CN103397520B - Fabric desinsection mosquito-repellent anti-static biologic product - Google Patents
Fabric desinsection mosquito-repellent anti-static biologic product Download PDFInfo
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- CN103397520B CN103397520B CN201310376622.XA CN201310376622A CN103397520B CN 103397520 B CN103397520 B CN 103397520B CN 201310376622 A CN201310376622 A CN 201310376622A CN 103397520 B CN103397520 B CN 103397520B
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- mosquito
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- 239000004744 fabric Substances 0.000 title claims abstract description 51
- 239000000077 insect repellent Substances 0.000 title claims abstract description 33
- 239000007788 liquid Substances 0.000 claims abstract description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 37
- 238000000605 extraction Methods 0.000 claims abstract description 33
- 239000000306 component Substances 0.000 claims abstract description 25
- RLLPVAHGXHCWKJ-UHFFFAOYSA-N permethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229960000490 permethrin Drugs 0.000 claims abstract description 25
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims abstract description 19
- -1 polyoxyethylene nonylphenol Polymers 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002904 solvent Substances 0.000 claims abstract description 17
- 239000004094 surface-active agent Substances 0.000 claims abstract description 17
- 235000005881 Calendula officinalis Nutrition 0.000 claims description 14
- 241000675108 Citrus tangerina Species 0.000 claims description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 14
- 239000009636 Huang Qi Substances 0.000 claims description 14
- 244000178870 Lavandula angustifolia Species 0.000 claims description 14
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 14
- 239000001102 lavandula vera Substances 0.000 claims description 14
- 235000018219 lavender Nutrition 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 12
- 239000000284 extract Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 239000004615 ingredient Substances 0.000 claims description 7
- 239000002893 slag Substances 0.000 claims description 7
- 240000000785 Tagetes erecta Species 0.000 claims 2
- 241000255925 Diptera Species 0.000 abstract description 6
- 241000238631 Hexapoda Species 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 5
- 230000001846 repelling effect Effects 0.000 abstract description 4
- 230000003115 biocidal effect Effects 0.000 abstract description 2
- 239000003139 biocide Substances 0.000 abstract description 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 244000045947 parasite Species 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 15
- 241000736851 Tagetes Species 0.000 description 12
- 238000012360 testing method Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000000575 pesticide Substances 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 241000256173 Aedes albopictus Species 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000000857 drug effect Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 230000003285 pharmacodynamic effect Effects 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000003197 gene knockdown Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000002728 pyrethroid Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of repelling mosquitoes and preventing insects biocide preparation, particularly relate to a kind of fabric desinsection mosquito repellent biologic product, be be prepared from by the aqueous solution of active component, surfactant, solvent, its active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; Its proportioning by weight mark is: Permethrin: biological extraction liquid: polyoxyethylene nonylphenol ether: ethanol=10 ~ 30:15 ~ 40:3 ~ 25:25 ~ 60, and to be dissolved in parts by weight be in the water of 1:13 ~ 30.This fabric desinsection mosquito-repellent anti-static biologic product contains natural botanical extraction liquid, and the mosquito-proof preparation of more general expelling parasite is safer, environmental protection, for soaking the fabrics such as clothes, trousers or mosquito net, can repelling mosquitoes and preventing insects for a long time, and harmless.
Description
Technical field
The present invention relates to a kind of repelling mosquitoes and preventing insects biocide preparation, particularly relate to a kind of fabric desinsection mosquito-repellent anti-static biologic product.
Background technology
Mosquito is not only sucked blood harassing and wrecking, and is the communication media of multiple serious disease, has relatively large people to suffer biting and attacking of mosquito, fly, flea, ant etc. every year, brings very large puzzlement to the live and work of people.At present, mosquito repellent product is on the market main raw material mainly with the chemicals that permethrin or Permethrin etc. are simple.Permethrin is a kind of pyrethroid insect to the synthesis repelling and knock down and kill activity.But under oxygen and ultraviolet existence, it can decompose inert matter, loses effect of desinsection.Permethrin is a kind of pesticide of state approval, although it meets national standard, not representing it does not have toxicity, if Long-Time Service still exists hidden danger.If publication number is CN101133741.B, name is called Vermins-expelling vermins-proof disinfection preparations for fabric, disclose a kind of composition of Vermins-expelling vermins-proof disinfection preparations, comprise active component Permethrin, surfactant polyoxyethylene nonylphenol ether, solvent medicinal alcohol, its main component is chemicals, particularly with the Vermins-expelling vermins-proof disinfection composition that Permethrin is main, although the pesticide that this composition uses for state approval, but this is also merely able to show, the pesticide that its toxicity is more general is less, if Long-Time Service also can bring certain injury with human body.Therefore, if a kind of biologic product can be found to replace chemical composition to a certain extent, also there is the function of desinsection mosquito repellent simultaneously, the injury to environment and human body will be reduced.
Summary of the invention
The present invention is intended to overcome the deficiencies in the prior art, provides a kind of fabric desinsection mosquito-repellent anti-static biologic product.
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention is prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 15 ~ 25 parts, biological extraction liquid 20 ~ 30, polyoxyethylene nonylphenol ether 5 ~ 20 parts and ethanol 25 ~ 60 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 20 ~ 30 parts by parts by weight, the moon tangerine of 15 ~ 25 parts, the lavender of 20 ~ 25 parts and 20 ~ 30 parts marigold to be dipped in parts by weight be in the water of 40 ~ 60 parts, airtightly be heated to 70 ~ 80 DEG C, after constant temperature 80 ~ 100min, continue to be heated to 90 ~ 100 DEG C, after constant temperature 45 ~ 50min, room temperature leaves standstill 6 ~ 12h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
As a further improvement on the present invention, it preferably selects component is Permethrin 18 ~ 23 parts, biological extraction liquid 23 ~ 28, polyoxyethylene nonylphenol ether 10 ~ 15 parts and ethanol 35 ~ 40 parts;
Prepare the method for desinsection mosquito-repellent anti-static fabric with fabric desinsection mosquito-repellent anti-static biologic product, realize through the following steps:
A, fabric desinsection mosquito-repellent anti-static biologic product claim 1 obtained and water are diluted to soak by 1:20-25 weight ratio;
B, fabric is dipped at 30 ~ 45 DEG C 75 ~ 95min in the obtained soak of a step, then takes out and dry;
C, the fabric obtained in b step is dipped in again 45 ~ 75 DEG C soak in 10 ~ 20min, dry, i.e. obtained desinsection mosquito-repellent anti-static fabric;
Wherein, in b, step c, the weight ratio of fabric and soak is 1:2 ~ 7.
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention, compatibility is reasonable, greatly reduces the use amount of Permethrin, can soak fabric, can mosquito repellent for a long time, alleviates harmless.The key technical indexes comprises: fabric pH6.1; Fabric scattering ratio 92%; Prevent biting rate 97%, fabric formaldehyde National Standards Technical requires content of formaldehyde≤300mg/kg, and actual measurement fabric formaldehyde content 137 mg/kg, is significantly less than national standard.In daily life, fabric washing still has the effect of Vermins-expelling vermins-proof for 50-70 time, harmless.
Detailed description of the invention
Embodiment 1
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention is prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 15 parts, biological extraction liquid 30, polyoxyethylene nonylphenol ether 5 parts and ethanol 60 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 20 parts by parts by weight, the moon tangerine of 25 parts, the lavender of 20 parts and 30 parts marigold to be dipped in parts by weight be in the water of 40 parts, airtightly be heated to 70 ~ 80 DEG C, after constant temperature 80 ~ 100min, continue to be heated to 90 ~ 100 DEG C, after constant temperature 45 ~ 50min, room temperature leaves standstill 6h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
Embodiment 2
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention, it is characterized in that being prepared from by active component, surfactant and solvent, described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 25 parts, biological extraction liquid 20, polyoxyethylene nonylphenol ether 20 parts and ethanol 25 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 30 parts by parts by weight, the moon tangerine of 15 parts, the lavender of 25 parts and 20 parts marigold to be dipped in parts by weight be in the water of 60 parts, airtightly be heated to 72 ~ 78 DEG C, after constant temperature 80min, continue to be heated to 90 ~ 90 DEG C, after constant temperature 50min, room temperature leaves standstill 12h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
Embodiment 3
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention is prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 18 parts, biological extraction liquid 28, polyoxyethylene nonylphenol ether 10 parts and ethanol 40 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 22 parts by parts by weight, the moon tangerine of 23 parts, the lavender of 22 parts and 22 parts marigold to be dipped in parts by weight be in the water of 45 parts, airtightly be heated to 74 ~ 76 DEG C, after constant temperature 85min, continue to be heated to 95 ~ 100 DEG C, after constant temperature 45min, room temperature leaves standstill 8h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
Embodiment 4
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention is prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 23 parts, biological extraction liquid 23, polyoxyethylene nonylphenol ether 15 parts and ethanol 35 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 28 parts by parts by weight, the moon tangerine of 17 parts, the lavender of 24 parts and 28 parts marigold to be dipped in parts by weight be in the water of 55 parts, airtightly be heated to 74 ~ 76 DEG C, after constant temperature 95min, continue to be heated to 90 ~ 100 DEG C, after constant temperature 45 ~ 50min, room temperature leaves standstill 10h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
Embodiment 5
Fabric desinsection mosquito-repellent anti-static biologic product of the present invention is prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 20 parts, biological extraction liquid 25, polyoxyethylene nonylphenol ether 13 parts and ethanol 37 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 25 parts by parts by weight, the moon tangerine of 20 parts, the lavender of 23 parts and 25 parts marigold to be dipped in parts by weight be in the water of 50 parts, be airtightly heated to 75 DEG C, after constant temperature 90min, continue to be heated to 95 DEG C, after constant temperature 48min, room temperature leaves standstill 10h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
Embodiment 6
With embodiment 1 ~ 5 obtained fabric desinsection mosquito-repellent anti-static biologic product, the method preparing desinsection mosquito-repellent anti-static fabric is as follows:
A, the fabric desinsection mosquito-repellent anti-static biologic product that embodiment 1 ~ 5 is obtained is diluted to soak with water by 1:20 ~ 25 weight ratio respectively;
B, anti-static fabric is dipped at 30 ~ 45 DEG C 75 ~ 95min in the obtained soak of a step, then takes out and dry;
C, the fabric obtained in b step is dipped in again 45 ~ 75 DEG C soak in 10 ~ 20min, dry, i.e. obtained desinsection mosquito-repellent anti-static fabric;
Wherein, in b, step c, the weight ratio of fabric and soak is 1:3 or 1:4 or 1:5 or 1:6 or 1:7.
The present invention's anti-static fabric used is the XHY-11 electrostatic fabric of my company's research and development, adopts special polyester long filament, warp-wise or warp-wise broadwise is embedding knits German Japanese series of conductive fiber, weaves form through special process.Through the clothes that special process is made, there is excellent antistatic anti-dust performance with this fabric.Technical indicator: meet GB12014-89 " anti-static clothing " standard-required, home washings expects surface density of charge≤1.0 μ c/m below 100 times
2, be far smaller than surface density of charge≤7 μ c/m
2requirement (GB12014-89 " anti-static clothing " standard).The anti-static clothing quantity of electric charge≤0.4 μ the c/m made
2.
Below, provide concrete test report and further illustrate main functional characteristics of the present invention and beneficial effect.
One, with the mosquito repellent evaluating drug effect of the fabric of fabric desinsection mosquito-repellent anti-static biologic product immersion of the present invention
Experimental basis: GB/T 13917.9-2009 " agricultural chemicals grade hygienic insecticide indoor pharmacodynamic test and evaluation the 9th part: repellant ";
For examination insect: aedes albopictus (
adeds albopictus), sprout wings rear adult of not sucking blood for 3 days;
Experimental condition: temperature is 26.1 DEG C ± 1 DEG C, and relative humidity is 65% ± 10%;
Result of the test:
As following table:
Conclusion (of pressure testing)
Carry out evaluating drug effect by GB/T 13917.9-2009 " agriculture chemical registration hygienic insecticide indoor pharmacodynamic test and evaluation the 9th part: repellant ", anophelifuge fabrics is 78.05% to the scattering ratio of aedes albopictus, has mosquito-proof effect.
Two, desinsection mosquito-repellent anti-static fabric of the present invention is made into the content of formaldehyde survey report of clothes
Test basis/judgment basis: GB18410-2010
Check conclusion:
As following table:
Test item title | Unit | Technical requirement (C class) | Assay | Individual event judges |
Content of formaldehyde | mg/kg | ≤300 | 137 | Meet |
Claims (3)
1. fabric desinsection mosquito-repellent anti-static biologic product, it is characterized in that being prepared from by active component, surfactant and solvent, and described active component is that Permethrin and biological extraction liquid, surfactant are polyoxyethylene nonylphenol ether, solvent is ethanol; The parts by weight of its each component are: Permethrin 15 ~ 25 parts, biological extraction liquid 20 ~ 30 parts, polyoxyethylene nonylphenol ether 5 ~ 20 parts and ethanol 25 ~ 60 parts;
Described biological extraction liquid be by the Radix Astragali, the moon tangerine, lavender, marigold and water is prepared from, its extracting method is:
Be the Radix Astragali of 20 ~ 30 parts by parts by weight, the moon tangerine of 15 ~ 25 parts, the lavender of 20 ~ 25 parts and 20 ~ 30 parts marigold to be dipped in parts by weight be in the water of 40 ~ 60 parts, airtightly be heated to 70 ~ 80 DEG C, after constant temperature 80 ~ 100min, continue to be heated to 90 ~ 100 DEG C, after constant temperature 45 ~ 50min, room temperature leaves standstill 6 ~ 12h; Filtering slag, extracts liquid, carries out separated, obtain the biological extraction liquid that effective ingredient is 60 ~ 70%.
2. fabric desinsection mosquito-repellent anti-static biologic product as claimed in claim 1, is characterized in that Permethrin 18 ~ 23 parts, biological extraction liquid 23 ~ 28 parts, polyoxyethylene nonylphenol ether 10 ~ 15 parts and ethanol 35 ~ 40 parts.
3. prepare the method for desinsection mosquito-repellent anti-static fabric with fabric desinsection mosquito-repellent anti-static biologic product as obtained in claim 1, be characterised in that and realize through the following steps:
A, fabric desinsection mosquito-repellent anti-static biologic product claim 1 obtained and water are diluted to soak by 1:20-25 weight ratio;
B, fabric is dipped at 30 ~ 45 DEG C 75 ~ 95min in the obtained soak of a step, then takes out and dry;
C, the fabric obtained in b step is dipped in again 45 ~ 75 DEG C soak in 10 ~ 20min, dry, i.e. obtained desinsection mosquito-repellent anti-static fabric;
Wherein, in b, step c, the weight ratio of fabric and soak is 1:2 ~ 7.
Priority Applications (1)
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CN201310376622.XA CN103397520B (en) | 2013-08-27 | 2013-08-27 | Fabric desinsection mosquito-repellent anti-static biologic product |
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CN201310376622.XA CN103397520B (en) | 2013-08-27 | 2013-08-27 | Fabric desinsection mosquito-repellent anti-static biologic product |
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CN103397520B true CN103397520B (en) | 2015-07-29 |
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CN201310376622.XA Expired - Fee Related CN103397520B (en) | 2013-08-27 | 2013-08-27 | Fabric desinsection mosquito-repellent anti-static biologic product |
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CN106973958A (en) * | 2017-03-29 | 2017-07-25 | 苏州艾菲罗化工科技有限公司 | A kind of special anti-mosquito agent of textile and preparation method thereof |
WO2018228303A1 (en) * | 2017-06-12 | 2018-12-20 | Cypress Bio-Tech Company Limited | Multi-applica tion insect repellent additive |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
CN101173485A (en) * | 2006-11-02 | 2008-05-07 | 上海鼎中保鲜科技有限公司 | Vermins-proof preparations for fabric |
CN101518365A (en) * | 2008-02-27 | 2009-09-02 | 上海服装集团品牌发展有限公司 | Manufacturing method of anti-mosquito clothes |
CN103015167A (en) * | 2012-12-24 | 2013-04-03 | 王建波 | Multifunctional cool shirt |
-
2013
- 2013-08-27 CN CN201310376622.XA patent/CN103397520B/en not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101173485A (en) * | 2006-11-02 | 2008-05-07 | 上海鼎中保鲜科技有限公司 | Vermins-proof preparations for fabric |
CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
CN101518365A (en) * | 2008-02-27 | 2009-09-02 | 上海服装集团品牌发展有限公司 | Manufacturing method of anti-mosquito clothes |
CN103015167A (en) * | 2012-12-24 | 2013-04-03 | 王建波 | Multifunctional cool shirt |
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Effective date of registration: 20161031 Address after: 163316, new industry incubator (Park), room 2, No. 105, hi tech Zone, Daqing, Heilongjiang, 702 Patentee after: Daqing Xin Li Li Biological Technology Co., Ltd. Address before: 163000 gate H-A, No. 1, weft two road, Saertu District, Heilongjiang, Daqing Patentee before: Dong Haiyan |
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Granted publication date: 20150729 Termination date: 20180827 |