CN101173485A - Vermins-proof preparations for fabric - Google Patents
Vermins-proof preparations for fabric Download PDFInfo
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- CN101173485A CN101173485A CNA2006101179029A CN200610117902A CN101173485A CN 101173485 A CN101173485 A CN 101173485A CN A2006101179029 A CNA2006101179029 A CN A2006101179029A CN 200610117902 A CN200610117902 A CN 200610117902A CN 101173485 A CN101173485 A CN 101173485A
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Abstract
The invention relates to a mothproof preparation for the fabric, which is characterized in that the materials and the water are prepared according to certain quality percentage; the materials comprise the active component, the solvent, the surface-active material, wherein, the active component is permethin and the content is 30 to 50 wt percent, and the surface-active material is nonyl phenol polyoxyethylene ether and the content is 10 to 30 wt percent, the content of the solvent is 30 to 50 wt percent. The invention has the advantages that: the invention can be sprayed on the fabric, such as the clothes, the pants, the mosquito net and the tent, can drive the mosquito away for long time, and is harmless to the human body.
Description
Technical field
The present invention relates to a kind of insect protected preparation, particularly a kind of Vermins-proof preparations for fabric.
Background technology
In the human puzzlement that always is in the virus infections that insect bites and bring thus, although the highly developed modern people of science have grasped the means of a lot of replies, annual still have a large amount of people to suffer biting and attacking of mosquito, fly, Lian, attagenus piceus, flea, mite and ant etc., particularly the people who lives or work in arduous area.
Permethrin is a kind of insect to be had repulsion, and knocks down and kill active synthetic pyrethroid.Permethrin is to plant, food, most of animal, human harmless, and can not generate other harmful material under daily condition.Although permethrin has so many beneficial features, because therefore its short relatively effective insecticidal activity, is difficult to be extensive use of in the mankind's daily life always.This be because oxygen and ultraviolet in the presence of, permethrin can resolve into inactive, the product of no pesticidal.
Summary of the invention
The object of the present invention is to provide the long Vermins-proof preparations for fabric of a kind of safe, efficient, term of validity, it can be sprayed on the fabric, plays the effect of longer-term mosquito repellent.
The present invention solves the problems of the technologies described above by the following technical programs, reaches goal of the invention of the present invention.
A kind of Vermins-proof preparations for fabric is characterized in that: formulated by certain quality percentage by raw material and water; Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 30%～50wt%, and surfactant is a polyoxyethylene nonylphenol ether, and content is 10～30wt%, and the content of solvent is 40%～60wt%.
In the present invention, the content of active component Permethrin is preferably 35～45%wt.
In the present invention, solvent is a medicinal alcohol, but is not limited thereto, so long as all kinds of solvents that can dissolve Permethrin all can, choice of Solvent is accomplished for the person of ordinary skill of the art very easily.
In the present invention, the mass percent of raw material and water is generally 1: 50～70, but is not limited to this.
Permethrin of the present invention, English name is: permethrin; Another name Permanone, permethrin, 3-phenoxy benzyl-2,2-dimethyl-3-(2, the 2-dichloroethylene)-1-cyclopropanecarboxylcompound; Molecular formula is: C
21H
20Cl
2O
3Formal name used at school: (3-benzyloxy phenoxy base) cis, trans-(±)-3-(2, the 2-dichloroethylene)-2,2-dimethyl cyclopropane carboxylic acid ester; The Latin chemical name is: (3-phenoxyphenyl) methyl (±) cis-trans-3-(2,2dichloroethenyl)-2,2-dimethyl-cyclopropanecarboxylatecis/trans isomers ratio:min 35% (±) cis and max 65% (±) trans; Structural formula is as follows:
Its outward appearance is faint yellow to little brown viscous liquid, and postpone for a long time can be formed solid.
Vermins-proof preparations for fabric of the present invention, as long as raw material is mixed with water, stirring gets final product, can hot a little hydrotropy during preparation.
Vermins-proof preparations for fabric of the present invention, its major function has:
1, prevents biting of insects such as mosquito, fly, mite, Lian, attagenus piceus, flea, flat lice and ant
2, anti-intensive ultraviolet (30+UV).
Thereby 3, make people avoid the generation of diseases such as invasion and attack, Lyme arthritis, encephalitis, dengue fever, yellow fever, typhoid fever as West Nile Virus owing to prevent biting of above insect
Its key property is:
1, effective: as to compare with similar pest repellant in the market and to have lasting effectiveness.
2, convenient: as, just again to need not to smear other culicifuge and insect protected articles for use as long as put on the clothing of handling by preparation of the present invention.
3, reliable: as to be not made of salt, to expose to the weather, sweat, laundry and flatiron.
4, continue: on clothing, use once, still effective after washing 50 times.
5, tasteless: without any peculiar smell.
6, colourless: as, to be applied in the sensation that can not give people's difference on the clothing without any color.
7, harmless: without any side effect and harm, more safer than present pest repellant to human body.
8, environmental protection: can not produce any pollution and harm to environment.
The Permethrin content that this Vermins-proof preparations for fabric finally is applied to clothes only is about 0.5%, and promptly the content on cloth is 0.12mg/cm
2About.It is than present any all safety and effectively lasting of pest repellant that skin smears that is applied to.Safety message is: the oral and Skin-test data on rat and the rabbit: skin LD50＞2000mg/kg (rabbit), oral LD50＞5000mg/kg (rat) has proved that it is one of former medicine of safe class in the world.
The packing of this Vermins-proof preparations for fabric adopts the steel drum of liner PE or PVF, net weight 25 or 50 kilograms.
This Vermins-proof preparations for fabric finished product is a cream preparation, behind the thin up, used up in two hours during use, diluted concentration is: the 17.5g medicament adds water 987.5g, directly spray on the heavy clothes of 1kg after making the liquid of 1kg, specifically have two kinds of spraying methods as follows:
1, uses the aerosol spray spraying method
At first sprayer is thoroughly cleaned up with clear water, the preparation after will diluting is then filled sprayer and is stirred and be forced into 0.55Mpa.Fine in the ventilation every suit is divided on the ground, every is evenly sprayed with above-mentioned 0.55Mpa pressure, and the time is preferably 50s, and turn-over carries out same processing then.Hang up after double treatment finishes and dry, and on every clothes, stamp marks for treatment and processing time.
2, special purpose machinery facture
By the operation of streamline, batch process on a large scale.
Below, provide concrete laboratory report and further specify major function characteristic of the present invention and beneficial effect.
One, the mosquito repellent evaluating drug effect of preparation of the present invention
1, examination criteria: detect by State Standard of the People's Republic of China GB/T 17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant " regulation;
2, testing conditions and sample
1) laboratory temperature: 26 ± 1 ℃, relative humidity: 65 ± 5%
2) mosquito kind: aedes albopictus (Aedes albopictus), the back 4～5 days (the standard examination worm that Prevention ﹠ Control Station of Parasitic Disease, China Diseases Prevention ﹠ C raises) of sprouting wings
3) mosquito number: 300 female insect/cages of not sucking blood (35 * 35 * 35cm)
4) test pre-treatment: before test with the jejunitas 18h of mosquito
5) test sample: the clothing (calling the insect protected clothing in the following text) that has sprayed preparation of the present invention by preceding method
6) control sample: the clothing of handling by preceding method of the same race (calling the contrast clothing in the following text) not
3, experimenter
5 volunteers participate in test
4, detect step
1) mosquito attack test: the experimenter stretches into left hand in the mosquito cage before the test, and it is qualified for attack to stop to fall to biting 30 above persons in the 2min, and this person and this cage mosquito can be used for repellency test
2) the insect protected clothing is inserted in the experimenter on hand, stretches in the mosquito cage, observe 2min, record the back of the hand mosquito stops falling and biting number
3) will contrast clothing and be inserted in the experimenter on hand, and stretch in the mosquito cage, and observe 2min, record the back of the hand mosquito stops falling and biting number
5, testing result
As following table
6, conclusion
With reference to State Standard of the People's Republic of China GB/T 17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant " relevant regulations, the clothing that has sprayed preparation of the present invention is 74.16% to the scattering ratio of aedes albopictus, and the clothing that has sprayed preparation of the present invention has repellent action to aedes albopictus.
Two, the insect protected of preparation of the present invention, mosquito repellent evaluating drug effect
1, detects foundation: State Standard of the People's Republic of China GB13917.1-92 " the indoor harmacological effect assay method of agriculture chemical registration hygienic insecticide indoor harmacological effect detection method propellant " and GB/T17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant "
2, test sample: the clothes, the trousers (calling insect protected clothing, insect protected trousers in the following text) that have sprayed preparation of the present invention by preceding method; Control sample: the clothing of handling by preceding method of the same race (calling the contrast clothing in the following text) not
3, testing conditions: laboratory temperature is 26 ± 1 ℃, relative humidity 65 ± 5%
4, for the examination insect: the standard examination worm that Prevention ﹠ Control Station of Parasitic Disease, China Diseases Prevention ﹠ C raises
Culex pipiens pallens (Culex pipiens pallens), the 2nd～3 day female adult of not sucking blood in back sprouts wings
Aedes albopictus (Aedes albopictus), emergence back 4～5 days
Housefly (Musca doestica), the 3rd～5 day adult in back that sprout wings, male and female half and half
Groton bug (Blatte germanica), two all adults, male and female half and half
Method is had a liking for skin mite (Dermatophagoides farinae), female male imago
Attagenus piceus (Attagenus unicolor japonicus), the 10-11 instar larvae
Xanthopsyllacheopis (Xenopsylla cheopis), back the 1st～2 all adults sprout wings
Monomorium pharaonis (Monomrium pharaonis), worker ant becomes ant
5, detection method
1) forces contact method
Evaluation of pesticide effectiveness step by the 2.4.2 residual spray among the State Standard of the People's Republic of China GB13917.1-92 " the indoor harmacological effect assay method of agriculture chemical registration hygienic insecticide indoor harmacological effect detection method propellant " detects.
Respectively each examination worm is placed and force in the contactor (GB13917.1-92 2.3 defineds force contactor), force to be contacted with insect protected clothing contact-making surface 30min.To try then to feed with feed and immersion cotton balls in the dependent insect cage (ware) that worm all is transferred to cleaning.Dead examination borer population when flight property examination worm is checked 24h.Dead examination borer population when creeping inspection 24,48 of examination worm and 72h.Detect triplicate, calculate average dead examination borer population.
2) anthelminthic effect detects
After the insect protected clothing is inserted in experimenter's hand, stretch in the mosquito cage, observe 2min, record the back of the hand mosquito stops the number that falls.
Parallel control: the hand that is inserted in the contrast clothing is observed mosquito and is stopped the number that falls in contrast.
6, testing result
Insect protected clothing insect protected drug effect testing result is as following table
The insect protected clothing is to aedes albopictus repellent effect testing result such as following table
7, conclusion
Estimate according to 3.2.2 among the State Standard of the People's Republic of China GB/T 17322.1-1998 " indoor harmacological effect of agriculture chemical registration hygienic insecticide is estimated propellant ".Insect protected clothing insect protected drug effect testing result is as follows:
The insect protected clothing is 100% to mosquito, fly, Lian and attagenus piceus 30min rate of knockdown, and the 24h death rate is respectively 100%, 90.0%, 90.0% and 90.0%, and the Lian and the attagenus piceus 72h death rate are respectively 90.0% and 90.0%; The insect protected clothing is respectively 90.0%, 89.54% and 93.33% to flea, mite and ant 30min rate of knockdown, and the 72h death rate is respectively 80.0%, 72.54% and 81.90%.
The insect protected clothing is 53.14% to the scattering ratio of aedes albopictus.
The insect protected clothing has the insect protected effect.
Three, the mosquito repellent evaluating drug effect of preparation of the present invention
1, detects foundation: State Standard of the People's Republic of China GB/T 17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant "
2, test sample: the clothes (calling insect protected clothing 1# in the following text) that has sprayed preparation of the present invention by preceding method; Sprayed the clothes (calling insect protected clothing 2# in the following text) of preparation of the present invention by preceding method; Control sample: the clothing of handling by preceding method of the same race (calling the contrast clothing in the following text) not
3, for the examination insect: the standard examination worm aedes albopictus (Aedes albopictus) that Prevention ﹠ Control Station of Parasitic Disease, China Diseases Prevention ﹠ C raises, emergence back 4～5 days
4, detection method
1) examination criteria: detect by State Standard of the People's Republic of China GB/T 17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant " regulation
2) testing conditions:
1. laboratory humiture: 26 ± 1 ℃, RH65 ± 5%
2. mosquito kind: aedes albopictus (Aedes albopictus), the back 4～5 days of sprouting wings
3. mosquito number: 300 female insect/cages of not sucking blood (35 * 35 * 35cm)
4. test pre-treatment: before test with the jejunitas 18h of mosquito
3) study subject
3 volunteers participate in test.
4) testing procedure
1. mosquito attack: the experimenter stretches into left hand in the mosquito cage before the test, and it is qualified for attack to stop to fall to biting 30 above persons in the 2min, and this person and this cage mosquito can be used for repellency test.
2. method of testing: respectively insect protected clothing and contrast clothing are inserted in the experimenter on hand
3. measure of merit: after the insect protected clothing is inserted in experimenter's hand, stretch in the mosquito cage, observe 2min, record the back of the hand mosquito stops falling and biting number.
4. parallel control: the hand that is inserted in the contrast clothing is observed mosquito and is stopped falling and biting number in contrast
5, testing result:
The insect protected clothing is to aedes albopictus repellent effect testing result such as following table
Effect detection such as following table that the anti-aedes albopictus of insect protected clothing is bitten
6, conclusion
With reference to State Standard of the People's Republic of China GB/T 17322.10-1998 " agriculture chemical registration hygienic insecticide indoor harmacological effect is estimated repellant ".
Insect protected clothing 1# is 77.11% to the scattering ratio of aedes albopictus, prevents that biting rate is 100%.Insect protected clothing 2# is 62.99% to the scattering ratio of aedes albopictus, prevents that biting rate is 100%.
Insect protected clothing 1# is better than insect protected clothing 2# to the repellent effect of aedes albopictus.
Insect protected clothing 1# and insect protected clothing 2# have repellent effect to aedes albopictus, and it is obvious to prevent biting effect.
The specific embodiment
For technological means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with the specific embodiment, further set forth the present invention.
Embodiment 1
A kind of Vermins-proof preparations for fabric is that 1: 50 ratio is formulated by raw material and water by mass ratio.Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 30%wt, and surfactant is a polyoxyethylene nonylphenol ether, and content is 10%wt, and solvent is a medicinal alcohol, and content is 60%wt.
Embodiment 2
A kind of Vermins-proof preparations for fabric is that 1: 60 ratio is formulated by raw material and water by mass ratio.Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 50%wt, and surfactant is a polyoxyethylene nonylphenol ether, and content is 10%wt, and solvent is a medicinal alcohol, and content is 40%wt.
Embodiment 3
A kind of Vermins-proof preparations for fabric, formulated by raw material and water by 1: 70 ratio.Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 35%wt, and surfactant is a polyoxyethylene nonylphenol ether, and content is 15%wt, and solvent is a medicinal alcohol, and content is 50%wt.
Embodiment 4
A kind of Vermins-proof preparations for fabric, formulated by raw material and water by 1: 70 ratio.Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 45%wt, and surfactant is a polyoxyethylene nonylphenol ether, and content is 15%wt, and solvent is a medicinal alcohol, and content is 40%wt.
Embodiment 5
A kind of Vermins-proof preparations for fabric, formulated by raw material and water by 1: 70 ratio.Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 40%wt, and surfactant is a polyoxyethylene nonylphenol ether, and content is 20%wt, and solvent is a medicinal alcohol, and content is 40%wt.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that describes in the foregoing description and the specification just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (4)
1. a Vermins-proof preparations for fabric is characterized in that: formulated by certain quality percentage by raw material and water; Raw material comprises active component, solvent, surfactant, and active component is a Permethrin, and content is 30%～50wt%, and surfactant is a polyoxyethylene nonylphenol ether, and content is 10～30wt%, and the content of solvent is 40%～60wt%.
2. a kind of Vermins-proof preparations for fabric according to claim 1 is characterized in that: the content of active component Permethrin is 35～45%wt.
3. a kind of Vermins-proof preparations for fabric according to claim 1 is characterized in that: solvent is a medicinal alcohol.
4. a kind of Vermins-proof preparations for fabric according to claim 1 is characterized in that: preparing the raw material of described insect protected preparation and the mass percent of water is 1: 50～70.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006101179029A CN101173485A (en) | 2006-11-02 | 2006-11-02 | Vermins-proof preparations for fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006101179029A CN101173485A (en) | 2006-11-02 | 2006-11-02 | Vermins-proof preparations for fabric |
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| Publication Number | Publication Date |
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| CN101173485A true CN101173485A (en) | 2008-05-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA2006101179029A Pending CN101173485A (en) | 2006-11-02 | 2006-11-02 | Vermins-proof preparations for fabric |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101133741B (en) * | 2007-07-20 | 2010-05-19 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| CN102517910A (en) * | 2011-12-06 | 2012-06-27 | 福建锦江科技有限公司 | Anti-mite polyamide fiber and preparation method thereof |
| CN103397520A (en) * | 2013-08-27 | 2013-11-20 | 董海燕 | Vermin-killing mosquito-repellent anti-static biological preparation for fabrics |
| CN104179385A (en) * | 2014-08-29 | 2014-12-03 | 句容市石狮冲压件厂 | Outdoor waterproof heat preservation tent |
| CN116122044A (en) * | 2023-01-17 | 2023-05-16 | 上海洁宜康化工科技有限公司 | Mite-proof finishing method for mattress cloth |
-
2006
- 2006-11-02 CN CNA2006101179029A patent/CN101173485A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101133741B (en) * | 2007-07-20 | 2010-05-19 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| CN102517910A (en) * | 2011-12-06 | 2012-06-27 | 福建锦江科技有限公司 | Anti-mite polyamide fiber and preparation method thereof |
| CN103397520A (en) * | 2013-08-27 | 2013-11-20 | 董海燕 | Vermin-killing mosquito-repellent anti-static biological preparation for fabrics |
| CN103397520B (en) * | 2013-08-27 | 2015-07-29 | 董海燕 | Fabric desinsection mosquito-repellent anti-static biologic product |
| CN104179385A (en) * | 2014-08-29 | 2014-12-03 | 句容市石狮冲压件厂 | Outdoor waterproof heat preservation tent |
| CN104179385B (en) * | 2014-08-29 | 2016-11-23 | 句容市石狮冲压件厂 | A kind of outdoor water-proof heat-preserving tent |
| CN116122044A (en) * | 2023-01-17 | 2023-05-16 | 上海洁宜康化工科技有限公司 | Mite-proof finishing method for mattress cloth |
| CN116122044B (en) * | 2023-01-17 | 2024-03-08 | 上海洁宜康化工科技有限公司 | Mite-proof finishing method for mattress cloth |
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Open date: 20080507 |