CN116122044A - Mite-proof finishing method for mattress cloth - Google Patents
Mite-proof finishing method for mattress cloth Download PDFInfo
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- CN116122044A CN116122044A CN202310059914.4A CN202310059914A CN116122044A CN 116122044 A CN116122044 A CN 116122044A CN 202310059914 A CN202310059914 A CN 202310059914A CN 116122044 A CN116122044 A CN 116122044A
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- mite
- parts
- mattress
- cloth
- solution
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
- D06M13/17—Polyoxyalkyleneglycol ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to an anti-mite finishing method of bed cloth, which solves the problem that the anti-mite effect of the anti-mite finishing method in the prior art needs to be improved, and comprises the following steps: (I) Contacting the to-be-anti-mite finishing bed mattress cloth with an anti-mite finishing working solution to obtain a fabric I with liquid; (II) drying; (III) heat setting; wherein the anti-mite finishing work comprises the following anti-mite agent composition for mattress cloth: an anti-mite composition for mattress cloths, comprising, by weight: 2-10 parts of permethrin; 0 to 10 parts of ethyl butyl levulinate; (c) 2-20 parts of emulsifying agent; (d) 10-30 parts of polar organic solvent; (e) 0-10 parts of urea or thiourea; (f) The technical proposal of water for the anti-mite agent composition to 100 parts solves the technical problem well, and can be used in the production of the anti-mite agent composition for mattress cloth.
Description
Technical Field
The invention relates to an anti-mite finishing method of mattress cloth.
Background
Mites are a serious hazard to human health, where dust mites present in the home environment are largely distributed in carpets, sofas, tapestry, curtains, cushions, back pads, throw pillows, quilts, bedsheets, coverlets, pillows, simmons (mattresses). The dust mites eat secretions of human bodies, fallen dander, fallen food residues and the like, so that the breeding speed is extremely high; secretions, excretions, hulls, cadavers, and the like of dust mites are allergens. These allergens enter the human lung and can cause dust mite asthma, manifested by chest distress, shortness of breath, dyspnea due to exhalation, cyanosis due to anoxia of lips and nails, and allergic rhinitis and allergic dermatitis.
The Simmons mattress has a large internal space, a multi-layer structure and a higher temperature and humidity in a family living environment, and is suitable for mass propagation of mites, in particular dust mites. Dust mites are most distributed on the mattress cloth of the outermost layer of the mattress. In addition, the mattress is large in size, and the mattress cannot be taken out for airing generally, so that if the anti-mite processing treatment is carried out on the mattress cloth, the number of dust mites in the whole living environment can be greatly reduced, and the possibility of dust mite asthma is reduced.
The permethrin is a common anti-mite agent for mattress cloth fabric, and how to improve the anti-mite effect of the agent is a subject of continuous attention in the field.
Disclosure of Invention
The invention aims to solve the technical problem that the mite-proof effect of mite-proof finishing is to be improved by adopting single permethrin in the prior art, and provides a novel mite-proof finishing method for mattress cloth, which has a better mite-proof effect.
In order to solve the technical problems, the technical scheme of the invention is as follows:
an anti-mite finishing method of mattress cloth, comprising the following steps:
(I) Contacting the to-be-anti-mite finishing bed mattress cloth with an anti-mite finishing working solution to obtain a fabric I with liquid;
(II) drying;
(III) heat setting;
wherein the anti-mite finishing work comprises the following anti-mite agent composition for mattress cloth:
an anti-mite composition for mattress cloths, comprising, by weight:
(a) 2-10 parts of permethrin;
(b) 0-10 parts of ethyl butyl levulinate;
(c) 2-20 parts of emulsifying agent;
(d) 10-30 parts of polar organic solvent;
(e) Urea or thiourea, 0-10 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
Those skilled in the art know that when the anti-mite composition is in a range with a relatively low concentration of an effective substance (the effective substance is the general term of the component (a), the component (b) and the component (e), and the whole term is the same), the anti-mite composition is convenient to use, for example, the anti-mite composition can be directly used as an anti-mite finishing working solution for anti-mite finishing of bedding cloth fabrics. When the anti-mite composition is in a range with higher effective matter concentration, the composition occupies relatively smaller space per unit effective matter content, so that the storage and transportation cost is reduced, and the person skilled in the art also knows that the anti-mite composition with high effective concentration can be used as an anti-mite finishing working solution only by simply diluting the composition with water to the required concentration.
In the above technical solution, the material of the to-be-anti-mite finishing mattress cloth fabric in the step (I) is not particularly limited, and may be cotton, acrylic, polyester, polypropylene or spandex.
In the technical scheme, the form of the bedding cloth fabric to be anti-mite finished can be textile, knitwear or non-woven fabric.
The raw material fabrics in the embodiment and the comparative example of the invention are all mattress cloth fabrics provided by the company of the division of the like furniture, which are just the same ratio, the double-sided circular knitting machine sandwich jacquard fabric is a composite fabric which is formed by combining a front side, a sandwich and a back side into a whole through joint, and has the following specific specification:
in the above technical solution, the manner of contacting in the step (I) is not particularly limited, and may be dip contact, spray contact, roll contact, or the like. Further, the impregnation may be a batch impregnation or a continuous impregnation. The specific mode of the anti-mite finishing mattress cloth to be contacted with the anti-mite finishing working solution can be reasonably selected by the person skilled in the art, comparable technical effects can be achieved, and creative labor is not required.
In the above technical scheme, the contact time is not particularly limited, as long as the contact between the fabric deodorant finishing working solution and the fabric reaches or is basically balanced, the contact time is prolonged without particularly influencing the technical effect, but the contact time is too long to cause the increase of the production time cost, and the contact time is too short to influence the load capacity of the photocatalyst, based on the principle of the contact time, the person skilled in the art can comprehensively consider the factors to reasonably select the dipping time, and can obtain the comparable technical effect without carrying out creative labor.
By way of example only, when step (I) is contacted by batch impregnation, such as, but not limited to, not less than 1 minute for a period of time of impregnation, further non-limiting examples of impregnation periods may be 2 minutes, 3 minutes, 4 minutes, 5 minutes, 6 minutes, 7 minutes, 8 minutes, 9 minutes, 10 minutes, 11 minutes, 15 minutes, 30 minutes, 40 minutes, 50 minutes, 60 minutes, and the like. The impregnation times were 10 minutes in both the examples and comparative examples, which are merely comparable.
Those skilled in the art will recognize that the impregnation process will involve the ratio of the amount of anti-mite finishing working liquid to the amount of mattress pad to be anti-mite finished, and that those skilled in the art can reasonably select this ratio to achieve comparable technical results without the need for creative effort. By way of non-limiting example only, when step (I) is performed by batch impregnation, the ratio of the amount of the anti-mite finishing working liquid to the amount of the anti-mite finishing mattress pad to be used is 10 or more by weight, for example, but not limited to, 12, 14, 16, 18, 20, 30, etc., and further, by the same ratio, the weight ratio is 15 in the examples of the present invention and the comparative examples.
The impregnation in the examples and comparative examples of the present invention was batch impregnation, by way of comparison only.
In the above technical solution, the solution carrying rate in the solution carrying fabric I in the step (I) is not particularly limited, and a person skilled in the art can reasonably control the solution carrying rate according to the concentration of the effective matters in the anti-mite finishing working solution, the ability of the fabric to adsorb the anti-mite finishing working solution, the amount of the effective matters loaded with the anti-mite agent in the anti-mite mattress cloth fabric to be obtained, whether the fabric is extruded or not after impregnation, and the extrusion degree. The specification of the invention adopts the meaning of the liquid carrying rate commonly used in the field, and the liquid carrying rate, namely the ratio of the mattress cloth fabric to the anti-mite finishing working liquid, is based on the weight and relative to the mattress cloth fabric to be anti-mite finished. By way of example only, the fluid carrying rate in the fluid carrying fabric I may be 50-100%, such as, but not limited to, 55%, 60%, 65%, 70%, 75%, 80%, 85%, 90%, 95% and the like. The liquid carrying rate was controlled to 80% in the same comparative example and comparative example.
In the above-mentioned embodiments, the temperature of the drying in the step (II) is preferably 80 to 110℃such as, but not limited to, 85℃90℃95℃100℃105 ℃. The drying temperatures in the examples and comparative examples of the present invention were 100℃for the same comparison only.
In the above technical solution, the drying time of the step (II) is preferably 3 to 10 minutes, for example, but not limited to, 3.5 minutes, 4 minutes, 4.5 minutes, 5 minutes, 5.5 minutes, 6 minutes, 6.5 minutes, 7 minutes, 7.5 minutes, 8 minutes, 8.5 minutes, 9 minutes, 9.5 minutes, and the like. The drying time was 5 minutes in the examples and comparative examples of the present invention, which were merely comparable.
In the above-mentioned embodiments, the heat-setting temperature in the step (III) is preferably 120 to 180℃such as, but not limited to, 125℃130℃135℃140℃145℃150℃155℃160℃165℃170℃175℃and the like. The heat setting temperatures in the examples and comparative examples of the present invention were 150℃by comparison only.
In the above embodiment, the heat setting time of the step (III) is preferably 1 to 5 minutes, for example, but not limited to, 1.5 minutes, 2 minutes, 2.5 minutes, 3 minutes, 3.5 minutes, 4 minutes, 4.5 minutes, and the like. The heat setting time was 3 minutes in the examples and comparative examples of the present invention, which were comparable only.
By way of non-limiting example, permethrin is 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts, 9.5 parts, and the like.
Preferably, the ethyl butyllevulinate is more than 0 part and 10 parts or less, and the ethyl butyllevulinate and the permethrin have a mutual synergistic effect in terms of improving the anti-mite effect, namely, the ethyl butyllevulinate is a synergistic agent of the permethrin in terms of improving the anti-mite effect.
By way of non-limiting example, ethyl butyllevulinate is 0.5 part, 1 part, 1.5 part, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts, 9.5 parts, and the like. More preferably 1 to 9 parts.
By way of non-limiting example, the emulsifier is 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts, 9.5 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, and the like. More preferably 5 to 20 parts, most preferably 5 to 15 parts.
As non-limiting examples, the polar organic solvents are 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts, and the like. More preferably 10 to 25 parts.
Preferably, the component (e) is more than 0 parts and 10 parts or less, and the component (e) has an enhancing effect on the fenpropathrin in terms of improving the anti-mite effect.
By way of non-limiting example, component (e) is 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4.0 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts, 9.5 parts, and the like. More preferably 0.5 to 9 parts, most preferably 1 to 8 parts.
In the above technical solution, preferably, the emulsifier includes a nonionic surfactant.
In the above-described embodiments, the nonionic surfactant includes, for example, at least one selected from the group consisting of fatty alcohol polyoxyethylene ether, fatty acid polyoxyethylene ether, tween (i.e., polyoxyethylene sorbitan fatty acid ester), and hydrogenated castor oil ethylene oxide adduct.
In the above technical solution, the tween is, for example, at least one selected from the group consisting of tween-20, tween-40, tween-60 and tween-80.
Tween-80 was used for the emulsifier in examples and comparative examples only in the same manner.
In the above technical solution, preferably, the polar organic solvent is an alcoholic hydroxyl group-containing compound, abbreviated as solvent alcohol. The solvent alcohol is at least one selected from the group consisting of C1-C4 alcohols, glycol monoalkyl ethers, and glycols containing ether linkages.
In the above technical scheme, preferably, the C1-C4 alcohol is monohydric alcohol or dihydric alcohol. Such as, but not limited to, methanol, ethanol, ethylene glycol, n-propanol, isopropanol, 1, 2-propanediol, 1, 3-propanediol, n-butanol.
In the above technical scheme, preferably, the glycol monoalkyl ether corresponds to the following formula 1:
R1O (CH 2CH 2O) nH, formula 1;
wherein R is 1 Is C1-C4 alkyl, n is 1-3.
In the above technical scheme, preferably, the dihydric alcohol containing ether bond accords with the following formula 2:
m is the average degree of polymerization, number average molecular weight = ethylene oxide molecular weight m + molecular weight of water; wherein the number average molecular weight is 100 to 700. Such as, but not limited to, number average molecular weights of 100, 150, 200, 250, 300, 350, 400, 450, 500, 550, 600, 650, and the like.
By way of non-limiting example only of a specific ether linkage-containing glycol, the glycol series being the name of a commercially available variety, includes at least one selected from the group consisting of: diethylene glycol (or diethylene glycol), m is 2, and the number average molecular weight is 106; triethylene glycol (or triethylene glycol), m is 3, and the number average molecular weight is 150; and tetraethylene glycol (or tetraethylene glycol), m is 4, and the number average molecular weight is 194; etc.
Only as a non-limiting example of a commercial variety of PEG with "PEG (also called polyethylene glycol) +number average molecular weight" as a series name, a specific ether bond-containing diol includes at least one selected from the group consisting of: PEG-200, PEG-300, PEG-400, PEG-500, and PEG-600, and the like.
The polar organic solvents used in the examples and comparative examples of the present invention were PEG-400, by way of comparison only.
The technical key of the invention is the selection of the components of the composition, and when the composition formula is disclosed by the specification of the invention, the person skilled in the art can select and use the method commonly used in the art to obtain the anti-mite composition for mattress cloth according to the understanding of the person skilled in the art, and the obtained composition has comparable technical effects without the need of creative labor.
By way of example only, the anti-mite composition of the present invention may be obtained by a preparation method comprising the steps of:
(1) Dissolving the emulsifier into the polar organic solvent to obtain an emulsifier solution;
(2) Dispersing ethyl butyllevulinate in an emulsifier solution when the anti-mite composition contains ethyl butyllevulinate to obtain a solution A;
(3) Dispersing the solution A into water or dispersing the solution A into an aqueous solution of the component (e) when the anti-mite composition contains the component (e) to obtain emulsion B, wherein the emulsion B is less than or equal to 100 parts;
(4) When emulsion B is less than 100 parts, the required amount of water to the anti-mite composition is made up.
Moreover, the technical key of the invention is the selection of the components of the anti-mite agent composition, and the person skilled in the art can reasonably select the methods commonly used in the art to obtain comparable technical effects without the need of creative labor for how to apply the composition to the anti-mite finishing of mattress cloths.
The mite-proof performance evaluation of the mite-proof agent composition for the bed cloth adopts a repelling method specified in section 9.1 of the standard GB/T24253-2009 evaluation of the mite-proof performance of textiles, the mite-proof finishing bed cloth fabric to be mite-proof finished without mite-proof treatment is used as a reference sample, the mite-proof finishing bed cloth fabric subjected to mite-proof treatment, namely the mite-proof bed cloth is used as a sample, and the reference sample and the sample are not subjected to washing treatment specified in section 8.3 of the standard. The greater the repellency of the test sample, the better the anti-mite effect.
The present invention will be described in detail with reference to examples and comparative examples.
Detailed Description
[ comparative example 1 ]
1. Anti-mite agent composition for mattress cloth
1.1 formulation of an anti-mite composition for mattress cloths
An anti-mite composition for mattress cloths, comprising, by weight:
(a) 8 parts of permethrin;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 8 parts of permethrin into the emulsifier solution, and uniformly stirring to obtain a solution A;
adding the solution A into 61 parts of water under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has a mite repellent rate of 76%.
[ comparative example 2 ]
1. Anti-mite agent composition for mattress cloth
1.1 formulation of an anti-mite composition for mattress cloths
An anti-mite composition for mattress cloths, comprising, by weight:
(b) 8 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 8 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
adding the solution A into 61 parts of water under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has 65% of mite repellent rate.
[ comparative example 3 ]
1. Anti-mite agent composition for mattress cloth
1.1 formulation of an anti-mite composition for mattress cloths
An anti-mite composition for mattress cloths, comprising, by weight:
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 8 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
dissolving 8 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the emulsifier solution into the thiourea solution under stirring to obtain a mixed solution B;
water was added to the mixed solution B under stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has a mite repellent rate of 45%.
[ example 1 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(a) 6 parts of permethrin;
(b) 2 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 6 parts of permethrin and 2 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
adding the solution A into 61 parts of water under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has 91% of mite repellent rate.
[ example 2 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(a) 6 parts of permethrin;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 2 parts of the total of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 6 parts of permethrin into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 2 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has a mite repellent rate of 85%.
[ example 3 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(b) 2 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 6 parts of the total amount of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 2 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 6 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has 55% of mite repellent rate.
[ example 4 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(b) 6 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 2 parts of the total of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 6 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 2 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has a mite repellent rate of 70%.
[ example 5 ]
1. Anti-mite agent composition for mattress cloth
1.1 formulation of an anti-mite composition for mattress cloths
An anti-mite composition for mattress cloths, comprising, by weight:
(a) 4 parts of permethrin;
(b) 2 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 2 parts of the total of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 4 parts of permethrin and 2 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 2 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has a mite repellent rate of 93 percent.
[ example 6 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(a) 8 parts of permethrin;
(b) 2 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 4 parts of the total amount of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 8 parts of permethrin and 2 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 4 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has the repellent rate of more than 99 percent to mites.
[ example 7 ]
1. An anti-mite composition for mattress cloths, comprising, by weight:
(a) 6 parts of permethrin;
(b) 4 parts of ethyl butyl levulinate;
(c) Tween-80,8 parts;
(d) PEG-400, 16 parts;
(e) Thiourea, 2 parts of the total of the components,
(f) Water, such that the anti-mite composition is up to 100 parts.
1.2 preparation of an anti-mite composition for mattress cloths
Dissolving 8 parts of Tween-80 in 16 parts of PEG-400 to obtain an emulsifier solution;
adding 6 parts of permethrin and 4 parts of ethyl butyl levulinate into the emulsifier solution, and uniformly stirring to obtain a solution A;
dissolving 2 parts of thiourea in 61 parts of water to obtain a thiourea solution;
adding the solution A into thiourea solution under stirring to obtain emulsion B;
water was added to emulsion B with stirring until the total parts of the anti-mite composition for mattress cloths was 100 parts.
2. Preparation of anti-mite finishing working solution
Under stirring, adding 40 parts of the anti-mite agent composition into 960 parts of water, and uniformly stirring to obtain the anti-mite finishing working solution for the mattress cloth.
3. Anti-mite finishing method for bedding cloth fabric
Immersing the mattress cloth fabric to be subjected to mite-proof arrangement in the mite-proof arrangement working solution for mattress cloth in the section 2 for 10 minutes, wherein the weight ratio of the fabric to the mite-proof arrangement working solution for mattress cloth (also called bath ratio in the industry) is 1:15, then extruding to enable the liquid carrying rate to be 80%, then drying at 100 ℃ for 5 minutes by a shaping dryer, and shaping at 150 ℃ for 3 minutes to obtain the mite-proof mattress cloth.
Through tests, the anti-mite mattress cloth has the repellent rate of more than 99 percent to mites.
It should be noted that the above-described embodiments are only for explaining the present invention and do not constitute any limitation of the present invention. The invention has been described with reference to exemplary embodiments, but it is understood that the words which have been used are words of description and illustration, rather than words of limitation. Modifications may be made to the invention as defined in the appended claims, and the invention may be modified without departing from the scope and spirit of the invention. Although the invention is described herein with reference to particular means, materials and embodiments, the invention is not intended to be limited to the particulars disclosed herein, as the invention extends to all other means and applications which perform the same function.
Claims (10)
1. An anti-mite finishing method of mattress cloth, comprising the following steps:
(I) Contacting the to-be-anti-mite finishing bed mattress cloth with an anti-mite finishing working solution to obtain a fabric I with liquid;
(II) drying;
(III) heat setting;
wherein the anti-mite finishing work comprises the following anti-mite agent composition for mattress cloth:
an anti-mite composition for mattress cloths, comprising, by weight:
(a) 2-10 parts of permethrin;
(b) 0-10 parts of ethyl butyl levulinate;
(c) 2-20 parts of emulsifying agent;
(d) 10-30 parts of polar organic solvent;
(e) Urea or thiourea, 0-10 parts;
(f) Water, such that the anti-mite composition is up to 100 parts.
2. The anti-mite finishing method according to claim 1, wherein the material of the bed pad cloth to be anti-mite finished in the step (I) is cotton, acrylic, terylene, polypropylene or spandex, and the bed pad cloth to be anti-mite finished is in the form of textile, knitwear or non-woven fabric.
3. The anti-mite finishing method according to claim 1, wherein the liquid carrying rate of the liquid carrying fabric I is 50 to 100% by weight and based on the bed pad cloth to be anti-mite finished.
4. The anti-mite finishing method according to claim 1, wherein the temperature of the drying in the step (II) is 80-110 ℃.
5. The anti-mite finishing method according to claim 1, wherein the drying time in the step (II) is 3 to 10 minutes.
6. The anti-mite finishing method according to claim 1, wherein the heat setting temperature in the step (III) is 120 to 180 ℃.
7. The method of anti-mite finishing according to claim 1, wherein the time for heat setting in the step (III) is 1 to 5 minutes.
8. The method according to claim 1, wherein the parts of ethyl butyllevulinate in the anti-mite agent composition is more than 0 parts and 10 parts or less, and/or the parts of component (e) is more than 0 parts and 10 parts or less.
9. The anti-mite finishing method according to claim 1, wherein the emulsifier comprises a nonionic surfactant.
10. The mite-preventing finishing method according to claim 1, wherein the mite-preventing agent composition is obtained by a preparation method comprising the steps of:
(1) Dissolving the emulsifier into the polar organic solvent to obtain an emulsifier solution;
(2) Dispersing ethyl butyllevulinate in an emulsifier solution when the anti-mite composition contains ethyl butyllevulinate to obtain a solution A;
(3) Dispersing the solution A into water or dispersing the solution A into an aqueous solution of the component (e) when the anti-mite composition contains the component (e) to obtain emulsion B, wherein the emulsion B is less than or equal to 100 parts;
(4) When emulsion B is less than 100 parts, the required amount of water to the anti-mite composition is made up.
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Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060000025A1 (en) * | 2004-07-02 | 2006-01-05 | Dixon Timothy R | Insecticidally treated fabric having improved wash durability and insecticidal efficacy and method for its production |
| CN1807751A (en) * | 2006-01-12 | 2006-07-26 | 上海公泰纺织制品有限公司 | Method for preparing anti-insect textile by using pyrethroid-dyed synthetic fiber |
| CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| CN101173485A (en) * | 2006-11-02 | 2008-05-07 | 上海鼎中保鲜科技有限公司 | Vermins-proof preparations for fabric |
| CN101309583A (en) * | 2003-12-22 | 2008-11-19 | 巴斯福股份公司 | Composition for the impregnation of fibers, fabrics and nettings imparting a protective activity against pests |
| CN101718042A (en) * | 2009-11-24 | 2010-06-02 | 上海公泰纺织制品有限公司 | Mothproof fabric and preparation method thereof |
| CN102021830A (en) * | 2010-09-20 | 2011-04-20 | 吴江市龙申纺业有限公司 | Method for manufacturing agricultural insect-proof net |
| CN103103752A (en) * | 2012-12-10 | 2013-05-15 | 苏州尊元纺织有限公司 | Production method of fragrant cotton fabric |
| CN106808542A (en) * | 2017-01-13 | 2017-06-09 | 李水金 | A kind of timber preservative and preparation method thereof |
| CN107761374A (en) * | 2016-08-16 | 2018-03-06 | 牛绍英 | A kind of antibacterial, the fabric/fiber dressing liquid of insecticidal medium and its application method and textile article/fibre/paper products |
| CN112127150A (en) * | 2020-09-16 | 2020-12-25 | 无锡恒诺纺织科技有限公司 | Textile anti-mosquito finishing agent and using method thereof |
| CN112442779A (en) * | 2020-11-12 | 2021-03-05 | 汪爱国 | Stretch-proof and fracture-resistant blended fabric and preparation method thereof |
-
2023
- 2023-01-17 CN CN202310059914.4A patent/CN116122044B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101309583A (en) * | 2003-12-22 | 2008-11-19 | 巴斯福股份公司 | Composition for the impregnation of fibers, fabrics and nettings imparting a protective activity against pests |
| US20060000025A1 (en) * | 2004-07-02 | 2006-01-05 | Dixon Timothy R | Insecticidally treated fabric having improved wash durability and insecticidal efficacy and method for its production |
| CN1807751A (en) * | 2006-01-12 | 2006-07-26 | 上海公泰纺织制品有限公司 | Method for preparing anti-insect textile by using pyrethroid-dyed synthetic fiber |
| CN101173485A (en) * | 2006-11-02 | 2008-05-07 | 上海鼎中保鲜科技有限公司 | Vermins-proof preparations for fabric |
| CN101133741A (en) * | 2007-07-20 | 2008-03-05 | 季建萍 | Vermins-expelling vermins-proof disinfection preparations for fabric |
| CN101718042A (en) * | 2009-11-24 | 2010-06-02 | 上海公泰纺织制品有限公司 | Mothproof fabric and preparation method thereof |
| CN102021830A (en) * | 2010-09-20 | 2011-04-20 | 吴江市龙申纺业有限公司 | Method for manufacturing agricultural insect-proof net |
| CN103103752A (en) * | 2012-12-10 | 2013-05-15 | 苏州尊元纺织有限公司 | Production method of fragrant cotton fabric |
| CN107761374A (en) * | 2016-08-16 | 2018-03-06 | 牛绍英 | A kind of antibacterial, the fabric/fiber dressing liquid of insecticidal medium and its application method and textile article/fibre/paper products |
| CN106808542A (en) * | 2017-01-13 | 2017-06-09 | 李水金 | A kind of timber preservative and preparation method thereof |
| CN112127150A (en) * | 2020-09-16 | 2020-12-25 | 无锡恒诺纺织科技有限公司 | Textile anti-mosquito finishing agent and using method thereof |
| CN112442779A (en) * | 2020-11-12 | 2021-03-05 | 汪爱国 | Stretch-proof and fracture-resistant blended fabric and preparation method thereof |
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Effective date of registration: 20240426 Address after: 312001 Xilinmen Industrial Park, No. 1 Second Ring North Road, Yuecheng District, Shaoxing City, Zhejiang Province Patentee after: XILINMEN FURNITURE Co.,Ltd. Country or region after: China Address before: Room 403-A, Building 10, Lane 658, Jinzhong Road, Changning District, Shanghai, 200335 Patentee before: Shanghai jieyikang Chemical Technology Co.,Ltd. Country or region before: China Patentee before: Shanghai Guofan chemical new material Co.,Ltd. |