KR101812675B1 - Composite of Natural soap and Method of manufacturing thereof - Google Patents

Abstract

The present invention relates to a natural soap composition and a manufacturing method thereof. The natural soap composition of the present invention does not comprise artificial synthetic materials, has an excellent antibacterial effect such as removal of Demodex, and is helpful for skin condition improvement. Also, the natural soap composition does not comprise artificial synthetic materials, thereby preventing environmental pollution caused by artificial synthetic materials which are non-biodegradable. To this end, the natural soap composition comprises a pyrethrum flower, an anti-inflammatory agent, an exfoliator, an astringent, an antioxidant and perfume.

Description

TECHNICAL FIELD [0001] The present invention relates to a natural soap composition,

The present invention relates to a soap composition and a method for preparing the same, and more particularly, to a natural soap composition and a method for producing the same, which are effective for eliminating folliculitis without containing an artificial synthetic material and capable of improving skin.

Microcystic mite is an ex vivo parasite that is often observed under a microscope that infects the fur branching unit of the skin. Of the various species reported, at least Demodex folliculorum and Demodex brevis are found on the outside of the human body. The two shigies are often coexisting and preferentially gather in the same skin area of the face, cheeks, forehead, nose and outer ear canal, where active sebum secretion is beneficial to the environment and reproduction.

The adult phytoplankton mites are 14 to 18 days in life and eventually die, and their multiplication depends on successful mating by adult mite. Mating occurs at the follicular opening (near the skin surface). Thereafter, the pregnant females migrate to the sebaceous glands to lay eggs and become larvae and first nymphs. The first nymph goes to the opening of the hair follicle to become the second nymph, and goes out into the skin and enters the hair follicle again to become an adult. Thus, if the adult epididymis can successfully mate and produce the next generation in the life cycle process, the degree of infection in the host will increase. Fungicide infections do not appear in healthy children, but they increase in an age-dependent manner and are found in nearly 100% of middle-aged skin unless an abortion is taken. The incidence of fungal infection is higher in unhealthy skin than in normal skin. Excessive growth of these mites is associated with skin disease and hair loss.

In general, the soap is prepared by adding a sodium hydroxide solution to an animal fat, heating it, saponifying it, adding concentrated sodium chloride to the colloid solution, extracting the colloid solution, adding a predetermined flavor thereto, Molded. These general soaps are generally referred to as natural soaps. They contain natural glycerin as a natural soap, and do not have a salting process in comparison with general soaps. In addition, they contain preservatives, surfactants, coagulants , Pigment, artificial fragrance, and the like. In this regard, Korean Patent Laid-Open No. 10-2008-0110323 discloses a process for producing natural soap made only of natural materials. All of these natural soaps are made using only natural vegetable materials, so they are good for skin. They contain glycerin and can show moisturizing effect when they are used. In addition, various additives such as plant powders such as herbs and herbal powders are added So that the effect can be seen. Thus, the demand for the soap is higher than that of the general soap although it is expensive. However, most of the natural soaps are not fully saponified compared to regular solid soaps. In this case, the natural soap has an effective fat content.

The fungus is a mite that parasitizes in the hair follicles and sebaceous glands of the skin. It grows from few to several dozens of pores, and feeds on the fat from the sebaceous glands. Therefore, the effective fat content remaining in the natural soap is left on the skin when the soap is used, and the fat remaining on the skin causes the growth of the phosgenation. When the hair follicle is inhabited, hair loss starts and dry skin changes to oily skin.

In addition, insecticidal effects can be expected when natural materials are added to prevent the growth of the folliculum. However, the nature of the natural soap has the problem of skin exfoliation after exfoliation, pore contraction and cleansing, Which is the biggest problem of the natural soap which is contained in the soap, is still not solved.

Patent Publication No. 2008-0110323 (Publication Date: December 18, 2008)

Disclosure of the Invention The present invention has been made in view of the above points, and it is an object of the present invention to provide a cosmetic composition which does not contain an artificial synthetic material and is effective for removing folliculitis, It is an object of the present invention to provide a soap composition and a method for producing the same.

In order to solve the above-mentioned problems, the natural soap composition according to the present invention provides a soap composition comprising a pest control agent, an anti-inflammatory agent, an exfoliant, an astringent agent, an antioxidant and a fragrance as an active ingredient.

According to one preferred embodiment, 50 to 80 parts by weight of the anti-inflammatory agent, 50 to 80 parts by weight of the exfoliant, 50 to 80 parts by weight of the astringent agent, 50 to 80 parts by weight of the antioxidant, And 80 to 120 parts by weight of the perfume.

According to another preferred embodiment of the present invention, 50 to 80 parts by weight of papaya enzyme, 50 to 80 parts by weight of lavender, 150 to 250 parts by weight of jojoba oil, 150 to 250 parts by weight of castor oil, 150 to 250 parts by weight of oil and 500 to 700 parts by weight of honey.

According to one preferred embodiment, the anti-inflammatory agent comprises at least one member selected from the group consisting of gelite, calamine, castor oil and lemon grass, and the exfoliating agent is selected from the group consisting of papaya enzyme, gelite and white clay Wherein the astringent agent comprises at least one selected from the group consisting of white clay, gelite and papaya enzymes, and the antioxidant is at least one selected from the group consisting of allantoin lavender and calamine, And the fragrance may include at least one selected from the group consisting of lemon grass lavender and tea tree.

In one preferred embodiment, the composition may satisfy the following relationships:

 1) The weight ratio of calamine / trephine is 0.5 ~ 0.8

 2) The weight ratio of lemon grass / insect repellent is 0.8-1.2.

Further, in one preferred embodiment, the composition may further satisfy the following relation (3)

3) Stem repellant + lemongrass weight> Calamine + gel light weight.

In one preferred embodiment, the bug station may be a bug bug extract.

According to one preferred embodiment, 50 to 80 parts by weight of an anti-inflammatory agent, 50 to 80 parts by weight of an exfoliating agent, 50 to 80 parts by weight of an astringent agent, 50 to 80 parts by weight of an antioxidant, And 80 to 120 parts by weight of a perfume.

In one preferred embodiment, the bug extract extract may be prepared by tincture extraction.

Specifically, the tincture extraction method comprises a first step of mixing 10 to 30 parts by weight of a bug insecticide with 100 parts by weight of an alcoholic solution having a concentration of 60 to 95%; A second step of mixing 10 to 20 parts by weight of a moisturizing additive with 100 parts by weight of the alcohol solution; And a third step of aging the prepared mixture.

According to a preferred embodiment of the present invention, the moisturizing additive may include at least one selected from the group consisting of glycerin, betaine, and sorbitol.

According to a preferred embodiment of the present invention, the alcohol solution may be prepared by mixing a 90 to 100% fermented alcohol and a solvent at a weight ratio of 6: 4 to 8: 2.

According to a preferred embodiment of the present invention, the solvent may be water, but is not limited thereto.

The natural soap composition of the present invention does not contain an artificial synthetic material and is effective for eliminating folliculitis, and also has the effect of eliminating exfoliation, shrinking pores, preventing pushing of natural soap, and helping skin.

1 is a photograph of a natural soap according to an embodiment of the present invention.

Hereinafter, embodiments of the present invention will be described in detail with reference to the accompanying drawings so that those skilled in the art can easily carry out the present invention. It should be understood, however, that the embodiments are not intended to limit the scope of the present invention, which should be construed to facilitate understanding of the present invention.

As described above, the conventional natural soap is not completely saponified as compared with the general solid soap. In this case, the effective fat component remains in the natural soap, and the bacteria such as the fungus grows. Removal of pores, shrinkage of pores, skin pulling after cleansing, as well as a pressing shape of the soap outer shape during prolonged use.

Accordingly, the present invention provides a soap composition comprising an insect repellent, an anti-inflammatory agent, an exfoliation agent, an astringent agent, an antioxidant, and a perfume as an active ingredient, . Accordingly, it is possible to provide a natural soap composition and a method for producing the natural soap composition, which include a pest control station that is excellent in removing folliculitis from only natural materials by including a certain amount of a pest control station used as a natural pesticide without including an artificial synthetic substance.

Specifically, the compositions of the natural soap composition according to the present invention are described below.

First, a pest control station which is an effective component of the soap composition according to the present invention will be described.

Chrysanthemum cinerariaefolium belongs to the Asteraceae. Its perennial herbaceous stem is 15 ~ 45㎝ long. Leaves are ovate or elliptical, and are diverged like feathers. see. One flower is usually on the end of the branch, and the color of the flowers around it is white. Similar plants are red coccineum (C. coccineum), which is native to Southeast Asia, but the surrounding flowers are red rather than white. The bug bureau contains a large amount of natural insecticides, pyrethrin. Pyretrin is harmless to warm-blooded animals and livestock, but it has an insecticidal action that causes paralysis and death of the motor neurons of cold-blooded insects. The content of pyrethrin, which is an effective insecticide, is 10 ~ 20 times higher than that of flower buds, leaves and stems, and is most abundant in the full bloom period.

Here, according to the present invention, the bug station may be a bug bug extract derived from a bug bug.

In the present invention, as described above, the insect pest extract extracted from the flower part of the insecticide having excellent antimicrobial effect is contained in an amount of 0.3 to 0.7 g based on 100 g of natural soap. Preferably 0.4 to 0.6 g, and more preferably 0.5 g. In this case, when the extract is less than 0.3 g, it may be difficult to effectively remove the phytopathogenic fungus due to insufficient content. When the extract is more than 0.7 g, the soap may be decomposed and bubbles may not be produced.

The anti-inflammatory agent which is an active ingredient of the soap composition according to the present invention will be described.

An anti-inflammatory agent acts to eliminate the inflammation source, reduce the vital reaction and symptom to lose inflammation. In general, the indomethacin used as an anti-inflammatory agent is a substance which can not be used in cosmetics. The amount of hydrocotisin is limited. The licorice acid and its derivatives are difficult to stabilize or have poor solubility, There is a problem that it is difficult to achieve the effect, and the known anti-inflammatory agents have problems in terms of skin safety and stability in mixing cosmetics, and their use is limited. Therefore, it is possible to inhibit the production of NO effectively and without any side-effect or cytotoxic effect with a natural-substance-derived substance, so that the anti-inflammatory effect is excellent, and the inflammation can be suppressed without any side effects. Materials that can be used in cosmetics are needed.

Therefore, according to the present invention, the anti-inflammatory agent may include at least one selected from the group consisting of gelite, calamine, castor oil and lemon grass. Preferably a chalamin or gelite, and more preferably a chalamin.

This calamine is a light pink powder mixed with zinc oxide (iron oxide) and iron oxide. Calamine powder evaporates water quickly and exerts cooling effect, absorbs secretion and dries the surface, and relieves inflammation. , It absorbs dirt and oil due to inflammation of the skin and prevents secondary infection and trouble. It is also effective in disinfecting and cooling to sink heat. Calamine is used as a raw material for quasi-drugs, and is effective for inflammation, itching, eczema and the like and is generally applied to lotion-type quasi-drugs. These calamins were classified as medicines before the revision of Notification No. 2007-48 of the Ministry of Health and Welfare, but their efficacy and safety were proved, and the lotion containing calamine was classified as quasi-drugs according to the quasi-drug specification rule. Calamine lotions, commonly marketed as quasi-commercial products, are used to relieve the symptoms of sunburn, eczema, rashes, urticaria, poisoning by plants, chickenpox and insect bites

According to the present invention, the calamine may be contained in an amount of 50 to 80 parts by weight based on 100 parts by weight of the extract. Preferably 55 to 75 parts by weight, and more preferably 60 to 70 parts by weight. At this time, if the calamine content is less than 50 parts by weight, the anti-inflammatory ability may be deteriorated. If the calamine content is 80 parts by weight or more, there is a problem that the soap becomes very hard and foaming is difficult.

The exfoliating agent which is an effective component of the soap composition according to the present invention will be described.

An exfoliant is generally a method of removing the exfoliation of the skin. It is a method of chemically dissolving the exfoliation or shortening the turnover period and physically peeling it. However, sometimes the exfoliant has too high a hardness, the surface is uneven, and the skin often has fine scratches on the skin. Therefore, there is a need for an exfoliating agent having a natural scrub function which is superior in skin stability because it effectively removes keratin and does not harm skin moisture, compared to keratin removal using scrub particles or acid.

Therefore, according to the present invention, the exfoliant may include at least one selected from the group consisting of papaya enzyme, gelite and white clay. Preferably gelite or white clay, and more preferably gelite.

The Geltite is a natural minerals mineralized by the deposition of volcanic ash produced as a result of the volcanic activity of the peninsula during the Mesozoic Cretaceous period 65 million years ago. GELITE has a germanium content of 2.0 ppm and contains a large amount of far-infrared rays and anions, and shows a content of components other than the generally known pozzolans. GELITE is an eco-friendly material minerals which has 187 times of ingredient effect (germanium content, deodorization effect, sterilization, mold removal, anion, far infrared rays)

Such gelite may be contained in an amount of 50 to 80 parts by weight based on 100 parts by weight of the insect repellent according to the present invention. Preferably 55 to 75 parts by weight of the gelite, and more preferably 60 to 70 parts by weight of the gelite. At this time, when the gel weight is 50 parts by weight or less, it may be difficult to reduce the detergency and prevent the soap from becoming cloudy, and when the gel weight is 80 parts by weight or more, the soap may become hard as stone, There is a problem that does not work well.

The astringent agent which is an effective component of the soap composition according to the present invention will be described.

Astringent usually acts on the skin or mucous membrane to coagulate proteins to remove inflammation and protect the skin. Mainly, zinc oxide, tannic acid, etc. are used as a material for a hydroxyl group. Plant extracts from green tea and various astringents such as Witch-hazel, Hammailes, and evening primrose oil have been used as natural materials for such astringents.

According to the present invention, the astringent agent may include at least one selected from the group consisting of white clay, gelite and papaya enzymes. Preferably white clay or gelite, and more preferably white clay.

Clay is a clayey material that exists underground in uncontaminated rivers and contains silica as a main component and includes minerals such as iron, calcium, magnesium, potassium, and zinc. Clay varies in color depending on the proportion of minerals contained in it, but there are different types such as white, yellow, red, green and pink. White clay is the most mild and suitable for all skin types, especially for sensitive skin. White clay removes detoxification and sebum and tightens the pores by converging action.

Thus, according to the present invention, the white clay may be contained in an amount of 50 to 80 parts by weight based on 100 parts by weight of the insect repellent extract. Preferably 55 to 75% by weight, and more preferably 60 to 70% by weight. At this time, when the white clay is 50 parts by weight or less, it may be difficult to have skin elasticity such as a desired level of pore shrinkage. When the white clay is 80 parts by weight or more, the soap may become hard as a stone, There is a problem that does not work well.

The antioxidant which is an effective component of the soap composition according to the present invention will be described.

The antioxidant is an organic compound having a property of suppressing the action of oxygen under various conditions such as light and heat for various kinds of auto oxidizing substances and is used for the purpose of preventing deterioration due to oxidation, Butylhydroxyanilide (BHA), butylhydroxytoluene (BHT), and the like are used as materials. Natural antioxidants are natural spices, sesame extracts, tea catechin and natural α-tocopherol.

According to the present invention, the antioxidant extracted from nature may contain at least one or more selected from the group consisting of allantoin lavender and calamine. Preferably allantoin or lavender, and more preferably allantoin.

The allantoin is a natural substance extracted from places such as oat, comfrey root, sugar beet, and wheat germ. It is a non-allergenic safety product that activates cell activity either directly or indirectly.

In the present invention, the allantoin may be contained in an amount of 50 to 80 parts by weight with respect to 100 parts by weight of the extract of the insect repellent. Preferably 55 to 75% by weight, and more preferably 60 to 70% by weight. At this time, when the allantoin content is 50 parts by weight or less, skin activation may be difficult. When the allantoin content is 80 parts by weight or more, there is a problem that the soap is hard as a stone or bubble is not produced well.

The perfume which is an effective component of the soap composition according to the present invention will be described.

Spices are generally organic substances with a strong aroma added to add flavor to household products such as cosmetics and foodstuffs. They are excellent in volatility at room temperature. It is divided into natural fragrance and artificial fragrance. Natural fragrances include four kinds of animal spices such as musk, civet, ambergris, castor and flowers of oriental plants, flower buds, fruit, leaves, branches, stems, roots, And vegetable flavors such as natural resins.

According to the present invention, the perfume may include at least one selected from the group consisting of lemon grass lavender and tea tree. It may be preferably lemon grass or lavender, more preferably lemon grass.

The lemon grass is a herb that comes from the meaning of grass with a fresh smell similar to lemon. Lemongrass essential oil contains Citral, which is widely used as soap and medicine fragrance. Like lemon oil, it stimulates and refreshens (refreshes), helping to clear the mind and improve concentration. Lemon grass is also used as an insect chaser in summer with citronella.

According to the present invention, the lemon grass may be contained in an amount of 80 to 120 parts by weight with respect to 100 parts by weight of the extract of the insect repellent. Preferably 90 to 110% by weight, and more preferably 95 to 105% by weight. When the lemon grass is less than 80 parts by weight, it may be difficult to smell when using soap. When the lemon grass is more than 120 parts by weight, irritation to sensitive skin may be caused.

According to the present invention, the soap composition prepared from such compositions can satisfy all of the following relational formulas 1 to 3.

1) The weight ratio of calamine / trephine is 0.5 ~ 0.8

2) The weight ratio of lemon grass / insect repellent is 0.8 ~ 1.2

3) Stem repellant + lemongrass weight> Calamine + gel light weight.

Meanwhile, according to the present invention, it is possible to further include papaya enzyme, lavender, jojoba oil, castor oil, laurel oil and honey as effective ingredients including the above-described soap compositions.

Specifically, the compositions described above in addition to the natural soap composition according to the present invention are described below.

First, the papaya enzyme, which is a further active ingredient of the present invention, is an enzyme extracted from papaya fruit of about 20 to 40 cm. It has a special property of hydrolyzing protein, and is suitable for cleaning skin that has been accumulated on the skin for a long time.

In the present invention, the papaya enzyme may be contained in an amount of 50 to 80 parts by weight based on 100 parts by weight of the insect repellent. Preferably 60 to 75% by weight, and more preferably 65 to 73 parts by weight. At this time, when the papaya enzyme is 50 parts by weight or less, it may be difficult to exfoliate the skin, and when the papaya enzyme is 80 parts by weight or more, the soap hardens like stones or bubbles are not produced.

In addition, the active ingredient of the present invention, lavender, blooms in June-August, and lavender flowers are used as insecticides to chase pests. As such, lavender has a germicidal effect and is effective in skin regeneration and inflammation treatment.

The lavender according to the present invention may be contained in an amount of 50 to 80 parts by weight based on 100 parts by weight of the insect repellent. Preferably 55 to 75% by weight, and more preferably 60 to 70% by weight. At this time, if the amount of the lavender is less than 50 parts by weight, it may be difficult to exhibit a sterilizing effect. If the amount of the lavender is more than 80 parts by weight, the soap may not be hard like stones or bubbles may be generated.

In addition, jojoba oil, which is an active ingredient of the present invention, contains a large amount of wax components unlike other vegetable oils. While the other vegetable oil has a triglyceride structure, the jojoba oil has a wax structure which is an ester of a higher fatty acid and a higher alcohol. Jojoba oil is a liquid wax which contains more than 70% of Gadoleic acid (C20: 1) with high carbon number in double fatty acid and many Erucic acid (C22: 1) in rape oil. It is a long-lasting oil that has good thermal stability and is not easily oxidized by heating up to 285 ° C or heating at 370 ° C for 4 days. It also contains an antioxidant component which can be blended together to help extend the shelf life of other oils used and thus increase the shelf life of the soap. Especially, it has a structure similar to that of human skin, so it has good affinity for skin and it is well absorbed and sticky.

The jojoba oil according to the present invention may be contained in an amount of 150 to 250 parts by weight. Preferably from 170 to 230% by weight, and more preferably from 190 to 210% by weight. At this time, if the jojoba oil is 150 parts by weight or less, it may be difficult to prevent the oxidation of the soap. When the jojoba oil is 250 parts by weight or more, the soap may be decomposed and bubbles may not be generated.

The castor oil, which is an active ingredient according to the present invention, has a property of dissolving in alcohol, unlike other fatty oils in most of the fatty oils obtained by pressing castor seeds. Castor oil contains about 45% oil in the seeds. Seeds are toxic, but during the pressing process, the toxicity is left in the remnant residue, and the oil obtained by squeezing is not toxic. The main ingredient is ricinoleic acid and is contained as glyceride. A typical effect of ricinoleic acid is anti-inflammatory and analgesic, and is effective in eliminating germs and epidermis on the skin surface.

The castor oil according to the present invention may be contained in an amount of 150 to 250 parts by weight. Preferably from 170 to 230% by weight, and more preferably from 190 to 210% by weight. If the amount of the castor oil is less than 150 parts by weight, the antimicrobial effect may not be expected. If the amount of the castor oil is more than 250 parts by weight, the soap may be decomposed and the foam may not be produced.

In addition, the laurel oil as an effective ingredient according to the present invention contains a lot of lauric acid, so that it has excellent washing power and bubbles. In addition, it has high antimicrobial activity and is effective for acne and troublesome skin.

The laurel oil according to the present invention may be contained in an amount of 150 to 250 parts by weight. Preferably from 170 to 230% by weight, and more preferably from 190 to 210% by weight. At this time, if the laurel oil is 150 parts by weight or less, it may be difficult to obtain an expected washing power. If the laurel oil is 250 parts by weight or more, the soap may be decomposed and bubbles may not be generated.

In addition, honey as an active ingredient according to the present invention is rich in antioxidants and is effective in removing waste products. It also has anti-bacterial properties, which helps prevent and prevent acne and also acts as a natural preservative. Honey has excellent moisturizing power, which absorbs moisture on the skin and keeps it moist for a long time.

The honey according to the present invention may be contained in an amount of 500 to 700 parts by weight. Preferably from 550 to 650% by weight, and more preferably from 600 to 600% by weight. At this time, if the honey content is less than 500 parts by weight, the expected moisturizing effect may be difficult to manifest. If the honey content is more than 700 parts by weight, the soap may be decomposed and bubbles may not be formed.

50 to 80 parts by weight of the anti-inflammatory agent, 50 to 80 parts by weight of the exfoliant, 50 to 80 parts by weight of the astringent agent, 50 to 80 parts by weight of the antioxidant and 80 to 120 parts by weight of the perfume And a method for producing the soap composition.

First, a method for preparing the bug extract of the present invention will be described.

According to the present invention, the insect repellent extract is not particularly limited as long as it can be prepared through a conventional method for producing an extract, but preferably a tincture extraction method is used to simultaneously extract water-soluble and lipophilic components, And the advantage of being able to extract pure ingredients of the material without chemical modification.

Specifically, the tincture extraction method comprises a first step of mixing 10 to 30 parts by weight of a pest control station with 100 parts by weight of an alcohol solution having a concentration of 60 to 95%; A second step of mixing 10 to 20 parts by weight of a moisturizing additive with 100 parts by weight of the alcohol solution; And a third step of aging the prepared mixture.

First, in the first extraction step, 10 to 30 parts by weight of a pest control station is mixed with 100 parts by weight of an alcohol solution having a concentration of 60 to 95%.

Preferably, the alcohol solution may be ethanol. At this time, if the concentration of the alcohol solution is 95% or more, there may be a problem of irritating sensitive skin, so the above range is appropriate.

In addition, the bug bug is preferably a bug bug extract derived from a bug bug. If the bug king is less than 10 parts by weight, it is difficult to obtain the desired antimicrobial effect. If the bug body is more than 30 parts by weight, the soap may be retracted and the skin may be irritated.

Next, as the second step, 10 to 20 parts by weight of a moisturizing additive is mixed with 100 parts by weight of the alcohol solution.

The moisturizing additive is a moisturizing agent that generally helps regenerate the skin and improve the wrinkles of the skin due to the moisture control action, and protease is mainly used as a material. These proteases are collectively referred to as proteolytic enzymes having proteolytic activities such as papain and trypsin. When these substances are applied to the epidermis, they decompose proteins such as keratin, which form peel or epidermal keratin, and digestion and absorption And peptone, which is an easy nutrient, to facilitate the epidermal metabolism and normalization of the skin function, and has excellent properties as a moisturizing additive.

According to the present invention, the moisturizing additive may include at least one member selected from the group consisting of moietin, hyaluronic acid, glycerin, betaine and sorbitol. Preferably, glycerin, betaine or sorbitol may be used, May include both glycerin, betaine and sorbitol.

Here, the moisturizing additive may be prepared by mixing the glycerin, betaine, and sorbitol at a weight ratio of 1: 1: 1, respectively. If the amount of the moisturizing additive is less than 10 parts by weight with respect to 100 parts by weight of the alcohol solution, there is a problem that the expected moisturizing effect can not be obtained. When the amount is more than 20 parts by weight, Is good.

Finally, the third step may include a method of aging the prepared mixture, and a method of aging the mixture by adding a common solvent. However, there is no limitation on the particular aging method, And then kept in a shaded area at room temperature for about 10 days to 20 days in a sealed state so as not to allow air to flow.

The alcohol solution may be prepared by mixing a 90 to 100% fermented alcohol and a solvent at a weight ratio of 6: 4 to 8: 2.

Preferably, the solvent may be water but may be any solvent that can be dissolved in the fermentation alcohol, but is not limited thereto.

According to the present invention, 50 to 80 parts by weight of papaya enzyme, 50 to 80 parts by weight of lavender, 150 to 250 parts by weight of jojoba oil, 150 to 250 parts by weight of castor oil, 250 parts by weight of laurel oil, 150 to 250 parts by weight of laurel oil, and 500 to 700 parts by weight of honey.

Hereinafter, exemplary embodiments of the present invention will be described in order to facilitate understanding of the present invention. However, the following examples are intended to aid understanding of the present invention, and the present invention is not limited by the following experimental examples.

[Preparation Example] Preparation of extract

After mixing 95% fermented liquor and purified water at a weight ratio of 7: 3, 20% by weight of the total solution is added to the pest control station and 5% by weight of glycerin, betaine and sorbitol are added, respectively. Thereafter, the prepared mixture is sealed, aged in a cool place for about 15 days, and then the aged mixture is filtered through a filter paper to extract pure liquid to prepare a pest control extract.

[Example] Preparation of natural soap containing insect repellent extract

≪ Example 1 >

First, natural soap (100 g) was prepared using the pest control extract prepared in the preparation example. First, a fatty acid purified from palm oil and coconut oil was saponified to prepare a weakly alkaline soap base After the preparation, 91 g of a liquid soap base was prepared by dissolving in a hot plate.

On the other hand, as shown in the following Table 1, 0.33 g of calamine powder, 0.33 g of allantoin powder, 0.35 g of papaya enzyme powder, 0.33 g of lavender powder, (0.33 g) and white clay powder (0.33 g) were mixed in the same ratio of 1: 1: 1: 1: 1: 1, respectively, and 2 g of the blended powder was weighed. Further, 3 g of blending oil prepared by mixing 1 g of jojoba oil, 1 g of castor oil (1 g) and laurel oil (1 g) in an equal ratio of 1: 1: 1, respectively, and 3 g of honey were further added to the glass beaker. Then, 15 drops of lemon grass essential oil and 15 drops of the insect repellent extract prepared in the preparation example were added.

Then, all the additives were weighed in the glass beaker, stirred until the blending powder was completely dissolved, and then mixed with the soap base in a liquid state dissolved in a hot plate and further stirred. At this time, the final mixture was prepared by filtering 3-4 times so that no solid matter remained in the glass beaker.

Finally, ethanol was injected into the silicon mold of the desired shape, and the prepared final mixture was injected. The foams generated in this process were further removed by spraying ethanol, and then cured at room temperature for about 40 minutes to obtain natural Soaps were prepared.

≪ Examples 2 to 5 >

Natural soap was prepared in the same manner as in Example 1, except that the composition ratio of the insect repellent station was changed as shown in Table 1 below.

≪ Examples 6 to 10 &

Natural soaps were prepared in the same manner as in Example 1, except that the composition was changed as shown in Table 1 below.

≪ Example 11 >

Natural soap was prepared in the same manner as in Example 1, except that the method of extracting the insect pest extract was changed as shown in Table 1 below.

Kinds Example (g) One 2 3 4 5 6 7 8 9 10 11 Soap base 91 91 91 91 91 91 91 91 91 91 91 Bug land 0.5 0.45 0.65 0.27 0.85 0.5 0.5 0.5 0.5 0.5 0.5 Calamine powder 0.33 0.33 0.33 0.33 0.33 0.22 0.33 0.33 0.33 0.33 0.33 Gel light 0.33 0.33 0.33 0.33 0.33 0.33 0.21 0.33 0.33 0.33 0.33 White clay 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.19 0.33 0.33 0.33 Allantoin 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.27 0.33 0.33 Lemon grass 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.73 0.5 Papaya enzyme 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.35 Lavender Powder 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 0.33 Jojoba oil One One One One One One One One One One One Palm oil One One One One One One One One One One One Laurel oil One One One One One One One One One One One honey 3 3 3 3 3 3 3 3 3 3 3 Extraction method Tincture Tincture Tincture Tincture Tincture Tincture Tincture Tincture Tincture Tincture Other Total: 100 (g)

(Other: freeze-dried flowers of the bug bug, and then pulverized to a size of 0.1 mm to 0.5 mm to prepare 0.33 g of powder to make a soap)

 [Comparative Example]

≪ Comparative Example 1 &

A natural soap containing a pest control extract was prepared in the same manner as in Example 1, except that chrysanthemum was used instead of a pest control station as shown in Table 1 below.

≪ Comparative Examples 2 to 6 >

A natural soap containing a pest control extract was prepared in the same manner as in Example 1, except that the composition was changed as shown in Table 2 below.

division Comparative Example (g) One 2 3 4 5 6 Natural soap
Composition type Soap base Soap base Soap base Soap base Soap base Soap base Chrysanthemum extract Bug land Bug land Bug land Bug land Bug land Calamine powder - Calamine powder Calamine powder Calamine powder Calamine powder Gel light Gel light - Gel light Gel light Gel light White clay White clay White clay - White clay White clay Allantoin Allantoin Allantoin Allantoin - Allantoin Lemon grass Lemon grass Lemon grass Lemon grass Lemon grass - Papaya enzyme Papaya enzyme Papaya enzyme Papaya enzyme Papaya enzyme Papaya enzyme Lavender Powder Lavender Powder Lavender Powder Lavender Powder Lavender Powder Lavender Powder Jojoba oil Jojoba oil Jojoba oil Jojoba oil Jojoba oil Jojoba oil Palm oil Palm oil Palm oil Palm oil Palm oil Palm oil Laurel oil Laurel oil Laurel oil Laurel oil Laurel oil Laurel oil honey honey honey honey honey honey

[Experimental Example]

1. Usability evaluation (detergency and exfoliation power)

Using the natural soap prepared in Examples 1 to 11 and Comparative Examples 1 to 6, the cleaning power and exfoliation power of the natural soap were evaluated in 30 women aged 25 to 50 years. The results are shown in Table 3 below . (Washing power, exfoliation power 5 points scale)

division Example Comparative Example One 2 3 4 5 6 7 8 9 10 11 One 2 3 4 5 6 Cleaning power 4.54 4.35 4.55 4.43 4.57 4.36 3.02 4.23 4.78 4.02 4.54 4.21 4.75 4.05 4.53 4.07 4.51 Exfoliation power 3.68 3.58 3.48 3.51 3.35 3.25 2.06 3.66 3.32 3.43 3.08 3.65 3.31 3.42 3.67 3.42 3.65

As shown in Table 3, in contrast to Example 1, Comparative Example 1 which does not include a pest control station even though the pest control station is included, and Comparative Example 2 to Comparative Example 6 that does not include any one of the natural soap compositions, And the exfoliation power was decreased. Particularly, in the case of Comparative Example 2 and Comparative Example 3 in which calamine and gelite were omitted, it was confirmed that the detergency and exfoliation power were further reduced.

2. Measurement of skin aesthetic effect

The skin cosmetic effects of the natural soaps prepared in Examples 1 to 11 and Comparative Examples 1 to 6 were clinically measured.

A total of 56 Korean women aged 28-32 years who were interested in skin health were selected and the following tests were conducted. 56 women were treated for 5 weeks. In order to reduce errors caused by the habit between the subjects, the standard method of washing was designated and cleansed three times a day. After 5 weeks, skin health was checked by measuring skin moisture and skin elasticity, and skin moisturizers and skin protectants were not used at all.

Skin moisture content was measured by using a corneometer to measure changes in skin moisture before and after use of a human body cleanser. Skin elasticity was measured using a cutometer to measure skin elasticity before and after use of a human body cleanser Table 4 shows the results.

division Example One 2 3 4 5 6 7 8 9 10 11 Skin moisture content Before use 78 78.5 79.6 78.6 77.9 79.5 78.4 77.2 78.1 79.4 78.6 5 weeks
after use 85.9 82.6 85.7 81.08 84.5 82.6 81.2 71.4 82.6 83.4 83.9 Skin elasticity Before use 0.82 0.88 0.85 0.87 0.86 0.84 0.81 0.87 0.88 0.82 0.79 5 weeks
after use 0.81 0.80 0.83 0.88 0.86 0.79 0.83 0.35 0.81 0.83 0.73 division Comparative Example One 2 3 4 5 6 Skin moisture content Before use 78.6 77.9 79.5 78.4 79.4 78.6 5 weeks
after use 77.5 76.4 77.9 73.5 75.4 74.2 Skin elasticity Before use 0.88 0.78 0.87 0.86 0.84 0.81 5 weeks
after use 0.74 0.71 0.75 0.45 0.77 0.79

As shown in Table 4, in comparison with Example 1, in Comparative Example 1 which does not include a pest control station and Comparative Examples 2 to 6 which does not include any of the natural soap compositions, the skin moisture content and skin elasticity And it was confirmed that it fell. In particular, in the case of Comparative Example 4 in which white clay was not added, it was found that the skin moisture content and skin elasticity were reduced.

3. Evaluation of antibacterial ability

Antimicrobial activity tests were conducted to confirm the antibacterial effects of the natural soaps prepared in Examples 1 to 11 and Comparative Examples 1 to 6.

The test for antibacterial activity is described in L. J. Vinson et al., "J, Pharm. Sci. , 50,827-830, 1961, and the degree of incubation with the strains shown in Table 4 was graded in five stages from 0 (no inhibition of growth) to 4 (complete inhibition of growth) Table 5 shows the results.

Test strain Example One 2 3 4 5 6 7 8 9 10 11 S. Aureus 4 3 4 2 4 3 3 4 3 4 4 E. coli 4 4 4 2 4 4 2 3 4 3 4 P.aeruginosa 4 3 4 3 4 4 3 4 4 3 3 C.albicans 4 3 4 2 4 3 2 3 4 3 3 K.kneumoniae 4 4 4 2 4 3 3 4 3 4 3 Test strain Comparative Example One 2 3 4 5 6 S. Aureus One 3 4 4 3 4 E. coli 2 3 3 4 4 3 P.aeruginosa One 3 3 3 4 4 C.albicans One 4 3 3 4 4 K.kneumoniae One 3 3 3 3 3

As shown in Table 5, in the case of Example 2 in which the pest control station contained 5 g or less, the pest control station had antibacterial ability It is possible to confirm that it is somewhat reduced. In addition, the antibacterial ability of Example 4 was significantly reduced as compared with that of Example 1, and the antimicrobial ability was substantially the same as that of Example 1 when the insect repellent containing 0.7 g or more was obtained through Example 5. In addition, it was confirmed that the antibacterial ability was slightly lower in Examples 6 to 10 in which the content of each composition was less than that in Example 1.

In addition, it was confirmed that the antibacterial ability of Comparative Example 1 was decreased as compared with that of Example 1, and the antibacterial ability was further improved when the extracting country and the calamine were used simultaneously as in Example 1 .

4. Assessment of the inhibitory effect on survival

The antimicrobial activity tests were conducted to confirm the effect of suppressing the survival of shrubs in the natural soaps prepared in Examples 1 to 11 and Comparative Examples 1 to 6, and the results are shown in Table 6 below.

Attach the electron microscope to the CCD camera and connect it to the computer. After removing the sample from the hair follicle by using a blade, the sample was dropped on a slide glass, and the reagent required for the destruction of the follicle was dropped under the three electron microscopes. The cover glass was set at a right angle, Observe the movement of the legs. At this time, the electron microscope observes the external shape of the folliculitis using a low magnification, observes the detail at increasingly high magnification, confirms the time, and measures the survival time. In the experiment, the survival time means that the body of the folliculitis changes gradually from the time when the sample is dropped, to the time when the follicle body is crumbled and the movement is finished.

division Example One 2 3 4 5 6 7 8 9 10 11 Shovel survival time 13m45s 14m15s 13m54s 30m54s 13m33s 15m25s 14m05s 13m89s 13m78s 13m62s 14m92s Comparative Example One 2 3 4 5 6 Shovel survival time 34m42 15m02s 13m89s 13m51s 13m42s 14m12s

As can be seen from the above Table 6, in the case of Example 2 containing 0.45 g of insect repellent as compared with Example 1, the survival time of the insecticidal insecticide slightly increased and in the case of Example 4 containing 0.27 g of insect repellent It was confirmed that the survival time of the fungus larvae was greatly increased. In comparison with Example 1, the survival time of the phytopathogenic fungus was slightly increased in Example 6, which is presumably due to the fact that the anti-inflammatory effect was somewhat reduced by the addition of 0.26 g of calamine, .

In addition, in the case of using the extract of chrysanthemum in Comparative Example 1, it was confirmed that the survival time of the fungus larvae was greatly increased as compared with Example 1.

5. Evaluation of pore shrinkage

To examine the pore-shrinking effect of the natural soap prepared in Examples 1 to 11 and Comparative Examples 1 to 6, ten male and female subjects were selected and subjected to a pore shrinkage evaluation test. The results are shown in Table 7 below .

The paired t-test method of SPSS program package 11.5 was used as the analysis method used to analyze the difference between the two groups.

division Example One 2 3 4 5 6 7 8 9 10 11 Area of pores Before use 40.70 40.80 40.70 41.50 40.20 40.60 40.70 40.80 40.20 40.30 after use 33.80 33.60 33.40 36.50 33.30 35.20 32.10 37.20 33.70 33.30 Number of pores Before use 336.40 335.30 339.10 336.30 334.20 338.20 337.20 337.10 337.10 336.80 after use 312.60 310.90 312.40 319.50 313.10 319.70 311.10 323.70 312.10 312.60 Comparative Example One 2 3 4 5 6 Area of pores Before use 40.10 40.50 40.20 40.20 40.10 40.90 after use 33.70 33.60 33.40 38.75 32.10 32.20 Number of pores Before use 336.40 336.04 335.47 338.6 337.4 339.6 after use 312.20 312.60 313.50 329.4 313.10 312.60

As can be seen from Table 7, in Example 8, the pore shrinkage degree was estimated to be greatly reduced as compared with that in Example 1, with the white clay being less in composition ratio. However, It is considered that the addition of the minerals increases the removal of the phos- phorus and the anti-inflammatory effect, and consequently contributes to the improvement of the pore shrinkage.

6. Evaluation after cleansing

To determine the feeling of use of the natural soap prepared in Examples 1 to 11 and Comparative Examples 1 to 6, 10 persons were selected for each of the subjects and the degree of skin pulling, refreshing feeling and soapiness were evaluated, Table 8 shows the results. (Based on 5 points)

division Example One 2 3 4 5 6 7 8 9 10 11 Skin pull 5 5 5 4 5 5 4 5 5 5 4 Refreshing feeling 5 5 5 4 4 4 4 4 3 4 4 Soap incense 5 4 4 5 3 5 4 5 4 4 3 division Comparative Example One 2 3 4 5 6 Skin pull 3 2 3 4 3 3 Refreshing feeling 3 4 4 3 4 3 Soap incense 3 2 3 3 3 2

As can be seen in Table 8, in contrast to Example 1, in the case of Comparative Example 1, which does not contain a bug bug, and Comparative Example 2 to Comparative Example 6, which does not include any of the natural soap compositions, The feeling of use was evaluated low. Particularly, Comparative Example 2 in which no calamine was added showed high skin pulling, and Comparative Example 6 in which no lemon grass was added was evaluated to have the lowest soap flavor.

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that the invention is not limited to the disclosed exemplary embodiments. It will be apparent to those skilled in the art that the present invention, Various modifications and variations are possible.

Claims (12)

60 to 70 parts by weight of calamine, 60 to 70 parts by weight of gelite, 60 to 70 parts by weight of white clay, 60 to 70 parts by weight of allantoin, 95 to 105 parts by weight of lemon glass, 50 to 100 parts by weight of papaya enzyme 50 Wherein the composition comprises 50 to 80 parts by weight of lavender, 150 to 250 parts by weight of jojoba oil, 150 to 250 parts by weight of castor oil, 150 to 250 parts by weight of laurel oil and 500 to 700 parts by weight of honey. .
delete delete delete delete delete delete 60 to 70 parts by weight of calamine, 60 to 70 parts by weight of gelite, 60 to 70 parts by weight of white clay, 60 to 70 parts by weight of allantoin, 95 to 105 parts by weight of lemon glass, 50 to 100 parts by weight of papaya enzyme 50 To 50 parts by weight of lavender, 150 to 250 parts by weight of jojoba oil, 150 to 250 parts by weight of castor oil, 150 to 250 parts by weight of laurel water, and 500 to 700 parts by weight of honey. ≪ / RTI >
9. The method of claim 8, wherein the bug extract extract is prepared by a tincture extraction method.
10. The method of claim 9,
In the tincture extraction method,
Mixing 10 to 30 parts by weight of the insecticide with 100 parts by weight of an alcoholic solution having a concentration of 60 to 95%;
A second step of mixing 10 to 20 parts by weight of a moisturizing additive with 100 parts by weight of the alcohol solution; And
And a third step of aging the prepared mixture.
11. The method of claim 10, wherein the moisturizing additive comprises at least one member selected from the group consisting of glycerin, betaine, and sorbitol.
The method of claim 10, wherein the alcohol solution is prepared by mixing 90 to 100% fermented alcohol and a solvent at a weight ratio of 6: 4 to 8: 2.

Images