CN104997644B - A kind of dual-purpose oil-control spraying of hair skin - Google Patents
A kind of dual-purpose oil-control spraying of hair skin Download PDFInfo
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Abstract
A kind of dual-purpose oil-control spraying of hair skin, it is composed of the following components：(A) the oil-control compounding powder agent of composition weight 2.65% to 12% is accounted for, (B) accounts for the suspension thickener bentonite of composition weight 0.1 5.0%；(C) at least one of 1,2 propylene glycol of cool feeling agent () peppermint oxygroup, () menthone glycerol acetal, () menthyl lactate of composition weight 0.5 2.0% are accounted for；(D) ethyl alcohol of composition weight 2.0 10% is accounted for；(E) surplus is cosmetically acceptable carrier.Oil-control composition application in the form of suspending agent type spray product of the present invention, oil-control composition of the invention have the oil-control effect to work immediately.
Description
Technical field
The present invention relates to a kind of dual-purpose oil-control composition of hair skin, more particularly to the floating type oil-control of a kind of quick acting is sprayed
Mist.
Background technology
Matter of utmost importance, that is, the fat secretion for perplexing Oily consumer is superfluous, shows as that skin is glossy, coarse and acne.
And sebum secretion surplus also usually makes that scalp is greasy, itches, the greasy peculiar smell of hair, or even the root as dandruff and alopecia problem
Source also results in the problem of body odour exception waits " upsetting orders of life ".Therefore " oil-control " effect becomes one weight of personal care articles
The effect of wanting.Face cleaning cream, shower cream, shampoo and facial mask, the toner declared in the market with " oil-control ", though can be consumer
There is provided to a certain degree, the oil-control nursing role of certain timeliness, but still cannot meet most Oilys when hot summer
The salubrious demand of consumer's whole day.Moreover, modern life rhythm is accelerated, social activity is more frequent, therefore, it is necessary to develop one
It kind can quickly eliminate glossy, keep salubrious convenient product to meet the possible period of want or need of consumer.
Invention content
The object of the present invention is to provide a kind of oil-control sprayings of the hair dual-purpose quick acting of skin.
The object of the present invention is achieved like this：
A kind of dual-purpose oil-control spraying of hair skin, it is composed of the following components：
(A) the oil-control compounding powder agent of composition weight 2.65% to 12% is accounted for, the group of the compounding powder agent is divided into：
(I) accounts for the porous type oil suction particle of composition weight 2.0-5.0%；
(II) accounts for the modified tapioca starch of composition weight 0.5-5.0%；
(III) accounts for the zinc pyrrolidone carboxylate of composition weight 0.1-1.0%；
(IV) accounts for the pepo extract of composition weight 0.05-1.0%；
(B) the suspension thickener of composition weight 0.1-5.0% is accounted for；
(C) the cool feeling agent of composition weight 0.5-2.0 is accounted for；
(D) ethyl alcohol of composition weight 0-10% is accounted for；
(E) surplus is cosmetically acceptable carrier.
Technical scheme of the present invention further includes：
Porous type oil absorbent of the present invention is in spherical cellulose acetate or porous type methyl methacrylate microsphere
At least one.
Spherical cellulose acetate selected by the present invention is made of cellulose acetate, degree of acetylation 58-60%, average
Grain size is 6-10 microns, oil factor 2.0-3.0ml/g；The porous type methyl methacrylate microsphere is methacrylic acid
Methacrylate polymer, average grain diameter are 8 microns, oil factor 1.2-2.4ml/g.
The modified tapioca starch is poly methyl silsesquioxane oil modification tapioca.
Effective Zn content of the zinc pyrrolidone carboxylate is 19.4-21.3%.
Suspension thickener is at least one of bentonite, xanthan gum, carbomer in the present invention.Preferable scheme, which suspends, to be increased
Thick dose of selection bentonite, and bentonite is water-soluble bentonite, layer structure contains the charge less than 0.9 unit per lattice.
Cool feeling agent of the present invention is (-)-peppermint Oxy-1,2- propylene glycol, (-)-menthone glycerol acetal, (-) lactic acid
At least one of menthyl ester.
Beneficial effects of the present invention：Thick and disorderly powder on the market is the oil-control product of professional hairdressing, but operates with inconvenience,
And it is unsuitable for the large-scale production of traditional daily chemical industry.Antihidrotic spray is due to its emphractic hidroschesis principle, it is impossible to be used in
Scalp and facial-care, and can not achieve and eliminate glossy effect at once.Therefore, the invention is intended to overcome the disadvantage of the said goods
The oil-control spraying of not grease-contained suspension formula system is prepared using efficient, non-stimulated porous type oil suction raw material in end.Again
Person, compared with traditional oil-control shampoo, shower cream, face cleaning product, oil-control spraying of the present invention is disposable product, both can be direct
Hair (including scalp) can be directly applied to by being applied to skin (including face) also, easy to use.The oil-control spraying of the present invention
Most outstanding advantages are the oil-control effect of its quick acting, and greasy feeling can be eliminated in 10 minutes, eliminate glossy and white without rising
Phenomenon.
Description of the drawings
Attached drawing 1 is that light transmission value reading of the SEBUMETER method test oil-control nebulised samples I-Ⅹ in 0-12 hours is average
Value, the reading smaller display oil-control effect of average value are better.
Specific implementation mode
The present invention is discussed further with reference to embodiment：
The porous type oil absorbent that the present invention selects is spherical cellulose acetate and porous type methyl methacrylate microsphere
At least one of.
The spherical cellulose acetate that the present invention selects is made of cellulose acetate, degree of acetylation 58-60%, average
Grain size is 6-10 microns, oil factor 2.0-3.0ml/g.The spherical shape cellulose acetate structural formula such as following formula I, wherein R are second
The ratio of acyl group is 58-60%.
The spherical cellulose acetate that the present invention selects is that white arrives off-white color spherical shape fine granular.There are following characteristics：High object
Manage intensity, highly porous, high-specific surface area；Safe and non-toxic and low stimulation, water, oil are compatible.It can also be used for making emulsification cosmetic
With facial treatment milk without will produce particle from caking, stability and keeping quality are good.Spherical cellulose acetate class oil absorbent is more fine than spherical
The large specific surface area for tieing up element, can absorb the grease of 2-3 times of own wt.Spherical cellulose acetate is microporous spherical acetic acid
Cellulose solution pearl, then it is dispersed into spherical liquid by the way that cellulose acetate dissolving is obtained in organic solvent.
Its feature includes soft-touch, low skin irritability and good gas permeability.
The porous type methyl methacrylate microsphere that the present invention selects is methylmethacrylate polymer, average grain diameter
It is 8 microns, oil factor 1.2-2.4ml/g；It is preferred that 1.7-2.4ml/g.The porous type methyl methacrylate microsphere category
It in one kind of methyl methacrylate cross-linked polymer, is made of methyl methacrylate monomer, structural formula such as following formula II.
The porous type methyl methacrylate microsphere selective absorbing grease that the present invention selects, dispersibility are better than silicon
Powder, polyurethane, nylon-type adsorbent disperse 10% porous type methyl methacrylate microsphere in 10% ethanol solution
Do not assemble in 3 months, can be used for making emulsification cosmetic and spraying, is particularly suitable for before shaking up class product.The porous type first
Base methyl acrylate microsphere can for Sunjin Chemical SUNPMMA-COCO130, SUNPMMA-COCO170,
SUNPMMA-P、 SUNPMMA-PH；It is preferred that SUNPMMA-P, SUNPMMA-PH.
The zinc pyrrolidone carboxylate that the present invention selects is white to yellow powder, and chemical name is Bis (5-oxo-L-
Prolinato-N1, O2) Zinc, INCI title PCAZn, chemical structural formula is formula III.
The zinc pyrrolidone carboxylate that the present invention selects, effective Zn content are 19.4-21.3% (in terms of anhydrous product), can be had
Effect inhibits the release of 5α-reductase, to adjust sebum secretion, inhibits propionibacterium acnes, fatty oxydasis, free acid, from
And reaches oil-control, reduces the multiple effect for stimulating inflammation of releiving.
The modified tapioca starch that the present invention selects, the entitled tapiocas of INCI (and) polymethylsilsesquioxane
Tapioca Starch (and) Polymethylsilsesquioxane appearances are white to beige white powder, no aluminium innovation wood
Sweet potato starch is compatible with, and softness, powdery sense are strong, can improve the skin sense of various types of cosmetics；Especially having reduces oil
Soapy feeling is eliminated glossy；Do not whiten on the skin, the easily dispersible advantage in cold water.In addition, it can be effectively reduced formula
Cost.The modified tapioca starch can be Akzo Nobel'sTS and DRY-FLO TS PURE.
The pepo extract that the present invention selects, the entitled Cucurbita pepo extract. Summer of INCI
Squash, Pattypan Squash, Field Pumpkin, for yellow to brown color fine powder；The pepo extraction
Object is 10:1-20:1 alcohol extracting thing crosses 120 mesh sieve, adjusting fat secretion is played in oil-control compound, restrains pore, disappear
Scorching and antibacterial is a kind of to multiple efficacies.
Suspension thickener bentonite of the present invention, also referred to as volcanic clay, silicon bentonite are natural hydrated aluminium silicate
(Al2O3.4(SiO2).H2O), sallow or milky superfine powder, a diameter of 1~150 μm, wherein often containing quartz, feldspar, in vain
The mineral such as marble, calcite, it is not soluble in water or sour, but expand in water, about 10 times of volume increase, form high viscosity and have thixotroping
Property and pseudoplastic gel.Using the thixotropy of thixotrope, the i.e. property of gel and colloidal sol isothermal transformation, when standing, forms gel
Prevent particle from settling, when shaking becomes colloidal sol and is conducive to pour out.There are certain sun for the layer structure formed due to bentonite structure cell
Ion, such as Cu2+、Mg2+、Na+、K+Deng the fewer inter-layer bonding force of amount of ions is smaller, the easier expansion of bentonite, therefore does
Suspension thickener selects the bentonite of low cation or anionic charge, preferably each structure cell charge to be less than the swelling of 0.9 unit
Soil.Be conducive to the stabilization of suspending system using swelling great soil group thixotropy suspension thickener.There is described bentonite itself convergence to make
With the oil-control effect of formula system can be promoted.The suspension thickener dosage is to realize formula system viscosity for 2000-
10000cps is preferred.
The cool feeling agent that the present invention selects is (-)-peppermint Oxy-1,2- propylene glycol, (-)-menthone glycerol acetal, (-)-breast
One kind in sour menthyl ester.
(-)-peppermint Oxy-1 that the present invention selects, 2- propylene glycol, by two kinds of optical isomerisms of 2R (formula IV) and 2S (formula V)
Body, the wherein intensity of 2S ratio 2R are 2-3 times big, 1.5-2 multiples stronger than the isomers of racemization.(-)-peppermint Oxy-1,2- third
Glycol is takasago coolant agent 10 (coolant agent 10), its threshold values is 1ppm, is menthol 20%-100%, and (-)-is thin
Lotus Oxy-1, the cold air intensity of 2- propylene glycol are 2-2.5 times of menthol.
(-)-menthone glycerol acetal that the present invention selects, is levo form (VI), also known as 6- isopropyls -9- methyl-1s,
4- dioxies spiral shell (4,5)-decane -2- methanol；L-9- methyl -6- (1- Methylethyls) -1,4- dioxies spiral shell (4,5)-decane -2- first
Alcohol, 5~10mg/kg concentration can feel that the cool sense of taste gradually increased is felt in oral cavity；10% concentration does not have the gas of menthol
Taste.(-)-menthone glycerol acetal is water solubility, can be the FRESCOLAT MGA of the fragrant company of moral.
(-)-menthyl lactate that the present invention selects is levo form (formula VII), also known as 2 hydroxy propanoic acid -5- methyl -2-
Isopropyl cyclohexyl), lactic acid Meng ester, (-)-menthanol lactic acid ester, 2 hydroxy propanoic acid -5- methyl -2- isopropyl cyclohexyls, be
A kind of peppermint derivative；There is slight peppermint fragrance, taste almost without taste, but with lasting, it is pleasant clear
Cool effect can be the FRESCOLAT ML of the fragrant company of moral.
The cool feeling agent that the present invention selects plays antipruritic part, analgesic, refrigerant effect, is used in oil-control composition of the present invention cool
The effect of sense agent also resides in the cold receptor on the stimulation skin of cool feeling agent transmission, though do not lead to actual temperature change, human body life
Slight chill in the air is produced in reason, be transmitted to brain cool feeling information can cause nervous system feed back inhibition sweat gland, smegma signal,
Therefore it can enhance oil-control effect.In the oil-control spray composite of the present invention, other cosmetically acceptable carriers further include fitting
Measure essence, preservative, chelating agent, antioxidant, astringent etc..The preferred methyl p-hydroxybenzoate of the preservative, para hydroxybenzene
Propyl formate etc., the preferred disodium ethylene diamine tetraacetate of chelating agent, the antioxidant is di-tert-butyl p-cresol, the receipts
Hold back the preferred polymeric aluminum chloride of agent.
The oil-control composition of the present invention is milky white to translucent liquid product, can be used with Sprayable.Institute of the present invention
It is liquid that state spraying, which refer under room temperature, passes through the auto spraying dress containing propellant for commonly holding pump spray or routine
It sets, content can be administered on subject matter using finger pressure mode.Solid particle in the spraying must reach sufficiently small
Grain size when using conventional spraying device, nozzle can be reached by conduit in 0.05-50 micron ranges.
Here is the non-limiting example of the dual-purpose oil-control spraying of hair skin of the present invention.These embodiments be only given for
The purpose of explanation, can not be interpreted as limitation of the invention, because on the basis for not departing from the spirit and scope of the present invention
On, many changes can be carried out to the present invention.In these embodiments, unless stated otherwise, all concentration is all weight hundred
Divide ratio.
Prepare embodiment I-Ⅹ
The oil-control spray composite of the present invention can be by any known or other effective suitable for providing spraying combination
Prepared by the technology of object, the method for preparing the oil-control spray composite of the present invention includes conventional preparation and hybrid technology.Suitably
The method for preparing spray composite described in embodiment I-Ⅹ is as follows：Suitable quantity of water is added in retort, efficient oil-control is added
Compound powder, is dispersed with stirring；Then suspension thickener is added, is sufficiently stirred dispersion, adjusts suitable for viscosity；It is dissolved with ethyl alcohol fragrant
It is added in aforementioned mixture, stirs after essence, cool feeling agent.
Embodiment I-V
Embodiment VI-Ⅹ
Optimum embodiment of the present invention：
Efficacy assessments embodiment
Efficacy assessments are using universally acknowledged in the worldThe method that method and sensory evaluation are combined.Method, it is to be based on photometer principle, a kind of special delustring adhesive tape absorption oil on human skin of 0.1mm thickness
After fat, a kind of translucent adhesive tape will be become, its light transmission capacity will change, and the grease of absorption is more, and light transmission capacity is just
It can be bigger.
Preparation embodiment I-Ⅹ is issued 30 Oilys (light transmittance is more than 70) tester to try out.Sample is applied respectively
For the facial blocks T and head close to scalp portion；Unified outdoor sports in 30 minutes are carried out before on probation, then in 23 ± 2 DEG C of constant temperature,
Relative humidity is maintained at the test of rooms 50 ± 10%.It uses within (0 minute) before useSM815 tests background, uses
10 minutes afterwards, 30 minutes, 1 hour, 6 hours and 12 hours measure transparency value respectively, its average reading value is taken to draw oil-control effect
Fruit curve (Fig. 1).Wherein data result average value ＜ 50 is that oil-control effect is extremely notable；Average value 50-70 is oil-control significant effect；
Average value ＞ 70 is not notable for no oil-control effect or oil-control effect.Sensory evaluation is that trier's instrument test voluntarily gives a mark simultaneously,
It is oil-control significant effect that 0-1, which divides for no oil-control effect or oil-control effect be not notable, 1-2 divides, and 2-3 points extremely show for oil-control effect
It writes；Its appraisal result average score after ten minutes on probation close with instrument test is 1.6, that is, tries out the oil-control spraying of the present invention,
Mitigation greasy feeling can significantly be experienced within 10 minutes.
Claims (3)
1. a kind of dual-purpose oil-control spraying of hair skin, composed of the following components：
(A) the oil-control compounding powder agent of composition weight 2.65% to 12% is accounted for, the group of the compounding powder agent is divided into：
(I) accounts for the porous type oil suction particle of composition weight 2.0-5.0%；
(II) accounts for the modified tapioca starch of composition weight 0.5-5.0%；
(III) accounts for the zinc pyrrolidone carboxylate of composition weight 0.1-1.0%；
(IV) accounts for the pepo extract dry powder of composition weight 0.05-1.0%；
(B) the suspension thickener bentonite of composition weight 0.1-5.0% is accounted for；
(C) cool feeling agent (-)-peppermint Oxy-1 of composition weight 0.5-2.0%, 2- propylene glycol, the contracting of (-)-menthone glycerin are accounted for
At least one of aldehyde, (-)-menthyl lactate；
(D) ethyl alcohol of composition weight 2-10% is accounted for；
(E) surplus is cosmetically acceptable carrier；
Wherein porous type oil suction particle is at least one of spherical cellulose acetate or porous type methyl methacrylate microsphere,
Modified tapioca starch is poly methyl silsesquioxane oil modification tapioca；
Spherical cellulose acetate is made of cellulose acetate, degree of acetylation 58-60%, and average grain diameter is 6-10 microns, is inhaled
Oil value is 2.0-3.0ml/g；Porous type methyl methacrylate microsphere is methylmethacrylate polymer, and average grain diameter is
8 microns, oil factor 1.2-2.4ml/g.
2. wanting the oil-control described in 1 to spray according to right, it is characterised in that effective Zn content of the zinc pyrrolidone carboxylate is
19.4-21.3%.
3. wanting the oil-control described in 1 to spray according to right, it is characterised in that the bentonite is layer structure, contains per lattice and is less than
The charge of 0.9 unit.
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| CN201510413867.4A CN104997644B (en) | 2015-07-14 | 2015-07-14 | A kind of dual-purpose oil-control spraying of hair skin |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726646B (en) * | 2016-12-16 | 2019-11-15 | 广州市白云联佳精细化工厂 | A kind of clarity oil-control matifying lotion and preparation method thereof |
| CN108771635B (en) * | 2018-08-15 | 2021-05-25 | 广州艾蓓生物科技有限公司 | Foundation make-up composition and preparation method thereof |
| US11147775B2 (en) * | 2018-09-04 | 2021-10-19 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| US11229610B2 (en) * | 2018-09-04 | 2022-01-25 | Babak Ghalili | Cannabinoid and menthol gel compositions, patches and methods |
| CN111631965A (en) * | 2020-07-07 | 2020-09-08 | 美丽链接生物科技研究院(广东)有限公司 | Plant-derived facial mask with cleaning and makeup removing functions |
| CN111728892A (en) * | 2020-08-14 | 2020-10-02 | 宋家豪 | Oil-control cosmetic cream for improving oily skin and preparation method thereof |
| CN112641640A (en) * | 2020-12-31 | 2021-04-13 | 彭氏(惠州)实业发展有限公司 | Powder-containing oil-control spray and preparation method thereof |
| CN114272156B (en) * | 2021-12-10 | 2023-06-16 | 广州融汇化妆品有限公司 | Deoiling fluffy washing-free hair drying spray and preparation method thereof |
| CN115779131B (en) * | 2022-10-09 | 2024-02-23 | 湖南中腾湘岳生物科技有限公司 | Processing technology of medical dressing and medical dressing thereof |
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