CN103321375A - Composite inorganic thermal-insulation decoration plate and manufacturing method thereof - Google Patents
Composite inorganic thermal-insulation decoration plate and manufacturing method thereof Download PDFInfo
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Abstract
The invention discloses a composite inorganic thermal-insulation decoration plate and a manufacturing method thereof and belongs to the technical field of novel construction materials. The composite inorganic thermal-insulation decoration plate comprises a thermal-insulation layer and a decoration layer and is characterized in that the thermal-insulation layer is composed of the following components by weight: 30-40 parts of cement, 2.5-5 parts of gypsum powder, 55-63 parts of glass beads, 0.3-0.5 part of water reducer, 0.6-1.0 part of hydrophobe emulsion powder, 0.2-0.4 part of silane waterproof agents and 0.5-1.0 part of capillary crystalline master batches, and the decoration layer is composed of the following components by weight: 15-25 parts of silicone acrylic emulsion, 2-5 parts of silica solution, 65-75 parts of silica sand, 0.1-0.2 part of hydroxyethyl cellulose, 0.2-0.5 part of methanesiliconic acid sodium salt and 1-5 parts of water. The decoration plate manufactured by a formula and the manufacturing method has the effect of thermal-insulation and decoration, and further has the advantages of being fireproof, waterproof, capable of automatically repairing microcracks, long in service life, low in manufacturing cost and short in production period.
Description
Technical field
The invention belongs to the New Building Materials technical field, be specifically related to a kind of composite inorganic heat insulation decorative panel and preparation method thereof.
Background technology
Along with country more and more payes attention to Building Energy-saving, building external wall energy-saving insulation industry more and more receives publicity.Because the deficiency that the heat insulating materials such as thin plastoring system, glue powder polyphenyl particle system exist, exterior-wall heat insulation is gradually to the heat preservation decoration integrative transition at present.
Heat preservation decoration integrative in the architectural energy saving system refers to heat insulating material and metal finishing sheet material or inorganic pre-coating decorative plaques organic composites such as EPS, XPS, polyurethane, phenol formaldehyde foam or inorganic foamed materials.The shortcomings such as the manual efficiency of construction that the heat preservation decoration integrative system can overcome current other external-wall external-insulation energy-saving system is low, and easily cracking is ornamental poor, and application life is short are the superior exterior wall insulation energy efficient systems of a kind of comprehensive cost performance.Its appearance will produce great change to traditional coating industry and insulation industry, have good future develop, and it will become a development trend of China's building energy conservation industry.
But, the problem such as it is high that existing heat insulating decorative board ubiquity the sheet material water absorption rate, and water resistance is poor.From more existing sample projects, through exposing to the sun and rain more than a year, appearance slab-joint cracking, the plate sweat in various degree of the warming plate on the metope phenomenon such as grow dim.In the warm and humid deformation of inorganic composite heat-preserving plate, rainwater tends to be penetrated into thus insulation layer, causes insulation layer imbibition, distortion, and this not only affects the usefulness of warming plate, also can destroy the adhesion strength of insulating composite layer, can cause coming unstuck when serious, the phenomenon such as cracking.Simultaneously, some inorganic pre-coating decorative plaques is often ignored plate side and backboard face is carried out waterproofing work, particularly sheet material after building-site carries out cutting processing, does not carry out waterproofing work, causes rainwater to be penetrated into coating surface along edge of crack, and coating is grown dim.
Present existing heat insulating decorative board often lays particular emphasis on the improvement and bring new ideas to the thermal and insulating performance of warming plate, and research and attention to the heat insulating decorative board water resistance have been ignored, make heat insulating decorative board many problems in use occur, bring certain trouble to the user.
Summary of the invention
For problems of the prior art, the object of the invention is providing a kind of composite inorganic heat insulation decorative panel and preparation method thereof.
The present invention is realized by the following technical programs:
Described composite inorganic heat insulation decorative panel; comprise insulation layer and decorative layer; it is characterized in that described insulation layer is comprised of the component of following parts by weight: cement 30-40 part; land plaster 2.5-5 part; glass bead 55-63 part; water reducing agent 0.3-0.5 part; hydrophobic latex powder 0.6-1.0 part; silane waterproof agent 0.2-0.4 part; penetrant crystalline masterbatch 0.5-1.0 part, described decorative layer is comprised of the component of following parts by weight: Silicone acrylic emulsion 15-25 part; Ludox 2-5 part; quartz sand 65-75 part; hydroxyethylcellulose 0.1-0.2 part; sodium methyl silicate 0.2-0.5 part; water 1-5 part.
Described composite inorganic heat insulation decorative panel; it is characterized in that described insulation layer is comprised of the component of following parts by weight: cement 35-40 part, land plaster 3-4 part, glass bead 57-61 part, water reducing agent 0.3-0.4 part, hydrophobic latex powder 0.8-1.0 part, silane waterproof agent 0.2-0.3 part, penetrant crystalline masterbatch 0.8-1.0 part, described decorative layer is comprised of the component of following parts by weight: Silicone acrylic emulsion 15-20 part, Ludox 3-4 part, quartz sand 70-72 part, hydroxyethylcellulose 0.1-0.2 part, sodium methyl silicate 0.3-0.4 part, water 2.6-4.5 part.
Described composite inorganic heat insulation decorative panel is characterized in that described cement is common 425 label portland cements.
Described composite inorganic heat insulation decorative panel is characterized in that described glass bead bulk density is 110-130 kg/m
3
Described composite inorganic heat insulation decorative panel is characterized in that described water reducing agent is the NF naphthalene series high-efficiency water-reducing agent.
Described composite inorganic heat insulation decorative panel is characterized in that described quartz sand is the 70-100 order.
The preparation method of described composite inorganic heat insulation decorative panel is characterized in that by following processing step:
1) preparation of insulation layer slurry: with cement, land plaster, glass bead, water reducing agent, hydrophobic latex powder, silane waterproof agent, penetrant crystalline masterbatch, add the insulation layer dry powder that stirs to get in the kneader in described ratio, then in insulation layer dry powder, add entry, stir and make the insulation layer slurry, for subsequent use;
2) preparation of decorative layer slurry: in another kneader, slowly add entry and hydroxyethylcellulose, make the hydroxyethylcellulose dissolving evenly, then add successively Silicone acrylic emulsion, quartz sand, Ludox, sodium methyl silicate, stir and make the decorative layer slurry, for subsequent use;
3) preparation of insulation layer: fix mould, the insulation layer slurry for preparing in the step 1) is poured in the mould, by forcing press closed and pressurization to mould, make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer, wherein press pressure is 20～30 kg/cm
3
4) preparation of decorative layer: adjusting press pressure is 10～20 kg/cm
3, with step 2) in the decorative layer slurry that stirs pour into above the wet embryo of insulation layer that step 3) makes, by the closed and pressurization to mould, make decorative layer become consolidation with insulation layer, be the warming plate idiosome after the demoulding;
5) thermostatic curing: with the warming plate idiosome that step 4) makes, send in 40～60 ℃ the constant temperature oven, oven dry maintenance 5～8 hours namely gets composite inorganic heat insulation decorative panel of the present invention.
The preparation method of described composite inorganic heat insulation decorative panel is characterized in that the ratio of insulation layer dry powder and water is 100:20-30 in the step 1).
The preparation method of described composite inorganic heat insulation decorative panel is characterized in that step 1) and step 2) described in the speed of agitator of kneader be 30-50 rev/min.
Compared to existing technology, the present invention has the following advantages:
1. the insulation layer of composite inorganic heat insulation decorative panel and decorative layer; the inorganics such as cement, gypsum, glass bead, quartz sand have been adopted; fireproof performance and the fire-protection rating of sheet material have been heightened; simultaneously bilevel physical property approaches, and distortion, be full of cracks, the layering of having avoided causing because expanding with heat and contract with cold, the phenomenon such as come off.
2. insulation layer has adopted and has had the hydrophobicity redispersable latex powder, organosilicon powder hydrophober, make goods have excellent water resistance and hydrophobicity performance, no matter be that sheet material is inner, or the surface all has excellent water resistance, greatly reduce the water absorption rate of sheet material self, solved be full of cracks that existing heat insulating decorative board causes because of the suction problem, rise rouse, come off, the problem such as mouldy, bleeding.Simultaneously after the sheet material suction, active chemistry in the penetrant crystalline masterbatch that adds permeates to inside concrete take water as carrier, in concrete, form water-fast crystalline solid, stop up capillary channel, thereby make the finer and close more waterproof of sheet material, thereby make sheet material have the function of the defectives such as automatic reparation micro-crack, make sheet material have the effect of permanent waterproof.The prepared composite inorganic heat insulation decorative panel of the present invention, through check, water absorption rate≤0.3%, its water resistance is higher than the market like product far away.
3. decorative layer, abandon the way of traditional polymer cement mortar decorative layer, adopted the splendid Silicone acrylic emulsion of water resistance and weatherability and sodium methyl silicate waterproof agent, greatly promoted waterproof and the hydrophobicity performance of decorative layer, the simultaneously adding of Ludox has also improved the adhesion strength of decorative layer.
4. composite inorganic heat insulation decorative panel, adopt the brand-new production technology of the compressing and constant temperature drying maintenance of twice on mould, the techniques such as bonding between traditional insulation layer and the decorative layer, anchoring, spraying have been abandoned, carry out workshop production, the heat insulating decorative board of machine-shaping, technique is advanced, and mechanization degree is high, reduce the production and processing cost, save the production cycle.
Description of drawings
Fig. 1 is structural representation of the present invention;
Among the figure: 1-insulation layer, 2-decorative layer.
The specific embodiment
Below in conjunction with Figure of description the present invention is described in further detail, and provides the specific embodiment.
As shown in Figure 1, composite inorganic heat insulation decorative panel of the present invention is suppressed successively by insulation layer 1 and decorative layer 2 and is formed.Wherein insulation layer 1 is comprised of cement, land plaster, glass bead, water reducing agent, hydrophobic latex powder, silane waterproof agent, penetrant crystalline masterbatch, and decorative layer 2 is comprised of Silicone acrylic emulsion, Ludox, quartz sand, hydroxyethylcellulose, sodium methyl silicate, water.
Wherein, in the insulation layer, cement is common 425 label portland cements, and the glass bead bulk density is 110～130kg/m
3Water reducing agent is the NF naphthalene series high-efficiency water-reducing agent, the hydrophobic latex powder is Germany's watt 8031H latex powder that the gram chemical company is produced, the silane waterproof agent is Germany's watt Powder D organosilicon powder hydrophober that the gram chemical company is produced, the penetrant crystalline masterbatch is that the Activated-Crystal 8106 that company far away produces is composed in Shanghai, in the decorative layer, quartz sand is 70～100 orders, and the molecular weight of hydroxyethylcellulose is about 100,000.
With 30 parts of cement, 5 parts of land plasters, 63 parts of glass beads, 0.3 part of water reducing agent, 1 part of hydrophobic latex powder, 0.2 part of silane waterproof agent, 0.5 part of penetrant crystalline masterbatch; add in the kneader by above-mentioned weight ratio; under 45 rev/mins rotating speed, stir and make insulation layer dry powder; under stirring; in insulation layer dry powder, add entry; by insulation layer dry powder total amount: the weight ratio of water=100:20 adds entry, stirs to make the insulation layer slurry, and is for subsequent use.In another kneader, by weight slowly adding 2.6 parts of entry, 0.1 part of hydroxyethylcellulose, both stirring and dissolving are even, be to add successively 25 parts of Silicone acrylic emulsions, 70 parts of quartz sands, 2 parts of Ludox, 0.3 part of sodium methyl silicate under 45 rev/mins the condition at the kneader speed of agitator, stirring makes the decorative layer slurry, for subsequent use.
Fixing mould, the insulation layer slurry that stirs is poured in the mould, by forcing press closed and pressurization to mould, is 20kg/cm in press pressure
3Pressure condition under.Make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer.After the wet embryo of insulation layer prepared, the adjustment press pressure was 15kg/cm
3, the decorative layer slurry that stirs is poured into above the wet embryo of insulation layer, then by forcing press closed and pressurization to mould, insulation layer and decorative laminate are integrated, be the warming plate idiosome after the demoulding.With the warming plate idiosome after the demoulding, to send in 40 ℃ the constant temperature oven, oven dry maintenance 7 hours namely makes composite inorganic heat insulation decorative panel of the present invention.
With 35 parts of cement, 3 parts of land plasters, 59.7 parts of glass beads, 0.4 part of water reducing agent, 0.8 part of hydrophobic latex powder, 0.3 part of silane waterproof agent, 0.8 part of penetrant crystalline masterbatch; add in the kneader by above-mentioned weight ratio; under 30 rev/mins rotating speed, stir and make insulation layer dry powder; under stirring; in insulation layer dry powder, add entry; by insulation layer dry powder total amount: the weight ratio of water=100:25 adds entry, stirs to make the insulation layer slurry, and is for subsequent use.In another kneader, by weight slowly adding 4.5 parts of entry, 0.1 part of hydroxyethylcellulose, both stirring and dissolving are even, be to add successively 20 parts of Silicone acrylic emulsions, 72 parts of quartz sands, 3 parts of Ludox, 0.4 part of sodium methyl silicate under 30 rev/mins the condition at the kneader speed of agitator, stirring makes the decorative layer slurry, for subsequent use.
Fixing mould, the insulation layer slurry that stirs is poured in the mould, by forcing press closed and pressurization to mould, is 15kg/cm in press pressure
3Pressure condition under.Make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer.After the wet embryo of insulation layer prepared, the adjustment press pressure was 10kg/cm
3, the decorative layer slurry that stirs is poured into above the wet embryo of insulation layer, then by forcing press closed and pressurization to mould, insulation layer and decorative laminate are integrated, be the warming plate idiosome after the demoulding.With the warming plate idiosome after the demoulding, to send in 50 ℃ the constant temperature oven, oven dry maintenance 6 hours namely makes composite inorganic heat insulation decorative panel of the present invention.
Embodiment 3
With 40 parts of cement, 2.5 parts of land plasters, 55 parts of glass beads, 0.5 part of water reducing agent, 0.6 part of hydrophobic latex powder, 0.4 part of silane waterproof agent, 1.0 parts of penetrant crystalline masterbatch; add in the kneader by above-mentioned weight ratio; under 50 rev/mins rotating speed, stir and make insulation layer dry powder; under stirring; in insulation layer dry powder, add entry; by insulation layer dry powder total amount: the weight ratio of water=100:30 adds entry, stirs to make the insulation layer slurry, and is for subsequent use.In another kneader, by weight slowly adding 5 parts of entry, 0.2 part of hydroxyethylcellulose, both stirring and dissolving are even, be to add successively 18 parts of Silicone acrylic emulsions, 65 parts of quartz sands, 4 parts of Ludox, 0.5 part of sodium methyl silicate under 50 rev/mins the condition at the kneader speed of agitator, stirring makes the decorative layer slurry, for subsequent use.
Fixing mould, the insulation layer slurry that stirs is poured in the mould, by forcing press closed and pressurization to mould, is 20kg/cm in press pressure
3Pressure condition under.Make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer.After the wet embryo of insulation layer prepared, the adjustment press pressure was 10kg/cm
3, the decorative layer slurry that stirs is poured into above the wet embryo of insulation layer, then by forcing press closed and pressurization to mould, insulation layer and decorative laminate are integrated, be the warming plate idiosome after the demoulding.With the warming plate idiosome after the demoulding, to send in 60 ℃ the constant temperature oven, oven dry maintenance 5 hours namely makes composite inorganic heat insulation decorative panel of the present invention.
Embodiment 4
With 38 parts of cement, 4 parts of land plasters, 61 parts of glass beads, 0.35 part of water reducing agent, 0.9 part of hydrophobic latex powder, 0.25 part of silane waterproof agent, 0.9 part of penetrant crystalline masterbatch; add in the kneader by above-mentioned weight ratio; under 50 rev/mins rotating speed, stir and make insulation layer dry powder; under stirring; in insulation layer dry powder, add entry; by insulation layer dry powder total amount: the weight ratio of water=100:30 adds entry, stirs to make the insulation layer slurry, and is for subsequent use.In another kneader, by weight slowly adding 3.5 parts of entry, 0.15 part of hydroxyethylcellulose, both stirring and dissolving are even, be to add successively 15 parts of Silicone acrylic emulsions, 65 parts of quartz sands, 5 parts of Ludox, 0.2 part of sodium methyl silicate under 50 rev/mins the condition at the kneader speed of agitator, stirring makes the decorative layer slurry, for subsequent use.
Fixing mould, the insulation layer slurry that stirs is poured in the mould, by forcing press closed and pressurization to mould, is 15kg/cm in press pressure
3Pressure condition under.Make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer.After the wet embryo of insulation layer prepared, the adjustment press pressure was 10kg/cm
3, the decorative layer slurry that stirs is poured into above the wet embryo of insulation layer, then by forcing press closed and pressurization to mould, insulation layer and decorative laminate are integrated, be the warming plate idiosome after the demoulding.With the warming plate idiosome after the demoulding, to send in 55 ℃ the constant temperature oven, oven dry maintenance 6 hours namely makes composite inorganic heat insulation decorative panel of the present invention.
Adopt the composite inorganic heat insulation decorative panel of above-described embodiment prescription and method preparation, except the dual-use function that has insulation and decorate, also have fire prevention and excellent water resistance.Because the physical property of insulation layer and decorative layer approaches, the phenomenon such as can effectively avoid distortion, be full of cracks, the layering that causes because expanding with heat and contract with cold and come off; The hydrophobic latex powder of adding in the insulation layer and silane waterproof agent, make product surface and the inner water resistance that all has excellence, can greatly reduce the water absorption rate of sheet material self, even if after a small amount of suction of sheet material, active chemistry in the penetrant crystalline masterbatch that adds permeates to inside concrete take water as carrier, in concrete, form water-fast crystalline solid, stop up capillary channel, thereby make the finer and close more waterproof of sheet material, through check, this product water absorption rate≤0.3%, water resistance is higher than the market like product.
Claims (9)
1. composite inorganic heat insulation decorative panel; comprise insulation layer and decorative layer; it is characterized in that described insulation layer is comprised of the component of following parts by weight: cement 30-40 part, land plaster 2.5-5 part, glass bead 55-63 part, water reducing agent 0.3-0.5 part, hydrophobic latex powder 0.6-1.0 part, silane waterproof agent 0.2-0.4 part, penetrant crystalline masterbatch 0.5-1.0 part, described decorative layer is comprised of the component of following parts by weight: Silicone acrylic emulsion 15-25 part, Ludox 2-5 part, quartz sand 65-75 part, hydroxyethylcellulose 0.1-0.2 part, sodium methyl silicate 0.2-0.5 part, water 1-5 part.
2. composite inorganic heat insulation decorative panel according to claim 1; it is characterized in that described insulation layer is comprised of the component of following parts by weight: cement 35-40 part, land plaster 3-4 part, glass bead 57-61 part, water reducing agent 0.3-0.4 part, hydrophobic latex powder 0.8-1.0 part, silane waterproof agent 0.2-0.3 part, penetrant crystalline masterbatch 0.8-1.0 part, described decorative layer is comprised of the component of following parts by weight: Silicone acrylic emulsion 15-20 part, Ludox 3-4 part, quartz sand 70-72 part, hydroxyethylcellulose 0.1-0.2 part, sodium methyl silicate 0.3-0.4 part, water 2.6-4.5 part.
3. composite inorganic heat insulation decorative panel according to claim 1 and 2 is characterized in that described cement is common 425 label portland cements.
4. composite inorganic heat insulation decorative panel according to claim 1 and 2 is characterized in that described glass bead bulk density is 110-130kg/m
3
5. composite inorganic heat insulation decorative panel according to claim 1 and 2 is characterized in that described water reducing agent is the NF naphthalene series high-efficiency water-reducing agent.
6. composite inorganic heat insulation decorative panel according to claim 1 and 2 is characterized in that described quartz sand is the 70-100 order.
7. the preparation method of composite inorganic heat insulation decorative panel is characterized in that by following processing step:
1) preparation of insulation layer slurry: with cement, land plaster, glass bead, water reducing agent, hydrophobic latex powder, silane waterproof agent, penetrant crystalline masterbatch, add the insulation layer dry powder that stirs to get in the kneader in described ratio, then in insulation layer dry powder, add entry, stir and make the insulation layer slurry, for subsequent use;
2) preparation of decorative layer slurry: in another kneader, slowly add entry and hydroxyethylcellulose, make the hydroxyethylcellulose dissolving evenly, then add successively Silicone acrylic emulsion, quartz sand, Ludox, sodium methyl silicate, stir and make the decorative layer slurry, for subsequent use;
3) preparation of insulation layer: fix mould, the insulation layer slurry for preparing in the step 1) is poured in the mould, by forcing press closed and pressurization to mould, make the extrusion forming of insulation layer slurry make the wet embryo of insulation layer, wherein press pressure is 20～30kg/cm
3
4) preparation of decorative layer: the adjustment press pressure is 10～20kg/cm
3, with step 2) in the decorative layer slurry that stirs pour into above the wet embryo of insulation layer that step 3) makes, by the closed and pressurization to mould, decorative layer and insulation layer are become one, be the warming plate idiosome after the demoulding;
5) thermostatic curing: with the warming plate idiosome that step 4) makes, send in 40～60 ℃ the constant temperature oven, oven dry maintenance 5～8 hours namely gets composite inorganic heat insulation decorative panel of the present invention.
8. the preparation method of composite inorganic heat insulation decorative panel according to claim 7 is characterized in that the ratio of insulation layer dry powder and water is 100:20-30 in the step 1).
9. the preparation method of composite inorganic heat insulation decorative panel according to claim 7 is characterized in that step 1) and step 2) described in the speed of agitator of kneader be 30-50 rev/min.
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