CN103274893A - 1,1,1,3,3-五氯丙烷的制备方法 - Google Patents

1,1,1,3,3-五氯丙烷的制备方法 Download PDF

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Publication number
CN103274893A
CN103274893A CN2013101863032A CN201310186303A CN103274893A CN 103274893 A CN103274893 A CN 103274893A CN 2013101863032 A CN2013101863032 A CN 2013101863032A CN 201310186303 A CN201310186303 A CN 201310186303A CN 103274893 A CN103274893 A CN 103274893A
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starting material
catalyst
haloalkane
cocatalyst
product stream
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CN2013101863032A
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Chinese (zh)
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童雪松
I.尚克兰
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Honeywell International Inc
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Honeywell International Inc
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/01Acyclic saturated compounds containing halogen atoms containing chlorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/08Acyclic saturated compounds containing halogen atoms containing fluorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN2013101863032A 2006-10-11 2007-10-10 1,1,1,3,3-五氯丙烷的制备方法 Pending CN103274893A (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US85091006P 2006-10-11 2006-10-11
US60/850,910 2006-10-11
US11/869,274 US9738577B2 (en) 2006-10-11 2007-10-09 Process for the manufacture of 1,1,1,3,3-pentachloropropane
US11/869,274 2007-10-09

Related Parent Applications (1)

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CNA2007800458520A Division CN101558031A (zh) 2006-10-11 2007-10-10 1,1,1,3,3-五氯丙烷的制备方法

Publications (1)

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CN103274893A true CN103274893A (zh) 2013-09-04

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CN2013101863032A Pending CN103274893A (zh) 2006-10-11 2007-10-10 1,1,1,3,3-五氯丙烷的制备方法

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US (2) US9738577B2 (enExample)
JP (1) JP5588173B2 (enExample)
CN (1) CN103274893A (enExample)
MX (1) MX2009003714A (enExample)
WO (1) WO2008045910A1 (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105348033A (zh) * 2015-11-24 2016-02-24 淄博澳宏化工科技有限公司 一种1,1,1,3,3-五氯丙烷的制备方法
TWI770558B (zh) * 2014-10-16 2022-07-11 捷克商史波克專業化學杭尼維洛普合股公司 用於製備高純度1,1,1,2,3-五氯丙烷產物之方法
CN117886665A (zh) * 2023-12-11 2024-04-16 江西中欣埃克盛新材料有限公司 合成1,1,1,3,3-五氟丙烷的全流程连续工艺

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9738577B2 (en) * 2006-10-11 2017-08-22 Honeywell International Inc. Process for the manufacture of 1,1,1,3,3-pentachloropropane
CA2708643C (en) * 2007-12-19 2017-05-30 Occidental Chemical Corporation Methods of making chlorinated hydrocarbons
US8426655B2 (en) 2010-03-26 2013-04-23 Honeywell International Inc. Process for the manufacture of hexafluoro-2-butene
US8373010B2 (en) 2010-09-03 2013-02-12 Honeywell International Inc. Methods to produce 3,3,3-trifluoropropene
RU2010147002A (ru) * 2010-11-17 2012-05-27 Е.И.Дюпон де Немур энд Компани (US) Каталитический синтез галогенированных углеводородов
US9156752B2 (en) * 2011-01-04 2015-10-13 Honeywell International Inc. High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same
US8722946B2 (en) * 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
US10112166B2 (en) * 2011-06-03 2018-10-30 Honeywell International Inc. Method for capturing and recycling iron catalyst used in the production of haloalkane compounds
US8835702B2 (en) 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
US8889924B2 (en) * 2012-02-14 2014-11-18 Honeywell International Inc. Process for the production of 1,3,3,3-tetrafluoropropene
US9289758B2 (en) 2013-01-22 2016-03-22 Axiall Ohio, Inc. Processes for producing chlorinated hydrocarbons and methods for recovering polyvalent antimony catalysts therefrom
US8889930B2 (en) 2013-01-22 2014-11-18 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons
US8859829B2 (en) * 2013-03-14 2014-10-14 Honeywell International Inc. Stabilizer and inhibitor for chloropropenes, such as tetrachloropropene 1,1,2,3-tetrachloropropene (1230xa), used in the manufacture of 2,3,3,3-tetrafluoropropene (1234yf)
US9090531B2 (en) * 2013-03-14 2015-07-28 Honeywell International Inc. Method for mitigating HCL generation during 1,1,2,3-tetrachloropropene purification
US9139497B2 (en) 2013-10-23 2015-09-22 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons in the presence of a polyvalent bismuth compound
CN106061929A (zh) * 2014-02-19 2016-10-26 阿科玛股份有限公司 用于制造氢氯氟烯烃的方法
JP5928549B2 (ja) 2014-10-09 2016-06-01 ダイキン工業株式会社 ハロオレフィン化合物の製造方法及び安定剤の除去方法
US9896400B2 (en) 2014-10-16 2018-02-20 Spolek Pro Chemickou A Hutni Vyrobu A.S. Process for producing a chlorinated C3-6 alkane
CN105622330A (zh) * 2016-01-26 2016-06-01 巨化集团技术中心 一种氯代烃的连续制备方法
WO2019195258A1 (en) * 2018-04-03 2019-10-10 Blue Cube Ip Llc Improved process for preparing chloroalkanes and/or chlorofluoroalkanes

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3651019A (en) * 1961-09-28 1972-03-21 Yeda Res & Dev Production of adducts of carbon tetrachloride or chloroform with olefinically unsaturated substances
WO1995004021A1 (en) * 1993-07-29 1995-02-09 Alliedsignal Inc. Process for the preparation of hydrofluorocarbons having 3 to 7 carbon atoms
CN1130614A (zh) * 1994-09-26 1996-09-11 埃尔夫阿托化学有限公司 1,1,1,3,3-五氟丙烷的合成
EP0787707A1 (fr) * 1996-02-01 1997-08-06 Elf Atochem S.A. Préparation du 1,1,1,3,3-pentachlorobutane et du 1,1,1,3,3-pentafluorobutane
US5902914A (en) * 1995-08-14 1999-05-11 Alliedsignal Inc. Process for the preparation of halogenated alkanes
US6040487A (en) * 1996-07-31 2000-03-21 E. I. Du Pont De Nemours And Company Process for the manufacture of halocarbons
CN1384812A (zh) * 1999-05-12 2002-12-11 联合讯号公司 制备卤代化合物的连续方法
WO2002102750A2 (en) * 2001-06-14 2002-12-27 Vulcan Chemicals Water-enhanced production of 1,1,1,3,3-pentachloropropane
US20060122441A1 (en) * 2004-12-08 2006-06-08 Honeywell International Inc. Continuous process for preparing halogenated compounds

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3862978A (en) 1967-08-24 1975-01-28 Dow Chemical Co Catalytic synthesis of organic halogen compounds from an ethylenically unsaturated compound and a halogenated organic compound
US4605802A (en) 1982-04-01 1986-08-12 Halocarbon Products Corp. Production of 1,1,1,3-tetrachloropropane
ATE22877T1 (de) 1983-07-06 1986-11-15 Monsanto Co Verfahren zur herstellung von monoaddukten von olefinen und damit reagierfaehigen telogenen.
US5608127A (en) 1990-02-09 1997-03-04 E. I. Dupont De Nemours And Company Halogen exchange process for manufacture of hydrochlorofluoropropanes
KR930004510B1 (ko) 1990-10-18 1993-05-27 한국과학기술연구원 1,1,1-트리플루오로-2,2-디클로로에탄의 제조방법
JP3105793B2 (ja) 1996-08-13 2000-11-06 住友バイエルウレタン株式会社 硬質ポリウレタンフォームの製造方法および硬質ポリウレタンフォーム用組成物
DE19639121A1 (de) 1996-09-24 1998-03-26 Basf Ag Verfahren zur Herstellung von Polyurethan-Hartschaumstoffen
US5792898A (en) 1996-09-27 1998-08-11 Uop Llc Process for the management of mononuclear and polynuclear aromatic compounds produced in a hydrocarbon dehydrogenation reaction zone
CZ297256B6 (cs) 1997-05-05 2006-10-11 Solvay (Societe Anonyme) Zpusob výroby 1,1,1,3,3-pentachlorbutanu
WO1999007659A1 (fr) 1997-08-08 1999-02-18 Solvay (Societe Anonyme) Procede de preparation d'hydrocarbures halogenes
US6339840B1 (en) 1997-06-02 2002-01-15 Iowa State University Research Foundation, Inc. Apparatus and method for parallelizing legacy computer code
JP2000063301A (ja) 1998-08-18 2000-02-29 Central Glass Co Ltd フッ素化プロパンの製造方法
BE1012268A3 (fr) 1998-11-05 2000-08-01 Solvay Procede de preparation d'hydrocarbures halogenes.
US6300532B1 (en) * 1998-12-15 2001-10-09 Alliedsignal Inc. Process for addition of haloalkanes to alkenes catalyzed by an organophosphite compound
AU7908900A (en) 1999-10-06 2001-05-10 Solvay (Societe Anonyme) Method for obtaining halogenated hydrocarbons in the presence of a co-catalyst
WO2001025176A1 (fr) 1999-10-06 2001-04-12 Solvay (Société Anonyme) Procede de preparation d'hydrocarbures halogenes
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
US6534688B2 (en) 2001-06-11 2003-03-18 Vulcan Chemicals Dehydrochlorination stabilization of polychlorinated alkanes
US20050177012A1 (en) 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US6720466B2 (en) 2002-04-17 2004-04-13 Vulcan Chemicals, a division of Vulcan Materials Company 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery
US20040225166A1 (en) 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US20050049443A1 (en) 2003-08-28 2005-03-03 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes using a copper catalyst
US7091388B2 (en) 2003-09-26 2006-08-15 Honeywell International Inc. Method of making 1,1,3,3,3-pentafluoropropene
US9738577B2 (en) * 2006-10-11 2017-08-22 Honeywell International Inc. Process for the manufacture of 1,1,1,3,3-pentachloropropane

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3651019A (en) * 1961-09-28 1972-03-21 Yeda Res & Dev Production of adducts of carbon tetrachloride or chloroform with olefinically unsaturated substances
WO1995004021A1 (en) * 1993-07-29 1995-02-09 Alliedsignal Inc. Process for the preparation of hydrofluorocarbons having 3 to 7 carbon atoms
CN1130614A (zh) * 1994-09-26 1996-09-11 埃尔夫阿托化学有限公司 1,1,1,3,3-五氟丙烷的合成
US5902914A (en) * 1995-08-14 1999-05-11 Alliedsignal Inc. Process for the preparation of halogenated alkanes
EP0787707A1 (fr) * 1996-02-01 1997-08-06 Elf Atochem S.A. Préparation du 1,1,1,3,3-pentachlorobutane et du 1,1,1,3,3-pentafluorobutane
US6040487A (en) * 1996-07-31 2000-03-21 E. I. Du Pont De Nemours And Company Process for the manufacture of halocarbons
CN1384812A (zh) * 1999-05-12 2002-12-11 联合讯号公司 制备卤代化合物的连续方法
WO2002102750A2 (en) * 2001-06-14 2002-12-27 Vulcan Chemicals Water-enhanced production of 1,1,1,3,3-pentachloropropane
US20060122441A1 (en) * 2004-12-08 2006-06-08 Honeywell International Inc. Continuous process for preparing halogenated compounds
US7102041B2 (en) * 2004-12-08 2006-09-05 Honeywell International Inc. Continuous process for preparing halogenated compounds

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI770558B (zh) * 2014-10-16 2022-07-11 捷克商史波克專業化學杭尼維洛普合股公司 用於製備高純度1,1,1,2,3-五氯丙烷產物之方法
CN105348033A (zh) * 2015-11-24 2016-02-24 淄博澳宏化工科技有限公司 一种1,1,1,3,3-五氯丙烷的制备方法
CN117886665A (zh) * 2023-12-11 2024-04-16 江西中欣埃克盛新材料有限公司 合成1,1,1,3,3-五氟丙烷的全流程连续工艺
CN117886665B (zh) * 2023-12-11 2025-06-10 江西中欣埃克盛新材料有限公司 合成1,1,1,3,3-五氟丙烷的全流程连续工艺

Also Published As

Publication number Publication date
JP2010506848A (ja) 2010-03-04
US20180127337A1 (en) 2018-05-10
US9738577B2 (en) 2017-08-22
US10676414B2 (en) 2020-06-09
WO2008045910A1 (en) 2008-04-17
JP5588173B2 (ja) 2014-09-10
MX2009003714A (es) 2009-04-22
US20080091053A1 (en) 2008-04-17

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