CN103141787B - Acerola cherry preparation and preparation method thereof - Google Patents
Acerola cherry preparation and preparation method thereof Download PDFInfo
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- CN103141787B CN103141787B CN201310118423.9A CN201310118423A CN103141787B CN 103141787 B CN103141787 B CN 103141787B CN 201310118423 A CN201310118423 A CN 201310118423A CN 103141787 B CN103141787 B CN 103141787B
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Abstract
The invention provides an acerola cherry preparation which is characterized by comprising 1-50 parts by mass of acerola cherry powder, 20-96 parts by mass of diluent, 2-15 parts by mass of synthetic vitamin C and 0.5-15 parts by mass of additives. The preparation method comprises the following steps of: pulping acerola cherry fruits after pretreatment, adding deastringent liquid into the obtained acerola cherry pulp to agitate, colloid-milling, homogenizing and filtering the mixture to obtain first filter liquid for later use, adding pectinase and cellulose into the obtained first filter residue for enzymolysis treatment, and colloid-milling, homogenizing and filtering the mixture once again to obtain second filter liquid, wherein the deastringent liquid is mixed water solution of citric acid and sodium chloride; and mixing the first filter liquid and the second filter liquid, homogenizing the mixture, carrying out vacuum concentration to obtain concentrated liquid, adding auxiliary materials comprising resistant starch and isomaltooligosaccharide into the concentrated liquid, homogenizing the mixture, and then carrying out vacuum drying to obtain the acerola cherry powder. The acerola cherry preparation provided by the invention has quick vitamin C dissolution speed and high bioavailability.
Description
Technical field
The present invention relates to health food technology field, relate in particular to acerola concentrate preparation and preparation method thereof
Background technology
Vitamin C is the water soluble vitamin that a kind of people early find and are familiar with, and is to maintain normal human's metabolism and the requisite material of physiological function.Ascorbic physiological function mainly contains antioxidation, promote that connective tissue forms, removing toxic substances, promote neurotransmitter and carnitine synthetic, promote iron to absorb, improve immunologic function, reduce artery sclerosis, prevent and control inflammation etc.Vitamin C can be helped immune system opposing virus and bacterium infection by the increase of the bacterial activity of immunologic function and Acute toxicity cell, and therefore vitamin C and human immune system are closely related.Vitamin C is divided into natural complex C and synthetic vitamin C.Natural complex C is mainly present in the wholefoods such as fruits and vegetables, has higher biologically active, is more easily absorbed by the body than synthetic vitamin C.Though and synthetic vitamin C has the structure identical with natural complex C, its biologically active is lower, human body is difficult for absorbing.
Acerola concentrate is the Chinese appellation of A Xi roller cherry (Acerola Cherry), originates in Caribbean, the West Indies, tropical America, therefore have another name called malpighia glabra (West Indies Cherry).Research shows, at present in the plant of plantation, in acerola concentrate, Vitamin C content is the highest, in every 100 grams of fruits, Vc content reaches more than 1000 milligrams, is approximately 35 times of lemon, 17 times of strawberry, also higher 11 times than being considered to the high guava of vitamin C, be genuine " king of vitamin C ", also contain the elements such as dimension A, dimension B1, dimension B2, iron, calcium simultaneously, the citrin wherein containing can help ascorbic absorption.
Prior art discloses the preparation method of multivitamin C sheet, as CN101861990A discloses a kind of pearl vitamin C buccal tablets, by water soluble pearl powder, VC microcapsules, sorbierite, L～malic acid, Sucralose, dolomol mix to be made through compressing dry granulation.But the vitamin C of its use is synthetic vitamin C, and activity is lower, and bioavailability is not high.
Summary of the invention
In view of this, the technical problem to be solved in the present invention is to provide a kind of acerola concentrate preparation and preparation method thereof, and the ascorbic dissolution rate of acerola concentrate preparation provided by the invention is fast, and bioavailability is high.
The invention provides a kind of acerola concentrate preparation, it is characterized in that, comprising:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
The additive of 0.5～15 mass parts;
Described acerola concentrate powder is prepared in accordance with the following methods:
To after the pretreatment of acerola concentrate fruit, pull an oar, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate is for subsequent use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material being made up of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Preferably, comprising: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
Preferably, described diluent is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch.
Preferably, described additive is selected from one or more in flavouring, lubricant, wetting agent and adhesive.
Preferably, described flavouring is selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame; Described lubricant is selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder; Described wetting agent is the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
Preferably, described acerola concentrate preparation is acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
Preferably, the preparation method of described acerola concentrate powder is:
The synthetic vitamin C of the acerola concentrate powder of 1～50 mass parts and 2～10 mass parts is pulverized respectively, crosses 100 mesh sieves;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained to acerola concentrate powder.
Preferably, the preparation method of described acerola concentrate granule is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture;
In said mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, make softwood;
Softwood is crossed to 14 mesh sieves, obtain wet granular;
By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle;
By dry particle, sieve whole grain, classification;
Dry particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained to acerola concentrate granule.
Preferably, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents;
By acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture;
Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture;
The second mixture is mixed with the flavouring of 0.5～2 mass parts, airtight 2～4 hours, obtain the 3rd mixture;
The 3rd mixture compressing tablet is obtained to acerola concentrate tablet.
Preferably, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture;
In the first mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, prepare softwood;
Above-mentioned softwood is crossed to 14 mesh sieves, make wet granular;
By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle, described dry pellet moisture content is 1%～3%;
Dry particle is crossed to 16 mesh sieves;
Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join after above-mentioned sieving in dry particle, mix, obtain the second mixture;
By the second mixture compressing tablet, prepare acerola concentrate tablet.
The invention provides a kind of acerola concentrate preparation, it is characterized in that, comprising: the acerola concentrate powder of 1～50 mass parts; The diluent of 20～96 mass parts; The synthetic vitamin C of 2～15 mass parts; The additive of 0.5～15 mass parts; To after the pretreatment of acerola concentrate fruit, pull an oar, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate is for subsequent use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride; Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material being made up of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.The preparation method of acerola concentrate powder provided by the invention has introduced special pre-treatment and has protected look and complex enzyme treatment process, retain the nutritional labeling in acerola concentrate fruit, particularly effective reservation of vitamin C etc., adds suitable auxiliary material simultaneously and carries out vacuum drying and increase fruit powder collection powder rate.In whole technique, not adding food additives and the auxiliary materials such as any essence, sweetener, is that a kind of color and luster is good, dissolubility is high, the nutrient fruit powder of pure natural; Acerola concentrate preparation provided by the invention is to be diluent by above-mentioned acerola concentrate powder and hydrophilicity condiment, and ascorbic dissolution rate is fast, and bioavailability is high.There is in addition mouthfeel good, steady quality, the advantage that cost is low.Experimental result shows, the cumulative leaching rate of acerola concentrate preparation provided by the invention in 45min is more than 95%.
Detailed description of the invention
The invention provides a kind of acerola concentrate preparation, comprising:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
The additive of 0.5～15 mass parts;
Described acerola concentrate powder is prepared in accordance with the following methods:
To after the pretreatment of acerola concentrate fruit, pull an oar, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate is for subsequent use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material being made up of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Acerola concentrate preparation provided by the invention, comprising: the acerola concentrate powder of 1～50 mass parts; The diluent of 20～96 mass parts; The synthetic vitamin C of 2～15 mass parts; The additive of 0.5～15 mass parts;
Described acerola concentrate powder is prepared in accordance with the following methods: will after the pretreatment of acerola concentrate fruit, pull an oar, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate is for subsequent use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride; Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material being made up of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Acerola concentrate preparation provided by the invention preferably includes: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
The present invention is directed to the problem that acerola concentrate fruit powder nutrition content too much runs off and collection powder rate is lower, color and luster is darker, former fruit local flavor is weak that the defect of the preparation technology in patent CN102835713A causes, select special Treatment Solution, complex enzyme reagent and auxiliary material to process, changing traditional spray-dired method is vacuum drying, not only improve the content of individual nutritional labeling but also improved the collection powder rate of acerola concentrate fruit, ensured stronger former fruit taste and acerola concentrate fruit primary colors.
In the preparation method of acerola concentrate powder, described pretreatment is preferably:
After acerola concentrate fruit is rinsed, be immersed in 2min in the sodium hydroxide solution that 80 DEG C of mass percents are 2%, after flushing, add sodium sulfite to content of sulfur dioxide to reach 100mg/L.The present invention selects NaOH and sodium sulfite to carry out pretreatment can to reduce the oxidation of tannin, pigment in acerola concentrate fruit, suppresses the breeding of wild yeasts, mould etc., increases the effect of crushing and beating, is conducive to maintaining and the increase of nutritional labeling of fruit pink colour pool.
Astringent liquid of the present invention is preferably to add and accounts for the citric acid of acerola concentrate pulp quality 0.5% and 0.2% sodium chloride; Described stirring is preferably at 50 DEG C and stirs 10-30min.Citric acid and sodium chloride are combined use by the present invention, utilizes citric acid to increase osmotic pressure effect, promotes Na
+enter cell and be combined with soluble tannin and change insolubility into, eliminate the puckery sense of fruit.Citric acid, sodium chloride suppress enzymatic browning effect in addition simultaneously, prevent the brown stain of polyphenols in fruit, play certain color-protecting function.
In enzymolysis processing of the present invention, use cellulase and pectase by combining, pectin and cellulose in degraded fruit, fully discharge fruit inclusion, improves nutrient composition content in fruit powder.Preferably, add and account for the pectase of the first filter residue quality 0.2% and 0.1% cellulase, be heated to 40～55 DEG C, homogeneous, leaves standstill 2.5～5h.It is that 620mmHg, evaporating temperature are preferably at 45～60 DEG C and are concentrated into 60～70Bx that Vacuum Concentration of the present invention is specially in vacuum, and wherein, Bx refers to Baume degrees, represents soluble solids content, and mmHg is millimetres of mercury, the size of tolerance atmospheric pressure.
The present invention adopts vacuum drying, and described vacuum drying is preferably:
Be that 680～740mmHg, temperature are dry 5～6h at 50～60 DEG C in vacuum.
Because the content of material such as pectin, reduced sugar in fruit powder are high, in being dried to powder there is sticky wall, collection powder rate declines, have influence on the dissolubility of finished product fruit powder, the present invention has increased resistant starch (non-converted starch and oxidized starch) and dextrinosan for this reason in concentrate, increase the collection powder rate of fruit powder, reduce sticky wall, increase the brew of fruit powder simultaneously.As preferably, described auxiliary material addition is the 10-30% of concentrate quality, and the mass ratio of described resistant starch and dextrinosan is 4:1.
Preferably, described making beating adopts the making beating of two pass beater, and slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm.
The acerola concentrate fruit powder of preparing according to preparation method of the present invention has the content of higher vitamin C, vitamin A, vitamin B1, vitamin B2 and niacin, and there is acerola concentrate fruit primary colors and strong local flavor, there is the collection powder rate of higher acerola concentrate fruit simultaneously and reconstitute preferably effect.
In the preparation method of acerola concentrate powder of the present invention, introduce special pre-treatment and protected look and complex enzyme treatment process, retain the nutritional labeling in acerola concentrate fruit, particularly effective reservation of vitamin C etc., adds suitable auxiliary material simultaneously and carries out vacuum drying and increase fruit powder collection powder rate.In whole technique, not adding food additives and the auxiliary materials such as any essence, sweetener, is that a kind of color and luster is good, dissolubility is high, the nutrient fruit powder of pure natural, can be widely used in the industry such as food and health products.
Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, is more preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; The present invention is also unrestricted for the source of described synthetic vitamin C, can be commercially available, the present invention is also unrestricted for the source of described sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, can be commercially available.
In the present invention, described additive is preferably selected from one or more in flavouring, lubricant, wetting agent and adhesive.Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, be most preferably selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose.The present invention is also unrestricted for the source of described peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, can be commercially available.
In the present invention, described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.The present invention is also unrestricted for the source of described stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, can be commercially available.
In the present invention, described wetting agent is preferably the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.The present invention is also unrestricted for the source of described PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement, can be commercially available.
In the present invention, described acerola concentrate preparation is preferably acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
In the present invention, preferably preparation in accordance with the following methods of acerola concentrate powder:
The synthetic vitamin C of the acerola concentrate powder of 1～50 mass parts and 2～10 mass parts is pulverized respectively, crosses 100 mesh sieves;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained to acerola concentrate powder.
First the present invention pulverizes the synthetic vitamin C of the acerola concentrate powder of 1～50 mass parts and 2～10 mass parts respectively, crosses 100 mesh sieves; Described acerola concentrate powder is preferably according to the acerola concentrate powder preparing described in technique scheme, does not repeat them here; The present invention is for described grinding mode and the mode unrestricted of sieving, grinding mode well known to those skilled in the art.Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained to acerola concentrate powder.The present invention is also unrestricted for the source of described synthetic vitamin C, can be commercially available.The present invention is for described hybrid mode unrestricted, hybrid mode well known to those skilled in the art.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, is more preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, be most preferably selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
In the present invention, preferably preparation in accordance with the following methods of acerola concentrate granule:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring; Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture; In said mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, make softwood; Softwood is crossed to 14 mesh sieves, obtain wet granular; By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle; By dry particle, sieve whole grain, classification; Dry particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained to acerola concentrate granule.
The present invention for described pulverizing, sieve.Mix, the mode of whole grain, classification unrestricted, pulverizing well known to those skilled in the art, sieve.Mix.Whole grain, hierarchical approaches.The present invention is also unrestricted for the source of described synthetic vitamin C, can be commercially available.Described acerola concentrate powder is preferably according to the acerola concentrate powder preparing described in technique scheme, does not repeat them here; Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, is more preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, be most preferably selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
In the present invention, the preparation method of acerola concentrate tablet is preferably:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents; By acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture; Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture; The second mixture is mixed with the flavouring of 0.5～2 mass parts, airtight 2～4 hours, obtain the 3rd mixture; The 3rd mixture compressing tablet is obtained to acerola concentrate tablet.
The present invention for described pulverizing, sieve, mixing, compressing tablet mode unrestricted, pulverizing well known to those skilled in the art, sieve, mixing, compressing tablet mode.Described acerola concentrate powder is preferably according to the acerola concentrate powder preparing described in technique scheme, does not repeat them here; The present invention is also unrestricted for the source of described synthetic vitamin C, can be commercially available.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, is more preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, be most preferably selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
In the present invention, the preparation method of described acerola concentrate tablet is preferably:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring; Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture; In the first mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, prepare softwood; Above-mentioned softwood is crossed to 14 mesh sieves, make wet granular; By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle, described dry pellet moisture content is 1%～3%; Dry particle is crossed to 16 mesh sieves; Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join after above-mentioned sieving in dry particle, mix, obtain the second mixture; By the second mixture compressing tablet, prepare acerola concentrate tablet.
The present invention for described pulverizing, sieve, mixing, compressing tablet mode unrestricted, pulverizing well known to those skilled in the art, sieve, mixing, compressing tablet mode.Described acerola concentrate powder is preferably according to the acerola concentrate powder preparing described in technique scheme, does not repeat them here; The present invention is also unrestricted for the source of described synthetic vitamin C, can be commercially available.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, is more preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, be most preferably selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described wetting agent is preferably the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
Acerola concentrate preparation provided by the invention is to be diluent by above-mentioned acerola concentrate powder and hydrophilicity condiment, and ascorbic dissolution rate is fast, and bioavailability is high.There is in addition mouthfeel good, steady quality, the advantage that cost is low.
In order to further illustrate the present invention, below in conjunction with embodiment, acerola concentrate preparation provided by the invention and preparation method thereof is described in detail.
Embodiment 1
The ripening degree of selection is higher, full bright-coloured, without the fruit that rots to go mouldy.Acerola concentrate fruit is rinsed well, add the 5%NaOH solution of 80 DEG C, soak 2min left and right, pull out be placed in can leakage container, control flow rate and rinse acerola concentrate, then pour in glass container, and with wooden stick stirring, add appropriate sodium sulfite, make SO
2content reaches 100mg/L, firmly stirs the mixture, and sieves and removes acerola concentrate seed and the pericarp coming off.
Acerola concentrate mixture is sent into stoning two pass beater making beating (slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm), obtain acerola concentrate pulp; Account for pulp quality 0.5% citric acid and account for pulp quality 0.2% sodium chloride (being astringent liquid) adding in the pulp of above-mentioned separation, processing 20min at 50 DEG C.
Pulp after treatment, after glue mill is processed, then is sent into and in high pressure homogenizer, is carried out trickle pulverizing for the second time; The slurry obtaining carries out slag liquid separation (gained filtrate is that the first filtrate is for subsequent use), the thick slag leaching (the first filter residue) is added to enzyme preparation (pectase 0.2% and cellulase 0.2%), be heated to 45 DEG C, homogeneous leaves standstill 2.5-5h, by the slurry obtaining after glue mill is processed, send into again homogenizer and carry out miniaturization processing, obtain the second filtrate.
Mix the first filtrate and the second filtrate, enter subsequently vacuum decker concentrated, temperature is 50 DEG C, and vacuum is 620mmHg, is concentrated into 68Bx.Slurry after concentrated, by 20% of its quality, adds resistant starch and dextrinosan to prepare burden, add resistant starch and isomalto-oligosaccharide mass ratio be 4:1.Homogeneous disposed slurry is drying to obtain acerola concentrate fruit powder under 55 DEG C of vacuum 710mmHg conditions of temperature.The acerola concentrate fruit powder of dry gained is crossed to 80 mesh sieves, under ultraviolet ray, after sterilization, adopt the vacuum-packed finished product of composite plastic film.
Embodiment 2
The ripening degree of selection is higher, full bright-coloured, without the fruit that rots to go mouldy.Acerola concentrate fruit is rinsed well, add the 5%NaOH solution of 80 DEG C, soak 2min left and right, pull out be placed in can leakage container, control flow rate and rinse acerola concentrate, then pour in glass container, and with wooden stick stirring, add appropriate sodium sulfite, make SO
2content reaches 100mg/L, firmly stirs the mixture, and sieves and removes acerola concentrate seed and the pericarp coming off.
Acerola concentrate mixture is sent into stoning two pass beater making beating (slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm), obtain acerola concentrate pulp; Account for pulp quality 0.5% citric acid and account for pulp quality 0.2% sodium chloride (being astringent liquid) adding in the pulp of above-mentioned separation, processing 10min at 50 DEG C.
Pulp after treatment, after glue mill is processed, then is sent into and in high pressure homogenizer, is carried out trickle pulverizing for the second time; The slurry obtaining carries out slag liquid separation (gained filtrate is that the first filtrate is for subsequent use), the thick slag leaching (the first filter residue) is added to enzyme preparation (pectase 0.2% and cellulase 0.2%), be heated to 40 DEG C, homogeneous leaves standstill 2.5-5h, by the slurry obtaining after glue mill is processed, send into again homogenizer and carry out miniaturization processing, obtain the second filtrate.
Mix the first filtrate and the second filtrate, enter subsequently vacuum decker concentrated, temperature is 45 DEG C, and vacuum is 620mmHg, is concentrated into 60Bx.Slurry after concentrated, by 20% of its quality, adds resistant starch and dextrinosan to prepare burden, add resistant starch and isomalto-oligosaccharide mass ratio be 4:1.Homogeneous disposed slurry is drying to obtain acerola concentrate fruit powder under temperature 50 C vacuum 680mmHg condition.The acerola concentrate fruit powder of dry gained is crossed to 80 mesh sieves, under ultraviolet ray, after sterilization, adopt the vacuum-packed finished product of composite plastic film.
Embodiment 3
Get respectively acerola concentrate powder 100g prepared by embodiment 1, sweet mellow wine 450g, lactose 450g, flavoring orange essence 1g pulverizes, cross 80 mesh sieves, being placed in beveller grinds 10min and makes fully to mix, prepare softwood with the ethanolic solution of 200mL3% PVP (PVP), softwood is crossed to 14 mesh sieves, obtain wet granular, wet granular is laid on porcelain dish, thickness is no more than 3mm, at the temperature of 60 DEG C, dry 30min obtains dry particle, use sieving of screen-dividing machine, whole grain, classification, 1g talcum powder will be added in dry particle after classification, mix rear sub-dose packaging and obtain acerola concentrate granule.
Embodiment 4
Get respectively acerola concentrate powder 100g prepared by embodiment 2, sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, lactose 350g, glucose 50g pulverizes, cross 80 mesh sieves, put and in beveller, grind 10min and make fully to mix, prepare softwood with the aqueous solution of 20% ethanol, softwood is crossed to 14 mesh sieves, obtain wet granular, wet granular is laid on porcelain dish, thickness is no more than 3mm, at the temperature of 60 DEG C, dry 1h obtains dry particle, use sieving of screen-dividing machine, carry out whole grain and classification, 1g talcum powder will be added in dry particle after classification, mix, sub-dose packaging obtains acerola concentrate granule.
Embodiment 5
Get respectively acerola concentrate powder 100g, xylitol 100g, synthetic vitamin C100g, lactose 700g prepared by embodiment 1, by above-mentioned acerola concentrate powder and vitamin C, pulverize respectively, cross 100 mesh sieves, add 10g xylitol, mix with 300g lactose, 0.5g lauryl sodium sulfate, sub-dose packaging obtains acerola concentrate powder.
Embodiment 6
Get respectively acerola concentrate powder 100g prepared by embodiment 2, sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, lactose 400g, flavoring orange essence 1g pulverizes respectively, cross 80 mesh sieves, being placed in beveller grinds 10min and fully mixes, prepare softwood with the aqueous solution of 200mL20% ethanol, softwood is crossed to 14 mesh sieves, obtain wet granular, wet granular is laid on porcelain dish, thickness is no more than 3mm, at the temperature of 60 DEG C, dry 1h obtains dry particle, with the whole grain of 16 mesh sieves, in dry particle, add 0.5g polyethylene glycol, mix, compressing tablet obtains acerola concentrate tablet.
Embodiment 7
Get respectively acerola concentrate powder 100g, sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, glucose 400g, lemon extract 5g pulverizing prepared by embodiment 1, cross 80 mesh sieves, being placed in beveller grinds 10min and makes fully to mix, add the 10g stearic acid of mistake 100 mesh sieves that crush, being placed in beveller grinds 10min and makes fully to mix, airtight 3 hours, compressing tablet obtained acerola concentrate tablet.
Embodiment 8
" Chinese pharmacopoeia " 2005 editions two annex VC dissolution method one methods of employing, the dissolution rate of the Ai Lan get natural complex C chewable tablets of the ascorbic and Jiangsu Jiangshan Pharmaceutical Co of the acerola concentrate preparation that the embodiment of the present invention 1～6 is provided is tested, the results are shown in Table 1, the acerola concentrate preparation that table 1 provides for the embodiment of the present invention and the dissolution determination result of commercially available VC sheet.
The acerola concentrate preparation that table 1 embodiment of the present invention provides and the dissolution determination result of commercially available VC sheet
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. an acerola concentrate preparation, is characterized in that, is made up of following component:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
The additive of 0.5～15 mass parts;
Described acerola concentrate powder is prepared in accordance with the following methods:
To after the pretreatment of acerola concentrate fruit, pull an oar, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate is for subsequent use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Described pretreatment is:
After acerola concentrate fruit is rinsed, be immersed in 2min in the sodium hydroxide solution that 80 DEG C of mass percents are 2%, after flushing, add sodium sulfite to content of sulfur dioxide to reach 100mg/L;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material being made up of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
2. acerola concentrate preparation according to claim 1, is characterized in that, comprising: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
3. acerola concentrate preparation according to claim 1, is characterized in that, described diluent is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch.
4. acerola concentrate preparation according to claim 1, is characterized in that, described additive is selected from one or more in flavouring, lubricant, wetting agent and adhesive.
5. acerola concentrate preparation according to claim 4, it is characterized in that, described flavouring is selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame; Described lubricant is selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder; Described wetting agent is the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
6. acerola concentrate preparation according to claim 2, is characterized in that, described acerola concentrate preparation is acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
7. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate powder is:
The synthetic vitamin C of the acerola concentrate powder of 1～50 mass parts and 2～10 mass parts is pulverized respectively, crosses 100 mesh sieves;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained to acerola concentrate powder.
8. acerola concentrate granulation agent according to claim 6, is characterized in that, the preparation method of described acerola concentrate granule is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture;
In said mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, make softwood;
Softwood is crossed to 14 mesh sieves, obtain wet granular;
By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle;
By dry particle, sieve whole grain, classification;
Dry particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained to acerola concentrate granule.
9. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents;
By acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture;
Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture;
The second mixture is mixed with the flavouring of 0.5～2 mass parts, airtight 2～4 hours, obtain the 3rd mixture;
The 3rd mixture compressing tablet is obtained to acerola concentrate tablet.
10. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture;
In the first mixture, add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts, prepare softwood;
Above-mentioned softwood is crossed to 14 mesh sieves, make wet granular;
By wet granular dry 0.5～2h at 50～70 DEG C, obtain dry particle, described dry pellet moisture content is 1%～3%;
Dry particle is crossed to 16 mesh sieves;
Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join after above-mentioned sieving in dry particle, mix, obtain the second mixture;
By the second mixture compressing tablet, prepare acerola concentrate tablet.
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