CN103141787A - Acerola cherry preparation and preparation method thereof - Google Patents
Acerola cherry preparation and preparation method thereof Download PDFInfo
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- CN103141787A CN103141787A CN2013101184239A CN201310118423A CN103141787A CN 103141787 A CN103141787 A CN 103141787A CN 2013101184239 A CN2013101184239 A CN 2013101184239A CN 201310118423 A CN201310118423 A CN 201310118423A CN 103141787 A CN103141787 A CN 103141787A
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Abstract
The invention provides an acerola cherry preparation which is characterized by comprising 1-50 parts by mass of acerola cherry powder, 20-96 parts by mass of diluent, 2-15 parts by mass of synthetic vitamin C and 0.5-15 parts by mass of additives. The preparation method comprises the following steps of: pulping acerola cherry fruits after pretreatment, adding deastringent liquid into the obtained acerola cherry pulp to agitate, colloid-milling, homogenizing and filtering the mixture to obtain first filter liquid for later use, adding pectinase and cellulose into the obtained first filter residue for enzymolysis treatment, and colloid-milling, homogenizing and filtering the mixture once again to obtain second filter liquid, wherein the deastringent liquid is mixed water solution of citric acid and sodium chloride; and mixing the first filter liquid and the second filter liquid, homogenizing the mixture, carrying out vacuum concentration to obtain concentrated liquid, adding auxiliary materials comprising resistant starch and isomaltooligosaccharide into the concentrated liquid, homogenizing the mixture, and then carrying out vacuum drying to obtain the acerola cherry powder. The acerola cherry preparation provided by the invention has quick vitamin C dissolution speed and high bioavailability.
Description
Technical field
The present invention relates to the health food technology field, relate in particular to the acerola concentrate preparation and preparation method thereof
Background technology
Vitamin C is the water soluble vitamin that a kind of people early find and are familiar with, and is to keep normal human's metabolism and the requisite material of physiological function.Ascorbic physiological function mainly contains antioxidation, promote that connective tissue forms, detoxifcation, promote neurotransmitter and carnitine synthetic, promote iron to absorb, improve immunologic function, reduce artery sclerosis, prevent and control inflammation etc.Vitamin C can be by immunologic function and Acute toxicity cell the increase of bacterial activity help immune system opposing virus and bacterium infection, so vitamin C and the human immune system closely related.Vitamin C is divided into natural complex C and synthetic vitamin C.Natural complex C mainly is present in the wholefoods such as fruits and vegetables, has higher biologically active, more easily is absorbed by the body than synthetic vitamin C.Though and synthetic vitamin C has the structure identical with natural complex C, its biologically active is lower, and human body is difficult for absorbing.
Acerola concentrate is the Chinese appellation of A Xi roller cherry (Acerola Cherry), originates in the West Indies, tropical America Caribbean, therefore have another name called malpighia glabra (West Indies Cherry).Studies show that, at present in the plant of plantation, in acerola concentrate, Vitamin C content is the highest, in every 100 grams fruits, Vc content reaches more than 1000 milligrams, is approximately 35 times of lemon, 17 times of strawberry, also high 11 times than being considered to the high guava of vitamin C, be genuine " king of vitamin C ", also contain simultaneously the elements such as dimension A, dimension B1, dimension B2, iron, calcium, the citrin that wherein contains can help ascorbic absorption.
Prior art discloses the preparation method of multivitamin C sheet, a kind of pearl vitamin C buccal tablets is disclosed as CN101861990A, by water soluble pearl powder, VC microcapsules, sorbierite, L～malic acid, Sucralose, dolomol mix to be made through compressing dry granulation.But its vitamin C that uses is synthetic vitamin C, and activity is lower, and bioavailability is not high.
Summary of the invention
In view of this, the technical problem to be solved in the present invention is to provide a kind of acerola concentrate preparation and preparation method thereof, and the ascorbic dissolution rate of acerola concentrate preparation provided by the invention is fast, and bioavailability is high.
The invention provides a kind of acerola concentrate preparation, it is characterized in that, comprising:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
0.5 the additive of～15 mass parts;
Described acerola concentrate powder prepares in accordance with the following methods:
To pull an oar after the pretreatment of acerola concentrate fruit, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate for later use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, and described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material that is comprised of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Preferably, comprising: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
Preferably, described diluent is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch.
Preferably, described additive is selected from one or more in flavouring, lubricant, wetting agent and adhesive.
Preferably, described flavouring is selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame; Described lubricant is selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder; Described wetting agent is the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
Preferably, described acerola concentrate preparation is acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
Preferably, the preparation method of described acerola concentrate powder is:
100 mesh sieves are pulverized respectively, crossed to the acerola concentrate powder of 1～50 mass parts and the synthetic vitamin C of 2～10 mass parts;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained acerola concentrate powder.
Preferably, the preparation method of described acerola concentrate granule is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture;
Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in said mixture, make softwood;
Softwood is crossed 14 mesh sieves, obtain wet granular;
With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle;
With dried particle, sieve whole grain, classification;
Dried particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained the acerola concentrate granule.
Preferably, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents;
With acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture;
Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture;
The flavouring of the second mixture with 0.5～2 mass parts mixed, airtight 2～4 hours, obtain the 3rd mixture;
The 3rd mixture compressing tablet is obtained the acerola concentrate tablet.
Preferably, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture;
Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in the first mixture, prepare softwood;
Above-mentioned softwood is crossed 14 mesh sieves, make wet granular;
With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle, described dried pellet moisture content is 1%～3%;
Dried particle is crossed 16 mesh sieves;
Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join in the above-mentioned rear dried particle that sieves, mix, obtain the second mixture;
With the second mixture compressing tablet, prepare the acerola concentrate tablet.
The invention provides a kind of acerola concentrate preparation, it is characterized in that, comprising: the acerola concentrate powder of 1～50 mass parts; The diluent of 20～96 mass parts; The synthetic vitamin C of 2～15 mass parts; 0.5 the additive of～15 mass parts; To pull an oar after the pretreatment of acerola concentrate fruit, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate for later use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, and described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride; Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material that is comprised of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.The preparation method of acerola concentrate powder provided by the invention has introduced special pre-treatment and has protected look and complex enzyme treatment process, kept the nutritional labeling in the acerola concentrate fruit, particularly effective reservation of vitamin C etc. is added simultaneously suitable auxiliary material and is carried out vacuum drying and increase fruit powder collection powder rate.Not adding food additives and the auxiliary materials such as any essence, sweetener in whole technique, is that a kind of color and luster is good, dissolubility is high, the nutrient fruit powder of pure natural; Acerola concentrate preparation provided by the invention is to be diluent by above-mentioned acerola concentrate powder and hydrophilicity condiment, and ascorbic dissolution rate is fast, and bioavailability is high.Has in addition mouthfeel good, steady quality, the advantage that cost is low.Experimental result shows, the cumulative leaching rate of acerola concentrate preparation provided by the invention in 45min is more than 95%.
The specific embodiment
The invention provides a kind of acerola concentrate preparation, comprising:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
0.5 the additive of～15 mass parts;
Described acerola concentrate powder prepares in accordance with the following methods:
To pull an oar after the pretreatment of acerola concentrate fruit, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate for later use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, and described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material that is comprised of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Acerola concentrate preparation provided by the invention comprises: the acerola concentrate powder of 1～50 mass parts; The diluent of 20～96 mass parts; The synthetic vitamin C of 2～15 mass parts; 0.5 the additive of～15 mass parts;
Described acerola concentrate powder prepares in accordance with the following methods: will pull an oar after the pretreatment of acerola concentrate fruit, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate for later use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, and described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride; Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material that is comprised of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
Acerola concentrate preparation provided by the invention preferably includes: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
The present invention is directed to the problem that acerola concentrate fruit powder nutrition content too much runs off and collection powder rate is lower, color and luster is darker, former fruit local flavor is weak that the defective of the preparation technology in patent CN102835713A causes, select special Treatment Solution, complex enzyme reagent and auxiliary material to process, changing traditional spray-dired method is vacuum drying, not only improve the content of individual nutritional labeling but also improved the collection powder rate of acerola concentrate fruit, guaranteed stronger former fruit taste and acerola concentrate fruit primary colors.
In the preparation method of acerola concentrate powder, described pretreatment is preferably:
Be immersed in 80 ℃ of mass percents after acerola concentrate is really rinsed and be 2min in 2% sodium hydroxide solution, add sodium sulfite to content of sulfur dioxide to reach 100mg/L after flushing.The present invention selects NaOH and sodium sulfite to carry out the oxidation that pretreatment can reduce tannin, pigment in acerola concentrate fruit, suppresses the breeding of wild yeasts, mould etc., increases the effect of crushing and beating, is conducive to keeping and the increase of nutritional labeling of fruit pink colour pool.
Astringent liquid of the present invention is preferably and adds the citric acid that accounts for acerola concentrate pulp quality 0.5% and 0.2% sodium chloride; Described stirring is preferably under 50 ℃ and stirs 10-30min.The present invention unites use with citric acid and sodium chloride, utilizes citric acid to increase the osmotic pressure effect, promotes Na
+Enter cell and be combined with soluble tannin and change insolubility into, eliminate the puckery sense of fruit.Citric acid, sodium chloride suppress the enzymatic browning effect in addition simultaneously, prevent the brown stain of polyphenols in fruit, play certain color-protecting function.
In enzymolysis processing of the present invention, use cellulase and pectase by uniting, pectin and cellulose in the degraded fruit fully discharge the fruit inclusion, improve nutrient composition content in the fruit powder.Preferably, add the pectase that accounts for the first filter residue quality 0.2% and 0.1% cellulase, be heated to 40～55 ℃, homogeneous, standing 2.5～5h.It is that 620mmHg, evaporating temperature are preferably under 45～60 ℃ and are concentrated into 60～70Bx that Vacuum Concentration of the present invention is specially in vacuum, and wherein, Bx refers to Baume degrees, represents soluble solids content, and mmHg is millimetres of mercury, the size of tolerance atmospheric pressure.
The present invention adopts vacuum drying, and described vacuum drying is preferably:
Be that 680～740mmHg, temperature are dry 5～6h under 50～60 ℃ in vacuum.
Because the content of material such as pectin, reduced sugar in the fruit powder are high, when being dried to powder so that sticking wall to occur, collection powder rate descends, have influence on the dissolubility of finished product fruit powder, the present invention has increased resistant starch (non-converted starch and oxidized starch) and dextrinosan for this reason in concentrate, increase the collection powder rate of fruit powder, reduce sticking wall, increase simultaneously the brew of fruit powder.As preferably, described auxiliary material addition is the 10-30% of concentrate quality, and the mass ratio of described resistant starch and dextrinosan is 4:1.
Preferably, the making beating of two pass beater is adopted in described making beating, and slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm.
The content that has higher vitamin C, vitamin A, vitamin B1, vitamin B2 and niacin according to the acerola concentrate fruit powder of preparation method of the present invention preparation, and have acerola concentrate fruit primary colors and strong local flavor, have simultaneously the collection powder rate of higher acerola concentrate fruit and reconstitute preferably effect.
Introduce special pre-treatment in the preparation method of acerola concentrate powder of the present invention and protected look and complex enzyme treatment process, kept the nutritional labeling in the acerola concentrate fruit, particularly effective reservation of vitamin C etc. is added simultaneously suitable auxiliary material and is carried out vacuum drying and increase fruit powder collection powder rate.Not adding food additives and the auxiliary materials such as any essence, sweetener in whole technique, is that a kind of color and luster is good, dissolubility is high, the nutrient fruit powder of pure natural, can be widely used in the industries such as food and health products.
Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, more preferably is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; The present invention is also unrestricted for the source of described synthetic vitamin C, can be for commercially available, the present invention is also unrestricted for the source of described sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, can be for commercially available.
In the present invention, described additive is preferably selected from one or more in flavouring, lubricant, wetting agent and adhesive.Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, most preferably be selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose.The present invention is also unrestricted for the source of described peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, can be for commercially available.
In the present invention, described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.The present invention is also unrestricted for the source of described stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, can be for commercially available.
In the present invention, described wetting agent is preferably the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.The present invention is also unrestricted for the source of described PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement, can be for commercially available.
In the present invention, described acerola concentrate preparation is preferably acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
In the present invention, preferably preparation in accordance with the following methods of acerola concentrate powder:
100 mesh sieves are pulverized respectively, crossed to the acerola concentrate powder of 1～50 mass parts and the synthetic vitamin C of 2～10 mass parts;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained acerola concentrate powder.
At first the present invention pulverizes respectively, crosses 100 mesh sieves with the acerola concentrate powder of 1～50 mass parts and the synthetic vitamin C of 2～10 mass parts; Described acerola concentrate powder is preferably according to the described acerola concentrate powder for preparing of technique scheme, does not repeat them here; The present invention is for described grinding mode and the mode and unrestricted of sieving, and grinding mode well known to those skilled in the art gets final product.Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained acerola concentrate powder.The present invention is also unrestricted for the source of described synthetic vitamin C, can be for commercially available.The present invention is for described hybrid mode and unrestricted, and hybrid mode well known to those skilled in the art gets final product.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, more preferably is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, most preferably be selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
In the present invention, preferably preparation in accordance with the following methods of acerola concentrate granule:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring; Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture; Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in said mixture, make softwood; Softwood is crossed 14 mesh sieves, obtain wet granular; With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle; With dried particle, sieve whole grain, classification; Dried particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained the acerola concentrate granule.
The present invention for described pulverizing, sieve.Mix, the mode of whole grain, classification and unrestricted, pulverizing well known to those skilled in the art, sieve.Mix.Whole grain, hierarchical approaches get final product.The present invention is also unrestricted for the source of described synthetic vitamin C, can be for commercially available.Described acerola concentrate powder is preferably according to the described acerola concentrate powder for preparing of technique scheme, does not repeat them here; Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, more preferably is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, most preferably be selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
In the present invention, the preparation method of acerola concentrate tablet is preferably:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents; With acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture; Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture; The flavouring of the second mixture with 0.5～2 mass parts mixed, airtight 2～4 hours, obtain the 3rd mixture; The 3rd mixture compressing tablet is obtained the acerola concentrate tablet.
The present invention for described pulverizing, sieve, mixing, compressing tablet mode and unrestricted, pulverizing well known to those skilled in the art, sieve, mixing, compressing tablet mode get final product.Described acerola concentrate powder is preferably according to the described acerola concentrate powder for preparing of technique scheme, does not repeat them here; The present invention is also unrestricted for the source of described synthetic vitamin C, can be for commercially available.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, more preferably is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, most preferably be selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
In the present invention, the preparation method of described acerola concentrate tablet is preferably:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring; Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture; Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in the first mixture, prepare softwood; Above-mentioned softwood is crossed 14 mesh sieves, make wet granular; With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle, described dried pellet moisture content is 1%～3%; Dried particle is crossed 16 mesh sieves; Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join in the above-mentioned rear dried particle that sieves, mix, obtain the second mixture; With the second mixture compressing tablet, prepare the acerola concentrate tablet.
The present invention for described pulverizing, sieve, mixing, compressing tablet mode and unrestricted, pulverizing well known to those skilled in the art, sieve, mixing, compressing tablet mode get final product.Described acerola concentrate powder is preferably according to the described acerola concentrate powder for preparing of technique scheme, does not repeat them here; The present invention is also unrestricted for the source of described synthetic vitamin C, can be for commercially available.Described diluent is preferably selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch, more preferably is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite; Described flavouring is preferably selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame, more preferably be selected from one or more in orange oil, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, honey, xylitol, maltose, most preferably be selected from one or more in flavoring orange essence, lemon extract, cherry essence, xylitol, maltose; Described wetting agent is preferably the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is preferably selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement; Described lubricant is preferably selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder, preferred one or more that are selected from stearic acid, dolomol, calcium stearate, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate and Stepanol MG.
Acerola concentrate preparation provided by the invention is to be diluent by above-mentioned acerola concentrate powder and hydrophilicity condiment, and ascorbic dissolution rate is fast, and bioavailability is high.Has in addition mouthfeel good, steady quality, the advantage that cost is low.
In order to further illustrate the present invention, below in conjunction with embodiment, acerola concentrate preparation provided by the invention and preparation method thereof is described in detail.
Embodiment 1
The ripening degree of selection is higher, and is full bright-coloured, without the fruit that rots to go mouldy.Acerola concentrate is really rinsed well, added the 5%NaOH solution of 80 ℃, soak the 2min left and right, pull out be placed in can leakage container, control flow rate and rinse acerola concentrate, then pour in glass container, and stir with wooden stick, add appropriate sodium sulfite, make SO
2Content reaches 100mg/L, firmly stirs the mixture, and sieves and removes acerola concentrate seed and the pericarp that comes off.
The acerola concentrate mixture is sent into stoning two pass beater making beating (slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm), obtain the acerola concentrate pulp; Add in pulp with above-mentioned separation account for pulp quality 0.5% citric acid and account for pulp quality 0.2% sodium chloride (being astringent liquid), process 20min under 50 ℃.
Pulp after processing then is sent into and is carried out trickle pulverizing for the second time in high pressure homogenizer after glue mill is processed; The slurry that obtains carries out slag liquid and separates (gained filtrate is the first filtrate for later use), the thick slag (the first filter residue) that leaches is added enzyme preparation (pectase 0.2% and cellulase 0.2%), be heated to 45 ℃, the standing 2.5-5h of homogeneous, with the slurry that obtains after the glue mill is processed, send into again homogenizer and carry out the miniaturization processing, obtain the second filtrate.
Mix the first filtrate and the second filtrate, enter subsequently vacuum decker concentrated, temperature is 50 ℃, and vacuum is 620mmHg, is concentrated into 68Bx.Slurry after concentrated adds resistant starch and dextrinosan to prepare burden by 20% of its quality, add resistant starch and isomalto-oligosaccharide mass ratio be 4:1.The homogeneous disposed slurry is drying to obtain acerola concentrate fruit powder under 55 ℃ of vacuum 710mmHg conditions of temperature.The acerola concentrate fruit powder of dry gained is crossed 80 mesh sieves, adopt the vacuum-packed finished product of composite plastic film after sterilization under ultraviolet ray.
Embodiment 2
The ripening degree of selection is higher, and is full bright-coloured, without the fruit that rots to go mouldy.Acerola concentrate is really rinsed well, added the 5%NaOH solution of 80 ℃, soak the 2min left and right, pull out be placed in can leakage container, control flow rate and rinse acerola concentrate, then pour in glass container, and stir with wooden stick, add appropriate sodium sulfite, make SO
2Content reaches 100mg/L, firmly stirs the mixture, and sieves and removes acerola concentrate seed and the pericarp that comes off.
The acerola concentrate mixture is sent into stoning two pass beater making beating (slubbing beater sieve diameter is 3mm, and two road beater sieve diameters are 0.6mm), obtain the acerola concentrate pulp; Add in pulp with above-mentioned separation account for pulp quality 0.5% citric acid and account for pulp quality 0.2% sodium chloride (being astringent liquid), process 10min under 50 ℃.
Pulp after processing then is sent into and is carried out trickle pulverizing for the second time in high pressure homogenizer after glue mill is processed; The slurry that obtains carries out slag liquid and separates (gained filtrate is the first filtrate for later use), the thick slag (the first filter residue) that leaches is added enzyme preparation (pectase 0.2% and cellulase 0.2%), be heated to 40 ℃, the standing 2.5-5h of homogeneous, with the slurry that obtains after the glue mill is processed, send into again homogenizer and carry out the miniaturization processing, obtain the second filtrate.
Mix the first filtrate and the second filtrate, enter subsequently vacuum decker concentrated, temperature is 45 ℃, and vacuum is 620mmHg, is concentrated into 60Bx.Slurry after concentrated adds resistant starch and dextrinosan to prepare burden by 20% of its quality, add resistant starch and isomalto-oligosaccharide mass ratio be 4:1.The homogeneous disposed slurry is drying to obtain acerola concentrate fruit powder under temperature 50 C vacuum 680mmHg condition.The acerola concentrate fruit powder of dry gained is crossed 80 mesh sieves, adopt the vacuum-packed finished product of composite plastic film after sterilization under ultraviolet ray.
Embodiment 3
get respectively the acerola concentrate powder 100g of embodiment 1 preparation, sweet mellow wine 450g, lactose 450g, flavoring orange essence 1g pulverizes, cross 80 mesh sieves, being placed in beveller grinds 10min and makes fully and mix, ethanolic solution with 200mL3% PVP (PVP) prepares softwood, softwood is crossed 14 mesh sieves, obtain wet granular, wet granular is tiled on porcelain dish, thickness is no more than 3mm, dry 30min obtains dried particle at the temperature of 60 ℃, use sieving of screen-dividing machine, whole grain, classification, the 1g talcum powder will be added in dried particle after classification, after mixing, sub-dose packaging obtains the acerola concentrate granule.
Embodiment 4
get respectively the acerola concentrate powder 100g of embodiment 2 preparations, sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, lactose 350g, glucose 50g pulverizes, cross 80 mesh sieves, put in beveller and to grind 10min and make fully and mix, the aqueous solution with 20% ethanol prepares softwood, softwood is crossed 14 mesh sieves, obtain wet granular, wet granular is tiled on porcelain dish, thickness is no more than 3mm, dry 1h obtains dried particle at the temperature of 60 ℃, use sieving of screen-dividing machine, carry out whole grain and classification, the 1g talcum powder will be added in dried particle after classification, mixing, sub-dose packaging obtains the acerola concentrate granule.
Embodiment 5
Get respectively acerola concentrate powder 100g, xylitol 100g, synthetic vitamin C100g, the lactose 700g of embodiment 1 preparation, with above-mentioned acerola concentrate powder and vitamin C, pulverize respectively, cross 100 mesh sieves, add the 10g xylitol, with 300g lactose, 0.5g lauryl sodium sulfate mixing, sub-dose packaging obtains acerola concentrate powder.
Embodiment 6
get respectively the acerola concentrate powder 100g of embodiment 2 preparations, sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, lactose 400g, flavoring orange essence 1g pulverizes respectively, cross 80 mesh sieves, being placed in beveller grinding 10min fully mixes, the aqueous solution with 200mL20% ethanol prepares softwood, softwood is crossed 14 mesh sieves, obtain wet granular, wet granular is tiled on porcelain dish, thickness is no more than 3mm, dry 1h obtains dried particle at the temperature of 60 ℃, with the 16 whole grains of mesh sieve, add the 0.5g polyethylene glycol in dried particle, mixing, compressing tablet obtains the acerola concentrate tablet.
Embodiment 7
Acerola concentrate powder 100g, the sweet mellow wine 300g, xylitol 100g, synthetic vitamin C100g, glucose 400g, the lemon extract 5g that get respectively embodiment 1 preparation pulverize, cross 80 mesh sieves, being placed in beveller grinds 10min and makes fully and mix, the 10g stearic acid that adds mistake 100 mesh sieves that crush, be placed in beveller grinding 10min and make abundant mixing, airtight 3 hours, compressing tablet obtained the acerola concentrate tablet.
Embodiment 8
" 2005 editions two appendix VC dissolution method one methods of Chinese pharmacopoeia of employing, the dissolution rate of the Ai Lande natural complex C chewable tablets of the ascorbic and Jiangsu Jiangshan Pharmaceutical Co of the acerola concentrate preparation that the embodiment of the present invention 1～6 is provided is tested, the results are shown in Table 1, the acerola concentrate preparation that table 1 provides for the embodiment of the present invention and the dissolution determination result of commercially available VC sheet.
The acerola concentrate preparation that table 1 embodiment of the present invention provides and the dissolution determination result of commercially available VC sheet
The above is only the preferred embodiment of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. an acerola concentrate preparation, is characterized in that, comprising:
The acerola concentrate powder of 1～50 mass parts;
The diluent of 20～96 mass parts;
The synthetic vitamin C of 2～15 mass parts;
0.5 the additive of～15 mass parts;
Described acerola concentrate powder prepares in accordance with the following methods:
To pull an oar after the pretreatment of acerola concentrate fruit, gained acerola concentrate pulp adds astringent liquid to stir, then glue mill, homogeneous, filtration, gained the first filtrate for later use, gained the first filter residue adds pectase and cellulase carries out enzymolysis processing, and then glue mill, homogeneous, filtration obtain the second filtrate, and described astringent liquid is the mixed aqueous solution of citric acid and sodium chloride;
Mix homogeneous after the first filtrate obtained above and the second filtrate, then carry out Vacuum Concentration and obtain concentrate, concentrate adds homogeneous after the auxiliary material that is comprised of resistant starch and dextrinosan, and then vacuum drying obtains acerola concentrate fruit powder.
2. acerola concentrate preparation according to claim 1, is characterized in that, comprising: the acerola concentrate powder of 20～40 mass parts; The diluent of 40～90 mass parts; The synthetic vitamin C of 4～8 mass parts; The additive of 1～8 mass parts.
3. acerola concentrate preparation according to claim 1, is characterized in that, described diluent is selected from one or more in sweet mellow wine, lactose, glucose, sorbierite, sucrose, microcrystalline cellulose, starch, dextrin and pregelatinized starch.
4. acerola concentrate preparation according to claim 1, is characterized in that, described additive is selected from one or more in flavouring, lubricant, wetting agent and adhesive.
5. acerola concentrate preparation according to claim 4, it is characterized in that, described flavouring is selected from one or more in peppermint oil, orange oil, caryophyllus oil, oil of ginger, flavoring orange essence, lemon extract, cherry essence, flavoring banana essence, syrup, sucrose, honey, xylitol, maltose, stevioside and aspartame; Described lubricant is selected from one or more in stearic acid, dolomol, calcium stearate, talcum powder, hydrogenated vegetable oil, polyethylene glycol, lauryl sodium sulfate, Stepanol MG and superfine silica gel powder; Described wetting agent is the aqueous solution of ethanol or the ethanolic solution of PVP; Described adhesive is selected from one or more in PVP, cellulose derivative adhesive, starch slurry, syrup and rubber cement.
6. acerola concentrate preparation according to claim 2, is characterized in that, described acerola concentrate preparation is acerola concentrate powder, acerola concentrate tablet or acerola concentrate granule.
7. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate powder is:
100 mesh sieves are pulverized respectively, crossed to the acerola concentrate powder of 1～50 mass parts and the synthetic vitamin C of 2～10 mass parts;
Acerola concentrate powder after sieving, synthetic vitamin C and 20～93 mass parts diluents, 1～5 mass parts flavouring, 0.1～3 mass parts mix lubricant are obtained acerola concentrate powder.
8. acerola concentrate granulation agent according to claim 6, is characterized in that, the preparation method of described acerola concentrate granule is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Acerola concentrate powder, synthetic vitamin C, diluent and flavouring are mixed, obtain mixture;
Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in said mixture, make softwood;
Softwood is crossed 14 mesh sieves, obtain wet granular;
With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle;
With dried particle, sieve whole grain, classification;
Dried particle after above-mentioned classification and 0.1～3 mass parts mix lubricant are obtained the acerola concentrate granule.
9. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents;
With acerola concentrate powder, synthetic vitamin C, mixing diluents, obtain the first mixture;
Get 0.1～3 mass parts lubricant, pulverize, cross 100 mesh sieves and add in the first mixture, obtain the second mixture;
The flavouring of the second mixture with 0.5～2 mass parts mixed, airtight 2～4 hours, obtain the 3rd mixture;
The 3rd mixture compressing tablet is obtained the acerola concentrate tablet.
10. acerola concentrate preparation according to claim 6, is characterized in that, the preparation method of described acerola concentrate tablet is:
80 mesh sieves are pulverized respectively, crossed to 1～50 mass parts acerola concentrate powder, 2～10 mass parts synthetic vitamin C, 20～93 mass parts diluents, 1～5 mass parts flavouring;
Described acerola concentrate powder, synthetic vitamin C, diluent are mixed with flavouring, obtain the first mixture;
Add the wetting agent of 3～20 mass parts or the adhesive of 3～20 mass parts in the first mixture, prepare softwood;
Above-mentioned softwood is crossed 14 mesh sieves, make wet granular;
With wet granular dry 0.5～2h under 50～70 ℃, obtain dried particle, described dried pellet moisture content is 1%～3%;
Dried particle is crossed 16 mesh sieves;
Get the lubricant of 0.1～3 mass parts, cross 100 mesh sieves and join in the above-mentioned rear dried particle that sieves, mix, obtain the second mixture;
With the second mixture compressing tablet, prepare the acerola concentrate tablet.
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| CN104473088A (en) * | 2015-01-19 | 2015-04-01 | 杨俊� | Production process for cerasus humilis fruit extracting and cerasus humilis fruit preparation |
| CN104970316A (en) * | 2015-07-01 | 2015-10-14 | 海南金芝麟保健食品有限公司 | Composite acerola cherry fruit powder |
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| CN108065286A (en) * | 2018-01-03 | 2018-05-25 | 江苏海王健康生物科技有限公司 | A kind of chewable tablets containing acerola concentrate powder, VC and taurine and preparation method thereof |
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| CN111528387A (en) * | 2020-05-19 | 2020-08-14 | 天津尖峰弗兰德医药科技发展有限公司 | Plant-based composition for enhancing immunity and protecting respiratory system and preparation thereof |
| CN113995066A (en) * | 2021-11-05 | 2022-02-01 | 海南振业英涛科技集团有限公司 | Preparation method of acerola cherry collagen peptide beverage |
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