CN102952455A - Ultraviolet light curing transparent priming paint and preparation method and use method thereof - Google Patents
Ultraviolet light curing transparent priming paint and preparation method and use method thereof Download PDFInfo
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Abstract
The invention discloses an ultraviolet light curing transparent priming paint and a preparation method and a use method thereof. The ultraviolet light curing transparent priming paint comprises the following components in percentage by weight: 20-30% of bisphenol A epoxy acrylate resin, 15-25% of polyester acrylate, 1-10% of urethane acrylate, 5-10% of reagent type hydroxyethyl acrylate, 10-20% of tripropylene glycol diacrylate, 12-25% of trimethylolpropane triacrylate, 4-6% of photoinitiator, 10-25% of filling powder and 0.4-0.8% of promotor. The ultraviolet light curing transparent priming paint is suitable for laser roller construction, has good grittiness and transparency, has the characteristics that sanding is not needed for semi-curing recoating between film layers and the like, and has thick coating performance and the performance that the surface is similar to a mirror surface, and compared with conventional roller coating, the coating weight is greatly increased, roller coating processes are saved, the priming paint is sanded by a sanding machine without large pressure and with a small number of sanded films, a workpiece has no bright spots, the fullness of a product is guaranteed, the product quality is improved, the loss of the machine is smallreduced, and the use amount of sanding belts is greatly reduced.
Description
Technical field
The present invention relates to a kind of ultraviolet cured primer, relate in particular to a kind of ultraviolet curing transparent priming and preparation method thereof and using method of the radium-shine roller that is applied to woodenware.
Background technology
At present, the roll coating model that generally adopts in UV wood lacquer field all is coated with construction with ganoid General Purpose Rubber roller or silica gel roller, the method existing problems are that disposable glue spread is few, and average glue spread is 15～20g/ ㎡, and surface effect is more coarse, be pitted skin, and the more coarse more difficult sand milling in the larger surface of glue spread if sand milling is done finish paint to the surface again without bright spot, then needs the grinder intensified pressure, sand falls more paint and just can sand flat without bright spot, and is very large to the loss in abrasive band.Because sand falls too many paint paint film, the product fullness ratio of carrying out finish paint can be relatively poor, needs the more number of times of roller coat could satisfy customer requirement.
Begin on the market at present to have released the radium-shine roller roller coat priming paint of laser sculpture wire casing for above-mentioned phenomenon, common UV roller coat transparent priming by radium-shine roller roller application after paint glue spread 15～20g/ ㎡, and rugged by the roller plate surface, cause the sand milling operation of back to go on, can not reach desired thick being coated with of radium-shine roller (25～35g/ ㎡) and surfacing close to the effect of minute surface.Its reason is that common UV roller coat transparent priming can not complete wetting arrive the wire casing the inside of the radium-shine roller of laser sculpture, and paints after the radium-shine roller roller coat plate and can not spread rapidly levelling out onboard, so can not be applicable to radium-shine roller coating machine fully.
Summary of the invention
The object of the present invention is to provide a kind of glue spread large, coating surface is smooth, has semicure recoat between good sanding and transparency, paint film layer without ultraviolet curing transparent priming of the radium-shine roller that is applied to woodenware of the characteristics such as sand milling and preparation method thereof and using method.
For achieving the above object, the invention provides a kind of ultraviolet curing transparent priming, comprise the component of following weight percent:
Described auxiliary agent is comprised of the flow agent of the anti-settling agent that accounts for coating gross weight 0.2%, 0.1-0.2% and the wetting dispersing agent of 0.1-0.2%;
Described filling powder is comprised of the talcum powder that accounts for coating gross weight 6-12% and the transparent powder of 4-8%.
Described bisphenol A epoxy acrylate resin is by bisphenol A epoxide resin and acrylic or methacrylic acid-respons and get, and contains aromatic ring and side position hydroxyl in its molecular structure.
Described polyester acrylate is the polyester acrylate resin of two functional groups of modification.
Described urethane acrylate is the UV light-cured resin by synthetic a kind of two senses of aliphatics carbimide and polyester, HEA.
Described light trigger adopts 6420 models and the combination of Tianjin English power 1173 models of Changxing chemistry.
Described anti-settling agent is hydrophobic type silicon-dioxide, and flow agent is the esters of acrylic acid flow agent.
The present invention also provides a kind of preparation method of described ultraviolet curing transparent priming, may further comprise the steps:
Step 1, by weight percentage the bisphenol A epoxy acrylate resin in the component, polyester acrylate, urethane acrylate, reagent type Hydroxyethyl acrylate (2-HEA), tripropylene glycol diacrylate (TPGDA), trimethylolpropane tris vinylformic acid (TMPTA), light trigger, wetting dispersing agent and flow agent are added container successively, rotate and disperse 3-5 minute to evenly;
Step 2, while stirring in the component after by weight percentage anti-settling agent, filling powder being joined step 1 and being uniformly dispersed, rotate and disperse 15-20 minute to fineness≤60 μ m, filter and namely get described ultraviolet curing transparent priming.
In the described step 1 with 500PRM(rev/min) rotating speed disperses; Disperse with the 1200PRM rotating speed in the step 2.
The present invention also provides a kind of using method of described ultraviolet curing transparent priming, may further comprise the steps:
Step 1, the wooden skin ground of subsides;
Step 2, roller coat compound type transparent putty, glue spread 15～20g/ ㎡ carries out semicure;
Step 3, roller coat transparent priming, glue spread 15～20g/ ㎡ carries out semicure;
Step 4, the described ultraviolet curing transparent priming of roller coat, glue spread 25～35g/ ㎡ carries out semicure;
Step 5, the described ultraviolet curing transparent priming of roller coat again, glue spread 25～35g/ ㎡ solidifies entirely;
Sanding is carried out in step 6, employing 400 order abrasive bands;
Step 7, roller coat or spray paint.
In the described step 7, roller coat or spraying UV finish paint, or spraying PU or PE finish paint.
Above technique priming paint effect is very smooth close to minute surface, grinder sand falls 10g/ ㎡ just can obtain sanding effect without bright spot, also has paint film 100g/ ㎡ on the plate, if step 4, five secondary roller coat change common roller coat transparent priming into and cooperate the conventional roller use then can obtain maximum paint film 80g/ ㎡, because it is more little more smooth that common roller coating machine is the roller coat amount, and the roller coat amount is larger just uneven, cause grinder to need intensified pressure, the unfairness part that sand falls the surface just can reach does the desired priming paint sanding of finish paint without bright spot, like this minimum that sand falls paint film 20g/ ㎡, just can reach requirement, only have paint film 60g/ ㎡ on the last plate.
By above contrast, carry out finish paint and the furniture after paint film 60g/ ㎡ carries out finish paint at paint film 100g/ ㎡, fullness ratio differs greatly, and is two kinds of different effects, two kinds of different class, and to the contrast of the wear pattern of grinder also clearly.Grinder is joined one of import abrasive band sand conventional roller transparent priming can sand 300 square metres, one of the transparent priming of sand radium-shine roller special use of the present invention can sand 500 square metres, general 180/ of import abrasive band price, a normal UV furniture coating line one day can 1200 square metres of furniture boards of roller coat, calculate (all the other times calculate dull season and have a rest) in 330 days by actual production in 1 year so:
Sand normal transparent priming paint=(330 * 1200) ÷ 300 * 180=237600 unit
The radium-shine roller dedicated transparent of sand the present invention priming paint=(330 * 1200) ÷ 500 * 180=129600 unit
Differ price=108000 yuan
Conclusion is: the present invention has not only lacked with abrasive band province money but also has promoted quality product in the situation that assurance UV production line machine loss is less, and application prospect is boundless.
Ultraviolet curing transparent priming of the present invention, be highly suitable for radium-shine roller construction, have common UV transparent priming good sanding and transparency, and between paint film layer the semicure recoat without characteristics such as sand millings, have again thick being coated with property (25～35g/ ㎡) and surfacing close to the performance of mirror effect, significantly improved glue spread than traditional roller coat, save the roller coat operation, make grinder not need to transfer too large pressure sand to fall less paint film, just can reach without bright spot by the good priming paint workpiece of sand, guaranteed that the product fullness ratio has promoted quality product, machine loss has been reduced, significantly reduced the abrasive band usage quantity.The whole coating efficiency that improves, application prospect is boundless.
Embodiment
The invention will be further described below in conjunction with specific embodiment.
Each component of the present invention all adopts currently available products, the bisphenol A epoxy acrylate resin that the present invention adopts is by bisphenol A epoxide resin and vinylformic acid (or methacrylic acid) reaction and get, contain aromatic ring and side position hydroxyl in its molecular structure, favourable to improving sticking power, principal feature is: photocuring reaction speed is very fast, cured strength and tensile strength are large, and the chemicals-resistant corrosive nature is excellent.
The polyester acrylate that the present invention adopts is the polyester acrylate resin of two functional groups of modification, and be characterized in: curing speed is fast, and at the bottom of the shrinking percentage, surface drying Canon obtains good grinability.
The urethane acrylate that the present invention adopts is the UV light-cured resin of a kind of two senses of being synthesized by aliphatics carbimide and polyester, HEA etc., its reactive behavior is not as epoxy acrylate, but the snappiness of the increase cured layer that it is unique, improve sticking power, highly polishedly well help improving product fullness ratio and levelling property, the adding of this resin is that transparent priming of the present invention is applicable to one of important factor of radium-shine roller.
The reactive thinner that the present invention adopts is: reagent type Hydroxyethyl acrylate (2-HEA), chemical formula: CH
2=CHCOOCH
2CHOH, contain ethylene double bond in the molecule and can generate side chain with the polymkeric substance of hydroxy functional group with various unsaturated monomer copolymerization, this functional group is fit to the cross-linking polymerization of prepolymerization and post polymerization, be characterized in that consumption is few, dilution property is strong, strengthen the levelling property of product, can play crucial effect at transparent priming of the present invention, can make paint roller on the radium-shine roller spread rapidly levelling out after being coated onto on the furniture board.
Described tripropylene glycol diacrylate (TPGDA) has low viscosity and better snappiness is arranged, and the medium dilution capacity of described trimethylolpropane tris vinylformic acid (TMPTA) provides high curing rate and high crosslink density.
The light trigger that the present invention adopts be Changxing chemistry 6420 and Ying Li 1173, the filling powder of employing is: talcum powder guarantees good grinability with the LH-667 of Liaoning modest and amiable talcum powder group; Transparent powder reduces cost with the TM-2500 of the holy chemical industry of monkey when guaranteeing transparency.
The auxiliary agent that the present invention uses is: anti-settling agent is a kind of ultra-fine, hydrophobic type silicon-dioxide that specific surface area is 220 ㎡/g; Flow agent is the esters of acrylic acid flow agent, has quick levelling and consistency good, but recoatability, and have the performance that presses down bubble, froth breaking concurrently; Wetting dispersing agent adopts EFKA4010, its chemical constitution is modified polyurethane, more than the active ingredient 50-52%, be mainly that stable inorganic pigment comprises carbon black and the macromolecule dispersing agent developed, can reduce jitter time, improve gloss, prevent loose colour and the problem of growing dim, improve pigmenting power, cost performance is good.
Each component that embodiment 1～4 selects and weight and part component model can be but listed product type in being not limited to show as shown in Table 1.
Table one
Below in conjunction with embodiment 1-4 technical scheme of the present invention is described.
Embodiment 1
One, the special-purpose ultraviolet curing transparent priming of preparation radium-shine roller of the present invention:
Get each component according to " embodiment 1 " listed weight in the table one, the preparation method in accordance with the following steps:
Step 1, bisphenol A epoxy acrylate resin, polyester acrylate, urethane acrylate, reagent type Hydroxyethyl acrylate (2-HEA), tripropylene glycol diacrylate (TPGDA), trimethylolpropane tris vinylformic acid (TMPTA), light trigger (Changxing 6420, Tianjin English power 1173), wetting dispersing agent (dust not blocks EFKA4010) and flow agent (prosperous titanium gram MAS) are added container successively, disperse 3-5 minute to evenly with 500PRM;
Step 2, add anti-settling agent (Degussa A200), talcum powder (the modest and amiable LH-667 in Liaoning), transparent powder (the holy chemical industry TM-2500 of monkey) while stirring, after adding, disperse 15-20 minute to fineness≤60 μ m with 1200RPM, 100 orders filter and namely get the special-purpose ultraviolet curing transparent priming of described radium-shine roller.
Two, the using method of the special-purpose ultraviolet curing transparent priming of radium-shine roller of the present embodiment has the following steps:
Paste wooden skin ground-roller coat compound type transparent putty 15～20g/ ㎡, semicure-roller coat transparent priming 15～20g/ ㎡, semicure-radium-shine roller roller coat dedicated transparent priming paint 25～35g/ ㎡, semicure-radium-shine roller roller coat dedicated transparent priming paint 25～35g/ ㎡, full curing-sanding (400 order abrasive band)-roller coat (spraying) UV finish paint or spraying PU(or PE) finish paint.
The traditional performance detected result is shown in " embodiment 1 " corresponding data in the table two.
Embodiment 2
With each listed composition weight of " embodiment 2 " in the table one, repeat example 1 described method (only each composition weight changes), make the special-purpose ultraviolet curing transparent priming of radium-shine roller of embodiment 2, construct according to the using method of the special-purpose ultraviolet curing transparent priming of example 1 radium-shine roller.
The traditional performance detected result is shown in " embodiment 2 " corresponding data in the table two.
Embodiment 3
With each listed composition weight of " embodiment 3 " in the table one, repeat example 1 described method (only each composition weight changes), make the special-purpose ultraviolet curing transparent priming of radium-shine roller of embodiment 3, construct according to the using method of the special-purpose ultraviolet curing transparent priming of example 1 radium-shine roller.
The traditional performance detected result is shown in " embodiment 3 " corresponding data in the table two.
Embodiment 4
With each listed composition weight of " embodiment 4 " in the table one, repeat example 1 described method (only each composition weight changes), make the special-purpose ultraviolet curing transparent priming of radium-shine roller of embodiment 4, construct according to the using method of the special-purpose ultraviolet curing transparent priming of example 1 radium-shine roller.
The traditional performance detected result is shown in " embodiment 4 " corresponding data in the table two.
Table two
Claims (10)
1. a ultraviolet curing transparent priming is characterized in that, comprises the component of following weight percent:
Described auxiliary agent is comprised of the flow agent of the anti-settling agent that accounts for coating gross weight 0.2%, 0.1-0.2% and the wetting dispersing agent of 0.1-0.2%;
Described filling powder is comprised of the talcum powder that accounts for coating gross weight 6-12% and the transparent powder of 4-8%.
2. ultraviolet curing transparent priming as claimed in claim 1 is characterized in that, described bisphenol A epoxy acrylate resin is by bisphenol A epoxide resin and acrylic or methacrylic acid-respons and get, and contains aromatic ring and side position hydroxyl in its molecular structure.
3. ultraviolet curing transparent priming as claimed in claim 2 is characterized in that, described polyester acrylate is the polyester acrylate resin of two functional groups of modification.
4. the ultraviolet curing transparent priming that is applied to the radium-shine roller of woodenware as claimed in claim 1 is characterized in that, described urethane acrylate is the UV light-cured resin by synthetic a kind of two senses of aliphatics carbimide and polyester, HEA.
5. ultraviolet curing transparent priming as claimed in claim 1 is characterized in that, described light trigger adopts 6420 models and the combination of Tianjin English power 1173 models of Changxing chemistry.
6. ultraviolet curing transparent priming as claimed in claim 5 is characterized in that, described anti-settling agent is hydrophobic type silicon-dioxide, and flow agent is the esters of acrylic acid flow agent.
7. the preparation method of a ultraviolet curing transparent priming as claimed in claim 1 is characterized in that, may further comprise the steps:
Step 1, by weight percentage the bisphenol A epoxy acrylate resin in the component, polyester acrylate, urethane acrylate, reagent type Hydroxyethyl acrylate, tripropylene glycol diacrylate, trimethylolpropane tris vinylformic acid, light trigger, wetting dispersing agent and flow agent are added container successively, rotate and disperse 3-5 minute to evenly;
Step 2, while stirring in the component after by weight percentage anti-settling agent, filling powder being joined step 1 and being uniformly dispersed, rotate and disperse 15-20 minute to fineness≤60 μ m, filter and namely get described ultraviolet curing transparent priming.
8. the preparation method of ultraviolet curing transparent priming as claimed in claim 7 is characterized in that, disperses with the 500PRM rotating speed in the described step 1; Disperse with the 1200PRM rotating speed in the step 2.
9. the using method of a ultraviolet curing transparent priming as claimed in claim 1 is characterized in that, may further comprise the steps:
Step 1, the wooden skin ground of subsides;
Step 2, roller coat compound type transparent putty, glue spread 15～20g/ ㎡ carries out semicure;
Step 3, roller coat transparent priming, glue spread 15～20g/ ㎡ carries out semicure;
Step 4, the described ultraviolet curing transparent priming of roller coat, glue spread 25～35g/ ㎡ carries out semicure;
Step 5, the described ultraviolet curing transparent priming of roller coat again, glue spread 25～35g/ ㎡ solidifies entirely;
Sanding is carried out in step 6, employing 400 order abrasive bands;
Step 7, roller coat or spray paint.
10. the using method of ultraviolet curing transparent priming as claimed in claim 9 is characterized in that, in the described step 7, and roller coat or spraying UV finish paint, or spraying PU or PE finish paint.
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