CN102926237B - Wetting liquid for fabric pattern transfer - Google Patents
Wetting liquid for fabric pattern transfer Download PDFInfo
- Publication number
- CN102926237B CN102926237B CN201210463946.2A CN201210463946A CN102926237B CN 102926237 B CN102926237 B CN 102926237B CN 201210463946 A CN201210463946 A CN 201210463946A CN 102926237 B CN102926237 B CN 102926237B
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- Prior art keywords
- acid
- fabric
- water
- fountain solution
- solvent
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- 239000004744 fabric Substances 0.000 title claims abstract description 126
- 239000007788 liquid Substances 0.000 title claims abstract description 11
- 238000009736 wetting Methods 0.000 title abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 60
- 238000000034 method Methods 0.000 claims abstract description 27
- 239000003960 organic solvent Substances 0.000 claims abstract description 27
- 239000002253 acid Substances 0.000 claims abstract description 25
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 239000002904 solvent Substances 0.000 claims abstract description 23
- 239000000835 fiber Substances 0.000 claims abstract description 18
- 229920000742 Cotton Polymers 0.000 claims abstract description 14
- 238000010023 transfer printing Methods 0.000 claims description 39
- 239000000975 dye Substances 0.000 claims description 32
- 210000002268 wool Anatomy 0.000 claims description 32
- 239000000463 material Substances 0.000 claims description 29
- 239000000985 reactive dye Substances 0.000 claims description 23
- 235000011837 pasties Nutrition 0.000 claims description 22
- 239000006096 absorbing agent Substances 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 9
- 229920003043 Cellulose fiber Polymers 0.000 claims description 9
- 239000004677 Nylon Substances 0.000 claims description 9
- 229920001778 nylon Polymers 0.000 claims description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical group CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 8
- 239000002585 base Substances 0.000 claims description 8
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N dimethyl sulfoxide Natural products CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 8
- 239000003292 glue Substances 0.000 claims description 8
- SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 claims description 7
- 229920002472 Starch Polymers 0.000 claims description 7
- 239000000980 acid dye Substances 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 7
- 235000019698 starch Nutrition 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 6
- 239000004202 carbamide Substances 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- 229920002972 Acrylic fiber Polymers 0.000 claims description 5
- 150000001768 cations Chemical class 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 150000001447 alkali salts Chemical class 0.000 claims description 4
- 239000001110 calcium chloride Substances 0.000 claims description 4
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 4
- 150000001720 carbohydrates Chemical class 0.000 claims description 4
- 235000014633 carbohydrates Nutrition 0.000 claims description 4
- 239000004359 castor oil Substances 0.000 claims description 4
- 150000004676 glycans Chemical class 0.000 claims description 4
- 150000007529 inorganic bases Chemical class 0.000 claims description 4
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 4
- 150000007522 mineralic acids Chemical class 0.000 claims description 4
- 150000007524 organic acids Chemical class 0.000 claims description 4
- 150000007530 organic bases Chemical class 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 229920001282 polysaccharide Polymers 0.000 claims description 4
- 239000005017 polysaccharide Substances 0.000 claims description 4
- 108090000623 proteins and genes Proteins 0.000 claims description 4
- 102000004169 proteins and genes Human genes 0.000 claims description 4
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 4
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical group [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 3
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical group N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 3
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 3
- 229920003086 cellulose ether Polymers 0.000 claims description 3
- 235000015165 citric acid Nutrition 0.000 claims description 3
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 3
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 3
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical group [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 3
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 3
- RPAJSBKBKSSMLJ-DFWYDOINSA-N (2s)-2-aminopentanedioic acid;hydrochloride Chemical compound Cl.OC(=O)[C@@H](N)CCC(O)=O RPAJSBKBKSSMLJ-DFWYDOINSA-N 0.000 claims description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 2
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical class CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 claims description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 2
- SAQSTQBVENFSKT-UHFFFAOYSA-M TCA-sodium Chemical compound [Na+].[O-]C(=O)C(Cl)(Cl)Cl SAQSTQBVENFSKT-UHFFFAOYSA-M 0.000 claims description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical group Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 claims description 2
- 235000011054 acetic acid Nutrition 0.000 claims description 2
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 2
- 239000000920 calcium hydroxide Substances 0.000 claims description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 2
- 235000019438 castor oil Nutrition 0.000 claims description 2
- 150000002016 disaccharides Chemical class 0.000 claims description 2
- 150000002170 ethers Chemical class 0.000 claims description 2
- 125000003916 ethylene diamine group Chemical group 0.000 claims description 2
- 235000019253 formic acid Nutrition 0.000 claims description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 2
- 239000001630 malic acid Substances 0.000 claims description 2
- 235000011090 malic acid Nutrition 0.000 claims description 2
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- 235000006408 oxalic acid Nutrition 0.000 claims description 2
- 229940072033 potash Drugs 0.000 claims description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 2
- 235000015320 potassium carbonate Nutrition 0.000 claims description 2
- 235000017550 sodium carbonate Nutrition 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- YNJBWRMUSHSURL-UHFFFAOYSA-N trichloroacetic acid Chemical compound OC(=O)C(Cl)(Cl)Cl YNJBWRMUSHSURL-UHFFFAOYSA-N 0.000 claims description 2
- 230000002209 hydrophobic effect Effects 0.000 abstract description 10
- 238000009941 weaving Methods 0.000 abstract description 5
- 239000002562 thickening agent Substances 0.000 abstract description 3
- 230000002745 absorbent Effects 0.000 abstract 1
- 239000002250 absorbent Substances 0.000 abstract 1
- 238000011109 contamination Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 16
- 235000002639 sodium chloride Nutrition 0.000 description 12
- 230000008595 infiltration Effects 0.000 description 10
- 238000001764 infiltration Methods 0.000 description 10
- 238000007639 printing Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- 238000005406 washing Methods 0.000 description 9
- 229920000297 Rayon Polymers 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 239000004519 grease Substances 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- 239000012752 auxiliary agent Substances 0.000 description 6
- 239000011248 coating agent Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- 239000000982 direct dye Substances 0.000 description 5
- 238000011049 filling Methods 0.000 description 5
- 238000010030 laminating Methods 0.000 description 5
- 239000012528 membrane Substances 0.000 description 5
- 239000002964 rayon Substances 0.000 description 5
- 238000004513 sizing Methods 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical class CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
- 230000007935 neutral effect Effects 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 230000001788 irregular Effects 0.000 description 3
- 238000009940 knitting Methods 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229960001760 dimethyl sulfoxide Drugs 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 210000004209 hair Anatomy 0.000 description 2
- 239000002985 plastic film Substances 0.000 description 2
- 229920006255 plastic film Polymers 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000010022 rotary screen printing Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- -1 10 kilograms Substances 0.000 description 1
- 241000223678 Aureobasidium pullulans Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 238000007774 anilox coating Methods 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 238000010020 roller printing Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 235000011008 sodium phosphates Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000009955 starching Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 150000007984 tetrahydrofuranes Chemical class 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Coloring (AREA)
Abstract
The invention discloses a wetting liquid for fabric pattern transfer. The wetting liquid comprises the following components by weight of 20-80% of water, 10-70% of organic solvent, 3-15% of water absorbent, 0.5-5% of base-releasing agent or acid-releasing agent and 0-20% of solvent-resistant thickener. By wetting the fabric with the wetting liquid, the problem that fabrics of a hydrophobic fabric in the wetting pattern transfer is difficult to wet uniformly is solved relatively thoroughly. The influence of the natural fiber such as cotton comprising the unremovable fat to the fabric wetting when performing the wetting pattern transfer is solved relatively thoroughly. The influence of the oil contamination on the fabric of the hydrophobic fabric in the wetting pattern transfer is removed relatively thoroughly in the process of fabric weaving.
Description
Technical field
The invention belongs to textile printing and dyeing field, fountain solution when particularly a kind of patterns of fabric shifts.
Background technology
It is that wet method shifts that the colored type of natural fabric and polyamide fibre and acrylic fabric shifts the best approach.When wet method shifts, most essential steps is the even dewing of fabric.And in the dewing operation of existing wet transfer printing, the producer only pays close attention to dewing equipment, by the difference of equipment, improve and control the object that reaches even dewing.Such as patent CN2844175 discloses a kind of method of soaking of side transfer printed fabric.Patent CN101643984 discloses the soaking device using in a kind of fabric wet transfer printing process.Patent CN201350725 discloses a kind of quantitative wetting apparatus of transfer printing machine.
These patents are all from equipment angle, to solve the even dewing of fabric.Yet in existing fabric, nylon fabric, acrylic fabric is hydrophobic fiber fabric, and in weaving process, often speckles with the greasy dirt that is difficult to thorough removal.Viscose fabric is artificial fibre, when fiber is manufactured, is often mixed with hydrophobic impurity, often speckles with the greasy dirt that is difficult to removal in weaving process.All-cotton fabric itself contains more hydrophobic impurity and grease, and it is very big that these impurity and grease are removed difficulty when pre-treatment, easily removes the bad fabric capillary effect that causes inconsistent, water capacity difference while causing wet transfer printing.
The fountain solution of existing wet transfer printing wet fabric, its main component is water, in its water, according to the difference of the difference of fabric and dyestuff, be added with a little different auxiliary agents, the surface tension of this fountain solution is large, is difficult to soak speckling with the fabric Quick uniform of greasy dirt in some hydrophobic fiber fabrics or the fabric that contains grease or weaving process.
So, only by the difference of the equipment of soaking, improve and control, want to reach the even dewing effect of the best, be to have suitable difficulty.
Summary of the invention
Fountain solution when technical problem to be solved by this invention is to provide a kind of low surface tension and can shifts the patterns of fabric of weaving greasy dirt or natural oil and have certain solvability and good wetting property on fabric.
For solving the problems of the technologies described above, thinking of the present invention is: water is mixed with organic solvent, become the mixed liquor of water and organic solvent, then add conventional auxiliary agent according to the difference of the difference of the difference of fabric or dyeing and printing process or dyestuff, the fountain solution while forming patterns of fabric transfer.
Concrete technical scheme is:
The fountain solution that patterns of fabric shifts, it comprises the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 0～15%, releasing alkaline agent or acid-releasing agent is 0.5～5%, resistance to solvent pasty materials 0～20%.
Wherein, described organic solvent is strong polarity, and can, with water arbitrarily than the organic solvent dissolving each other, be alcohols, ethers, cellosolve series, amide-type, acetonitrile, ketone, dimethyl sulfoxide (DMSO) or sulfonated castor oil.
Wherein, described water absorbing agent is the material of energy deliquescence water suction in air, and it comprises urea, glycerine, calcium chloride or magnesium chloride etc.
Wherein, described releases alkaline agent for can ionize the material that generates hydroxide ion in solution, it comprises inorganic base, organic base, basic salt or strong base-weak acid salt, wherein, described inorganic base is NaOH, calcium hydroxide or potassium hydroxide, described organic base is ethylenediamine or triethanolamine, and described basic salt is alkali formula calcium chloride, and described strong acid weak base salt is sodium bicarbonate, saleratus, potash, sodium trichloroacetate, tertiary sodium phosphate or soda ash; Described acid-releasing agent is in solution, can ionize to produce hydrionic material, it comprises organic acid, inorganic acid, acid salt or strong acid weak base salt, wherein, described organic acid is formic acid, acetic acid, oxalic acid, citric acid, malic acid or trichloroacetic acid, described inorganic acid is hydrochloric acid, sulfuric acid, phosphoric acid or nitric acid, described acid salt is niter cake or sodium dihydrogen phosphate, and described strong acid weak base salt is ammonium sulfate.
Wherein, described resistance to solvent pasty materials refers in the mixed liquor that can be dissolved in water and organic solvent, and can form polymer substance or the carbohydrate of thick liquid, wherein, described polymer substance is cellulose ether, starch ether, seed glue etherate or glucidtemns, and described carbohydrate is monose or disaccharide or polysaccharide.
Wherein, when adopting padding machine dipping dewing and spray gun spraying dewing, in fountain solution, can not need to add resistance to solvent pasty materials; When adopting wire mark dewing and intaglio plate anilox roll dewing, dewing liquid need to add certain resistance to solvent pasty materials, makes dewing liquid keep certain viscosity.These are all technological means well known to those skilled in the art, and those skilled in the art can, according to different dewing modes, select to add or do not add resistance to solvent pasty materials.
When fabric is cellulose fibre, real silk or wool, when dyestuff is direct dyes, fountain solution is comprised of the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 5～15%, resistance to solvent pasty materials 0.5～20%;
When fabric is cellulose fibre or real silk, when dyestuff is REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 5～15%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0.5～20%;
When fabric is real silk, nylon or wool, when dyestuff is ACID DYES or REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 5～15%, acid-releasing agent is 1～5%, resistance to solvent pasty materials 0.5～20%;
When fabric is acrylic fibers, when dyestuff is cation dyes, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 3～7%, acid-releasing agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
When fabric is all-cotton fabric, dyestuff is REACTIVE DYES, and when color fixing process is cold dome fixation, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0～20%;
When fabric is wool or real silk, dyestuff is REACTIVE DYES or ACID DYES, and when color fixing process is cold dome fixation, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, acid-releasing agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
When fabric is that cellulose fibre (as cotton, viscose glue, day silk etc.) interweaves with protein fibre (as real silk, wool, fibre and soya, milk fibre) or during blending, fountain solution formula is with reference to the fountain solution formula of cellulose base fiber fabric.
When fabric is cellulose fibre and protein fibre interweaves or during blending, when dyestuff is direct dyes, fountain solution is comprised of the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 5～15%, resistance to solvent pasty materials 0.5～20%;
When fabric is cellulose fibre and protein fibre interweaves or during blending, when dyestuff is REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 5～15%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
In addition, at kinds of fibers, be cellulose fibre, when dyestuff is direct dyes, in order to increase the affinity between dyestuff and fiber, increase the dye-uptake of dyestuff, in fountain solution, can add the neutral inorganic of 1～5wt%; At kinds of fibers, be cellulose fibre, cocoon fiber, when dyestuff is REACTIVE DYES, in order to increase the affinity between dyestuff and fiber, increase the dye-uptake of dyestuff, in fountain solution, can add the neutral inorganic of 1～5wt%.These are all technology well known to those skilled in the art, those skilled in the art can be according to different dyestuffs the infiltration on fabric and color depth situation, select to add or do not add neutral inorganic.
Wherein, neutral inorganic refers to the salt that the neutralization reaction of strong acid and strong base generates, and generally conventional is sodium chloride, sodium sulphate, potassium chloride, potassium sulfate etc.
Beneficial effect: compare with conventional fountain solution in fountain solution when patterns of fabric of the present invention shifts, because contain low surface tension, to greasy dirt, organic solvent that grease solvability is powerful, so, it has following beneficial effect: on the one hand, it is compared with conventional fountain solution, has very low surface tension, easily hydrophobic substance is infiltrated.On the other hand, the organic solvent of strong polarity has the extremely strong solvability to greasy dirt or grease, and fountain solution of the present invention can dissolve greasy dirt or grease, eliminates greasy dirt or grease to wetting impact.Also have, fountain solution of the present invention is larger to the solubility of dyestuff, and dissolution velocity is faster, and the rate of transform is higher.
Wetting to fabric by fountain solution of the present invention, the wet method that has solved more thoroughly hydrophobic fiber fabric spends fabric in type transfer to be difficult to evenly wetting problem.Solved more thoroughly natural fabric as cotton, the wetting impact of fabric when containing the grease that is difficult to remove on wool fabric wet method flower type being shifted.Solved more thoroughly the wetting impact of fabric when being infected with greasy dirt in face weave process wet method flower type being shifted.
The specific embodiment
According to following embodiment, the present invention may be better understood.Yet, those skilled in the art will readily understand, the described content of embodiment is only for the present invention is described, and should also can not limit the present invention described in detail in claims.
Embodiment 1:
Fetch water 100 kilograms, add 30 kilograms of ethanol, stir; Add 10 kilograms of urea, 2.5 kilograms of citric acids, stir, and until completely dissolved, add 8 kilograms of seed glue etherate PS-14, stir, and treat that PS-14 dissolves completely, form slurry, stand-by again.
Get 50 meters and be subject to oil pollution, the nylon elastic knitted cloth that is difficult to complete wipe oil is some, with single chromatography rotary screen printing machine, will coat nylon elastic knitted cloth surface with spreading mass, again by the pasting face laminating of the printing surface of ACID DYES transfer film and nylon elastic knitted cloth, pressurization, the ACID DYES on transfer film has just been transferred on nylon elastic fabric uniformly.Through decatize, washing, the rear arrangements such as sizing, transfer printing nylon elastic knit fabric.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good, and greasy dirt place Dry Sack is impact not.Comparative example 1:
More than, in formula, 30 kg of water are replaced to 30 kilograms of ethanol, all the other compositions and ratio are in full accord.
Get same fabric some, by same acid transfer membrane and same method transfer printing, obtain nylon elastic knitted cloth transfer printing fabric.
By range estimation, can obviously find out, color is relatively light, and Dry Sack is deep mixed, has the greasy dirt place fabric core that shows money or valuables one carries unintentionally, and the infiltration of flower type is bad.
Embodiment 2:
Fetch water 75 kilograms, add 17 kilograms of sulfonated castor oils, stir, then add 2 kilograms, caustic soda, 5 kilograms of salt, stir, and caustic soda and salt are dissolved completely, stand-by.
Get the irregular woven cotton fabric of kiering some, with above solution, insert in common evenness calender charging spout, regulate evenness calender pressure, allow cotton pass evenness calender quick humidification, again the printing surface of REACTIVE DYES transfer paper and wetting cotton are fitted, through cold-transfer printing machine, the REACTIVE DYES on REACTIVE DYES transfer paper has just been transferred on cotton.Use cold dome color fixing process, be about to this cotton PE plastic film wrapped, prevent moisture evaporation, after standing 10 hours, washing, dries, shape, transfer printing cotton.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good, and kiering is irregular on not impact of Dry Sack.
Comparative example 2:
More than, in formula, 10 kg of water are replaced to 10 kilograms of sulfonated castor oils, all the other compositions and ratio are in full accord.
Get same fabric some, by same REACTIVE DYES transfer paper and same method transfer printing, obtain cotton transfer printing fabric.
By range estimation, can obviously find out, color is relatively light, and Dry Sack is deep mixed, has obvious look shallow and white core at the irregular place of destarch.
Embodiment 3:
Fetch water 30 kilograms, add 70 kilograms of ethyl cellosolves, stir, then add 1.5 kilograms of ammonium sulfate, 3 kilograms of glycerine, 7 kilograms of urea, 1.2 kilograms of hydroxypropyl methylcelluloses (belonging to cellulose ether), stir, treat that auxiliary agent and resistance to solvent pasty materials dissolve completely, form slurry, stand-by.
Get wool knitted fabric some, in order to spreading mass, insert in the charging spout of intaglio plate coating roller, start intaglio plate coating roller, allow and with spreading mass, be coated on the surface of wool knitted fabric, again by the coated face laminating of the printing surface of reactive dye for wool transfer film and wool fabric, enter cold-transfer printing machine transfer printing, after reactive dye for wool is transferred on wool knitted fabric, dry, decatize, washing, sizing, transfer printing wool knitted fabric.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good.
Comparative example 3:
More than, in formula, 70 kg of water are replaced to 70 kilograms of ethyl cellosolves, all the other compositions are consistent with ratio.
Get same wool knitting fabrics some, by same reactive dye for wool transfer membrane and same method transfer printing, when intaglio plate coating roller rolling pulp material, can find, because wool fabric is hydrophobic fabric, slurry can not infiltrate wool fabric, and wool fabric can not be wetting by intaglio plate coating roller, and transfer printing can not complete.
Embodiment 4:
Fetch water 50 kilograms, 50 kilograms of dimethyl formamides, stir, and add 4 kilograms, sodium bicarbonate, 15 kilograms, urea, 3.5 kilograms of glauber salt, stir, and finally add 2.5 kilograms of sodium carboxymethyl starches (belonging to starch ether), stir, treat that sodium carboxymethyl starch dissolves completely, form pulpous state, stand-by.
Get and be woven oil pollution, it is some that pre-treatment is difficult to the rayon satin that removes, the charging spout of evenness calender will be placed in spreading mass, regulate evenness calender pressure, allow rayon satin pass evenness calender quick humidification, the printing surface of REACTIVE DYES transfer paper is fitted with wetting rayon satin, through cold-transfer printing machine, the REACTIVE DYES on REACTIVE DYES transfer paper has just been transferred on cotton again.Dry, decatize, washing, sizing, transfer printing rayon satin.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good, and greasy dirt place Dry Sack is impact not.Comparative example 4:
Dimethyl formamide in filling a prescription is above substituted by 50 kg of water, and all the other compositions are consistent with ratio.
Get same fabric some, by same REACTIVE DYES transfer paper and same method transfer printing, obtain rayon satin's transfer printing fabric.
By range estimation, can obviously find out, color is relatively light, and Dry Sack is deep mixed, at greasy dirt, has obvious look shallow and white core everywhere.
Embodiment 5:
Fetch water 60 kilograms, 40 kilograms, acetone, mixes, and stirs, and adds 1 kilogram of sodium chloride, 7 kilograms of glycerine, and 20 kilograms of sucrose, stir, and treat that sucrose and sodium chloride are dissolved into pulpous state completely, stand-by.
Get that to move back glue silk knitting fabric not to the utmost some, in order to spreading mass, insert in the charging spout of intaglio plate coating roller, start intaglio plate coating roller, allow and with spreading mass, be coated with the surface of silk knitting fabric, then the coated face of the printing surface of direct dyes transfer film and real silk knitted cloth fabric is fitted, enter cold-transfer printing machine transfer printing, dry decatize, washing, sizing, becomes transfer printing real silk knitted fabrics.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good, moves back glue not to the utmost on not impact of Dry Sack.
Comparative example 5:
In filling a prescription above, acetone substitutes by 40 kg of water, and all the other compositions are consistent with ratio.
Get same fabric some, by same direct dyes transfer membrane and same method transfer printing, obtain real silk knitted transfer printing fabric.
By range estimation, can obviously find out, color is relatively light, and Dry Sack is deep mixed, moves back glue and locates not to the utmost obviously to paint shallow and white core.
Embodiment 6:
Fetch water 80 kilograms, 30 kilograms of methyl-sulfoxides, mix, and stir, and add 3 kilograms of sodium dihydrogen phosphates, and 6 kilograms of glycerine, get 8 kilograms of yellow starch gums (belonging to glucidtemns), stir, and treat that auxiliary agent and yellow starch gum dissolve completely, and the slurry that poling is thin is stand-by.
Get acrylic fibers knitted cloth some, will add in spray gun with spreading mass, regulate spray gun air pressure, slurry is evenly sprayed on to fabric surface, gets the spray-coating surface laminating of cation dyes transfer film and fabric, put into cold-transfer printing machine, pressurization, cation dyes have just been dissolved on acrylic fabric.Dry, decatize, washing, sizing, transfer printing acrylic fabric.
By range estimation, can obviously find out, color is deeply dense, and Dry Sack is even, and infiltration is good.
Comparative example 6:
In filling a prescription above, methyl-sulfoxide substitutes by 30 kg of water, and all the other compositions are consistent with ratio.
Get same acrylic fibers knitted cloth some, by same cation dyes transfer membrane and same method transfer printing, because acrylic fibers knitted cloth is hydrophobic fabric, with spreading mass, can not permeate in fabric inside, and at fabric surface sediment, trickling, can not carry out transfer printing.
Embodiment 7:
Get 65 kg of water, add 35 kilograms of oxolanes, then add 0.6 kilogram of niter cake, add 2 kilograms of Aureobasidium pullulans polysaccharide, stir, treat that auxiliary agent and thickener are dissolved into thick liquid completely, stand-by.
On rotary screen printing machine, load onto 120Mu garden net, above thick liquid is coated on to wool fabric surface, by the printing surface of ACID DYES transfer film and the laminating of wool fabric coated face, put into wet transfer printing machine and shift, after transfer finishes, use cold dome fixation, both by plastic film wrapped, completed the wool fabric that dyestuff shifts, prevent moisture evaporation, after 24 hours, tear wrap film off, washing, dries.
By range estimation, can find, color is full, and infiltration is good, and the Dry Sack of the left, center, right of fabric is even, does not reveal white core phenomenon.
Comparative example 7:
Change the oxolane in filling a prescription above into 35 kg of water, all the other compositions and constant rate.After above identical printing transferring method and color-fixing method, washing, is dried into transfer printing wool fabric finished product.
By range estimation, can obviously see, on transfer membrane, dyestuff is residual many, wool stamp finished product of light color, fabric has very serious left, center, right aberration, has serious dew white core phenomenon.
Embodiment 8:
Fetch water 50 kilograms, 45 kilograms of acetonitriles, add 3 kilograms of tertiary sodium phosphates, 10 kilograms, urea, and 3 kilograms of pulullan polysaccharides, stir, and treat that auxiliary agent and thickener are dissolved into thick liquid completely, stand-by.
Get wool content 50%, the blending cut velvet hair wool fabric of viscose glue content 50%, with intaglio plate starching machine, use 50 order intaglio plate applicator rolls to be uniformly coated on cut velvet hair wool fabric surface with spreading mass, by the printing surface of REACTIVE DYES transfer paper and coated face laminating, enter wet transfer printing machine transfer printing, after transfer printing, tear transfer paper off, dry decatize, washing, dry again, transfer printing cut velvet hair wool fabric.
By range estimation, can find out, dyestuff penetration is dark, can be penetrated into the reverse side of mao wool fabric, and Dry Sack is rich and gaudy, and the suitable of the stamp place fine hair of cut velvet hair wool fabric can not cause colored type show-through.
Comparative example 8:
Acetonitrile in filling a prescription is above replaced to all the other compositions and constant rate by 45 kg of water.Use the same method transfer printing of same fabric, obtain wool blended vertical fluff woolen cloth transfer printing fabric.
By range estimation, can find out, the infiltration of dyestuff is shallow, only floats over cut velvet hair wool fabric surface, and the suitable of cut velvet fabric stamp place fine hair can cause serious grinning effect.
Claims (8)
1. the fountain solution that patterns of fabric shifts, is characterized in that, it comprises the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 0～15%, releasing alkaline agent or acid-releasing agent is 0.5～5%, resistance to solvent pasty materials 0～20%;
Described resistance to solvent pasty materials refers in the mixed liquor that can be dissolved in water and organic solvent, and can form polymer substance or the carbohydrate of thick liquid, wherein, described polymer substance is cellulose ether, starch ether, seed glue etherate or glucidtemns, and described carbohydrate is monose or disaccharide or polysaccharide.
2. the fountain solution that patterns of fabric according to claim 1 shifts, it is characterized in that, described organic solvent is strong polarity, and can, with water arbitrarily than the organic solvent dissolving each other, be alcohols, ethers, cellosolve series, amide-type, oxolane, acetonitrile, ketone, dimethyl sulfoxide (DMSO) or sulfonated castor oil.
3. the fountain solution that patterns of fabric according to claim 1 shifts, is characterized in that, described water absorbing agent is the material of energy deliquescence water suction in air, and described water absorbing agent is urea, glycerine, calcium chloride or magnesium chloride.
4. the fountain solution that patterns of fabric according to claim 1 shifts, it is characterized in that, described releases alkaline agent for can ionize the material that generates hydroxide ion in solution, the described alkaline agent of releasing is inorganic base, organic base, basic salt or strong base-weak acid salt, wherein, described inorganic base is NaOH, calcium hydroxide or potassium hydroxide, described organic base is ethylenediamine or triethanolamine, described basic salt is alkali formula calcium chloride, and described strong acid weak base salt is sodium bicarbonate, saleratus, potash, sodium trichloroacetate, tertiary sodium phosphate or soda ash; Described acid-releasing agent is in solution, can ionize to produce hydrionic material, it comprises organic acid, inorganic acid, acid salt or strong acid weak base salt, wherein, described organic acid is formic acid, acetic acid, oxalic acid, citric acid, malic acid or trichloroacetic acid, described inorganic acid is hydrochloric acid, sulfuric acid, phosphoric acid or nitric acid, described acid salt is niter cake or sodium dihydrogen phosphate, and described strong acid weak base salt is ammonium sulfate.
5. the fountain solution that patterns of fabric according to claim 1 shifts, is characterized in that,
When fabric is cellulose fibre or real silk, when dyestuff is REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 5～15%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0.5～20%;
When fabric is real silk, nylon or wool, when dyestuff is ACID DYES or REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 5～15%, acid-releasing agent is 0.5～5%, resistance to solvent pasty materials 0.5～20%;
When fabric is acrylic fibers, when dyestuff is cation dyes, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, water absorbing agent 3～7%, acid-releasing agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
6. the fountain solution that patterns of fabric according to claim 1 shifts, is characterized in that,
When fabric is all-cotton fabric, dyestuff is REACTIVE DYES, and when color fixing process is cold dome fixation, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0～20%;
When fabric is wool or real silk, dyestuff is REACTIVE DYES or ACID DYES, and when color fixing process is cold dome fixation, fountain solution is comprised of the component of following percentage by weight: water 20～80%, and organic solvent 10～70%, acid-releasing agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
7. the fountain solution that patterns of fabric according to claim 1 shifts, is characterized in that,
When fabric is cellulose fibre and protein fibre interweaves or during blending, when dyestuff is REACTIVE DYES, fountain solution is comprised of the component of following percentage by weight: water 20～80%, organic solvent 10～70%, water absorbing agent 5～15%, releasing alkaline agent is 1～5%, resistance to solvent pasty materials 0.5～20%.
8. the application of the fountain solution that patterns of fabric claimed in claim 1 shifts in wet transfer printing.
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| CN103243593B (en) * | 2013-05-17 | 2015-04-08 | 刘静 | Wetting solution for wet-process transfer printing of hydrophobic fiber fabric |
| CN103276611B (en) * | 2013-06-09 | 2015-07-08 | 东华大学 | Dyeing method adopting activated dye with high fixation rate |
| CN105951484B (en) * | 2016-05-24 | 2019-07-12 | 常州旭荣针织印染有限公司 | Wool fabric wet method transfer printing method |
| CN106012594B (en) * | 2016-06-24 | 2019-03-15 | 常州旭荣针织印染有限公司 | Milk protein fiber/cotton fiber union wet method transfer printing method |
| CN106120405B (en) * | 2016-07-26 | 2019-11-01 | 常州旭荣针织印染有限公司 | Terylene fibre/cotton fibre mixed union wet method transfer printing method |
| CN107034700A (en) * | 2016-11-03 | 2017-08-11 | 江苏海云花新材料有限公司 | A kind of dyeing nylon acid-releasing agent and preparation method thereof |
| CN108239887B (en) * | 2016-12-27 | 2020-07-31 | 长胜纺织科技发展(上海)有限公司 | Pretreatment method for plate-alignment liquid feeding |
| CN107083698B (en) * | 2017-04-07 | 2021-05-25 | 常州旭荣针织印染有限公司 | Padding liquid for wet transfer printing of chinlon fabric and its compounding process |
| CN111118717A (en) * | 2019-12-31 | 2020-05-08 | 江苏东源纺织科技实业有限公司 | Production process of natural antibacterial skin-friendly environment-friendly knitted fabric |
| CN116657413A (en) * | 2023-05-05 | 2023-08-29 | 中山市鸿盛生物科技有限公司 | Washing method of tencel jean garment |
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| US7604856B2 (en) * | 2000-10-31 | 2009-10-20 | Neenah Paper, Inc. | Heat transfer paper with peelable film and discontinuous coatings |
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