CN105862463A - Turquoise blue reserve printing method - Google Patents
Turquoise blue reserve printing method Download PDFInfo
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- CN105862463A CN105862463A CN201610315197.7A CN201610315197A CN105862463A CN 105862463 A CN105862463 A CN 105862463A CN 201610315197 A CN201610315197 A CN 201610315197A CN 105862463 A CN105862463 A CN 105862463A
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- printing
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- turquoise blue
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M1/00—Inking and printing with a printer's forme
- B41M1/26—Printing on other surfaces than ordinary paper
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67383—Inorganic compounds containing silicon
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention relates to a reactive dye reserve printing method, in particular to reactive turquoise blue reserve printing. A turquoise blue reserve printing method is characterized in that 2-10 wt% of at least one of tartaric acid, maleic acid, citric acid, itaconic acid and ammonium sulfate is taken as a reserve printing acid agent and is completely dissolved by a specified amount of deionized water; 0-5 wt% of water glass serving as an adhesive and a physical blocker is added, a stirrer is used for high-speed and even stirring, and the pH value of solution is controlled to be 2-4; 5-10% of at least one of solid hydroxyethyl gleditsia sinensis gum, guar gum, starch and tamarind gum is added and taken as reserve printing paste, reserve printing slurry is prepared after high-speed stirring for 1-2 hours, and the viscosity is controlled to be 30000 mPa.s-80000 mPa.s. During reserve printing, the reserve printing slurry is prepared firstly, then color paste scrapping and printing is performed, drying at 85 EDG C and ageing with saturated vapor at 102 DEG C for 8 min are performed, cold washing is performed twice, 1-5 g/L of a soaping agent for staining resistance is used for hot washing at 90-100 DEG C, and then cold washing and drying are performed.
Description
Technical field
The present invention relates to the resist printing stamp of reactive turquoise blue dyestuff, belong to textile printing and dyeing field.
Background technology
Resist printing stamp is the method utilizing over print (wet method over print) on printing machine, reaches the effect of resisting printing.Resist printing stamp is identical with resisting printing mechanism, but resist printing stamp production process is short, and technique is flexible, and a flower pattern can use multiple resist printing technique, and printing effect is good.Print the inverted style of the depth, dark completely in the special flower pattern such as fine little Hua, leaf and vein time, owing to these gradations enrich, third dimension is relatively strong, uses directly not only to spending difficulty, its profile is also difficult to obtain the effect of continuous and derivable, but resist printing stamp can solve these problems.
The widely used resist printing printing technology of current each printing and dyeing enterprise substantially has 2 types, the first is resist printing for reduction, sodium sulfite reacts generation vinyl sulfone(RemzaolHuo Xingranliaohuoxingjituan) sulfonate sodium so that vinylsulfone reactive dyes inactivation with the ethylene sulfuryl of vinyl-sulfone reactive dyes, utilizes this chemical reaction can realize white resist printing and the anti-stamp of color of a resist printing vinylsulfone reactive dyes of chloro-s-triazine reactive dye of vinylsulfone reactive dyes.The second is acid resist printing, i.e. by the alkaline agent in acidic materials and in printing with reactive dye mill base, destroys the environment that reactive dye are bonded with fiber.
Reactive turquoise blue dyestuff be a kind of parent be the reactive dye of C.I. Pigment Blue 15, beautiful in colour owing to it is cheap, after stamp, light fastness is high, and is widely used in printing with reactive dye, is usually used in bright green, the colorant match of gorgeous indigo plant.But reactive turquoise blue parent flatness is big, has the highest affinity to fiber, in resist printing stamp, it is particularly easy to that resist printing unclean problem occurs, has a strong impact on Printing quality and style.Chinese patent CN104562747A discloses Resist printing of cotton fabric with reactive dyestuffs technique, in this patent White-resistant pulp comprise that coating is white, binding agent, emulsion thickening and sodium sulfate, resist printing reactive dye require little to the affinity of cotton fiber, is easily there is the cleanest resist printing problem in the dyestuff that affinity is high.D Brierley and J R Provost article points out that sodium silicate can be used for resist printing carboxylic acid esters disperse dyes, first sodium silicate can make Dispersol PC type disperse dyes carboxyester hydrolysis become the higher carboxylate of water solublity as alkaline agent thus lose polyster fibre affinity, secondly sodium silicate can form polymer morphology after pH value reduces, this intermediary is similar to layer of gel thus intercepts disperse dyes and contact with polyster fibre, therefore sodium silicate has the resist printing effect of physics (D Brierley and J R Provost, JSDC Volume 99 December
1983), article but not being mentioned, sodium silicate is for the resist printing stamp of reactive dye.
Summary of the invention
In order to solve the problems referred to above, a kind of method that the invention provides resist printing reactive turquoise blue, use sodium silicate and non-volatile organic monoacid, use chemistry resist printing and physics resist printing mode that combines resist printing reactive turquoise blue dyestuff.
Reactive turquoise blue dyestuff is resist printing, and to be the most only primarily due to reactive turquoise blue parent flatness big, fiber is had the highest affinity, during stamp on bar magnet or spatual printing to cotton fiber, owing to it has high-affinity to cotton fiber thus it is difficult to eccysis thus occurs resist printing the cleanest.The present invention use non-volatile organic monoacid as resist printing acid agent, organic acid can neutralize the alkaline agent in mill base, sour environment is provided thus stops reactive dye to react with cellulose fibre, can reduce at the non-volatile organic monoacid of the process of evaporating and other site color are affected, reduce bafta strength loss.Use acid resistance thickener as thickening agent, control anti-printing paste high viscosity and be effectively reduced contacting of reactive dye and fiber.Sodium silicate can form polymer morphology in acid condition, and this intermediary is similar to layer of gel thus intercepts reactive dye and fiber contacts, and therefore sodium silicate has the resist printing effect of physics.In water-washing process hot water wash control temperature 90～100 DEG C and add releasing soaping agent can effective eccysis absorption reactive dye on fiber prevent the contamination of high-affinity reactive dye in vain.
At least one in 2～10wt% tartaric acid, maleic acid, citric acid, itaconic acid, ammonium sulfate is completely dissolved by the present invention as resist printing acid agent deionized water；Add 0～5wt% waterglass as binding agent and physical barrier agent, by agitator high-speed stirred uniformly, control solution ph 2～4；Add 5～10% solid hydroxyethyl saponin gum, guar gum, starch, tamarind gum at least one as resist printing thickener, make anti-printing paste through high-speed stirred 1～2 hours, control viscosity 30000 mPa s～80000 mPa s.Scraping mill base after first anti-printing paste being printed on fabric during resist printing stamp again, after 85 DEG C of drying, 102 DEG C of saturated vapors evaporate 8min, cold water washes twice, then soaps at 90～100 DEG C with 1～5 g/L releasing soaping agents, and last hot water wash, cold water are washed and dried.
Detailed description of the invention
Being further described technical scheme below by embodiment, following example are to further illustrate the present invention, but are not limitation of the present invention.
A kind of method of resist printing reactive turquoise blue, comprises the following steps:
(1) at least one in 2～10wt% tartaric acid, maleic acid, citric acid, itaconic acid, ammonium sulfate is completely dissolved as resist printing acid agent deionized water；Add 0～5wt% waterglass as binding agent and physical barrier agent, by agitator high-speed stirred uniformly, control solution ph 2～4；Add 5～10% solid hydroxyethyl saponin gum, guar gum, starch, tamarind gum at least one as resist printing thickener, make anti-printing paste through high-speed stirred 1～2 hours, control viscosity 30000 mPa s～80000 mPa s；
(2) mill base is scraped again after the anti-printing paste that step (1) prepares being printed on fabric, after 85 DEG C of drying, 102 DEG C of saturated vapors evaporate 8min, cold water washes twice, then soaps at 90～100 DEG C with 1～5 g/L releasing soaping agents, and last hot water wash, cold water are washed and dried.
Embodiment
1
Prepared by anti-printing paste: 6wt% citric acid is spent 86wt% deionized water and is completely dissolved, add 2wt% waterglass Glass rod to stir, solution ph 2～4 is controlled with extensive pH value reagent paper, under agitator stirs, 6wt% guar gum is added in solution, it is gradually increased rotating speed high-speed stirred 1～2 hours, with the resist printing slurry viscosity of viscosity meter at 30000～80000 mPa s, standby.
Prepared by reactive printing mill base: precise 80wt% deionized water, is sequentially added into 10wt% carbamide, 5wt% sodium bicarbonate, 1wt% reserve salt s, 4wt% solid sodium alginate, by agitator high-speed stirred 2 hours, expanded 24 hours the former paste of stamp.Precise 5wt% reactive turquoise blue WGFN, melts with 47.5wt% deionized water, adds the 47.5wt% former paste of above-mentioned sodium alginate and stirs to obtain reactive printing mill base.
The anti-printing paste prepared by above-mentioned formula and mill base are used for resist printing stamp of pure cotton fabric, dry, by saturated vapor decatize 8min, then carry out washing and soap.Concrete white resist printing flow process is as follows: pure cotton fabric → scrape anti-printing paste lines (3mm/s, 3V) → over print mill base (3mm/s, 5V) → dry (85 DEG C, 3min) → decatize (102 DEG C, 8min) → first room temperature washing → second room temperature wash → 90～100 DEG C of hot water soap → cold water washes → dries.Resist printing cloth specimen have excellence resist printing whiteness, resist printing lines fineness good.
Embodiment
2
Prepared by anti-printing paste: be completely dissolved by 7wt% citric acid 85wt% deionized water, add 2wt% waterglass Glass rod to stir, solution ph 2～4 is controlled with extensive pH value reagent paper, under agitator stirs, 6wt% hydroxyethyl saponin gum is added in solution, it is gradually increased rotating speed high-speed stirred 1～2 hours, with the resist printing slurry viscosity of viscosity meter at 30000～80000 mPa s, standby.
Prepared by reactive printing mill base: precise 80wt% deionized water, is sequentially added into 10wt% carbamide, 5wt% sodium bicarbonate, 1wt% reserve salt s, 4wt% solid sodium alginate, by agitator high-speed stirred 2 hours, expanded 24 hours the former paste of stamp.Precise 5wt% reactive turquoise blue BPSA, melts with 47.5wt% deionized water, adds the 47.5wt% former paste of above-mentioned sodium alginate and stirs to obtain reactive printing mill base.
The anti-printing paste prepared by above-mentioned formula and mill base are used for resist printing stamp of pure cotton fabric, dry, by saturated vapor decatize 8min, then carry out washing and soap.Concrete white resist printing flow process is as follows: pure cotton fabric → scrape anti-printing paste lines (3mm/s, 3V) → over print mill base (3mm/s, 5V) → dry (85 DEG C, 3min) → decatize (102 DEG C, 8min) → first room temperature washing → second room temperature wash → 90～100 DEG C of hot water soap → cold water washes → dries.Resist printing cloth specimen have excellence resist printing whiteness, resist printing lines fineness good.
Embodiment
3
Prepared by anti-printing paste: be completely dissolved by 7wt% citric acid 85wt% deionized water, add 2wt% waterglass Glass rod to stir, solution ph 2～4 is controlled with extensive pH value reagent paper, under agitator stirs, 6wt% hydroxyethyl saponin gum is added in solution, it is gradually increased rotating speed high-speed stirred 1～2 hours, with the resist printing slurry viscosity of viscosity meter at 30000～80000 mPa s, standby.
Prepared by reactive printing mill base: precise 80wt% deionized water, is sequentially added into 10wt% carbamide, 5wt% sodium bicarbonate, 1wt% reserve salt s, 4wt% solid sodium alginate, by agitator high-speed stirred 2 hours, expanded 24 hours the former paste of stamp.Precise 5wt% reactive turquoise blue BPSA, 0.3wt% reactive blue P-3R, melts with 47.4wt% deionized water, adds the 47.3wt% former paste of above-mentioned sodium alginate and stirs to obtain reactive printing mill base.
The anti-printing paste prepared by above-mentioned formula and mill base are used for resist printing stamp of pure cotton fabric, dry, by saturated vapor decatize 8min, then carry out washing and soap.Concrete white resist printing flow process is as follows: pure cotton fabric → scrape anti-printing paste lines (3mm/s, 3V) → over print mill base (3mm/s, 5V) → dry (85 DEG C, 3min) → decatize (102 DEG C, 8min) → first room temperature washing → second room temperature wash → 90～100 DEG C of hot water soap → cold water washes → dries.Resist printing cloth specimen have excellence resist printing whiteness, resist printing lines fineness good.
Claims (2)
1. the method for a resist printing reactive turquoise blue, it is characterised in that comprise the following steps:
(1) at least one in 2～10wt% tartaric acid, maleic acid, citric acid, itaconic acid, ammonium sulfate is completely dissolved as resist printing acid agent deionized water；Add 0～5wt% waterglass as binding agent and physical barrier agent, by agitator high-speed stirred uniformly, control solution ph 2～4；Add 5～10% solid hydroxyethyl saponin gum, guar gum, starch, tamarind gum at least one as resist printing thickener, make anti-printing paste through high-speed stirred 1～2 hours；
(2) mill base is scraped again after the anti-printing paste that step (1) prepares being printed on fabric, after 85 DEG C of drying, 102 DEG C of saturated vapors evaporate 8min, cold water washes twice, then soaps at 90～100 DEG C with 1～5 g/L releasing soaping agents, and last hot water wash, cold water are washed and dried.
The method of a kind of resist printing reactive turquoise blue the most according to claim 1, it is characterised in that the viscosity of described anti-printing paste is 30000
MPa s～80000 mPa s.
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| CN201610315197.7A CN105862463B (en) | 2016-05-14 | 2016-05-14 | A kind of method of resist printing reactive turquoise blue |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106592266A (en) * | 2016-11-25 | 2017-04-26 | 山东黄河三角洲纺织科技研究院有限公司 | Hot-melting anti-printing method for polyamide-ester fabric |
| CN107747241A (en) * | 2017-11-09 | 2018-03-02 | 沈阳工业大学 | A kind of White-resistant pulp resist printing for reactive dye physics and preparation method thereof |
| CN108517703A (en) * | 2018-05-11 | 2018-09-11 | 临清三和纺织集团有限公司 | A kind of preparation for the resist printing White-resistant pulp of reactive dye physics |
| CN109440496A (en) * | 2018-10-31 | 2019-03-08 | 山东华晨彩装科技有限公司 | A kind of white resist printing method for active emerald green orchid 21 |
| CN111118937A (en) * | 2020-02-25 | 2020-05-08 | 青岛德润宁纺织材料有限公司 | Preparation method of anti-printing auxiliary agent for reactive dye anti-printing |
| CN111593585A (en) * | 2020-05-27 | 2020-08-28 | 山东黄河三角洲纺织科技研究院有限公司 | Method for printing-proof reactive dye on cation modified cotton fabric |
| CN113897801A (en) * | 2021-11-18 | 2022-01-07 | 张启磊 | Preparation method of anti-printing auxiliary agent for reactive dye anti-printing |
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| CN103374840A (en) * | 2012-04-16 | 2013-10-30 | 谢红英 | Reactive dye color resisting printing |
| CN104562747A (en) * | 2013-10-15 | 2015-04-29 | 青岛三秀新科技复合面料有限公司 | Activated dye resist printing technology for cotton fabric |
| CN105133390A (en) * | 2015-10-14 | 2015-12-09 | 广东溢达纺织有限公司 | Novel dyeing method of reactive dyes |
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2016
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| WO2002066730A1 (en) * | 2001-02-22 | 2002-08-29 | Toa Kasei Co., Ltd. | Method for dyeing cellulose fiber containing material and cellulose fiber containing article dyed by said dyeing method |
| CN103374840A (en) * | 2012-04-16 | 2013-10-30 | 谢红英 | Reactive dye color resisting printing |
| CN104562747A (en) * | 2013-10-15 | 2015-04-29 | 青岛三秀新科技复合面料有限公司 | Activated dye resist printing technology for cotton fabric |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106592266A (en) * | 2016-11-25 | 2017-04-26 | 山东黄河三角洲纺织科技研究院有限公司 | Hot-melting anti-printing method for polyamide-ester fabric |
| CN106592266B (en) * | 2016-11-25 | 2019-02-22 | 山东黄河三角洲纺织科技研究院有限公司 | A kind of anti-impression method of polyamide -ester plus material hot melt |
| CN107747241A (en) * | 2017-11-09 | 2018-03-02 | 沈阳工业大学 | A kind of White-resistant pulp resist printing for reactive dye physics and preparation method thereof |
| CN107747241B (en) * | 2017-11-09 | 2020-04-14 | 沈阳工业大学 | White-proof pulp for physical anti-printing of reactive dye and preparation method thereof |
| CN108517703A (en) * | 2018-05-11 | 2018-09-11 | 临清三和纺织集团有限公司 | A kind of preparation for the resist printing White-resistant pulp of reactive dye physics |
| CN109440496A (en) * | 2018-10-31 | 2019-03-08 | 山东华晨彩装科技有限公司 | A kind of white resist printing method for active emerald green orchid 21 |
| CN109440496B (en) * | 2018-10-31 | 2021-03-30 | 山东华晨彩装科技有限公司 | White printing prevention method for active turquoise blue 21 |
| CN111118937A (en) * | 2020-02-25 | 2020-05-08 | 青岛德润宁纺织材料有限公司 | Preparation method of anti-printing auxiliary agent for reactive dye anti-printing |
| CN111593585A (en) * | 2020-05-27 | 2020-08-28 | 山东黄河三角洲纺织科技研究院有限公司 | Method for printing-proof reactive dye on cation modified cotton fabric |
| CN113897801A (en) * | 2021-11-18 | 2022-01-07 | 张启磊 | Preparation method of anti-printing auxiliary agent for reactive dye anti-printing |
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| Publication number | Publication date |
|---|---|
| CN105862463B (en) | 2017-09-22 |
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