CN102898413B - 含二氧杂饱和茚环类的液晶化合物及其组合物 - Google Patents
含二氧杂饱和茚环类的液晶化合物及其组合物 Download PDFInfo
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- CN102898413B CN102898413B CN201210387994.8A CN201210387994A CN102898413B CN 102898413 B CN102898413 B CN 102898413B CN 201210387994 A CN201210387994 A CN 201210387994A CN 102898413 B CN102898413 B CN 102898413B
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- 125000003454 indenyl group Chemical group C1(C=CC2=CC=CC=C12)* 0.000 title abstract description 10
- 125000003545 alkoxy group Chemical group 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 6
- 125000005842 heteroatom Chemical group 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 239000007788 liquid Substances 0.000 abstract description 14
- 239000000178 monomer Substances 0.000 abstract description 5
- 239000004983 Polymer Dispersed Liquid Crystal Substances 0.000 abstract description 4
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 abstract description 4
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- GVNVAWHJIKLAGL-UHFFFAOYSA-N 2-(cyclohexen-1-yl)cyclohexan-1-one Chemical compound O=C1CCCCC1C1=CCCCC1 GVNVAWHJIKLAGL-UHFFFAOYSA-N 0.000 description 6
- 101150065749 Churc1 gene Proteins 0.000 description 6
- 102100038239 Protein Churchill Human genes 0.000 description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
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- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- HEDRZPFGACZZDS-MICDWDOJSA-N Trichloro(2H)methane Chemical compound [2H]C(Cl)(Cl)Cl HEDRZPFGACZZDS-MICDWDOJSA-N 0.000 description 4
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- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 4
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- 238000005160 1H NMR spectroscopy Methods 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 239000004327 boric acid Substances 0.000 description 2
- CREMABGTGYGIQB-UHFFFAOYSA-N carbon carbon Chemical compound C.C CREMABGTGYGIQB-UHFFFAOYSA-N 0.000 description 2
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 2
- 238000004440 column chromatography Methods 0.000 description 2
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
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- 150000003839 salts Chemical class 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 2
- ZRYZBQLXDKPBDU-UHFFFAOYSA-N 4-bromobenzaldehyde Chemical compound BrC1=CC=C(C=O)C=C1 ZRYZBQLXDKPBDU-UHFFFAOYSA-N 0.000 description 1
- NFHOVIGMSHFLFI-KYZUINATSA-N Fc1cc(cc(F)c1F)[C@H]1CC[C@@H](CC1)C=O Chemical compound Fc1cc(cc(F)c1F)[C@H]1CC[C@@H](CC1)C=O NFHOVIGMSHFLFI-KYZUINATSA-N 0.000 description 1
- 238000003747 Grignard reaction Methods 0.000 description 1
- 239000007818 Grignard reagent Substances 0.000 description 1
- 238000006411 Negishi coupling reaction Methods 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000003477 Sonogashira cross-coupling reaction Methods 0.000 description 1
- 238000006069 Suzuki reaction reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- IYRWEQXVUNLMAY-UHFFFAOYSA-N carbonyl fluoride Chemical compound FC(F)=O IYRWEQXVUNLMAY-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000003098 cholesteric effect Effects 0.000 description 1
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- KVFDZFBHBWTVID-UHFFFAOYSA-N cyclohexanecarbaldehyde Chemical compound O=CC1CCCCC1 KVFDZFBHBWTVID-UHFFFAOYSA-N 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
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- 239000012065 filter cake Substances 0.000 description 1
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- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 1
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 1
- NFBAXHOPROOJAW-UHFFFAOYSA-N phenindione Chemical class O=C1C2=CC=CC=C2C(=O)C1C1=CC=CC=C1 NFBAXHOPROOJAW-UHFFFAOYSA-N 0.000 description 1
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- 229910052717 sulfur Inorganic materials 0.000 description 1
- -1 tosic acid monohydrate Chemical class 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Liquid Crystal Substances (AREA)
Abstract
Description
组分代码 | 重量百分数(%) | 性能参数测试结果 |
3CPO2 | 5 | △n=0.098 |
3CPP2 | 20 | Vth=2.15v |
5PP1 | 6 | Cp=78.6℃ |
3PPO2 | 10 | η=19.6mpa.s |
VCCP1 | 5 | △ε=6.7 |
3CCV | 34 | |
4PGUQUF | 6 | |
3PGUQUF | 6 | |
HCLC-07F | 8 |
组分代码 | 重量百分数(%) | 性能参数测试结果 |
3CPO2 | 5 | △n=0.108 |
3CPP2 | 20 | Vth=2.26v |
5PP1 | 6 | Cp=82.4℃ |
3PPO2 | 10 | η=14.2mpa.s |
VCCP1 | 5 | △ε=6.4 |
3CCV | 34 | |
4PGUQUF | 6 | |
3PGUQUF | 6 | |
3CPUQUF | 8 |
组分代码 | 重量百分数(%) | 性能参数测试结果 |
2CCUF | 15 | △n=0.134 |
HCLC-07 | 12 | Vth=1.64v |
1PP2V1 | 8 | Cp=80.1℃ |
2PGP3 | 12 | η=29.3mpa.s |
3CGUF | 6 | △ε=8.25 |
2CGUF | 7 | |
3CCV | 15 | |
3CCV1 | 5 | |
3PUQUF | 8 | |
3PGUQUF | 6 | |
2PGUQUF | 6 |
组分代码 | 重量百分数(%) | 性能参数测试结果 |
2CCUF | 15 | △n=0.140 |
3CCUF | 12 | Vth=1.75v |
1PP2V1 | 8 | Cp=85.5℃ |
2PGP3 | 12 | η=26.8mpa.s |
3CGUF | 6 | △ε=8.02 |
2CGUF | 7 | |
3CCV | 15 | |
3CCV1 | 5 | |
3PUQUF | 8 | |
3PGUQUF | 6 | |
2PGUQUF | 6 |
Claims (3)
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CN201210387994.8A CN102898413B (zh) | 2012-10-13 | 2012-10-13 | 含二氧杂饱和茚环类的液晶化合物及其组合物 |
TW102136575A TWI495710B (zh) | 2012-10-13 | 2013-10-09 | 具有二氧雜飽和茚環結構的液晶化合物及液晶組合物 |
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CN201210387994.8A CN102898413B (zh) | 2012-10-13 | 2012-10-13 | 含二氧杂饱和茚环类的液晶化合物及其组合物 |
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CN102898413B true CN102898413B (zh) | 2015-04-08 |
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CN103409146B (zh) * | 2013-04-01 | 2015-10-28 | 石家庄诚志永华显示材料有限公司 | 用于有源矩阵驱动液晶显示的液晶组合物 |
CN115124634B (zh) * | 2022-08-10 | 2023-10-20 | 杭州小菱科技有限公司 | 一种茂金属主催化剂及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101228251A (zh) * | 2005-06-23 | 2008-07-23 | 特拉根化学股份公司 | 包含氢化甘菊环结构的液晶分子 |
JP2011251931A (ja) * | 2010-06-01 | 2011-12-15 | Jnc Corp | 二つの酸素を有する縮合環からなる液晶化合物およびこれを用いた液晶組成物 |
CN102477305A (zh) * | 2010-11-25 | 2012-05-30 | 达兴材料股份有限公司 | 液晶化合物与液晶混合物 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
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TWI417368B (zh) * | 2010-10-04 | 2013-12-01 | Daxin Materials Corp | 液晶化合物與液晶混合物 |
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- 2012-10-13 CN CN201210387994.8A patent/CN102898413B/zh active Active
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101228251A (zh) * | 2005-06-23 | 2008-07-23 | 特拉根化学股份公司 | 包含氢化甘菊环结构的液晶分子 |
JP2011251931A (ja) * | 2010-06-01 | 2011-12-15 | Jnc Corp | 二つの酸素を有する縮合環からなる液晶化合物およびこれを用いた液晶組成物 |
CN102477305A (zh) * | 2010-11-25 | 2012-05-30 | 达兴材料股份有限公司 | 液晶化合物与液晶混合物 |
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Publication number | Publication date |
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CN102898413A (zh) | 2013-01-30 |
TW201414808A (zh) | 2014-04-16 |
TWI495710B (zh) | 2015-08-11 |
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CP02 | Change in the address of a patent holder | ||
CP02 | Change in the address of a patent holder |
Address after: Building 2, Sino Japan Cooperation Innovation Park, No. 16, Zidan Road, Qinhuai District, Nanjing, Jiangsu Province, 210000 Patentee after: JIANGSU HECHENG DISPLAY TECHNOLOGY Co.,Ltd. Patentee after: Daxin Materials Corp. Address before: 212212 East Side of Yangzhong Yangtze River Bridge, Zhenjiang City, Jiangsu Province Patentee before: JIANGSU HECHENG DISPLAY TECHNOLOGY Co.,Ltd. Patentee before: Daxin Materials Corp. |