CN102875949A - 增韧填充母粒及其制备方法 - Google Patents
增韧填充母粒及其制备方法 Download PDFInfo
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- CN102875949A CN102875949A CN2012103995173A CN201210399517A CN102875949A CN 102875949 A CN102875949 A CN 102875949A CN 2012103995173 A CN2012103995173 A CN 2012103995173A CN 201210399517 A CN201210399517 A CN 201210399517A CN 102875949 A CN102875949 A CN 102875949A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000000945 filler Substances 0.000 title abstract description 12
- 239000004594 Masterbatch (MB) Substances 0.000 title abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 25
- 239000002131 composite material Substances 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 239000000049 pigment Substances 0.000 claims abstract description 8
- 238000007599 discharging Methods 0.000 claims abstract description 5
- 239000008187 granular material Substances 0.000 claims description 35
- 239000003795 chemical substances by application Substances 0.000 claims description 31
- 239000012763 reinforcing filler Substances 0.000 claims description 31
- 239000004793 Polystyrene Substances 0.000 claims description 13
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 12
- 229920002223 polystyrene Polymers 0.000 claims description 12
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000006185 dispersion Substances 0.000 claims description 8
- 239000003112 inhibitor Substances 0.000 claims description 7
- 230000003647 oxidation Effects 0.000 claims description 7
- 238000007254 oxidation reaction Methods 0.000 claims description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 6
- 229920001684 low density polyethylene Polymers 0.000 claims description 6
- 239000004702 low-density polyethylene Substances 0.000 claims description 6
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical group CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims description 5
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims description 5
- 239000008116 calcium stearate Substances 0.000 claims description 5
- 235000013539 calcium stearate Nutrition 0.000 claims description 5
- RKISUIUJZGSLEV-UHFFFAOYSA-N n-[2-(octadecanoylamino)ethyl]octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NCCNC(=O)CCCCCCCCCCCCCCCCC RKISUIUJZGSLEV-UHFFFAOYSA-N 0.000 claims description 5
- 239000004408 titanium dioxide Substances 0.000 claims description 5
- 238000005469 granulation Methods 0.000 claims description 3
- 230000003179 granulation Effects 0.000 claims description 3
- 238000004080 punching Methods 0.000 claims description 2
- 229920000468 styrene butadiene styrene block copolymer Polymers 0.000 abstract description 46
- 239000003607 modifier Substances 0.000 abstract description 8
- FACXGONDLDSNOE-UHFFFAOYSA-N buta-1,3-diene;styrene Chemical compound C=CC=C.C=CC1=CC=CC=C1.C=CC1=CC=CC=C1 FACXGONDLDSNOE-UHFFFAOYSA-N 0.000 abstract description 6
- 239000002270 dispersing agent Substances 0.000 abstract description 3
- 238000005461 lubrication Methods 0.000 abstract description 3
- 235000012438 extruded product Nutrition 0.000 abstract description 2
- 238000001125 extrusion Methods 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000003963 antioxidant agent Substances 0.000 abstract 2
- 230000003078 antioxidant effect Effects 0.000 abstract 2
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 239000004743 Polypropylene Substances 0.000 description 12
- 229920001155 polypropylene Polymers 0.000 description 12
- -1 styrene-ethylene-butylene-styrene Chemical class 0.000 description 11
- 229920005669 high impact polystyrene Polymers 0.000 description 10
- 239000004797 high-impact polystyrene Substances 0.000 description 10
- 238000010438 heat treatment Methods 0.000 description 8
- 230000035939 shock Effects 0.000 description 7
- 229920001971 elastomer Polymers 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- 239000011347 resin Substances 0.000 description 6
- 239000005060 rubber Substances 0.000 description 6
- 229920006132 styrene block copolymer Polymers 0.000 description 5
- 239000010426 asphalt Substances 0.000 description 4
- 229920000346 polystyrene-polyisoprene block-polystyrene Polymers 0.000 description 4
- 229920002725 thermoplastic elastomer Polymers 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000001746 injection moulding Methods 0.000 description 2
- 239000000314 lubricant Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 150000003440 styrenes Chemical class 0.000 description 2
- 229920001897 terpolymer Polymers 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 1
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 1
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 229910052599 brucite Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- ZJOLCKGSXLIVAA-UHFFFAOYSA-N ethene;octadecanamide Chemical compound C=C.CCCCCCCCCCCCCCCCCC(N)=O.CCCCCCCCCCCCCCCCCC(N)=O ZJOLCKGSXLIVAA-UHFFFAOYSA-N 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical class C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 230000003116 impacting effect Effects 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 230000000051 modifying effect Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- XIVNZHXRIPJOIZ-UHFFFAOYSA-N octadecanoic acid;zinc Chemical compound [Zn].CCCCCCCCCCCCCCCCCC(O)=O XIVNZHXRIPJOIZ-UHFFFAOYSA-N 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000008262 pumice Substances 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
- 239000012815 thermoplastic material Substances 0.000 description 1
- 229920000428 triblock copolymer Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/88—Thermal treatment of the stream of extruded material, e.g. cooling
- B29C48/919—Thermal treatment of the stream of extruded material, e.g. cooling using a bath, e.g. extruding into an open bath to coagulate or cool the material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
- B29C48/04—Particle-shaped
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
- B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/88—Thermal treatment of the stream of extruded material, e.g. cooling
- B29C48/911—Cooling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/92—Measuring, controlling or regulating
Abstract
Description
应用例1 | 应用例2 | 应用例3 | 应用例4 | 对比应用例1 | |
高抗冲聚苯乙烯 | 80% | 85% | 90% | 95% | 100% |
增韧填充母粒 | 20% | 15% | 10% | 5% | - |
拉伸强度/MPa | 20.43 | 21.91 | 24.35 | 27.22 | 29.88 |
弯曲强度/MPa | 32.85 | 35.49 | 38.36 | 41.04 | 44.27 |
弯曲模量/MPa | 1584 | 1600 | 1650 | 1844 | 1717 |
悬臂梁缺口抗冲击强度/KJ·m-2 | 11.08 | 11.21 | 11.34 | 11.35 | 11.12 |
应用例5 | 应用例6 | 应用例7 | 应用例8 | 对比应用例2 | |
聚丙烯 | 80% | 85% | 90% | 95% | 100% |
增韧填充母粒 | 20% | 15% | 10% | 5% | - |
拉伸强度/MPa | 26.36 | 28.35 | 29.36 | 30.51 | 31.60 |
断裂伸长率/% | 22.86 | 23.18 | 25.28 | 40.24 | 26.42 |
弯曲强度/MPa | 30.42 | 32.44 | 33.01 | 33.19 | 33.94 |
弯曲模量/MPa | 887 | 914 | 948 | 938 | 894 |
悬臂梁缺口抗冲击强度/KJ·m-2 | 10.83 | 10.81 | 10.85 | 11.58 | 4.76 |
实施例3 | 实施例4 | 实施例5 | 实施例6 | 实施例7 | 实施例8 | |
冲油SBS | 25kg | 25kg | 25kg | 25kg | 25kg | 25kg |
乙撑双硬脂酰胺 | 1.1kg | 1.0kg | 1.2kg | 1.2kg | 1.2kg | 1.1kg |
硬脂酸钙 | 2.2kg | 2.0kg | 2.1kg | 2.2kg | 1.9kg | 2.3kg |
填充剂 | 70kg重质碳酸钙 | 75kg轻质碳酸钙 | 65kg重质碳酸钙 | 70kg轻质碳酸钙 | 65kg重质碳酸钙 | 70kg轻质碳酸钙 |
改性剂 | 10kg聚苯乙烯 | 12kg聚苯乙烯 | 8kg聚苯乙烯 | 10kg低密度聚乙烯 | 12kg低密度聚乙烯 | 8kg低密度聚乙烯 |
抗氧剂1010 | 0.15kg | 0.15kg | 0.15kg | 0.15kg | 0.15kg | 0.15kg |
钛白粉 | 0.15kg | 0.2kg | 0.15kg | 0.15kg | 0.2kg | 0.15kg |
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210399517.3A CN102875949B (zh) | 2012-10-19 | 2012-10-19 | 增韧填充母粒及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210399517.3A CN102875949B (zh) | 2012-10-19 | 2012-10-19 | 增韧填充母粒及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102875949A true CN102875949A (zh) | 2013-01-16 |
CN102875949B CN102875949B (zh) | 2014-10-15 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201210399517.3A Active CN102875949B (zh) | 2012-10-19 | 2012-10-19 | 增韧填充母粒及其制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN102875949B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105542292A (zh) * | 2015-12-15 | 2016-05-04 | 上海维凯光电新材料有限公司 | 一种功能性白色母粒及其制备方法 |
CN107446256A (zh) * | 2017-09-12 | 2017-12-08 | 贵州通汇塑料科技有限公司 | 一种增韧聚苯乙烯填充母料及其制备方法 |
CN109384990A (zh) * | 2018-09-21 | 2019-02-26 | 日彩复合塑料(深圳)有限公司 | 一种pe功能母粒材料及其制备工艺 |
CN114456476A (zh) * | 2022-01-24 | 2022-05-10 | 东莞市赛美塑胶制品有限公司 | 一种pc-abs片材用含碳酸钙的母粒及其制备方法、pc-abs片材及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1597752A (zh) * | 2004-08-23 | 2005-03-23 | 成都新柯力化工科技有限公司 | 生物降解淀粉树脂母料 |
WO2009045057A1 (en) * | 2007-10-04 | 2009-04-09 | Korea Kumho Petrochemical Co., Ltd. | Asphalt modifier compositions with an improved melting rate and modified asphalt prepared using the same |
CN102153829A (zh) * | 2011-01-04 | 2011-08-17 | 合肥美的荣事达电冰箱有限公司 | 高抗冲聚苯乙烯用增韧色母粒、复合板材和制冷设备内胆 |
CN102367320A (zh) * | 2011-06-24 | 2012-03-07 | 深圳市科聚新材料有限公司 | 一种通用白色母粒及其制备方法 |
-
2012
- 2012-10-19 CN CN201210399517.3A patent/CN102875949B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1597752A (zh) * | 2004-08-23 | 2005-03-23 | 成都新柯力化工科技有限公司 | 生物降解淀粉树脂母料 |
WO2009045057A1 (en) * | 2007-10-04 | 2009-04-09 | Korea Kumho Petrochemical Co., Ltd. | Asphalt modifier compositions with an improved melting rate and modified asphalt prepared using the same |
CN102153829A (zh) * | 2011-01-04 | 2011-08-17 | 合肥美的荣事达电冰箱有限公司 | 高抗冲聚苯乙烯用增韧色母粒、复合板材和制冷设备内胆 |
CN102367320A (zh) * | 2011-06-24 | 2012-03-07 | 深圳市科聚新材料有限公司 | 一种通用白色母粒及其制备方法 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105542292A (zh) * | 2015-12-15 | 2016-05-04 | 上海维凯光电新材料有限公司 | 一种功能性白色母粒及其制备方法 |
CN107446256A (zh) * | 2017-09-12 | 2017-12-08 | 贵州通汇塑料科技有限公司 | 一种增韧聚苯乙烯填充母料及其制备方法 |
CN107446256B (zh) * | 2017-09-12 | 2020-07-21 | 江苏中信国安新材料有限公司 | 一种增韧聚苯乙烯填充母料及其制备方法 |
CN109384990A (zh) * | 2018-09-21 | 2019-02-26 | 日彩复合塑料(深圳)有限公司 | 一种pe功能母粒材料及其制备工艺 |
CN109384990B (zh) * | 2018-09-21 | 2021-12-03 | 日彩复合塑料(深圳)有限公司 | 一种pe功能母粒材料及其制备工艺 |
CN114456476A (zh) * | 2022-01-24 | 2022-05-10 | 东莞市赛美塑胶制品有限公司 | 一种pc-abs片材用含碳酸钙的母粒及其制备方法、pc-abs片材及其制备方法 |
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CN102875949B (zh) | 2014-10-15 |
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