CN102875943A - Red semitransparent gluedots and preparation method thereof - Google Patents
Red semitransparent gluedots and preparation method thereof Download PDFInfo
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- CN102875943A CN102875943A CN2012101384705A CN201210138470A CN102875943A CN 102875943 A CN102875943 A CN 102875943A CN 2012101384705 A CN2012101384705 A CN 2012101384705A CN 201210138470 A CN201210138470 A CN 201210138470A CN 102875943 A CN102875943 A CN 102875943A
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- water
- borax
- glue
- nasal mucus
- translucent
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000003292 glue Substances 0.000 claims abstract description 74
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 229910021538 borax Inorganic materials 0.000 claims abstract description 40
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 40
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 40
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 31
- 229920002907 Guar gum Polymers 0.000 claims abstract description 20
- 239000000665 guar gum Substances 0.000 claims abstract description 20
- 229960002154 guar gum Drugs 0.000 claims abstract description 20
- 235000010417 guar gum Nutrition 0.000 claims abstract description 20
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims abstract description 16
- 235000010199 sorbic acid Nutrition 0.000 claims abstract description 16
- 239000004334 sorbic acid Substances 0.000 claims abstract description 16
- 229940075582 sorbic acid Drugs 0.000 claims abstract description 16
- VVUMWAHNKOLVSN-UHFFFAOYSA-N 2-(4-ethoxyanilino)-n-propylpropanamide Chemical compound CCCNC(=O)C(C)NC1=CC=C(OCC)C=C1 VVUMWAHNKOLVSN-UHFFFAOYSA-N 0.000 claims abstract description 15
- FQMZVFJYMPNUCT-UHFFFAOYSA-N geraniol formate Natural products CC(C)=CCCC(C)=CCOC=O FQMZVFJYMPNUCT-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000011187 glycerol Nutrition 0.000 claims abstract description 15
- CFNJLPHOBMVMNS-UHFFFAOYSA-N pentyl butyrate Chemical compound CCCCCOC(=O)CCC CFNJLPHOBMVMNS-UHFFFAOYSA-N 0.000 claims abstract description 14
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 13
- GHKOFFNLGXMVNJ-UHFFFAOYSA-N Didodecyl thiobispropanoate Chemical compound CCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCC GHKOFFNLGXMVNJ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 13
- 229960001631 carbomer Drugs 0.000 claims abstract description 13
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims abstract description 13
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 12
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 12
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 12
- 235000000380 Nyssa aquatica Nutrition 0.000 claims abstract description 10
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 5
- 210000003097 mucus Anatomy 0.000 claims description 57
- 238000004945 emulsification Methods 0.000 claims description 21
- 239000002253 acid Substances 0.000 claims description 14
- 239000011259 mixed solution Substances 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims description 13
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims description 12
- 229940043350 citral Drugs 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000003973 paint Substances 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 9
- 239000000049 pigment Substances 0.000 abstract description 9
- 239000003963 antioxidant agent Substances 0.000 abstract description 6
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract 2
- 239000003508 Dilauryl thiodipropionate Substances 0.000 abstract 1
- 230000003712 anti-aging effect Effects 0.000 abstract 1
- 235000019304 dilauryl thiodipropionate Nutrition 0.000 abstract 1
- 238000002845 discoloration Methods 0.000 abstract 1
- FGPPDYNPZTUNIU-UHFFFAOYSA-N pentyl pentanoate Chemical compound CCCCCOC(=O)CCCC FGPPDYNPZTUNIU-UHFFFAOYSA-N 0.000 abstract 1
- 235000013772 propylene glycol Nutrition 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
- 239000001054 red pigment Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 235000006708 antioxidants Nutrition 0.000 description 5
- 239000000976 ink Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- BBFYUPYFXSSMNV-HMGRVEAOSA-N quercetin 7-O-beta-D-glucoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC(O)=C2C(=O)C(O)=C(C=3C=C(O)C(O)=CC=3)OC2=C1 BBFYUPYFXSSMNV-HMGRVEAOSA-N 0.000 description 4
- 235000019832 sodium triphosphate Nutrition 0.000 description 4
- 239000000080 wetting agent Substances 0.000 description 4
- 230000003115 biocidal effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 230000003245 working effect Effects 0.000 description 3
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 2
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 2
- BBFYUPYFXSSMNV-UHFFFAOYSA-N quercetin-7-o-galactoside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC(O)=C2C(=O)C(O)=C(C=3C=C(O)C(O)=CC=3)OC2=C1 BBFYUPYFXSSMNV-UHFFFAOYSA-N 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241000209072 Sorghum Species 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 241001148470 aerobic bacillus Species 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- KZNIFHPLKGYRTM-UHFFFAOYSA-N apigenin Chemical compound C1=CC(O)=CC=C1C1=CC(=O)C2=C(O)C=C(O)C=C2O1 KZNIFHPLKGYRTM-UHFFFAOYSA-N 0.000 description 1
- 229940117893 apigenin Drugs 0.000 description 1
- XADJWCRESPGUTB-UHFFFAOYSA-N apigenin Natural products C1=CC(O)=CC=C1C1=CC(=O)C2=CC(O)=C(O)C=C2O1 XADJWCRESPGUTB-UHFFFAOYSA-N 0.000 description 1
- 235000008714 apigenin Nutrition 0.000 description 1
- POJOORKDYOPQLS-UHFFFAOYSA-L barium(2+) 5-chloro-2-[(2-hydroxynaphthalen-1-yl)diazenyl]-4-methylbenzenesulfonate Chemical compound [Ba+2].C1=C(Cl)C(C)=CC(N=NC=2C3=CC=CC=C3C=CC=2O)=C1S([O-])(=O)=O.C1=C(Cl)C(C)=CC(N=NC=2C3=CC=CC=C3C=CC=2O)=C1S([O-])(=O)=O POJOORKDYOPQLS-UHFFFAOYSA-L 0.000 description 1
- 235000012730 carminic acid Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- -1 easily decolouring Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- IINNWAYUJNWZRM-UHFFFAOYSA-L erythrosin B Chemical compound [Na+].[Na+].[O-]C(=O)C1=CC=CC=C1C1=C2C=C(I)C(=O)C(I)=C2OC2=C(I)C([O-])=C(I)C=C21 IINNWAYUJNWZRM-UHFFFAOYSA-L 0.000 description 1
- 235000012732 erythrosine Nutrition 0.000 description 1
- 229940011411 erythrosine Drugs 0.000 description 1
- 239000004174 erythrosine Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- QCUSKNIMUPQOES-UHFFFAOYSA-N quercetin 7-glucoside Natural products OCC1OC(C(O)C(O)C1O)c2cc(O)c3C(=O)C(=C(Oc3c2)c4ccc(O)c(O)c4)O QCUSKNIMUPQOES-UHFFFAOYSA-N 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Medicinal Preparation (AREA)
Abstract
The invention relates to gluedots and a preparation method thereof. The preparation method for red semitransparent gluedots comprises the following steps of: mixing water and guar gum; adding sorbic acid, sodium benzoate, dilauryl thiodipropionate, propylene glycol and glycerol, and emulsifying in an emulsifying pot; adding Carbomer resin to obtain a glue solution; pouring the glue solution into a stirrer, adding amyl valerate, amyl butyrate, geranialdehyde, geranyl formate and 1-(4'-sulfo-1'-azobenzol)-2-naphthol-6,8-trisodium disulfonate, and blending; and adding prepared borax water. The red semitransparent gluedots have high stability and good transparency, are naturally antibacterial and have high antiaging, antioxidant and water retaining capacity, so that the red semitransparent gluedots have long service life which is 12-15 months commonly, have bright color and stable pigment without discoloration, and have the transparency of 50-60 percent.
Description
Technical field
The invention belongs to the toy material field, particularly relate to a kind of nasal mucus glue and preparation method thereof.
Background technology
Nasal mucus glue is a kind of translucent thickness colloid, the colloid of its state between solid and liquid.Mainly for the preparation of the material of various nasal mucus glue toys, nasal mucus glue toy comprise be used to punish and enchant, the emerging toy of practical joke, market outlook are wide, divide according to color redness is arranged, green, blueness and yellow multiple.Existing nasal mucus glue main component comprises water, guar gum, tripoly phosphate sodium STPP and pigment, existing this nasal mucus glue poor stability, and easy deterioration by oxidation, transparency is bad, and easy breed bacteria.In addition, because lack the component of water retention, so that nasal mucus glue in use, easily dehydration is rotten, and work-ing life was short at 6～8 months lower work-ing life for normal temperature.Wherein the red pigments of red nasal mucus glue employing is industrial pigment, and not only color is not bright-coloured in nasal mucus glue for this red pigments, easily decolouring, and pigment state labile, and easily oxidation stain also affects transparency.The translucent nasal mucus glue of existing redness transparency is between 30～40%.
Summary of the invention
Deficiency for above-mentioned nasal mucus glue existence, the purpose of this invention is to provide the translucent nasal mucus glue of a kind of redness, the translucent nasal mucus glue of this redness is a kind of good stability, has anti-old oxidation-resistance, transparency is good, can be naturally antibiotic and the nasal mucus glue material of long service life; Aspect color, the translucent nasal mucus glue of this redness is bright-colored, color stable.
Another object of the present invention provides the preparation method of the translucent nasal mucus glue of this redness.
In order to realize the foregoing invention purpose, the present invention has adopted following technical scheme:
The translucent nasal mucus glue of a kind of redness, should be made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 2～5%;
Borax: 7～13%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.05～0.1%;
Sorbic Acid: 0.03～0.08%;
Sodium Benzoate: 0.01～0.03%;
Propylene glycol: 4～12%;
Glycerine: 1～7%;
Carbomer: 3～7%;
Tyox B: 0.08～0.15%;
Oil of apple: 0.008～0.013%;
Pentyl butyrate: 0.01～0.03%;
Citral: 0.01～0.03%;
Geranyl Formate: 0.005～0.012%;
Water: 70～80%;
The summation of above-mentioned all components percentage composition is 100%.
As preferably, should be made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 3.5%;
Borax: 9%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.07%;
Sorbic Acid: 0.05%;
Sodium Benzoate: 0.02%;
Propylene glycol: 7%;
Glycerine: 3%;
Carbomer: 5%;
Tyox B: 0.1%;
Oil of apple: 0.01%;
Pentyl butyrate: 0.02%;
Citral: 0.02%;
Geranyl Formate: 0.01%;
Water: 72.2%.
The preparation method of the translucent nasal mucus glue of a kind of redness, this preparation method may further comprise the steps:
(1) mixes, water and guar gum are mixed and poured container for stirring into 10～20 minutes, form mixed solution;
(2) emulsification is poured above-mentioned mixed solution into and was stirred in the emulsification pot 5～10 minutes, adds Sorbic Acid, Sodium Benzoate, Tyox B, propylene glycol and glycerine again, the mixed solution in heating emulsification pot and the stirring and emulsifying pot; Until mixeding liquid temperature rises to 90～100 ℃ in the emulsification pot, fully emulsification;
(3) glue liquid adds carbomer again to the good above-mentioned mixed solution of emulsification, stirs 20～30 minutes, until transparent glue solution is even, glue at this moment is the high thick liquid of transparency;
(4) the modulation borax water is crushed into powder borax first, water and borax is mixed to join in the warming pan again, heats to 90 ℃ and constantly stirring, until borax powder is fully water-soluble, makes borax water and heat preservation for standby use;
(5) paint and make finished product, the good transparent glue of emulsification pot internal modulation in the step (3) is poured in the stirrer, adding oil of apple, pentyl butyrate, citral, Geranyl Formate and 1-(4 '-sulfo group-1 '-nitrogen benzide)-beta naphthal-6,8-disulfonic acid trisodium salt, stirred 2～5 minutes, adding the borax solution that modulates in the step (4) stirred 5～10 minutes again, the effect of borax water is to solidify, be about to the semi-solid glue that above-mentioned glue becomes thickness, make red translucent nasal mucus glue finished product;
As preferably, the weight ratio of water and guar gum is 6～8:1 in the described step (1).
Red translucent nasal mucus glue by such scheme preparation of the present invention, in stability, anti-always anti-oxidant, all have on transparency and the water retention capacity significantly and improve, glycerine and propylene glycol belong to wetting Agent for Printing Inks, so glycerine wherein, propylene glycol, borax and water combination are so that nasal mucus glue water retention capacity is very good; Carbomer mixes with above-mentioned wetting Agent for Printing Inks, water and the guar gum mixed solution of comprising, so that nasal mucus glue transparency is high.The effect that borax also has water conservation and solidifies finished product in technological process, simultaneously also as a kind of stablizer and antioxidant, stability is high, and anti-old antioxidant effect is good.Tyox B also is a kind of oxidation inhibitor, its with include 1-(4 '-sulfo group-1 '-nitrogen benzide)-beta naphthal-6, the mixture of 8-disulfonic acid trisodium salt (red pigments), Sorbic Acid, Geranyl Formate is used in combination, the anti-old antioxidant effect of the red translucent nasal mucus glue that the present invention is made further promotes, possesses simultaneously antibacterial ability, and aspect color, redness shows more bright-colouredly and is stable not easy to change.In a word, the translucent nasal mucus glue of this redness is stable high, and transparency is good, can be naturally antibiotic, and anti-old anti-oxidant strong with water retention capacity, thus make it long with the life-span, work-ing life is generally at 12～15 months; Aspect color, bright-colored, pigment is stable not easy to change, so that the transparency of nasal mucus glue is between 50～60%.
Embodiment
The below does further to describe for example to the present invention by embodiment.
Embodiment 1:
The translucent nasal mucus glue of a kind of redness, should be made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 3.5%;
Borax: 9%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.07%;
Sorbic Acid: 0.05%;
Sodium Benzoate: 0.02%;
Propylene glycol: 7%;
Glycerine: 3%;
Carbomer: 5%;
Tyox B: 0.1%;
Oil of apple: 0.01%;
Pentyl butyrate: 0.02%;
Citral: 0.02%;
Geranyl Formate: 0.01%;
Water: 72.2%.
The preparation method of the red translucent nasal mucus glue of above-mentioned raw materials percentage composition proportioning may further comprise the steps:
(1) mix, water and guar gum are mixed and poured container for stirring into 10～20 minutes, form mixed solution, in this step, above-mentioned 72.2% water is not added fully, the weight ratio of water and guar gum is at 7:1, and namely water accounts for 24.5% of gross weight.
(2) emulsification is poured above-mentioned water and guar gum mixed solution into and was stirred in the emulsification pot 5～10 minutes, adds Sorbic Acid, Sodium Benzoate, Tyox B, propylene glycol and glycerine, the mixed solution in heating emulsification pot and the stirring and emulsifying pot again; Until mixeding liquid temperature rises to 90～100 ℃ in the emulsification pot, fully emulsification.
(3) glue liquid adds carbomer again to the good above-mentioned mixed solution of emulsification, stirs 20～30 minutes, until transparent glue solution is even, glue at this moment is the high thick liquid of transparency.
(4) modulation borax water, first borax is crushed into powder, again water and borax are mixed to join in the warming pan, namely wherein water accounts for 47.7% of gross weight, borax accounts for 9% of gross weight, this water and borax are heated to 90 ℃ and constantly stirring, until borax powder is fully water-soluble, make borax water and heat preservation for standby use.
(5) paint and make finished product, the good transparent glue of emulsification pot internal modulation in the step (3) is poured in the stirrer, adding oil of apple, pentyl butyrate, citral, Geranyl Formate and 1-(4 '-sulfo group-1 '-nitrogen benzide)-beta naphthal-6,8-disulfonic acid trisodium salt, cover and stir cover and stirred 2～5 minutes, add again the borax solution that modulates in the step (4), stirred 5～10 minutes, the effect of borax water is to solidify, be about to the semi-solid glue that above-mentioned glue becomes thickness, thereby prepare red translucent nasal mucus glue finished product.
Above steps is all carried out under normal pressure, and above-mentioned gross weight refers to the weight of red translucent nasal mucus glue finished product.
In above-mentioned various components, glycerine and propylene glycol belong to wetting Agent for Printing Inks, and borax replaces existing tripoly phosphate sodium STPP, have both had water retention, also are a kind of stablizers, so glycerine wherein, propylene glycol, borax and water combination are so that nasal mucus glue water retention capacity is very good.Carbomer mixes with above-mentioned wetting Agent for Printing Inks, water and the guar gum mixed solution of comprising, so that nasal mucus glue transparency is high.In addition, have borax or a kind of antioxidant of stabilizer function, under the effect of borax solution the borax homogeneous chemical composition is mixed wherein fully, so that nasal mucus glue stability is high, water-retentivity is strong, and anti-old antioxidant effect is good.1-(4 '-sulfo group-1 '-nitrogen benzide)-beta naphthal-6,8-disulfonic acid trisodium salt is a kind of natural red pigments, another name is carmine, English name Ponceau, water-soluble taking on a red color, maximum absorption wavelength 508 ± 2nm is heat-resisting, but can only under solutions of weak acidity, keep bright-coloured redness, meet alkali browning look.And above-mentioned Sorbic Acid and Sodium Benzoate are sanitass, and mould, yeast and aerobic bacteria are all had restraining effect, and the Sorbic Acid of selecting wherein is exactly acid sanitas, are intended to rot-resistant simultaneously, keep the bright-coloured nondiscoloration of red pigments.Similarly, as the oil of apple of essence, pentyl butyrate, each component of citral and Geranyl Formate can not only allow nasal mucus glue possess fruit aroma, and Geranyl Formate wherein also has the effect of regulating the mixture solutions of weak acidity, and protection is held pigment and is stablized nondiscoloration.Above-mentioned Sorbic Acid stink slightly with irritating, and oxidized painted easily in the medium-term and long-term placement of air.Oil of apple wherein, pentyl butyrate, citral and Geranyl Formate can be removed its pungent odour as essence, and Tyox B wherein and borax all are oxidation inhibitor, can prevent that Sorbic Acid is oxidized, affect the color of product.In a word, on the prepared red translucent nasal mucus glue final effect of this embodiment, it is high to have stability, can be naturally antibiotic, and anti-old anti-oxidant strong with water retention capacity, thus make it long with the life-span; Aspect color, bright-colored stable not easy to change, transparency is 54% simultaneously.
And with the red pigments 1-(4 ' in the said components-sulfo group-1 '-nitrogen benzide)-beta naphthal-6,8-disulfonic acid trisodium salt is replaced by other natural red pigments, repeat above-mentioned embodiment, the transparency of the nasal mucus glue of preparation can be reduced to below 50%, be 2 such as another name, 4,5,7-four sulphur fluorescent yellows, the red scarlet pigment of English name Erythrosine joins the red translucent nasal mucus glue for preparing in other components, and not only redness is not bright-coloured, and use for some time color partially blue unstable, so that the transparency of nasal mucus glue is 40%; Such as English Sorghum Pigment by name, major ingredient is that the red sorghum pigment of apigenin (5.74 '-trihydroxyflavone) and quercimeritrin (Quercetin-7-glucoside) joins the red translucent nasal mucus glue color for preparing in other components and is reddish brown, dimness is not bright-coloured, and the transparency of nasal mucus glue is 32%.
Embodiment 2
The translucent nasal mucus glue of a kind of redness, should be made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 5%;
Borax: 8%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.05%;
Sorbic Acid: 0.04%;
Sodium Benzoate: 0.03%;
Propylene glycol: 8%;
Glycerine: 1%;
Carbomer: 4%;
Tyox B: 0.12%;
Oil of apple: 0.008%;
Pentyl butyrate: 0.022%;
Citral: 0.025%;
Geranyl Formate: 0.005%;
Water: 73.7%.
The weight ratio of step (1) water and guar gum is at 6:1 among the preparation method of the red translucent nasal mucus glue of above-mentioned raw materials percentage composition proportioning, and namely water accounts for 30% of gross weight, and all the other water all mix adding in step (3) with borax.Other is identical with embodiment 1.
Embodiment 3
The translucent nasal mucus glue of a kind of redness, should be made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 2.5%;
Borax: 7%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.08%;
Sorbic Acid: 0.06%;
Sodium Benzoate: 0.03%;
Propylene glycol: 4%;
Glycerine: 6%;
Carbomer: 7%;
Tyox B: 0.09%;
Oil of apple: 0.008%;
Pentyl butyrate: 0.01%;
Citral: 0.013%;
Geranyl Formate: 0.009%;
Water: 73.2%.
The weight ratio of step (1) water and guar gum is at 8:1 among the preparation method of the red translucent nasal mucus glue of above-mentioned raw materials percentage composition proportioning, and namely water accounts for 20% of gross weight, and all the other water all mix adding in step (3) with borax.Other is identical with embodiment 1.
The below is existing red translucent nasal mucus glue and above-described embodiment 1,2,3 partial properties contrast table
Claims (4)
1. translucent nasal mucus glue of redness is characterized in that should being made by following component by the translucent nasal mucus glue of redness by weight percentage:
Guar gum: 2～5%;
Borax: 7～13%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.05～0.1%;
Sorbic Acid: 0.03～0.08%;
Sodium Benzoate: 0.01～0.03%;
Propylene glycol: 4～12%;
Glycerine: 1～7%;
Carbomer: 3～7%;
Tyox B: 0.08～0.15%;
Oil of apple: 0.008～0.013%;
Pentyl butyrate: 0.01～0.03%;
Citral: 0.01～0.03%;
Geranyl Formate: 0.005～0.012%;
Water: 70～80%;
Above-mentioned all components percentage composition sum is 100%.
2. the translucent nasal mucus glue of a kind of redness according to claim 1 is characterized in that should being made by following component by redness nasal mucus glue by weight percentage:
Guar gum: 3.5%;
Borax: 9%;
1-(4 '-sulfo group-1 '-nitrogen benzide)-and beta naphthal-6,8-disulfonic acid trisodium salt: 0.07%;
Sorbic Acid: 0.05%;
Sodium Benzoate: 0.02%;
Propylene glycol: 7%;
Glycerine: 3%;
Carbomer: 5%;
Tyox B: 0.1%;
Oil of apple: 0.01%;
Pentyl butyrate: 0.02%;
Citral: 0.02%;
Geranyl Formate: 0.01%;
Water: 72.2%.
3. the preparation method of the translucent nasal mucus glue of redness as claimed in claim 1 is characterized in that the method may further comprise the steps:
(1) mixes, water and guar gum are mixed and poured container for stirring into 10～20 minutes, form mixed solution;
(2) emulsification is poured above-mentioned mixed solution into and was stirred in the emulsification pot 5～10 minutes, adds Sorbic Acid, Sodium Benzoate, Tyox B, propylene glycol and glycerine again, the mixed solution in heating emulsification pot and the stirring and emulsifying pot; Until mixeding liquid temperature rises to 90～100 ℃ in the emulsification pot, fully emulsification;
(3) glue liquid adds carbomer again to the good above-mentioned mixed solution of emulsification, stirs 20-30 minute, until transparent glue solution is even;
(4) the modulation borax water is crushed into powder borax first, water and borax is mixed to join in the warming pan again, heats to 90 ℃ and constantly stirring, until borax powder is fully water-soluble, makes borax water and heat preservation for standby use;
(5) paint and make finished product, the good transparent glue of emulsification pot internal modulation in the step (3) is poured in the stirrer, adding oil of apple, pentyl butyrate, citral, Geranyl Formate and 1-(4 '-sulfo group-1 '-nitrogen benzide)-beta naphthal-6,8-disulfonic acid trisodium salt, stirred 2～5 minutes, add again the borax solution that modulates in the step (4), stirred 5～10 minutes, make red translucent nasal mucus glue finished product.
4. the preparation method of the translucent nasal mucus glue of described a kind of redness according to claim 3 is characterized in that the weight ratio of water and guar gum is 6～8:1 in the described step (1).
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114479202A (en) * | 2022-03-05 | 2022-05-13 | 丽妍塑料(惠州)有限公司 | Binkou water and preparation method thereof |
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| US20020025336A1 (en) * | 2000-04-17 | 2002-02-28 | Care Technologies Inc. | Lice remover composition |
| WO2007038855A1 (en) * | 2005-10-04 | 2007-04-12 | Sigmacon Medical Products Corporation | Medical gel |
| CN101525458A (en) * | 2008-11-17 | 2009-09-09 | 稂武忠 | Lava |
| CN102321443A (en) * | 2011-09-15 | 2012-01-18 | 宋仕良 | Environmental protection type transparent solid glue and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020025336A1 (en) * | 2000-04-17 | 2002-02-28 | Care Technologies Inc. | Lice remover composition |
| WO2007038855A1 (en) * | 2005-10-04 | 2007-04-12 | Sigmacon Medical Products Corporation | Medical gel |
| CN101525458A (en) * | 2008-11-17 | 2009-09-09 | 稂武忠 | Lava |
| CN102321443A (en) * | 2011-09-15 | 2012-01-18 | 宋仕良 | Environmental protection type transparent solid glue and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114479202A (en) * | 2022-03-05 | 2022-05-13 | 丽妍塑料(惠州)有限公司 | Binkou water and preparation method thereof |
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