CN102676084B - Transparent cleaning glue and preparation method thereof - Google Patents
Transparent cleaning glue and preparation method thereof Download PDFInfo
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- CN102676084B CN102676084B CN201210140110.9A CN201210140110A CN102676084B CN 102676084 B CN102676084 B CN 102676084B CN 201210140110 A CN201210140110 A CN 201210140110A CN 102676084 B CN102676084 B CN 102676084B
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Abstract
The invention relates to transparent cleaning glue and a preparation method thereof. The cleaning glue provided by the invention is prepared from water, guar gum, carrageenan, locust bean gum, triethanolamine, sorbic acid, carbomer, ethyl acetate, D-limonene, citral, glycerol, propylene glycol, didecyl dimethyl ammonium chloride, sodium sesquicarbonate and lauryl sodium sulfate. The yellow cleaning glue has the advantages of strong cleaning capability, high stability, oxidation resistance, acid and alkali resistance, heat and light resistance, and long use and storage life, wherein the storage life is more than one year at the temperature of 5DEG C below zero to 35DEG C, and the strong cleaning capability is represented on strong ash and powder sticking capability and also represented on the strong dirt cleaning and oil pollution removing capability. In addition, the transparency of the cleaning glue disclosed by the invention is 45-55%, whether dirt of various types is stuck on dead corners or not can be easily judged, and the dirt of various types on the dead corners can be cleaned.
Description
Technical field
The present invention relates to a kind of cleaning rubber and preparation method thereof.
Background technology
At present, a lot of product outer structure complexity, especially electric equipment products, can not water big area clean when clean, therefore can pinch into the cleaning rubber of different shape and just be pushed to the market and widespread use.Cleaning rubber is mainly used in clean all kinds of article dead angle, as clean computor-keyboard, and inner chamber of car, the electrical equipment of shoes and outer structure complexity, especially for the electric equipment products with dense arrangement button, applicability is very strong.Although existing cleaning rubber can be pinched into different shape and have stronger sticky ash to glue powder ability, but still there are many deficiencies, be mainly manifested in existing cleaning rubber to a little less than sticking to the knot Fouling Cleaning ability on electrical equipment outside surface, lack ability of cleaning greasy dirt, and unstable chemcial property, especially acid and alkali-resistance, anti-oxidant reduction and fast light hot ability, cause it under the normal temperature of 10～25 ℃, and the preservation life-span is not long, generally, at 6-8 month, work-ing life is shorter.
In addition, existing to have a class cleaning rubber be to be prepared from as tenderizer and polyvinyl alcohol combination by phthalic ester and analogue, and this class cleaning rubber also has toxicity, repeatedly uses naked manual manipulation very harmful to health when clean; Aspect color, existing cleaning rubber is mainly divided into redness, transparent and blue, and the Main Function of color is easily to see cleaned dirt and soot particle when clean as cleaning rubber background color clearly.After using repeatedly in coloured cleaning rubber prepared by the industrial pigment of these uses, easily decolouring variable color, especially clean metal surface easily becomes afterwards black and finally causes using, comparatively speaking, just there is not these problems in water white cleaning rubber, and not water white cleaning rubber product in the market.
Summary of the invention
Goal of the invention of the present invention is the deficiency existing for above-mentioned existing cleaning rubber, provide the sticky powder ability of a kind of sticky ash strong, and it is strong to settle accounts dirt ability, and degreasing result is good, and stability is high and use and preserve long transparent cleaning rubber of life-span.
Another object of the present invention is to provide the preparation method of above-mentioned transparent cleaning rubber.
In order to realize foregoing invention object, the present invention has adopted following technical scheme:
A kind of transparent cleaning rubber, should be made by following component according to weight percent meter:
Water: 70～85%;
Guar gum: 4～10%;
Carrageenin: 1～4%;
Locust bean gum: 3～8%;
Trolamine: 2～3%;
Sorbic Acid: 0.2～0.5%;
Carbomer: 2～4%;
Ethyl acetate: 0.01～0.03%;
D-ramie is rare: 0.01～0.03%;
Citral: 0.01～0.03%;
Glycerine: 0.5～2%;
Propylene glycol: 1～2%;
Timbercote 2000: 0.02～0.08%;
Sodium sesquicarbonate: 0.2～0.6%
Sodium lauryl sulphate: 1～1.8%;
Described above-mentioned each component percentage composition sum is 100%.
As preferably, should be made by following component according to weight percent meter:
Water: 74.91%;
Guar gum: 6%;
Carrageenin: 2%;
Locust bean gum: 5%;
Trolamine: 4%;
Sorbic Acid: 0.5%;
Carbomer: 3%;
Ethyl acetate: 0.01%;
D-ramie is rare: 0.02%;
Citral: 0.01%;
Glycerine: 2%;
Propylene glycol: 1%;
Timbercote 2000: 0.05%;
Sodium sesquicarbonate: 0.5%
Sodium lauryl sulphate: 1%.
A preparation method for above-mentioned transparent cleaning rubber, this preparation method comprises the following steps:
(1) water, propylene glycol, glycerine, carrageenin, carbomer, locust bean gum and guar gum are poured in container, stirred 5-10 minute; Add again sodium sesquicarbonate, sodium lauryl sulphate, Sorbic Acid and Timbercote 2000, stir and within 2-5 minute, obtain mixed glue solution, mixed liquor is poured in extruding machine and be heated to 120～130 ℃, treat that temperature is between 120～130 ℃, start extruding machine work, pour the most at last extruding completely of the interior mixed glue solution of extruding machine into;
(2) mixed glue solution of extruding in step (1) is added in stirrer, cover stirring cover, add again that ethyl acetate, D-ramie are rare, citral and trolamine, remain on temperature and stir 20-30 minute between 95～100 ℃, coolingly obtain transparent cleaning rubber finished product.
Above-mentioned transparent cleaning rubber provided by the invention, by water, guar gum, carrageenin and locust bean gum, as colloidal stroma, especially guar gum, carrageenin and locust bean gum combination, make colloidal stroma stability very good.Sodium lauryl sulphate is as tensio-active agent, its effect is the dissolving power that increases cleaning rubber, make it possess water-soluble and oil soluble simultaneously, tensio-active agent and above-mentioned colloidal stroma coordinate, it is the part that sodium lauryl sulphate is mixed into transparent cleaning rubber, make this transparent cleaning rubber can not only remove water-soluble dirt, and degreasing result is also very good.Timbercote 2000 is the cats product with germicidal action, is also a kind of sterilant.When Timbercote 2000 is used as tensio-active agent, can also strengthen cleaning effect, and sterilizing ability being very strong when the sterilant, is to go out and clean 2 times, and it also has excellent stability in hard water, inactivation of algae and mould fungus inhibition effect in addition.The Timbercote 2000 adding in the present invention plays above-mentioned dual function in final cleaning rubber, and its stability in hard water is dissolving after dirt the transparent cleaning rubber of preparation, still do not lose sterilizing ability, this is also going out and the unexistent performance of clean sterilant of commonly using.Glycerine and propylene glycol are wetting Agent for Printing Inkss, keep moisture not volatile, extend the work-ing life of this product.Rare and the ethyl acetate of citral, D-ramie is as food grade essence, and its effect is to remove the micro-irritating smell that trolamine brings, and increases citrus scented to this product simultaneously.Sodium sesquicarbonate or a kind of acid-base buffer agent, can stablize potential of hydrogen.Sorbic Acid is a kind of slightly acidic sanitas, can mould fungus inhibition, can also sterilization together with sterilant, and combination sterilization effect is good.Carbomer has very strong water-absorbent, absorbs water easily swelling, and be water-soluble thickener, the emulsifying agent simultaneously or in preparation method's process as residuite, is enhanced the transparency in above-mentioned pebble glue material composition.
The more important thing is, effect of the present invention focuses on cooperatively interacting between above-mentioned each component, and therefore most components possess selectivity and irreplaceability.Although glycerine and propylene glycol be all as wetting Agent for Printing Inks, another one effect is also for the character of combination of components is more stable, and if propylene glycol is as the solvent of citral, glycerine is as the solvent of citral, just can be finally that it is miscible between each component.Similarly, in cleaning course, the complicated of dirt is various, and it is particularly important that mixing ability seems, propylene glycol, glycerine, water and tensio-active agent are all made combination contribution on cleaning effect, and cleaning effect is very good.Aspect ph stability, component of the present invention is selected neutral component mostly, Sorbic Acid is wherein met water solvent and is extremely weak acidity, carbomer is also acidulous material, they coordinate sodium sesquicarbonate can stablize potential of hydrogen, make pH value between 6-7, also the external dirt dissolving in is possessed to very strong antiacid alkali changing capability, keep the ph stability of cleaning rubber.Carbomer can destroy alkaline sanitas, and therefore sanitas is selected Sorbic Acid; On the contrary, under alkaline condition, a little less than carbomer water absorption and swelling ability, select alkaline sanitas can suppress the performance of carbomer swelling behavior, cause the transparency of product to be affected.Carrageenin and locust bean gum while or emulsifing thickener, being convenient to a preparation process component emulsification mixes, also increased the viscosity of cleaning rubber, coordinated guar gum and water and the low component of other percentage compositions, outside finally showing is that in cleaning course, the sticky grey ability of sticky powder is strong.
In a word, this transparent cleaning rubber cleaning capacity of the present invention is strong, show that not only the sticky powder ability of sticky ash is strong, also settle accounts dirt and ability of cleaning greasy dirt is strong, stability is high, resistance to oxidation, soda acid, heat, light, and use and to preserve the life-span long, the preservation life-span is wherein can preserve more than 1 year at-5～35 ℃ of temperature.In addition, the transparency of cleaning rubber of the present invention, at 45-55%, is easy to differentiate all kinds of dirts that whether are stained with and remove on dead angle.
Embodiment
By embodiment, the present invention to be done further to describe for example below.
Embodiment 1:
A kind of above-mentioned transparent cleaning rubber, should be made by following component according to this transparent cleaning rubber of weight percent:
Water: 74.91%;
Guar gum: 6%;
Carrageenin: 2%;
Locust bean gum: 5%;
Trolamine: 4%;
Sorbic Acid: 0.5%;
Carbomer: 3%
Ethyl acetate: 0.01%;
D-ramie is rare: 0.02%;
Citral: 0.01%;
Glycerine: 2%;
Propylene glycol: 1%;
Timbercote 2000: 0.05%;
Sodium sesquicarbonate: 0.5%
Sodium lauryl sulphate: 1%.
The preparation method of this transparent cleaning rubber comprises the following steps:
(1) water, propylene glycol, glycerine, carbomer, carrageenin, locust bean gum and guar gum are poured in container, stirred 5-10 minute; Add again sodium sesquicarbonate, sodium lauryl sulphate, Sorbic Acid and Timbercote 2000, stir and within 2-5 minute, obtain mixed glue solution, mixed liquor is poured in extruding machine and be heated to 120～130 ℃, treat that temperature is between 120～130 ℃, start extruding machine work, pour the most at last extruding completely of the interior mixed glue solution of extruding machine into; Carrageenin wherein and locust bean gum, as emulsifying agent, are convenient to mix between each component, have also increased the viscosity of liquid simultaneously, after making to mix, become glue.
(2) mixed glue solution of extruding in step (1) is added in stirrer, cover stirring cover, add again that ethyl acetate, D-ramie are rare, citral and trolamine, remain on temperature and stir 20-30 minute between 95～100 ℃, coolingly obtain transparent cleaning rubber finished product.The effect of trolamine is that glue is frozen into deformable and flexible colloid, so just can obtain transparent cleaning rubber finished product.
Above steps is all carried out under normal pressure.
The preservation life-span of this transparent cleaning rubber is can preserve 18 months at-5～35 ℃ of temperature, and transparency is 50%.
Embodiment 2
A kind of above-mentioned transparent cleaning rubber, should be made by following component according to weight percent meter:
Water: 73.69%;
Guar gum: 4%;
Carrageenin: 3.8%;
Locust bean gum: 4%;
Trolamine: 7%;
Sorbic Acid: 0.4%;
Carbomer: 2%;
Ethyl acetate: 0.02%;
D-ramie is rare: 0.02%;
Citral: 0.01%;
Glycerine: 1.5%;
Propylene glycol: 2%;
Timbercote 2000: 0.06%;
Sodium sesquicarbonate: 0.4%
Sodium lauryl sulphate: 1.1%.
Its preparation method is identical with embodiment 1.
The preservation life-span of this transparent cleaning rubber is can preserve 16 months at-5～35 ℃ of temperature, and transparency is 48%.
Embodiment 3
A kind of above-mentioned transparent cleaning rubber, should be made by following component according to weight percent meter:
Water: 75.27%;
Guar gum: 8%;
Carrageenin: 1.2%;
Locust bean gum: 3.4%;
Trolamine: 3.2%;
Sorbic Acid: 0.3%;
Carbomer: 4%;
Ethyl acetate: 0.01%;
D-ramie is rare: 0.03%;
Citral: 0.01%;
Glycerine: 1.2%;
Propylene glycol: 1.3%;
Timbercote 2000: 0.03%;
Sodium sesquicarbonate: 0.55%
Sodium lauryl sulphate: 1.5%.
Its preparation method is identical with embodiment 1.
The preservation life-span of this transparent cleaning rubber is can preserve 16 months at-5～35 ℃ of temperature, and transparency is 52%.
Claims (3)
1. a transparent cleaning rubber, is characterized in that being made up of following component according to weight percent meter:
Water: 68～83%;
Guar gum: 4～10%;
Carrageenin: 1～4%;
Locust bean gum: 3～8%;
Trolamine: 2～8%;
Sorbic Acid: 0.2～0.5%;
Carbomer: 2～4%;
Ethyl acetate: 0.01～0.03%;
D-ramie is rare: 0.01～0.03%;
Citral: 0.01～0.03%;
Glycerine: 0.5～2%;
Propylene glycol: 1～2%;
Timbercote 2000: 0.02～0.08%;
Sodium sesquicarbonate: 0.2～0.6%
Sodium lauryl sulphate: 1～1.8%;
Described above-mentioned each component percentage composition sum is 100%.
2. the transparent cleaning rubber of one according to claim 1, is characterized in that being made up of following component according to weight percent meter:
Water: 74.91%;
Guar gum: 6%;
Carrageenin: 2%;
Locust bean gum: 5%;
Trolamine: 4%;
Sorbic Acid: 0.5%;
Carbomer: 3%;
Ethyl acetate: 0.01%;
D-ramie is rare: 0.02%;
Citral: 0.01%;
Glycerine: 2%;
Propylene glycol: 1%;
Timbercote 2000: 0.05%;
Sodium sesquicarbonate: 0.5%
Sodium lauryl sulphate: 1%.
3. a preparation method for transparent cleaning rubber as claimed in claim 1, and be characterised in that this preparation method comprises the following steps:
(1) water, propylene glycol, glycerine, carrageenin, carbomer, locust bean gum and guar gum are poured in container, stirred 5-10 minute; Add again sodium sesquicarbonate, sodium lauryl sulphate, Sorbic Acid and Timbercote 2000, stir and within 2-5 minute, obtain mixed glue solution, mixed liquor is poured in extruding machine and be heated to 120～130 ℃, treat that temperature is between 120～130 ℃, start extruding machine work, pour the most at last extruding completely of the interior mixed glue solution of extruding machine into;
(2) mixed glue solution of extruding in step (1) is added in stirrer, then add that ethyl acetate, D-ramie are rare, citral and trolamine, remain on temperature and stir 20-30 minute between 95～100 ℃, coolingly obtain transparent cleaning rubber finished product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210140110.9A CN102676084B (en) | 2012-05-06 | 2012-05-06 | Transparent cleaning glue and preparation method thereof |
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|---|---|---|---|
| CN201210140110.9A CN102676084B (en) | 2012-05-06 | 2012-05-06 | Transparent cleaning glue and preparation method thereof |
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| CN102676084A CN102676084A (en) | 2012-09-19 |
| CN102676084B true CN102676084B (en) | 2014-06-25 |
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| CN109679149B (en) * | 2018-11-28 | 2021-08-17 | 中国辐射防护研究院 | Decontamination daub and application thereof in radioactive graphite dust pollution removal |
| CN110862786B (en) * | 2019-11-20 | 2020-12-29 | 浙江国能科技有限公司 | Cleaning glue and preparation method thereof |
| CN113481065A (en) * | 2021-06-18 | 2021-10-08 | 中国辐射防护研究院 | Foam gel and preparation method thereof |
Citations (1)
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| CN101168648A (en) * | 2006-10-27 | 2008-04-30 | 保能科技股份有限公司 | Composition of hygroscopic coating with surface grain and manufacturing method for the coating |
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| JPH08295607A (en) * | 1995-04-26 | 1996-11-12 | Sumitomo Chem Co Ltd | Isecticidal incense stick |
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| CN101168648A (en) * | 2006-10-27 | 2008-04-30 | 保能科技股份有限公司 | Composition of hygroscopic coating with surface grain and manufacturing method for the coating |
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Granted publication date: 20140625 Termination date: 20170506 |