CN114736742A - Novel toilet bowl cleaning agent and preparation method thereof - Google Patents
Novel toilet bowl cleaning agent and preparation method thereof Download PDFInfo
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- CN114736742A CN114736742A CN202210504064.XA CN202210504064A CN114736742A CN 114736742 A CN114736742 A CN 114736742A CN 202210504064 A CN202210504064 A CN 202210504064A CN 114736742 A CN114736742 A CN 114736742A
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 78
- 238000003756 stirring Methods 0.000 claims abstract description 44
- 238000002156 mixing Methods 0.000 claims abstract description 34
- 239000004094 surface-active agent Substances 0.000 claims abstract description 29
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 28
- 239000003899 bactericide agent Substances 0.000 claims abstract description 28
- 239000000052 vinegar Substances 0.000 claims abstract description 26
- 235000021419 vinegar Nutrition 0.000 claims abstract description 26
- 238000001132 ultrasonic dispersion Methods 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 17
- 238000004140 cleaning Methods 0.000 claims abstract description 16
- 238000005303 weighing Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 8
- 230000002378 acidificating effect Effects 0.000 claims abstract description 6
- 238000004806 packaging method and process Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 239000008367 deionised water Substances 0.000 claims description 20
- 229910021641 deionized water Inorganic materials 0.000 claims description 20
- 239000000049 pigment Substances 0.000 claims description 20
- 239000000341 volatile oil Substances 0.000 claims description 20
- 239000000047 product Substances 0.000 claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 5
- 230000001376 precipitating effect Effects 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 239000011265 semifinished product Substances 0.000 claims description 5
- 238000003860 storage Methods 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- DODLPHVRNUZTBV-UHFFFAOYSA-N 2-sulfobutane-1,2,4-tricarboxylic acid Chemical compound OC(=O)CCC(S(O)(=O)=O)(C(O)=O)CC(O)=O DODLPHVRNUZTBV-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000686 essence Substances 0.000 claims 4
- -1 sprite Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 abstract description 5
- 230000001954 sterilising effect Effects 0.000 abstract description 4
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 238000005054 agglomeration Methods 0.000 abstract description 2
- 230000002776 aggregation Effects 0.000 abstract description 2
- 231100000419 toxicity Toxicity 0.000 abstract description 2
- 230000001988 toxicity Effects 0.000 abstract description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 239000000645 desinfectant Substances 0.000 description 3
- RDHZMYHPTPGFCO-UHFFFAOYSA-N 4-(2-carboxyethoxy)-4-oxo-3-sulfobutanoic acid Chemical compound C(COC(=O)C(CC(=O)O)S(=O)(=O)O)C(=O)O RDHZMYHPTPGFCO-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 230000000249 desinfective effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/40—Dyes ; Pigments
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/06—Ether- or thioether carboxylic acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a novel closestool cleaning agent and a preparation method thereof, comprising the following steps of firstly, weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing; the toilet cleanser has the advantages that the formula is reasonable, the raw materials are nontoxic and pollution-free, the toxicity and the hazard of the toilet cleanser are greatly reduced, hypochlorous acid is replaced by the white vinegar, the citric acid and the sprite, the damage to a human body in the using process is avoided, meanwhile, the environmental pollution is reduced, the cleaning effect of the cleanser is improved through the specially prepared surfactant, meanwhile, the white vinegar, the citric acid and the sprite are acidic, the alkaline substances in a toilet are effectively removed, the sterilization effect is improved through the addition of the bactericide, the quality of the cleanser is improved, the manufacturing process is simple, the operation is convenient, the raw materials are fully mixed and dispersed through twice stirring and ultrasonic dispersion, and the situations of agglomeration and uneven mixing are avoided.
Description
Technical Field
The invention relates to the technical field of toilet bowl cleaning agents, in particular to a novel toilet bowl cleaning agent and a preparation method thereof.
Background
The toilet cleanser is a cleaning product for cleaning, sterilizing and disinfecting toilets, and the toilet cleanser is mostly provided with more toxic or harmful substances, for example, application No. 201310479781.2 application No. 2013.10.15 discloses a toilet cleanser, which comprises the following components in parts by weight: 20-30 parts of acetic acid, 1-2 parts of hypochlorous acid, 2-3 parts of surfactant, 5-15 parts of bleaching powder, 1-3 parts of aromatic essence and 150 parts of 100-doped water, so as to obtain a finished product, wherein the hypochlorous acid is added into the toilet bowl cleaning agent of the formula and is used as a bactericide, contains chlorine and can generate certain chlorine to cause certain influence on human health, so that the safety of the toilet bowl cleaning agent is greatly reduced, meanwhile, the existing toilet bowl cleaning agent has poor cleaning effect, is particularly difficult to remove stubborn substances and reduces the practicability, and the existing toilet bowl cleaning agent is complex in production process, uneven in the preparation process, single in color and not favorable for sale.
Disclosure of Invention
The present invention is directed to a novel toilet cleanser and a method for preparing the same, which solves the above problems of the prior art.
In order to achieve the purpose, the invention provides the following technical scheme: a novel toilet bowl cleaner comprises the following formula: the water-based cleaning agent comprises a surfactant, white vinegar, essential oil, citric acid, sprite, a bactericide, essence, a pigment and deionized water, wherein the components are as follows in parts by weight: 3-4 parts of surfactant, 10-15 parts of white vinegar, 0.5-1 part of essential oil, 5-10 parts of citric acid, 3-5 parts of sprite, 3-5 parts of bactericide, 0.08-0.2 part of essence, 0.05-0.08 part of pigment and 80-100 parts of deionized water.
Preferably, the surfactant is prepared by mixing fatty acid methyl ester ethoxylate, carboxyethyl sulfosuccinate and D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1.
Preferably, the bactericide is prepared by mixing peroxyacetic acid and ethanol according to the mass part ratio of 2: 1.
A preparation method of a novel closestool cleaning agent comprises the following steps of weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing;
in the first step, 3-4 parts of surfactant, 10-15 parts of white vinegar, 0.5-1 part of essential oil, 5-10 parts of citric acid, 3-5 parts of sprite, 3-5 parts of bactericide, 0.08-0.2 part of essence, 0.05-0.08 part of pigment and 80-100 parts of deionized water are respectively weighed according to the parts by weight of the components;
in the second step, after the raw materials in the first step are weighed, a stirring kettle is used, the white vinegar, the essential oil, the citric acid and the sprite weighed in the first step are put into the stirring kettle, and the mixture is fully stirred to prepare an acid cleaning solution for later use;
in the third step, after the preparation of the acid cleaning solution in the second step is finished, adding the surfactant, the essence, the pigment and the deionized water weighed in the first step, continuously starting the stirring kettle to stir, and uniformly mixing to prepare a semi-finished product of the toilet bowl cleaning agent for later use;
in the fourth step, after the semi-finished toilet bowl cleaning agent in the third step is prepared, adding the semi-finished toilet bowl cleaning agent prepared in the third step and the bactericide weighed in the first step into an ultrasonic dispersion machine for sufficient ultrasonic dispersion, standing and precipitating after the dispersion is finished, and taking supernatant liquor after the precipitation is finished to prepare a finished toilet bowl cleaning agent;
and in the fifth step, after the finished product of the toilet bowl cleaning agent in the fourth step is manufactured, filling and weighing are carried out, and the finished product is delivered into a warehouse for storage.
Preferably, in the second step, the rotation speed of the stirring kettle is 350-500r/min, and the stirring time is 5-10 min.
Preferably, in the third step, the rotation speed of the stirring kettle is 500-.
Preferably, in the fourth step, the time for ultrasonic dispersion is 15-20 min.
Compared with the prior art, the invention has the beneficial effects that:
1. the formula of the toilet bowl cleaning agent is reasonable, the raw materials are nontoxic and pollution-free, the toxicity and the hazard of the toilet bowl cleaning agent are greatly reduced, the hypochlorous acid is replaced by the white vinegar, the citric acid and the sprite, the damage to a human body in the using process is avoided, and the environmental pollution is reduced;
2. according to the invention, the specially prepared surfactant is used, so that the cleaning effect of the cleaning agent is improved, meanwhile, the white vinegar, the citric acid and the sprite are acidic, the alkaline substances in the toilet bowl are effectively removed, the sterilization effect is improved by adding the bactericide, and the quality of the cleaning agent is improved;
3. the preparation method disclosed by the invention is simple in preparation process and convenient to operate, and through twice stirring and ultrasonic dispersion, the sufficient mixing and dispersion of the raw materials are ensured, and the situations of agglomeration and uneven mixing are avoided.
Drawings
FIG. 1 is a flow chart of the method of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, a technical solution provided by the present invention:
example 1:
a novel toilet bowl cleaner comprises the following formula: the water-based cleaning agent comprises a surfactant, white vinegar, essential oil, citric acid, sprite, a bactericide, essence, a pigment and deionized water, wherein the components are as follows in parts by weight: the disinfectant comprises the following components, by weight, 3 parts of a surfactant, 10 parts of white vinegar, 0.5 part of essential oil, 5 parts of citric acid, 3 parts of a sprite, 3 parts of a bactericide, 0.08 part of essence, 0.05 part of a pigment and 80 parts of deionized water, wherein the surfactant is formed by mixing fatty acid methyl ester ethoxylate, carboxyethyl sulfosuccinic acid and D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1, and the bactericide is formed by mixing peroxyacetic acid and ethanol according to the mass part ratio of 2: 1.
A preparation method of a novel closestool cleaning agent comprises the following steps of weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing;
in the first step, 3 parts of surfactant, 10 parts of white vinegar, 0.5 part of essential oil, 5 parts of citric acid, 3 parts of sprite, 3 parts of bactericide, 0.08 part of essence, 0.05 part of pigment and 80 parts of deionized water are weighed according to the parts by weight of the components;
in the second step, after the raw materials in the first step are weighed, a stirring kettle is used, the white vinegar, the essential oil, the citric acid and the sprite weighed in the first step are put into the stirring kettle for fully stirring, the rotating speed of the stirring kettle is 350r/min, the stirring time is 10min, and the acidic cleaning solution is prepared for later use;
in the third step, after the preparation of the acid cleaning solution in the second step is finished, adding the surfactant, the essence, the pigment and the deionized water weighed in the first step, continuously starting the stirring kettle to stir, wherein the rotating speed of the stirring kettle is 600r/min, the stirring time is 30min, and uniformly mixing to prepare a semi-finished product of the toilet bowl cleaning agent for later use;
in the fourth step, after the semi-finished toilet bowl cleaning agent in the third step is prepared, adding the semi-finished toilet bowl cleaning agent prepared in the third step and the bactericide weighed in the first step into an ultrasonic dispersion machine, performing sufficient ultrasonic dispersion for 20min, standing and precipitating after the dispersion is completed, and taking supernatant liquor after the precipitation is completed to prepare a finished toilet bowl cleaning agent;
and in the fifth step, after the toilet bowl cleaning agent finished product in the fourth step is manufactured, filling and weighing are carried out, and the finished product is delivered into a warehouse for storage.
Example 2:
a novel toilet bowl cleaner comprises the following formula: the water-based cleaning agent comprises a surfactant, white vinegar, essential oil, citric acid, sprite, a bactericide, essence, a pigment and deionized water, wherein the components are as follows in parts by weight: 3.5 parts of surfactant, 13 parts of white vinegar, 0.6 part of essential oil, 8 parts of citric acid, 3.5 parts of sprite, 3.5 parts of bactericide, 0.09 part of essence, 0.06 part of pigment and 90 parts of deionized water, wherein the surfactant is prepared by mixing fatty acid methyl ester ethoxylate, carboxyethyl sulfosuccinic acid and D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1, and the bactericide is prepared by mixing peroxyacetic acid and ethanol according to the mass part ratio of 2: 1.
A preparation method of a novel closestool cleaning agent comprises the following steps of weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing;
in the first step, 3.5 parts of surfactant, 13 parts of white vinegar, 0.6 part of essential oil, 8 parts of citric acid, 3.5 parts of sprite, 3.5 parts of bactericide, 0.09 part of essence, 0.06 part of pigment and 90 parts of deionized water are respectively weighed according to the parts by weight of the components;
in the second step, after the raw materials in the first step are weighed, a stirring kettle is used, the white vinegar, the essential oil, the citric acid and the sprite weighed in the first step are put into the stirring kettle for fully stirring, the rotating speed of the stirring kettle is 350r/min, the stirring time is 10min, and the acidic cleaning solution is prepared for later use;
in the third step, after the preparation of the acid cleaning solution in the second step is finished, adding the surfactant, the essence, the pigment and the deionized water weighed in the first step, continuously starting the stirring kettle to stir, wherein the rotating speed of the stirring kettle is 600r/min, the stirring time is 30min, and uniformly mixing to prepare a semi-finished product of the toilet bowl cleaning agent for later use;
in the fourth step, after the semi-finished toilet bowl cleaning agent in the third step is prepared, adding the semi-finished toilet bowl cleaning agent prepared in the third step and the bactericide weighed in the first step into an ultrasonic dispersion machine, performing sufficient ultrasonic dispersion for 20min, standing and precipitating after the dispersion is completed, and taking supernatant liquor after the precipitation is completed to prepare a finished toilet bowl cleaning agent;
and in the fifth step, after the finished product of the toilet bowl cleaning agent in the fourth step is manufactured, filling and weighing are carried out, and the finished product is delivered into a warehouse for storage.
Example 3:
a novel toilet bowl cleaner comprises the following formula: the water-based cleaning agent comprises a surfactant, white vinegar, essential oil, citric acid, sprite, a bactericide, essence, a pigment and deionized water, wherein the components are as follows in parts by weight: 4 parts of surfactant, 15 parts of white vinegar, 1 part of essential oil, 10 parts of citric acid, 5 parts of sprite, 5 parts of bactericide, 0.2 part of essence, 0.08 part of pigment and 100 parts of deionized water, wherein the surfactant is formed by mixing fatty acid methyl ester ethoxylate, carboxyethyl sulfosuccinic acid and D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1, and the bactericide is formed by mixing peroxyacetic acid and ethanol according to the mass part ratio of 2: 1.
A preparation method of a novel closestool cleaning agent comprises the following steps of weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing;
in the first step, respectively weighing 4 parts of surfactant, 15 parts of white vinegar, 1 part of essential oil, 10 parts of citric acid, 5 parts of sprite, 5 parts of bactericide, 0.2 part of essence, 0.08 part of pigment and 100 parts of deionized water according to the parts by weight of the components;
in the second step, after the raw materials in the first step are weighed, a stirring kettle is used, the white vinegar, the essential oil, the citric acid and the sprite weighed in the first step are put into the stirring kettle for fully stirring, the rotating speed of the stirring kettle is 350r/min, the stirring time is 10min, and the acidic cleaning solution is prepared for later use;
in the third step, after the preparation of the acid cleaning solution in the second step is finished, adding the surfactant, the essence, the pigment and the deionized water weighed in the first step, continuously starting the stirring kettle to stir, wherein the rotating speed of the stirring kettle is 600r/min, the stirring time is 30min, and uniformly mixing to prepare a semi-finished product of the toilet bowl cleaning agent for later use;
in the fourth step, after the semi-finished toilet bowl cleaning agent in the third step is prepared, adding the semi-finished toilet bowl cleaning agent prepared in the third step and the bactericide weighed in the first step into an ultrasonic dispersion machine, performing sufficient ultrasonic dispersion for 20min, standing and precipitating after the dispersion is completed, and taking supernatant liquor after the precipitation is completed to prepare a finished toilet bowl cleaning agent;
and in the fifth step, after the finished product of the toilet bowl cleaning agent in the fourth step is manufactured, filling and weighing are carried out, and the finished product is delivered into a warehouse for storage.
The properties of the examples are compared in the following table:
based on the above, the invention prepares the surfactant by mixing the fatty acid methyl ester ethoxylate, the carboxyethyl sulfosuccinate and the D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1, greatly improves the cleaning effect of the toilet cleaner, simultaneously, the acid of the white vinegar, the citric acid and the sprite is matched, so that the alkaline stubborn stains on the closestool are effectively removed, the disinfectant is prepared by mixing the peroxyacetic acid and the ethanol according to the mass ratio of 2: 1, which is favorable for improving the disinfection and sterilization effects of the cleanser, the formula of the disinfectant is reasonable, the raw materials are nontoxic and nuisanceless, the white vinegar, the citric acid and the sprite replace hypochloric acid, the safety of the cleanser is greatly improved, the environmental pollution is reduced, meanwhile, in the production process, mixing and ultrasonic dispersion are carried out twice, so that the uniform mixing degree of each raw material is improved, and the product quality is improved.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (7)
1. A novel toilet bowl cleaner comprises the following formula: surfactant, white vinegar, essential oil, citric acid, sprite, bactericide, essence, pigment and deionized water, and is characterized in that: the weight parts of the components are respectively as follows: 3-4 parts of surfactant, 10-15 parts of white vinegar, 0.5-1 part of essential oil, 5-10 parts of citric acid, 3-5 parts of sprite, 3-5 parts of bactericide, 0.08-0.2 part of essence, 0.05-0.08 part of pigment and 80-100 parts of deionized water.
2. A novel toilet bowl cleaner as claimed in claim 1, wherein: the surfactant is prepared by mixing fatty acid methyl ester ethoxylate, carboxyethyl sulfosuccinic acid and D-sulfo fatty acid ester salt according to the mass part ratio of 1: 1.
3. A novel toilet bowl cleaner as claimed in claim 1, wherein: the bactericide is prepared by mixing peroxyacetic acid and ethanol according to the mass part ratio of 2: 1.
4. A preparation method of a novel closestool cleaning agent comprises the following steps of weighing raw materials; step two, mixing for the first time; step three, mixing for the second time; step four, ultrasonic dispersion; step five, packaging and warehousing; the method is characterized in that:
in the first step, 3-4 parts of surfactant, 10-15 parts of white vinegar, 0.5-1 part of essential oil, 5-10 parts of citric acid, 3-5 parts of sprite, 3-5 parts of bactericide, 0.08-0.2 part of essence, 0.05-0.08 part of pigment and 80-100 parts of deionized water are respectively weighed according to the parts by weight of the components;
in the second step, after the raw materials in the first step are weighed, a stirring kettle is used, the white vinegar, the essential oil, the citric acid and the sprite weighed in the first step are put into the stirring kettle, and the mixture is fully stirred to prepare an acid cleaning solution for later use;
in the third step, after the preparation of the acidic cleaning solution in the second step is finished, adding the surfactant, the essence, the pigment and the deionized water weighed in the first step, continuously starting the stirring kettle for stirring, and uniformly mixing to prepare a semi-finished product of the toilet bowl cleaning agent for later use;
in the fourth step, after the semi-finished toilet bowl cleaning agent in the third step is prepared, adding the semi-finished toilet bowl cleaning agent prepared in the third step and the bactericide weighed in the first step into an ultrasonic dispersion machine for sufficient ultrasonic dispersion, standing and precipitating after the dispersion is finished, and taking supernatant liquor after the precipitation is finished to prepare a finished toilet bowl cleaning agent;
and in the fifth step, after the finished product of the toilet bowl cleaning agent in the fourth step is manufactured, filling and weighing are carried out, and the finished product is delivered into a warehouse for storage.
5. The method for preparing a novel toilet bowl cleanser according to claim 4, wherein: in the second step, the rotating speed of the stirring kettle is 350-500r/min, and the stirring time is 5-10 min.
6. The method for preparing a novel toilet bowl cleanser according to claim 4, wherein: in the third step, the rotating speed of the stirring kettle is 500-700r/min, and the stirring time is 20-30 min.
7. The method for preparing a novel toilet bowl cleanser according to claim 4, wherein: in the fourth step, the ultrasonic dispersion time is 15-20 min.
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| CN202210504064.XA CN114736742A (en) | 2022-05-10 | 2022-05-10 | Novel toilet bowl cleaning agent and preparation method thereof |
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| CN202210504064.XA CN114736742A (en) | 2022-05-10 | 2022-05-10 | Novel toilet bowl cleaning agent and preparation method thereof |
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Citations (3)
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| CN108004047A (en) * | 2017-12-25 | 2018-05-08 | 芜湖皖江知识产权运营中心有限公司 | Closestool cleanser and preparation method thereof |
| CN108060030A (en) * | 2017-12-25 | 2018-05-22 | 芜湖皖江知识产权运营中心有限公司 | A kind of Closestool cleanser and preparation method thereof |
| CN109499382A (en) * | 2018-12-28 | 2019-03-22 | 四川万潮科技有限公司 | A kind of reverse osmosis membrane cleaning combination and preparation method thereof |
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| CN108004047A (en) * | 2017-12-25 | 2018-05-08 | 芜湖皖江知识产权运营中心有限公司 | Closestool cleanser and preparation method thereof |
| CN108060030A (en) * | 2017-12-25 | 2018-05-22 | 芜湖皖江知识产权运营中心有限公司 | A kind of Closestool cleanser and preparation method thereof |
| CN109499382A (en) * | 2018-12-28 | 2019-03-22 | 四川万潮科技有限公司 | A kind of reverse osmosis membrane cleaning combination and preparation method thereof |
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| 徐铭勋: "脂肪酸甲酯乙氧基化物及其磺酸盐的生产技术与应用", 化学工业, vol. 30, no. 7, 31 July 2012 (2012-07-31), pages 30 - 32 * |
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