CN113855592A - Effervescent bath salt ball and preparation method thereof - Google Patents
Effervescent bath salt ball and preparation method thereof Download PDFInfo
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- CN113855592A CN113855592A CN202111374897.0A CN202111374897A CN113855592A CN 113855592 A CN113855592 A CN 113855592A CN 202111374897 A CN202111374897 A CN 202111374897A CN 113855592 A CN113855592 A CN 113855592A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Birds (AREA)
- Epidemiology (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
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- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention provides an effervescent bath salt ball and a preparation method thereof. The effervescent bath salt ball disclosed by the invention wraps the fragrance components in the water-soluble capsule wall to prepare the water-soluble fragrance capsule, and then the fragrance capsule is pressed in the bath salt ball body, so that the volatilization loss of the fragrance components in the processing and shelf life is avoided; when in use, the flavor capsule is dissolved with water together with the product, can timely and sufficiently release the flavor, indirectly reduce the addition of the flavor raw materials and reduce the cost of the raw materials.
Description
Technical Field
The invention belongs to the field of daily chemical products, and particularly relates to an effervescent bath salt ball and a preparation method thereof.
Background
The aroma is one of the important product characteristics of the effervescent bath salt ball, and is an important factor for consumers to consider the product preference and whether to buy the effervescent bath salt ball again. The fragrance mainly plays two roles, namely the effervescent bath salt ball releases fragrance to pleasure the sense of smell of a user in the using process, and the fragrance is left on the body after bathing is finished.
The main component of the fragrance raw material is a volatile component extracted from plants or chemically synthesized, an oily solvent is mostly used as a carrier, and the fragrance component is natural and volatile. The fragrance raw materials are mostly compounded by a plurality of fragrance components to achieve an ideal fragrance effect, and the fragrance is divided into top fragrance and middle fragrance which are blended and adjusted after being released.
At present, the process for adding the fragrance components in the effervescent bath salt ball industry is to directly add essential oil or essence into effervescent ball powder, mix the essential oil or the essence uniformly and press balls, in order to enable the coloring matter to develop color and enable the effervescent balls to be easy to press and form, a small amount of water or ethanol is added in the mixing process, after the pressing and forming, in order to remove water and prolong the quality guarantee period and the effervescent effect of the effervescent balls, the effervescent balls need to be placed into a drying chamber for drying for 24-48 hours. In the process of drying, the fragrance components are volatilized to lose nearly half of the fragrance components, and even the fragrance components are blended after the fragrance components are left, so that the optimal fragrance effect of the fragrance raw materials cannot be fully displayed. In addition, the flavor component continues to run off during the shelf life. In order to enable the fragrance components of the effervescent ball to achieve the ideal fragrance degree after loss, manufacturers generally increase the adding amount at present, which increases the raw material cost of the product, but cannot solve the problem that the characteristic fragrance cannot be shown.
Disclosure of Invention
In view of the above, in order to solve the above problems, the invention provides an effervescent bath salt ball and a preparation method thereof, wherein a fragrant component is wrapped in a water-soluble capsule wall to prepare a water-soluble capsule, and then the water-soluble capsule is pressed in a bath salt ball body, so that the fragrant component is prevented from volatilizing and losing in a drying process link and a shelf life link, and meanwhile, the water-soluble capsule can be dissolved in water to release fragrance in time when in use, so that the fragrance effect is ensured, the addition amount of the fragrant component raw materials is indirectly reduced, and the raw material cost is reduced.
In order to achieve the purpose, the technical scheme of the invention is realized as follows:
the invention provides an effervescent bath salt ball, which comprises a bath salt ball body and a fragrance capsule arranged in the bath salt ball body, wherein the fragrance capsule comprises a water-soluble capsule wall and a fragrance component serving as a capsule core.
Further, the bath salt ball body comprises the following raw materials in parts by weight: 55-60 parts of sodium bicarbonate, 0.1-0.2 part of pigment, 0.3-0.8 part of water, 0.4-1.2 parts of polyethylene glycol-4000.8, 0.5 part of vegetable oil, 0.01-0.02 part of cocoyl propyl betaine, 0.01-0.02 part of sodium lauroyl sarcosinate and 38-42 parts of citric acid.
Further, the vegetable oil comprises eucalyptus globulus oil, coconut oil, olive oil and avocado oil in a mass ratio of 6:1:1: 1.
Further, the weight portion of the fragrance component is 0.2-0.4 portion, and the fragrance component is essence or essential oil.
Further, the water-soluble capsule wall is selected from water-soluble capsule walls taking polyvinyl alcohol water-soluble film or gelatin as a main component.
Further, the water-soluble capsule wall is a polyvinyl alcohol water-soluble film; the fragrant capsule is obtained by filling fragrant components into a polyvinyl alcohol water-soluble film through a packaging machine and performing hot-press film sealing.
Polyvinyl alcohol is an organic compound of the formula [ C ]2H4O]nThe product is white flaky, flocculent or powdery solid, is odorless, is soluble in water (above 95 ℃), is slightly soluble in dimethyl sulfoxide, and is insoluble in gasoline, kerosene, vegetable oil, benzene, toluene, dichloroethane, carbon tetrachloride, acetone, ethyl acetate, methanol, ethylene glycol, etc. The water-soluble capsule wall material can be prepared by mixing and processing the polyvinyl alcohol and the macromolecular additive.
Further, the water-soluble capsule wall is a water-soluble capsule wall taking gelatin as a main component; the fragrant capsule is prepared by a dripping method through a dripping pill machine with double layers of dripping heads.
The dripping method comprises the following steps: gelatin solution and oily flavor component prepared from gelatin, plasticizer and water are respectively put into a liquid storage tank of a dripping pill machine with a double-layer dripper, and the two liquid materials are sprayed out at different speeds through a concentric tubular double-layer nozzle, so that a certain amount of oily flavor component is coated by a certain amount of gelatin solution and falls into cooling liquid, and the gelatin solution and the oily flavor component are gradually solidified into flavor capsules in the cooling liquid.
The invention provides a preparation method of the effervescent bath salt ball, which comprises the following steps of coating the fragrance components in the water-soluble capsule wall to form a fragrance capsule; uniformly mixing the components of the bath salt ball body to obtain a mixture, filling the mixture into a mold, and adding a fragrance capsule into the center of the mixture filled into the mold; pressing and forming; and (6) pumping and packaging.
Further, the method specifically comprises the following steps:
step one, cleaning and disinfecting production equipment and tools;
step two, preparing the flavor capsule: a) putting the flavor raw materials into a packaging machine, filling the flavor raw materials into a polyvinyl alcohol water-soluble film, and performing hot-press film sealing to obtain the flavor capsule; or b) taking gelatin solution prepared from gelatin, plasticizer and water as water-soluble capsule wall raw material, taking oily fragrant raw material as capsule core, and dripping to obtain the final product;
step three, weighing the components of the bath salt ball body according to the following weight parts: 55-60 parts of sodium bicarbonate, 0.1-0.2 part of pigment, 0.3-0.8 part of water, 0.4-1.2 parts of polyethylene glycol-4000.8, 0.5 part of vegetable oil, 0.01-0.02 part of cocoyl propyl betaine, 0.01-0.02 part of sodium lauroyl sarcosinate and 38-42 parts of citric acid;
step four, putting the sodium bicarbonate, the pigment and the water into stirring equipment, and uniformly stirring; adding polyethylene glycol-400 and vegetable oil, stirring, and sieving; adding cocoyl propyl betaine and sodium lauroyl sarcosinate, and stirring uniformly; finally, adding citric acid, and uniformly mixing to obtain a mixture;
filling the mixture into the mold, adding the flavor capsules into the center in the filling process, and performing compression molding;
and step six, putting the formed ball body into a drying chamber for drying to obtain the effervescent bath salt ball, and packaging. Further, the ratio of gelatin, plasticizer and water in the gelatin solution is 1: 0.4-0.6: 1
Compared with the prior art, the effervescent bath salt ball and the preparation method thereof have the following advantages:
the fragrant components are wrapped in the water-soluble capsule wall to prepare the water-soluble capsule, and then are pressed in the bath salt ball body, so that the volatilization loss of the fragrant components in a drying process link and a shelf life link is avoided, and the fragrant components can be sufficiently released when in use; meanwhile, the water-soluble capsule can be dissolved when being effervesced along with the product in use, so that the fragrance is released in time, the fragrance effect is ensured, the addition amount of the fragrance component raw materials is indirectly reduced, and the raw material cost is reduced.
Detailed Description
Unless defined otherwise, technical terms used in the following examples have the same meanings as commonly understood by one of ordinary skill in the art to which the present invention belongs. The test reagents used in the following examples, unless otherwise specified, are all conventional biochemical reagents; the experimental methods are conventional methods unless otherwise specified.
The present invention will be described in detail with reference to examples.
Example 1
Preparing an effervescent bath salt ball:
1) cleaning and disinfecting production equipment and tools;
2) weighing the components in the following proportion: 0.3 part of essence, 57.57 parts of sodium bicarbonate, 420900.15 parts of CI, 0.5 part of water, 1 part of polyethylene glycol-4001 parts of eucalyptus globulus leaf oil, 0.05 part of coconut oil, 0.05 part of olive oil, 0.05 part of avocado oil, 0.015 part of cocoyl propyl betaine, 0.015 part of sodium lauroyl sarcosinate and 40 parts of citric acid;
3) preparing a flavor capsule: putting the essence into a packaging machine, filling the essence into a polyvinyl alcohol water-soluble film, and performing hot-pressing film sealing to obtain a fragrant capsule;
4) putting sodium bicarbonate, pigment and water into a stirring pot, and uniformly stirring at a high speed; adding polyethylene glycol-400, Eucalyptus globulus Labill leaf oil, oleum Cocois, olive fruit oil and avocado oil, stirring, sieving, and removing large particle impurities; adding cocoyl propyl betaine and sodium lauroyl sarcosinate, and stirring uniformly; finally, adding citric acid, and uniformly mixing to obtain a mixture;
5) filling the mixture into the mold, adding the flavor capsule into the center during filling, and pressing to form;
6) and (3) putting the formed ball body into a drying chamber for drying for 24-48 h to obtain the effervescent bath salt ball, and packaging.
Example 2
On the basis of example 1, in contrast to example 1, a drop-wise process was used for the preparation of flavor capsules: mixing the components in a mass ratio of 1: 0.5: 1 gelatin solution prepared from gelatin, plasticizer and water and oily flavor component are respectively put into a liquid storage tank of a dripping pill machine with a double-layer dripper, and the two liquid materials are sprayed out at different speeds through a concentric tubular double-layer nozzle, so that the oily flavor component liquid drops are coated by the gelatin liquid drops and fall into cooling liquid, and are gradually solidified into flavor capsules in the cooling liquid.
The rest of the procedure was the same as in example 1.
When the prepared effervescent bath salt ball is not put into water for use, the fragrant substances can be well retained, the fragrance cannot be volatilized in a non-use stage, and the retained fragrant substances are more durable compared with bath salt balls prepared by directly adding essential oil or essence into effervescent ball powder.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. An effervescent bath salt ball, which is characterized in that: the bath salt ball comprises a bath salt ball body and a fragrance capsule arranged in the bath salt ball body, wherein the fragrance capsule comprises a water-soluble capsule wall and a fragrance component serving as a capsule core.
2. The effervescent bath salt ball of claim 1, wherein: the bath salt ball body comprises the following raw materials in parts by weight: 55-60 parts of sodium bicarbonate, 0.1-0.2 part of pigment, 0.3-0.8 part of water, 0.4-1.2 parts of polyethylene glycol-4000.8, 0.5 part of vegetable oil, 0.01-0.02 part of cocoyl propyl betaine, 0.01-0.02 part of sodium lauroyl sarcosinate and 38-42 parts of citric acid.
3. The effervescent bath salt ball of claim 2, wherein: the vegetable oil comprises eucalyptus globulus leaf oil, coconut oil, olive oil and avocado oil in a mass ratio of 6:1:1: 1.
4. The effervescent bath salt ball of claim 2, wherein: the weight portion of the fragrant component is 0.2-0.4 portion, and the fragrant component is essence or essential oil.
5. The effervescent bath salt ball of claim 1, wherein: the water-soluble capsule wall is selected from water-soluble capsule walls taking polyvinyl alcohol water-soluble film or gelatin as a main component.
6. The effervescent bath salt ball of claim 5, wherein: the water-soluble capsule wall is a polyvinyl alcohol water-soluble film; the fragrant capsule is obtained by filling fragrant components into a polyvinyl alcohol water-soluble film through a packaging machine and performing hot-press film sealing.
7. The effervescent bath salt ball of claim 5, wherein: the water-soluble capsule wall is a water-soluble capsule wall with gelatin as a main component; the fragrant capsule is prepared by a dripping method through a dripping pill machine with double layers of dripping heads.
8. A preparation method of an effervescent bath salt ball is characterized in that: wrapping the flavor component in the water-soluble capsule wall to form flavor capsule; uniformly mixing the components of the bath salt ball body to obtain a mixture, filling the mixture into a mold, and adding a fragrance capsule into the center of the mixture filled into the mold; pressing and forming; and (6) pumping and packaging.
9. The method of preparing effervescent bath salt balls of claim 8, wherein: the method specifically comprises the following steps:
step one, cleaning and disinfecting production equipment and tools;
step two, preparing the flavor capsule: a) putting the flavor components into a packaging machine, filling the flavor components into a polyvinyl alcohol water-soluble film, and performing hot-press film sealing to obtain the flavor capsule; or b) taking gelatin solution prepared from gelatin, plasticizer and water as water-soluble capsule wall raw material, taking oily flavor component as capsule core, and dripping to obtain the final product;
step three, weighing the components of the bath salt ball body according to the following weight parts: 55-60 parts of sodium bicarbonate, 0.1-0.2 part of pigment, 0.3-0.8 part of water, 0.4-1.2 parts of polyethylene glycol-4000.8, 0.5 part of vegetable oil, 0.01-0.02 part of cocoyl propyl betaine, 0.01-0.02 part of sodium lauroyl sarcosinate and 38-42 parts of citric acid;
step four, putting the sodium bicarbonate, the pigment and the water into stirring equipment, and uniformly stirring; adding polyethylene glycol-400 and vegetable oil, stirring, and sieving; adding cocoyl propyl betaine and sodium lauroyl sarcosinate, and stirring uniformly; finally, adding citric acid, and uniformly mixing to obtain a mixture;
filling the mixture into the mold, adding the flavor capsules into the center in the filling process, and performing compression molding;
and step six, putting the formed ball body into a drying chamber for drying to obtain the effervescent bath salt ball, and packaging.
10. The method of preparing effervescent bath salt balls of claim 9, wherein: the ratio of gelatin, plasticizer and water in the gelatin solution is 1: 0.4-0.6: 1.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111374897.0A CN113855592A (en) | 2021-11-19 | 2021-11-19 | Effervescent bath salt ball and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111374897.0A CN113855592A (en) | 2021-11-19 | 2021-11-19 | Effervescent bath salt ball and preparation method thereof |
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| CN113855592A true CN113855592A (en) | 2021-12-31 |
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| CN202111374897.0A Pending CN113855592A (en) | 2021-11-19 | 2021-11-19 | Effervescent bath salt ball and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114288193A (en) * | 2022-01-05 | 2022-04-08 | 中盐工程技术研究院有限公司 | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof |
| CN115054547A (en) * | 2022-06-07 | 2022-09-16 | 青海民族大学 | Notopterygium root effervescent bath salt ball and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3779932A (en) * | 1970-07-01 | 1973-12-18 | B Jaggers | Solid washing compositions |
| CN2912637Y (en) * | 2006-05-17 | 2007-06-20 | 义乌市庆鹏化妆品有限公司 | Solid bath salt with built-in cleaning ingredient |
| CN103140208A (en) * | 2010-06-25 | 2013-06-05 | 奇华顿股份有限公司 | Encapsulated compositions comprising aldehyde fragrance precursors |
| US20160143823A1 (en) * | 2013-06-13 | 2016-05-26 | Reckitt Benckiser (Brands) Limited | Bath Salt Composition |
| CN110101589A (en) * | 2019-05-21 | 2019-08-09 | 天津长芦海晶集团有限公司 | A kind of effervescent bath salt ball |
-
2021
- 2021-11-19 CN CN202111374897.0A patent/CN113855592A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3779932A (en) * | 1970-07-01 | 1973-12-18 | B Jaggers | Solid washing compositions |
| CN2912637Y (en) * | 2006-05-17 | 2007-06-20 | 义乌市庆鹏化妆品有限公司 | Solid bath salt with built-in cleaning ingredient |
| CN103140208A (en) * | 2010-06-25 | 2013-06-05 | 奇华顿股份有限公司 | Encapsulated compositions comprising aldehyde fragrance precursors |
| US20160143823A1 (en) * | 2013-06-13 | 2016-05-26 | Reckitt Benckiser (Brands) Limited | Bath Salt Composition |
| CN110101589A (en) * | 2019-05-21 | 2019-08-09 | 天津长芦海晶集团有限公司 | A kind of effervescent bath salt ball |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114288193A (en) * | 2022-01-05 | 2022-04-08 | 中盐工程技术研究院有限公司 | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof |
| CN115054547A (en) * | 2022-06-07 | 2022-09-16 | 青海民族大学 | Notopterygium root effervescent bath salt ball and preparation method thereof |
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