CN114288193A - Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof - Google Patents
Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof Download PDFInfo
- Publication number
- CN114288193A CN114288193A CN202210009446.5A CN202210009446A CN114288193A CN 114288193 A CN114288193 A CN 114288193A CN 202210009446 A CN202210009446 A CN 202210009446A CN 114288193 A CN114288193 A CN 114288193A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- release
- ball
- delaying
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 81
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 48
- 239000000843 powder Substances 0.000 claims abstract description 26
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 24
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 16
- 239000011148 porous material Substances 0.000 claims abstract description 9
- 238000001179 sorption measurement Methods 0.000 claims abstract description 6
- 239000011800 void material Substances 0.000 claims abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 238000002156 mixing Methods 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 16
- 229920002774 Maltodextrin Polymers 0.000 claims description 8
- 239000005913 Maltodextrin Substances 0.000 claims description 8
- 239000002202 Polyethylene glycol Substances 0.000 claims description 8
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 8
- 229940035034 maltodextrin Drugs 0.000 claims description 8
- 229920001223 polyethylene glycol Polymers 0.000 claims description 8
- 239000004094 surface-active agent Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 4
- 238000000465 moulding Methods 0.000 claims description 4
- 238000003825 pressing Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 238000007873 sieving Methods 0.000 claims description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- 230000003111 delayed effect Effects 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 5
- 239000013335 mesoporous material Substances 0.000 description 3
- 238000006555 catalytic reaction Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention provides a foot bath effervescent ball for delaying release of essential oil and a preparation method thereof, wherein the raw material comprises essential oil solidified powder, the essential oil solidified powder is mesoporous silicon dioxide absorbed with the essential oil, and the void volume of the mesoporous silicon dioxide is 0.8-1.5 cm3The adsorption average pore diameter is 10-20 nm. According to the foot bath effervescent ball for delaying the release of the essential oil, the mesoporous silicon dioxide is mixed with the essential oil, and the essential oil is adsorbed on the mesoporous silicon dioxide, so that the stability of the essential oil is improved to a certain extent, the volatilization of the essential oil is delayed, and the stable release of the essential oil is realized.
Description
Technical Field
The invention belongs to the technical field of daily necessities, and particularly relates to a foot bath effervescent ball for delaying release of essential oil and a preparation method thereof.
Background
The foot bath effervescent ball product is a leisure product which is popular in recent years, can generate an effervescent effect when in use, has high entertainment, has the functions of decontamination, moisture preservation and the like, and is gradually loved by consumers. The natural plant essential oil has the effects of aromatic physical therapy and skin moistening, is often used in the foot bath effervescent ball to improve the product value, but has the characteristics of volatility, instability and the like, and limits the use of the plant essential oil.
The mesoporous material is a porous material with the pore diameter of 2-50 nm, and has the characteristics of orderliness, pore diameter distribution unicity, controllability, mesoporous shape diversity and the like, so that the mesoporous material has an extremely important function in the fields of adsorption separation, industrial catalysis, biomedicine, environmental protection and the like. If the excellent adsorbability of the mesoporous material can be applied to the problem of volatilization of the essential oil in the effervescent ball, a new solution is provided for the problem of easy volatilization and instability of the essential oil.
Disclosure of Invention
In view of the above, in order to solve the above problems, the invention provides an essential oil release-delaying foot bath effervescent ball and a preparation method thereof.
In order to achieve the purpose, the technical scheme of the invention is realized as follows:
the invention provides a foot bath effervescent ball capable of delaying release of essential oil, which comprises essential oil solidified powder, wherein the essential oil solidified powder is mesoporous silicon dioxide adsorbed with the essential oil, and the release of the essential oil can be delayed through the adsorption slow release effect of the mesoporous silicon dioxide on the essential oil.
Further, the void volume of the mesoporous silica is 0.8-1.5 cm3The adsorption average pore diameter is 10-20 nm.
Further, the mass ratio of the essential oil to the mesoporous silica in the essential oil solidified powder is 1: 5-10: 5.
the mesoporous silica has the characteristics of high specific surface area, high pore volume, uniform and adjustable pore channel nanoscale in the range of 2-50 nm, good thermal stability, rich silicon hydroxyl in pore channels and the like, and is widely applied to the fields of catalysis, catalyst loading, adsorption separation and the like.
The essential oil can be natural plant essential oil with fragrance.
Further, the paint comprises the following components in parts by weight: 0.5-5 parts of essential oil curing powder, 30-50 parts of sodium bicarbonate, 0.1-1 part of water, 0.5-2 parts of polyethylene glycol, 1-10 parts of surfactant, 20-40 parts of citric acid and 1-5 parts of maltodextrin.
The invention also provides a preparation method of the foot bath effervescent ball for delaying the release of the essential oil, which comprises the following steps:
(1) weighing the components according to the proportion;
(2) adding essential oil into the mesoporous silicon dioxide under the condition of stirring, absorbing and mixing uniformly to obtain essential oil solidified powder, and sealing the essential oil solidified powder for later use;
(3) uniformly mixing sodium bicarbonate and water, sequentially adding polyethylene glycol and essential oil curing powder, uniformly mixing, sieving, adding a surfactant, uniformly mixing, adding citric acid, uniformly mixing, finally adding maltodextrin, uniformly mixing, and pressing and molding the obtained uniform mixture to obtain the foot bath effervescent ball for delaying the release of the essential oil.
Further, in the step (2), the stirring condition is specifically that essential oil is dropwise added while stirring under the condition of 100-300 r/min, and the stirring is carried out for 5-15 min.
Compared with the prior art, the foot bath effervescent ball for delaying the release of the essential oil and the preparation method thereof have the following advantages:
due to the good adsorbability of the mesoporous silicon dioxide, the essential oil is adsorbed in the mesoporous silicon dioxide in advance, so that the stability of the essential oil can be improved to a certain extent, and coordinated volatilization and stable release are realized; the mesoporous silicon dioxide and the essential oil are prepared into the essential oil solidified powder in advance, and then the essential oil solidified powder is mixed with other raw materials and pressed into a finished product, so that the essential oil can be prevented from volatilizing in the preparation process, the preparation process is simple, the production cost is low, and the application prospect is good.
Detailed Description
Unless defined otherwise, technical terms used in the following examples have the same meanings as commonly understood by one of ordinary skill in the art to which the present invention belongs. The test reagents used in the following examples, unless otherwise specified, are all conventional biochemical reagents; the experimental methods are conventional methods unless otherwise specified.
The present invention will be described in detail with reference to examples.
Example 1
Preparing essential oil solidified powder: the mass ratio of the essential oil to the mesoporous silicon dioxide is 3: 5; dropwise adding essential oil into the mesoporous silica while stirring at the speed of 150r/min, stirring for 8min to ensure that the essential oil is fully absorbed by the mesoporous silica and uniformly mixed, and sealing for later use;
weighing the components in the following proportion: 2 parts of essential oil solidified powder, 40 parts of sodium bicarbonate, 0.5 part of water, 1 part of polyethylene glycol, 2 parts of surfactant, 30 parts of citric acid and 2 parts of maltodextrin;
putting sodium bicarbonate and water into a stirring pot, stirring at a high speed, mixing uniformly, sequentially adding polyethylene glycol and essential oil curing powder, mixing uniformly, sieving, adding a surfactant, mixing uniformly, adding citric acid, mixing uniformly, finally adding maltodextrin, mixing uniformly, and pressing and molding the obtained uniform mixture to obtain the foot bath effervescent ball for delaying the release of essential oil.
Example 2
Preparing essential oil solidified powder: the mass ratio of the essential oil to the mesoporous silicon dioxide is 4: 5; dripping essential oil into the mesoporous silicon dioxide under the condition of 200r/min while stirring, stirring for 10min to ensure that the essential oil is fully absorbed by the mesoporous silicon dioxide and is uniformly mixed, and sealing for later use;
weighing the components in the following proportion: 4 parts of essential oil solidified powder, 40 parts of sodium bicarbonate, 1 part of water, 2 parts of polyethylene glycol, 5 parts of surfactant, 40 parts of citric acid and 3 parts of maltodextrin;
putting sodium bicarbonate and water into a stirring pot, stirring at a high speed, mixing uniformly, sequentially adding polyethylene glycol and essential oil curing powder, mixing uniformly, sieving, adding a surfactant, mixing uniformly, adding citric acid, mixing uniformly, finally adding maltodextrin, mixing uniformly, and pressing and molding the obtained uniform mixture to obtain the foot bath effervescent ball for delaying the release of essential oil.
Comparative example 1
The difference from example 1 is that no essential oil solidifying powder is prepared and added in the formulation, and the proportions of other components and the preparation process are the same as in example 1.
Comparative example 2
The difference from example 2 in the formulation of example 2 is that no essential oil curing powder was prepared, not added, and the proportions of other components and the preparation process were the same as in example 1.
And (3) performance testing:
the fragrance release period in the essential oil was measured by sensory evaluation, and the results are shown in table 1.
TABLE 1
As can be seen from table 1, in the sensory evaluation, different testers can obviously feel that the essential oil volatilization of the finished products of examples 1 and 2 added with the essential oil curing powder is more stable, and the addition of the mesoporous silica has a certain slow release effect on the release of the essential oil, so that the effect of delaying the release of the essential oil can be achieved.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. A footbath effervescent ball for delaying the release of essential oil is characterized in that: the essential oil curing powder is mesoporous silicon dioxide adsorbed with essential oil.
2. The footbath effervescent ball for delaying the release of essential oil according to claim 1, characterized in that: the void volume of the mesoporous silica is 0.8-1.5 cm3The adsorption average pore diameter is 10-20 nm.
3. The footbath effervescent ball for delaying the release of essential oil according to claim 1, characterized in that: the mass ratio of the essential oil to the mesoporous silica in the essential oil solidified powder is 1: 5-10: 5.
4. the footbath effervescent ball for delaying the release of essential oil according to any one of claims 1 to 3, which is characterized by comprising the following components in parts by weight: 0.5-5 parts of essential oil curing powder, 30-50 parts of sodium bicarbonate, 0.1-1 part of water, 0.5-2 parts of polyethylene glycol, 1-10 parts of surfactant, 20-40 parts of citric acid and 1-5 parts of maltodextrin.
5. The preparation method of the foot bath effervescent ball for delaying the release of essential oil, which is characterized by comprising the following steps:
(1) weighing the components according to the proportion;
(2) adding essential oil into the mesoporous silicon dioxide under the condition of stirring, absorbing and mixing uniformly to obtain essential oil solidified powder, and sealing the essential oil solidified powder for later use;
(3) uniformly mixing sodium bicarbonate and water, sequentially adding polyethylene glycol and essential oil curing powder, uniformly mixing, sieving, adding a surfactant, uniformly mixing, adding citric acid, uniformly mixing, finally adding maltodextrin, uniformly mixing, and pressing and molding the obtained uniform mixture to obtain the foot bath effervescent ball for delaying the release of the essential oil.
6. The preparation method of the foot bath effervescent ball for delaying the release of essential oil according to claim 5, which is characterized in that: in the step (2), the stirring condition is specifically that essential oil is dripped while stirring under the condition of 100-300 r/min, and the stirring is carried out for 5-15 min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210009446.5A CN114288193A (en) | 2022-01-05 | 2022-01-05 | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210009446.5A CN114288193A (en) | 2022-01-05 | 2022-01-05 | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114288193A true CN114288193A (en) | 2022-04-08 |
Family
ID=80975102
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210009446.5A Pending CN114288193A (en) | 2022-01-05 | 2022-01-05 | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114288193A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511133A (en) * | 2016-12-06 | 2017-03-22 | 广州睿森生物科技有限公司 | Essential oil nanoparticles and preparation method thereof as well as application of essential oil nanoparticles to preparation of mosquito-repelling product |
| CN110339258A (en) * | 2019-08-22 | 2019-10-18 | 新疆伊帕尔汗香料股份有限公司 | A kind of sleeping essential oil and its cured granulate preparation method |
| CN112973620A (en) * | 2021-02-23 | 2021-06-18 | 杭州云昇科技有限公司 | Mesoporous SiO based on joule heat effect2Essential oil controlled release material and preparation method thereof |
| CN113855592A (en) * | 2021-11-19 | 2021-12-31 | 中盐工程技术研究院有限公司 | Effervescent bath salt ball and preparation method thereof |
-
2022
- 2022-01-05 CN CN202210009446.5A patent/CN114288193A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511133A (en) * | 2016-12-06 | 2017-03-22 | 广州睿森生物科技有限公司 | Essential oil nanoparticles and preparation method thereof as well as application of essential oil nanoparticles to preparation of mosquito-repelling product |
| CN110339258A (en) * | 2019-08-22 | 2019-10-18 | 新疆伊帕尔汗香料股份有限公司 | A kind of sleeping essential oil and its cured granulate preparation method |
| CN112973620A (en) * | 2021-02-23 | 2021-06-18 | 杭州云昇科技有限公司 | Mesoporous SiO based on joule heat effect2Essential oil controlled release material and preparation method thereof |
| CN113855592A (en) * | 2021-11-19 | 2021-12-31 | 中盐工程技术研究院有限公司 | Effervescent bath salt ball and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104649640B (en) | Multi-stage porous regulation type diatom ooze | |
| CN101468304A (en) | Colour development methyl aldehyde adsorption material and preparation method thereof | |
| CN102792978A (en) | Preparation method of mosquito-repellent tablets and products | |
| CN103157448A (en) | Method for preparing amino-modified hierarchical pore adsorbent material for cigarette harm reduction | |
| CN110373052A (en) | A kind of modified zeolite purifying formaldehyde antibacterial and antimildew function water paint | |
| CN114288193A (en) | Foot bath effervescent ball capable of delaying release of essential oil and preparation method thereof | |
| CN111494337A (en) | ZIF-8 nano particle wrapping anti-aging drug and application thereof | |
| CN109110770A (en) | The method that silica-amine composite xerogel prepares porous silica microballoon as solid base | |
| CN109012009A (en) | A kind of dry powder material for air purification preparing environmental-friendly artistic product and preparation method | |
| CN103931981B (en) | A kind of preparation method of royal jelly microcapsules and application | |
| CN112961672B (en) | Preparation method of fluorescent bimetallic organic JLUE-MOG-6 aerogel material | |
| CN108976956A (en) | A kind of environment-friendly water-based paint composition and preparation method thereof | |
| CN114762814A (en) | Adsorbing material for solid air freshener, application and solid air freshener | |
| CN107649098A (en) | A kind of preparation method for the rich sulfydryl sorbing material for adsorbing heavy metal ion | |
| CN114045075A (en) | Anti-formaldehyde coating and preparation method and application thereof | |
| CN107352951A (en) | It is a kind of antibacterial except aldehyde diatom ooze coating and preparation method thereof | |
| CN107383982A (en) | A kind of negative ion putty powder and preparation method thereof | |
| CN105311063A (en) | Cordyceps sinensis tablet and preparation method thereof | |
| CN111870546A (en) | Hydrogen-rich mask and preparation method thereof | |
| CN109354026A (en) | A kind of preparation method of the uniform mesoporous silicon foam material in aperture | |
| CN108157364A (en) | A kind of pH responses slow-releasing pesticide preparation and preparation method thereof | |
| CN103739865B (en) | A kind of Antibiotic Membrane | |
| AU2021106183A4 (en) | Vitamin d3 complex and preparation method and application thereof | |
| JPS584006B2 (en) | Fun matsuyokuyouzainoseizouhouhou | |
| CN101767956B (en) | Bamboo carbon powder molding composition and molding method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |