CN102874857B - 一种水热法解聚贝壳制备片状碳酸钙的方法 - Google Patents
一种水热法解聚贝壳制备片状碳酸钙的方法 Download PDFInfo
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- CN102874857B CN102874857B CN201210331597.9A CN201210331597A CN102874857B CN 102874857 B CN102874857 B CN 102874857B CN 201210331597 A CN201210331597 A CN 201210331597A CN 102874857 B CN102874857 B CN 102874857B
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 65
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 32
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 claims abstract description 33
- 239000002994 raw material Substances 0.000 claims abstract description 33
- 239000000725 suspension Substances 0.000 claims abstract description 26
- 238000001914 filtration Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- 230000005484 gravity Effects 0.000 claims abstract description 11
- 238000000227 grinding Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 14
- 238000011049 filling Methods 0.000 claims description 10
- 238000009413 insulation Methods 0.000 claims description 10
- 230000009467 reduction Effects 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 10
- 241000237536 Mytilus edulis Species 0.000 claims description 9
- 235000020638 mussel Nutrition 0.000 claims description 9
- BAIIEUXIVAALCL-UHFFFAOYSA-M O.C(C)O.OO.[OH-].[Na+] Chemical compound O.C(C)O.OO.[OH-].[Na+] BAIIEUXIVAALCL-UHFFFAOYSA-M 0.000 claims description 7
- 229910001220 stainless steel Inorganic materials 0.000 claims description 7
- 239000010935 stainless steel Substances 0.000 claims description 7
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 6
- 235000005956 Cosmos caudatus Nutrition 0.000 claims description 5
- 244000293323 Cosmos caudatus Species 0.000 claims description 5
- 239000013505 freshwater Substances 0.000 claims description 5
- 241000237502 Ostreidae Species 0.000 claims description 4
- 241000237509 Patinopecten sp. Species 0.000 claims description 4
- 235000020636 oyster Nutrition 0.000 claims description 4
- 235000020637 scallop Nutrition 0.000 claims description 4
- 239000004567 concrete Substances 0.000 claims description 3
- 238000004062 sedimentation Methods 0.000 claims description 3
- 238000001238 wet grinding Methods 0.000 claims description 3
- 230000008901 benefit Effects 0.000 abstract description 5
- 239000011248 coating agent Substances 0.000 abstract description 3
- 238000000576 coating method Methods 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 abstract description 3
- 239000004033 plastic Substances 0.000 abstract description 3
- 229920003023 plastic Polymers 0.000 abstract description 3
- 239000005060 rubber Substances 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 239000004566 building material Substances 0.000 abstract description 2
- 239000003814 drug Substances 0.000 abstract description 2
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
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- 238000004519 manufacturing process Methods 0.000 description 2
- 239000011858 nanopowder Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 241000276489 Merlangius merlangus Species 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000009881 electrostatic interaction Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229920000592 inorganic polymer Polymers 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000012764 mineral filler Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 235000015170 shellfish Nutrition 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
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CN201210331597.9A CN102874857B (zh) | 2012-09-10 | 2012-09-10 | 一种水热法解聚贝壳制备片状碳酸钙的方法 |
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CN201210331597.9A CN102874857B (zh) | 2012-09-10 | 2012-09-10 | 一种水热法解聚贝壳制备片状碳酸钙的方法 |
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CN102874857B true CN102874857B (zh) | 2014-12-10 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110203957A (zh) * | 2019-06-10 | 2019-09-06 | 水恣意(厦门)科技有限公司 | 一种基于亚临界水解法制取纳米碳酸钙的方法 |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103086414A (zh) * | 2013-01-31 | 2013-05-08 | 南昌航空大学 | 贝壳水热处理制备高纯度方解石碳酸钙微粉的方法 |
CN103086415A (zh) * | 2013-01-31 | 2013-05-08 | 南昌航空大学 | 水热条件下贝壳制备片状文石结构碳酸钙粉体的方法 |
CN103274439B (zh) * | 2013-07-01 | 2015-12-09 | 广东海洋大学 | 一种牡蛎壳再生循环制取纳米碳酸钙的方法 |
CN103571235B (zh) * | 2013-10-28 | 2015-12-30 | 浙江大学舟山海洋研究中心 | 一种棱柱状生物碳酸钙的制备方法 |
CN104256654B (zh) * | 2014-09-08 | 2015-12-02 | 程梅雪 | 流水式文蛤壳加工工艺 |
CN108359273A (zh) * | 2018-01-29 | 2018-08-03 | 南昌航空大学 | 一种提高大理石粉体白度的方法 |
CN108675334B (zh) * | 2018-07-17 | 2019-07-12 | 北京航空航天大学 | 一种剥离贝壳文石片的方法 |
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CN101920982A (zh) * | 2010-07-16 | 2010-12-22 | 浙江大学 | 一种以贻贝壳为原料制备功能性碳酸钙的方法 |
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JP2007063080A (ja) * | 2005-08-31 | 2007-03-15 | Nippon Tennen Sozai Kk | 貝殻を原料とする高分散性炭酸カルシウム粉末とその製造方法 |
CN102205984B (zh) * | 2011-04-12 | 2012-12-05 | 广西大学 | 一种在常温常压下合成文石纳米棒的方法 |
CN102275966B (zh) * | 2011-07-25 | 2013-07-31 | 复旦大学 | 一种碳酸钙微粒的制备方法 |
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CN101920982A (zh) * | 2010-07-16 | 2010-12-22 | 浙江大学 | 一种以贻贝壳为原料制备功能性碳酸钙的方法 |
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Cited By (1)
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CN110203957A (zh) * | 2019-06-10 | 2019-09-06 | 水恣意(厦门)科技有限公司 | 一种基于亚临界水解法制取纳米碳酸钙的方法 |
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Inventor after: Ji Xiaosheng Inventor after: Chen Tao Inventor after: Ye Ying Inventor after: Xia Meisheng Inventor after: Jin Shidi Inventor after: Liu Shuting Inventor after: Zhu Zhenhong Inventor before: Ye Ying Inventor before: Chen Tao Inventor before: Xia Meisheng Inventor before: Jin Shidi Inventor before: Liu Shuting Inventor before: Zhu Zhenhong |
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Free format text: CORRECT: INVENTOR; FROM: YE YING CHEN TAO XIA MEISHENG JIN SHIDI LIU SHUTING ZHU ZHENHONG TO: JI XIAOSHENG CHEN TAO YE YING XIA MEISHENG JIN SHIDI LIU SHUTING ZHU ZHENHONG |
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Granted publication date: 20141210 Termination date: 20180910 |