CN102871864B - Antimicrobial and dandruff-removing nano-silver hair foaming emulsion - Google Patents
Antimicrobial and dandruff-removing nano-silver hair foaming emulsion Download PDFInfo
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- CN102871864B CN102871864B CN201210414344.8A CN201210414344A CN102871864B CN 102871864 B CN102871864 B CN 102871864B CN 201210414344 A CN201210414344 A CN 201210414344A CN 102871864 B CN102871864 B CN 102871864B
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Abstract
The invention relates to an antimicrobial and dandruff-removing hair foaming emulsion and belongs to the technical field of hair foaming agent. Antimicrobial materials of nano-silver and chitosan are taken as the main components and a thickener, an emulsifier, a co-emulsifier, a foaming agent, a preservative, a solvent and a propellent are added to prepare the emulsion. The preparation method comprises the following steps that: various components are mixed evenly and are subjected to ultrasonic emulsification for 30 minutes to prepare an emulsified solution; and the solution is poured into pressure-resistant bottles, and the propellent is added and the nano (50-100nm)-silver chitosan foaming gel preparation product is prepared. The product can clean hair, promote a physiological function and brighten hair. In addition, by the synergistic effect of chitosan and nano-silver, the antimicrobial effect is better and no drug resistance is caused. The hair foaming emulsion can be used for removing dandruff which is caused by scalp fungal infection.
Description
Technical field
The present invention relates to a kind of hair washing whipped cream, be specifically related to a kind of can be antibacterial, the nanometer silver leaves shampoo of dandruff, belong to hair-washing hair-care article of everyday use production technical field.
Background technology
The dandruff is medically being called capitis pityriasis, is a kind of dermatosis being caused by chlosma, the leaves shampoo of the antibacterial action going on the market at present, and as " adopting pleasure ", its antibacterials are miconazoles, this medicine life-time service can cause that an epithelial cell produces a drug resistance.
Nanometer silver is to take the novel antibacterial product that nanotechnology forms as foundation development, due to quantum effect, small-size effect with there is great specific surface area, thereby there is the incomparable antibacterial effect of traditional inorganic antiseptic, and safe, effect is lasting, is a kind of long-lasting and weatherability antibacterial of having.The principle of relevant bactericidal nano-silver effect, most scholars think, ultra-fine state silver surface is actively large, in water, be Ag+, therefore the bactericidal action of nanometer silver is main relevant with silver ion, can with pheron in thalline in-the rapid combination of SH, for key enzyme inactivation, make pathogenic bacterium not energy metabolism and death; Secondly, nanometer silver can be combined and form cross-linked with DNA of pathogenic base, replaces the hydrogen bond between adjacent nitrogen in purine and pyrimidine, makes DNA degeneration and reproducible not, causes pathogenic bacterium inactivation.The atomic arrangement surface of nanometer silver is " Jie's state " between solid and molecule, and the extremely strong Silver nanoparticles of this activity possesses superpower antibacterial ability, can kill the pathogenic microorganism such as antibacterial, fungus, mycoplasma, chlamydia.In addition, nanometer silver is again non-antibiotics antibacterial, without any antibacterial, silver is produced to drug resistance at present, have no adverse reaction, do not produce cross infection, visible, nanometer silver except wide spectrum, bacteriostasis and sterilization effect are strong, can also promote tissue repair and regeneration, safety, toxic and side effects are little.
CN101049279B discloses a kind of nanometer silver shampoo and preparation method thereof, but the method is used content of nanometer silver
Height, in order to reduce costs, and reaches better bactericidal effect, and the present invention has adopted different composition and engineerings to develop a kind of novel antibacterial hair washing of the nanometer silver except dandruff whipped cream.Because chitosan is a kind of have good biocompatibility and biodegradable macromolecular polysaccharide, nontoxic to human body, can promote wound healing and tissue reconstruction, by the synergism of chitosan and nanometer silver, can improve sterilization and the dandruff effect of leaves shampoo, and promotion physiological function, make hair light moist.This technical matters is simple, easy to operate.
Summary of the invention
The object of this invention is to provide a kind of hair washing whipped cream, there is effect antibacterial, dandruff.
Another object of the present invention is to provide a kind of preparation method of nanometer silver hair washing whipped cream.
For realizing the object of foregoing invention, the technical scheme that the present invention takes is as follows:
Have the antibacterial hair washing of the nanometer silver except a dandruff whipped cream, this whipped cream is comprised of drug delivery system and propellant, and the content of each component is:
100mL drug delivery system:
Nanometer silver sol solution 10 ~ 50ppm
Chitosan 5 ~ 10%
Oil phase emulsifier 5 ~ 10%
Emulsifying agent 0.5 ~ 1%
Co-emulsifier 0.5 ~ 1%
Thickening agent 0.1 ~ 0.5%
Antiseptic 0.1 ~ 0.5%
Foaming agent 1 ~ 5%
Propellant: 8-10%
Deionized water complements to 100mL
Wherein, nanometer silver particle diameter 25 ~ 50nm scope in described nanometer silver sol solution; Chitosan molecule amount is distributed in 2000 ~ 5000, and deacetylation is more than 95%.
Described oil phase emulsifier is Oleum sesami, Oleum Ricini or Rhizoma Alpiniae Officinarum oil 5 ~ 10%(W/L); Emulsifying agent is mixture (4:1) or the poloxamer 5 ~ 10%(g/L of tween 80, Arlacel-80, Tween 80 and sorbester p17); Co-emulsifier is glycerol or PEG400 (PEG400) 0.5 ~ 1%(g/L); Thickening agent is PVP polyvinyl pyrrolidone K30 (C-934), carbomer, microcrystalline Cellulose MCC, carboxymethyl cellulose (CMC-Na), hypromellose (HPMC), chitosan or polyoxyethylene--polyoxypropylene copolymer 0.1 ~ 0.5%(g/L), wherein first-selected carbomer and hypromellose; Antiseptic is benzalkonium bromide or ethyl hydroxybenzoate 0.1 ~ 0.5%(g/L); Foaming agent is sodium lauryl sulphate (K-12) 1 ~ 5%(g/L); Propellant is iso-butane, isopropyl alkane or hydrogen fluorohydrocarbon (HFC-134a) 8-10%(g/L).
A preparation method for nanometer silver hair washing whipped cream, comprises the steps:
(1) take appropriate thickening agent, be dissolved in deionized water, fully swelling is 24 hours, makes stream shape liquid A standby;
(2) by emulsifying agent, co-emulsifier, join in remaining deionized water, then add chitosan, stir, be heated to 80 ℃, fully dissolve to obtain B liquid;
(3) A, B liquid are mixed, after adding antiseptic to stir, add nano silver colloidal sol liquid, C liquid stirs to obtain;
(4) take oil phase emulsifier, foaming agent, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes;
(5) emulsified solution is filled in pressure bottle, (proportionally regulate the foam situation of spraying, adjusting is filled to add propellant
The amount of propellant, general preferred 8-10%(W/L)), be prepared into the silver-colored chitosan frothy gel of nanometer (50-100nm) preparation finished product.
The invention has the beneficial effects as follows:
(1) this product can clean hair, promotes physiological function, makes head light moist; There is bactericidal effect, overcome traditional dandruff control shampoo containing chafe, the shortcoming that drug resistance is poor; By the synergism of chitosan and nanometer silver, antibacterial effect is better, can eliminate scalp fungal infection and the dandruff that causes.
(2) product form is whipped cream type, easy to use, play a role fast and effect remarkable.
(3) by adding chitosan, make that the use amount of nanometer silver is very little can reach good bactericidal effect, reduced cost, and this technical matters is simple, easy to operate, be applicable to large-scale production.
The specific embodiment
Below by example, the present invention is described in further details, these examples are only used for illustrating the present invention, do not limit the scope of the invention.
Embodiment 1
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | In prescription, act on | Consumption 100g |
| Nanometer silver | Resist | 10ppm |
| Chitosan | Antibacterial, substrate | 5.0g |
| Carbomer | Thickening agent | ?0.1g |
| Tween 80 | Emulsifying agent | 0.5g ? |
| Glycerol | Co-emulsifier | 0.5g |
| K12 | Foaming agent | 2.0g |
| Benzalkonium bromide | Corrosion-proof and sterilization agent | 0.1 |
| Oleum sesami | Oil phase emulsifier | 5.0g |
| Propellant | Iso-butane | 10g |
| Deionized water | Solvent | Complement to 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.1g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 0.5g emulsifier tween 80,0.5g co-emulsifier glycerol joins (43.4g) in deionized water, adds chitosan 5g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic benzalkonium bromide 0.1g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 5g oil phase emulsifier Oleum sesami, 2.0g foaming agent K12, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant iso-butane 10g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 2
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | Effect | Consumption 100g |
| Nanometer silver | Resist | 20ppm(5g solution amount) |
| Chitosan | Antibacterial, substrate | 10g |
| Carbomer | Thickening agent | 0.3g |
| Tween 80 | Emulsifying agent | 1.0g |
| Glycerol | Co-emulsifier | 1.0g |
| K12 | Foaming agent | 3.0g |
| Benzalkonium bromide | Corrosion-proof and sterilization agent | 0.5g |
| Oleum sesami | Oil phase | 10g |
| Iso-butane | Propellant | 8g |
| Deionized water | Solvent | Complement to 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.3g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 1.0g emulsifier tween-80,0.5g co-emulsifier glycerol joins (32.2g) in deionized water, adds chitosan 10g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic benzalkonium bromide 0.1g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 10g oil phase emulsifier Oleum sesami, 0.5g foaming agent K12, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant 8g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 3
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | Effect | Consumption 100g |
| Nanometer silver | Resist | 50ppm(5g solution amount) |
| Chitosan | Antibacterial, substrate | 10g |
| Carbomer | Thickening agent | 0.5g |
| Tween 80 and Arlacel-80 mixture | Emulsifying agent | 1.0g |
| Glycerol | Co-emulsifier | 1.0g |
| K12 | Foaming agent | 1.0g |
| Benzalkonium bromide | Corrosion-proof and sterilization agent | 1.0g |
| Oleum Ricini | Oil phase | 10g |
| Hydrogen fluorohydrocarbon (HFC-134a) | Propellant | 10g |
| Deionized water | Solvent | Complement to 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.5g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 1.0g emulsifier tween-80 and Arlacel-80 mixture, 1.0g co-emulsifier glycerol joins (40.5g) in deionized water, adds chitosan 10g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic benzalkonium bromide 1g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 10g oil phase emulsifier Oleum Ricini, 1.0g foaming agent K12, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant 10g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 4
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | Effect | Consumption 100g |
| Nanometer silver | Resist | 50ppm(5g solution amount) |
| Chitosan | Antibacterial, substrate | 5.0g |
| Carbomer | Thickening agent | 0.5g |
| Poloxamer | Emulsifying agent | 0.5g ? |
| PEG400 | Co-emulsifier | 1.0g |
| TX-10 | Foaming agent | 5g |
| Ethyl hydroxybenzoate | Corrosion-proof and sterilization agent | 0.1g |
| Rhizoma Alpiniae Officinarum oil | Oil phase emulsifier | 10g |
| Isopropyl alkane | Propellant | 8g |
| Deionized water | Solvent | Supply 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.5g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 0.5g emulsifying agent poloxamer, co-emulsifier 1.0gPEG400 joins (34.4g) in deionized water, adds chitosan 5.0g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic ethyl hydroxybenzoate 0.1g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 10g oil phase emulsifier Rhizoma Alpiniae Officinarum oil, 0.5g foaming agent TX-10, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant 8g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 5
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | Effect | Consumption 100g |
| Nanometer silver | Resist | 50ppm(5g solution amount) |
| Chitosan | Antibacterial, substrate | 10g |
| Carbomer | Thickening agent | 0.5g |
| Tween 80 and Arlacel-80 mixture | Emulsifying agent | 2.0g |
| PEG400 | Co-emulsifier | 0.5g |
| Tx-10 | Foaming agent | 1.0g |
| Ethyl hydroxybenzoate | Corrosion-proof and sterilization agent | 0.1g |
| Rhizoma Alpiniae Officinarum oil | Oil phase | 5g |
| Iso-butane | Propellant | 10g |
| Deionized water | Solvent | Supply 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.5g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 2.0g emulsifier tween-80 and Arlacel-80 mixture, 0.5g co-emulsifier PEG400 joins (35 g) in deionized water, adds chitosan 10g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic ethyl hydroxybenzoate 0.1g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 5g oil phase emulsifier Rhizoma Alpiniae Officinarum oil, 1.0g foaming agent TX-10, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant 10g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 6
Hair washing whipped cream is comprised of the component of following weight portion:
| Component | Effect | Consumption 100g |
| Nanometer silver | Medicine | 10ppm(5g solution amount) |
| Chitosan | Antibacterial and gel-type vehicle | 8g |
| Carbomer | Thickening agent | 0.5g |
| Tween 80 and Arlacel-80 mixture | Emulsifying agent | 2.0g |
| PEG400 | Co-emulsifier | 0.5g |
| Tx-10 | Foaming agent | 1.0g |
| Benzalkonium bromide | Antiseptic | 0.5g |
| Oleum Ricini | Oil phase | 10g |
| Iso-butane | Propellant | 8g |
| Deionized water | Solvent | Supply 100g |
The preparation method of hair washing whipped cream, comprises the steps:
(1) take carbomer 0.5g, be dissolved in deionized water 30g, fully swelling is 24 hours, makes stream shape liquid A standby; By 2.0g emulsifier tween-80 and Arlacel-80 mixture, 0.5g co-emulsifier PEG400 joins (42.5g) in remaining deionized water, adds chitosan 8g, stirs and is heated to 80 ℃, fully dissolves to obtain B liquid; A, B liquid are mixed, after adding antiseptic benzalkonium bromide 0.5g to stir, add nano silver colloidal sol liquid 5g, C liquid stirs to obtain; Take 10g oil phase emulsifier Oleum Ricini, 1.0g foaming agent TX-10, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes.
(2) by 90g in above filled with solution pressure bottle, add propellant 8g, be prepared into the silver-colored chitosan frothy gel of nanometer (50 ~ 100nm) preparation finished product.
Embodiment 7
Whipped cream extracorporeal disinfecting experimental result of the present invention is in Table 1 and table 2.
Table 1 Emulsion of the present invention is to the dull and stereotyped bacterium base of pityrosporum furfur fungistatic effect
In table, data are antibacterial circle diameter (cm), and diameter is large antibacterial stronger.
Table 2 Emulsion of the present invention and listing are adopted happy to the dull and stereotyped bacterium base of pityrosporum furfur fungistatic effect
In table, data are antibacterial circle diameter (cm), and diameter is large antibacterial stronger, and Emulsion concentration of the present invention is 0.005ppm and adopt happy group (concentration is 2.50%) and have same fungistatic effect.Nanometer silver consumption is considerably less, and there is no drug resistance.
Claims (5)
1. have the antibacterial hair washing of the nanometer silver except a dandruff whipped cream, it is characterized in that: this whipped cream is comprised of drug delivery system and propellant, the content of each component is:
Nanometer silver sol solution 10 ~ 50ppm
Chitosan 5 ~ 10%
Oil phase emulsifier 5 ~ 10%
Emulsifying agent 1 ~ 10%
Co-emulsifier 0.5 ~ 1%
Thickening agent 0.1 ~ 0.5%
Antiseptic 0.1 ~ 0.5%
Foaming agent 1 ~ 5%
Propellant: 8-10%
Deionized water complements to 100mL
Described oil phase emulsifier is Oleum sesami, Oleum Ricini or Rhizoma Alpiniae Officinarum oil 5 ~ 10%(W/L); Emulsifying agent is that tween 80, Arlacel-80, Tween 80 and sorbester p17 are mixture or the poloxamer 1 ~ 10%(W/L of 4:1); Co-emulsifier is glycerol or PEG400 (PEG400) 0.5 ~ 1%(W/L); Thickening agent is polyvinyl pyrrolidone K30, carbomer, microcrystalline Cellulose MCC, sodium carboxymethyl cellulose (CMC-Na), hypromellose (HPMC), chitosan or polyoxyethylene--polyoxypropylene copolymer 0.1 ~ 0.5%(W/L), antiseptic is benzalkonium bromide or ethyl hydroxybenzoate 0.1 ~ 0.5%(W/L); Foaming agent is sodium lauryl sulphate 1 ~ 5%(W/L).
2. a kind of antibacterial hair washing of the nanometer silver except dandruff whipped cream that has according to claim 1, is characterized in that: nanometer silver particle diameter 25 ~ 50nm scope in described nanometer silver sol solution.
3. a kind of antibacterial hair washing of the nanometer silver except dandruff whipped cream that has according to claim 1, is characterized in that: described chitosan molecule amount is distributed in 2000 ~ 5000, and deacetylation is more than 95%.
4. a kind of antibacterial hair washing of the nanometer silver except dandruff whipped cream that has according to claim 1, is characterized in that: described propellant is iso-butane, isopropyl alkane or hydrogen fluorohydrocarbon HFC-134a 8-10%.
5. for the preparation of a method for nanometer silver hair washing whipped cream claimed in claim 1, it is characterized in that: comprise the following steps:
(1) take thickening agent, be dissolved in deionized water, fully swelling is 24 hours, makes stream shape liquid A standby;
(2) by emulsifying agent, co-emulsifier, join in remaining deionized water, then add chitosan, stir, be heated to 80 ℃, fully dissolve to obtain B liquid;
(3) A, B liquid are mixed, after adding antiseptic to stir, add nanometer silver sol solution, C liquid stirs to obtain;
(4) take oil phase emulsifier, foaming agent, joins respectively in C liquid, and ultrasonic emulsification is made emulsified solution for 30 minutes;
(5) emulsified solution is filled in pressure bottle, adds propellant, be prepared into nanometer silver hair washing whipped cream.
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| CN104306853B (en) * | 2014-10-22 | 2017-12-01 | 中国热带农业科学院农产品加工研究所 | Chitosan quaternary ammonium salt galangal essential oil composite antibacterial aerosol, its preparation method and its application |
| CN106176500A (en) * | 2016-09-06 | 2016-12-07 | 广西大学 | Hair growing shampoo and preparation method thereof |
| CN106377486A (en) * | 2016-09-06 | 2017-02-08 | 广西大学 | Method for preparing scurf-removing itching-relieving hair shampoo |
| TWI636794B (en) | 2017-11-06 | 2018-10-01 | 吳治增 | Nano composite material and application thereof |
| CN107970128B (en) * | 2017-12-06 | 2021-01-15 | 彭氏(惠州)实业发展有限公司 | Formula and production process of hair growth promoting liquid containing diaminopyrimidine oxide |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101049279A (en) * | 2007-04-30 | 2007-10-10 | 孙仲毅 | Antibacterial shampoo of Nano silver, and preparation method |
| CN102091017A (en) * | 2010-09-08 | 2011-06-15 | 成进学 | Nanometer-element traditional Chinese medicine negative ion far-infrared effective shampoo |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101049279A (en) * | 2007-04-30 | 2007-10-10 | 孙仲毅 | Antibacterial shampoo of Nano silver, and preparation method |
| CN102091017A (en) * | 2010-09-08 | 2011-06-15 | 成进学 | Nanometer-element traditional Chinese medicine negative ion far-infrared effective shampoo |
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Denomination of invention: A nano silver shampoo foam emulsion with antibacterial and dandruff removing properties Effective date of registration: 20230814 Granted publication date: 20140409 Pledgee: Industrial and Commercial Bank of China Limited Zhanjiang Chikan Branch Pledgor: GUANGDONG TONGDE PHARMACEUTICAL Co.,Ltd. Registration number: Y2023980051969 |
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