CN102835664A - Phyllanthus emblica fine powder containing high-activity superoxide dismutase and preparation method - Google Patents
Phyllanthus emblica fine powder containing high-activity superoxide dismutase and preparation method Download PDFInfo
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- CN102835664A CN102835664A CN2012103714216A CN201210371421A CN102835664A CN 102835664 A CN102835664 A CN 102835664A CN 2012103714216 A CN2012103714216 A CN 2012103714216A CN 201210371421 A CN201210371421 A CN 201210371421A CN 102835664 A CN102835664 A CN 102835664A
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Abstract
The invention discloses phyllanthus emblica fine powder containing high-activity superoxide dismutase and a preparation method. The phyllanthus emblica fine powder is prepared by juicing, purifying, concentrating and drying the raw materials, namely phyllanthus emblica fresh fruits, wherein the activity of superoxide dismutase is 0.45-0.55 million U/100g. The method specifically comprises the following steps of: raw material treatment: selecting decay-free and mildew-free phyllanthus emblica fresh fruits without exogenous impurities which can be seen with naked eyes and grinding the phyllanthus emblica fresh fruits until the grain sizes are 3-5mm after washing the phyllanthus emblica fresh fruits with running water; juicing: juicing the ground phyllanthus emblica and using the juice obtained after removing the fruit residues later; purifying: colating the fruit to remove the fruit residues and other impurities and carrying out high-speed centrifugal separation on the filtrate to obtain separation liquid; concentrating: carrying out vacuum concentration on the separation liquid until the relative density is 1.0-1.3; and drying: drying the concentrates to obtain the phyllanthus emblica fine powder containing high-activity superoxide dismutase. In the steps of concentrating and drying, the lower temperature at 40-50 DEG C is adopted, thus ensuring that the activities of superoxide dismutase and Vc are not easily damaged.
Description
Technical field
The invention belongs to natural plants deep process technology field, be specifically related to a kind of smart powder of emblic and preparation method who contains the high activity superoxide dismutase.
Background technology
Emblic belongs to the Euphorbiaceae phyllanthus plant, and it really eats raw sour-sweet crisp and little puckery, and aftertaste is sweet, so the name emblic has another name called pyhllanth usemhlica L., An Luoguo, Niuganguo etc.The emblic subtree is drought-enduring anti-lean, extremely well-adapted, and happiness light happiness temperature, at present, and China's seed selection or introduce nearly 10 excellent strains, these strain fruits are big, and output is high, and the life-span reaches more than a century, about single fruit weight 15g, is wild 2 ~ 3 times, high and stable yield.Planting the back promptly had output on the 2nd year, and 5 ~ 10kg is produced in living strain in 3 years, and entering in the 5th year is abounded with the phase, and 30 ~ 50kg, every 667m are produced in strain
2Field planting 110 strains, output 4000Kg/667 square metre.Emblic also has a peculiar place, is exactly that fruit is ripe 8 ~ September, and it is fresh-keeping to 2 ~ March of next year to bear fruit in the tree, and does not influence time annual production.Emblic also is that the leaf plant is really appreciated in rare sight.
Emblic contains abundant vitamin C, E, several amino acids, is rich in tannin, organic acid, phenols etc., also contains a considerable amount of superoxide dismutases (SOD) that can remove free radical, and wherein every gram content is up to 482.14 units.Put down in writing emblic " clothes are made light of one's life by commiting suicide for a long time; the growth of prolonging life " in the Compendium of Material Medica; Modern medicine study proves, emblic has effects such as lowering blood-fat and reducing weight, anti-angiogenic atherosis, anti-oxidant and old and feeble, nourishing the liver, is classified as one of the world's three big health plants by the World Health Organization.
At present, the deep process technology of emblic has all reduced the wherein activity of superoxide dismutase, makes the emblic deep processed product can not give play to original effect.Therefore, a kind of smart powder deep processed product of emblic of superoxide dismutase activity that keeps of exploitation is very important.
Summary of the invention
The present invention's first purpose is to provide a kind of smart powder of emblic that contains the high activity superoxide dismutase, and second purpose is the above-mentioned preparation method who contains the smart powder of emblic of high activity superoxide dismutase that provides.
The present invention's first purpose be achieved in that with the emblic fresh fruit be raw material through squeeze the juice, purifying, concentrate, the drying steps preparation, wherein superoxide dismutase activity is 45 ~ 550,000 U/100g.
The present invention's second purpose be achieved in that comprise that raw material is handled, squeezed the juice, purifying, concentrate, drying steps, be specially:
A, raw material are handled: the selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5mm after washing with flowing water;
B, squeeze the juice: get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use;
C, purifying: fruit juice is removed pomace and other impurity through coarse filtration, filtrating through high speed centrifugation separate parting liquid;
D, concentrated: the parting liquid vacuum is concentrated into relative density 1.0 ~ 1.3;
E, drying: with the smart powder of emblic that obtains containing the high activity superoxide dismutase after the concentrate drying.
The present invention is a raw material with the emblic fresh fruit, adopt squeeze the juice, combined filtering, high speed centrifugation separate, vacuum concentrates, dry, obtain the smart powder of emblic, method is easy.Wherein concentrated and drying steps adopts 40 ~ 50 ℃ lower temperature, has guaranteed that superoxide dismutase activity and Vc are difficult for being destroyed, and has kept the original color and luster of product, flavour, smell.
Description of drawings
Fig. 1 is a process chart of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing the present invention is further described, but never in any form the present invention is limited, any conversion or replacement based on training centre of the present invention is done all belong to protection scope of the present invention.
As shown in Figure 1, the present invention is a raw material with the emblic fresh fruit, through broken, squeeze the juice, purifying, concentrate, the drying steps preparation, superoxide dismutase activity is 45 ~ 550,000 U/100g.
Vc content is 2000 ~ 4500mg/100g in the smart powder of described emblic.
Preparation of the present invention contains the method for the smart powder of emblic of high activity superoxide dismutase, comprises that raw material is handled, squeezed the juice, purifying, concentrated, drying steps, is specially:
It is that nothing is rotten, nothing is gone mouldy, the emblic fresh fruit of the visible exogenous impurity of no naked eyes with selecting that described raw material is handled, with the granularity that is crushed to 3 ~ 5 mm after the flowing water flushing; Described squeezing the juice is to get broken emblic to squeeze the juice, and the fruit juice of removing behind the pomace is for use; Described purifying is that fruit juice is removed pomace and other impurity through coarse filtration, filtrating through 10000 ~ 45000 r/min high speed centrifugations separate parting liquid; Described concentrating is that the parting liquid vacuum is concentrated into relative density 1.0 ~ 1.3; Described drying is with the smart powder of emblic that obtains containing the high activity superoxide dismutase after the concentrate drying.
Described purification step high speed centrifugation rotating speed is 30000 ~ 40000r/min, further is optimized for 35000r/min.
The vacuum thickening temperature is 40 ~ 50 ℃ in the described concentration step.
Drying in the described drying steps is microwave drying or freeze drying, and baking temperature is 40 ~ 50 ℃.
Operation principle of the present invention:
The present invention is a raw material with the emblic fresh fruit; Adopt selected, clean, broken, squeeze the juice, filtration, high speed centrifugation separate, technology such as vacuum and low temperature concentrates, microwave low-temperature drying replace conventional arts; The high speed centrifugation isolation technics of uses advanced; Effectively remove the impurity in the fruit juice, improve utilization ratio of raw materials; Utilization low temperature concentrates, microwave low-temperature drying, guarantees that active ingredient is not destroyed, and has kept the original color and luster of product, flavour, smell.
Superoxide dismutase activity item in the embodiment of the invention is that the method according to B/T 5009.171-2003 detects.
Embodiment 1
The selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit 100kg of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5 mm after washing with flowing water; Get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use; Fruit juice is removed pomace and other impurity through preliminary the filtration, and filtrating is separated 5min through 25000 r/min high speed centrifugations and is got parting liquid; Parting liquid is concentrated into relative density 1.0 ~ 1.3 in 40 ℃ of vacuum; Described drying is the smart powder 6kg of emblic that concentrate is obtained containing the high activity superoxide dismutase after 40 ℃ of microwave dryings or freeze drying.
Through measuring, wherein superoxide dismutase activity is 460,000 U/100g, and natural Vc content is 3750 mg/100g.
Embodiment 2
The selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit 100kg of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5mm after washing with flowing water; Get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use; Fruit juice is removed pomace and other impurity through preliminary the filtration, and filtrating is separated 6min through 30000 r/min high speed centrifugations and is got parting liquid; Parting liquid is concentrated into relative density 1.0 ~ 1.3 in 50 ℃ of vacuum; Described drying is the smart powder 5.58kg of emblic that concentrate is obtained containing the high activity superoxide dismutase after 40 ℃ of microwave dryings or freeze drying.
Through measuring, wherein superoxide dismutase activity is 480,000 U/100g, and natural Vc content is 3845 mg/100g.
Embodiment 3
The selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit 100kg of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5 mm after washing with flowing water; Get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use; Fruit juice is removed pomace and other impurity through preliminary the filtration, and filtrating is separated 10min through the 45000r/min high speed centrifugation and is got parting liquid; Parting liquid is concentrated into relative density 1.0 ~ 1.3 in 45 ℃ of vacuum; Described drying is smart powder 5.47 kg of emblic that concentrate obtained containing the high activity superoxide dismutase after 45 ℃ of microwave dryings or freeze drying.
Through measuring, wherein superoxide dismutase activity is 500,000 U/100g, and natural Vc content is 3957 mg/100g.
Embodiment 4
The selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit 100kg of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5mm after washing with flowing water; Get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use; Fruit juice is removed pomace and other impurity through preliminary the filtration, and filtrating is separated 7min through 35000 r/min high speed centrifugations and is got parting liquid; Parting liquid is concentrated into relative density 1.0 ~ 1.3 in 50 ℃ of vacuum; Described drying is smart powder 5.58 kg of emblic that concentrate obtained containing the high activity superoxide dismutase after 50 ℃ of microwave dryings or freeze drying.
Through measuring, wherein superoxide dismutase activity is 500,000 U/100g, and natural Vc content is 4000mg/100g.
Embodiment 5
The selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit 100kg of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5 mm after washing with flowing water; Get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use; Fruit juice is removed pomace and other impurity through preliminary the filtration, and filtrating is separated 8min through 40000 r/min high speed centrifugations and is got parting liquid; Parting liquid is concentrated into relative density 1.0 ~ 1.3 in 40 ℃ of vacuum; Described drying is smart powder 5.46 kg of emblic that concentrate obtained containing the high activity superoxide dismutase after 40 ℃ of microwave dryings or freeze drying.
Through measuring, wherein superoxide dismutase activity is 520,000 U/100g, and natural Vc content is 4023 mg/100g.
Claims (7)
1. smart powder of the emblic that contains the high activity superoxide dismutase, it is characterized in that: with the emblic fresh fruit is raw material, through broken, squeeze the juice, purifying, concentrate, the drying steps preparation, superoxide dismutase activity is 45 ~ 550,000 U/100g.
2. the smart powder of emblic that contains the high activity superoxide dismutase according to claim 1, it is characterized in that: Vc content is 2000 ~ 4500mg/100g in the smart powder of described emblic.
3. methods that prepare claim 1 or the smart powder of the 2 described emblics that contain the high activity superoxide dismutase is characterized in that comprising that raw material is handled, squeezed the juice, purifying, concentrated, drying steps, are specially:
A, raw material are handled: the selection nothing is rotted, nothing is gone mouldy, the emblic fresh fruit of the visible exogenous impurity of no naked eyes, is crushed to the granularity of 3 ~ 5 mm after washing with flowing water;
B, squeeze the juice: get broken emblic and squeeze the juice, the fruit juice of removing behind the pomace is for use;
C, purifying: fruit juice is removed pomace and other impurity through coarse filtration, filtrating through high speed centrifugation separate parting liquid;
D, concentrated: the parting liquid vacuum is concentrated into relative density 1.0 ~ 1.3;
E, drying: with the smart powder of emblic that obtains containing the high activity superoxide dismutase after the concentrate drying.
4. the smart powder, preparation method thereof of emblic that contains the high activity superoxide dismutase according to claim 3 is characterized in that: described C step high speed centrifugation rotating speed is 10000 ~ 45000 r/min.
5. the smart powder, preparation method thereof of emblic that contains the high activity superoxide dismutase according to claim 3 is characterized in that: described C step high speed centrifugation rotating speed is 30000 ~ 40000r/min.
6. the smart powder, preparation method thereof of emblic that contains the high activity superoxide dismutase according to claim 3, it is characterized in that: the vacuum thickening temperature is 40 ~ 50 ℃ in the described D step.
7. the smart powder, preparation method thereof of emblic that contains the high activity superoxide dismutase according to claim 3, it is characterized in that: the drying in the described E step is microwave drying or freeze drying, baking temperature is 40 ~ 50 ℃.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103445180A (en) * | 2013-09-17 | 2013-12-18 | 王喜军 | Application of physalis pubescens in preparing anti-oxidization health-care food |
| CN106387904A (en) * | 2016-09-30 | 2017-02-15 | 楚雄州百草岭药业发展有限公司 | Composition, preparation method of composition, preparation and use |
| CN106418537A (en) * | 2016-09-30 | 2017-02-22 | 楚雄州百草岭药业发展有限公司 | Composition, as well as preparation method, preparation and application thereof |
| CN113854446A (en) * | 2021-09-02 | 2021-12-31 | 广州市东鹏食品饮料有限公司 | Phyllanthus emblica juicing method |
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| CN1078620A (en) * | 1992-05-09 | 1993-11-24 | 昆明市轻工研究所 | emblic powder (Phyllanthus emblica powder) and processing method thereof |
| CN1121783A (en) * | 1995-05-31 | 1996-05-08 | 刘国柱 | Phyllanthus emblica fruit SOD health food additive formulation and preparing process thereof |
| CN1124598A (en) * | 1995-07-19 | 1996-06-19 | 昆明天成食品工业有限公司 | Clear Yunnan Chinese olive beverage |
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2012
- 2012-09-29 CN CN2012103714216A patent/CN102835664A/en active Pending
Patent Citations (3)
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| CN1078620A (en) * | 1992-05-09 | 1993-11-24 | 昆明市轻工研究所 | emblic powder (Phyllanthus emblica powder) and processing method thereof |
| CN1121783A (en) * | 1995-05-31 | 1996-05-08 | 刘国柱 | Phyllanthus emblica fruit SOD health food additive formulation and preparing process thereof |
| CN1124598A (en) * | 1995-07-19 | 1996-06-19 | 昆明天成食品工业有限公司 | Clear Yunnan Chinese olive beverage |
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| 《中国民族民间医药杂质》 20021231 侯开卫 "余甘子的化学成分及在民族民间传统医药中的应用" 第345-348页 1-7 , 第59期 * |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103445180A (en) * | 2013-09-17 | 2013-12-18 | 王喜军 | Application of physalis pubescens in preparing anti-oxidization health-care food |
| CN103445180B (en) * | 2013-09-17 | 2015-05-06 | 王喜军 | Application of physalis pubescens in preparing anti-oxidization health-care food |
| CN106387904A (en) * | 2016-09-30 | 2017-02-15 | 楚雄州百草岭药业发展有限公司 | Composition, preparation method of composition, preparation and use |
| CN106418537A (en) * | 2016-09-30 | 2017-02-22 | 楚雄州百草岭药业发展有限公司 | Composition, as well as preparation method, preparation and application thereof |
| CN113854446A (en) * | 2021-09-02 | 2021-12-31 | 广州市东鹏食品饮料有限公司 | Phyllanthus emblica juicing method |
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Application publication date: 20121226 |