CN107937201A - A kind of preparation method of wild grape wine - Google Patents

A kind of preparation method of wild grape wine Download PDF

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Publication number
CN107937201A
CN107937201A CN201810056807.5A CN201810056807A CN107937201A CN 107937201 A CN107937201 A CN 107937201A CN 201810056807 A CN201810056807 A CN 201810056807A CN 107937201 A CN107937201 A CN 107937201A
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grape
days
preparation
grape wine
mixed liquor
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胡江宇
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G1/00Preparation of wine or sparkling wine
    • C12G1/02Preparation of must from grapes; Must treatment and fermentation
    • C12G1/0203Preparation of must from grapes; Must treatment and fermentation by microbiological or enzymatic treatment
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/59Menispermaceae (Moonseed family), e.g. hyperbaena or coralbead
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/75Rutaceae (Rue family)
    • A61K36/752Citrus, e.g. lime, orange or lemon
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/87Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine

Abstract

It is more particularly to a kind of to reduce the wild grape wine preparation method of this product acidity by adding Caulis Sinomenii extract the invention discloses a kind of preparation method of wild grape wine, include selection, broken, yeast fermentation, lactic fermentation and the ageing of grape.Contain substantial amounts of small molecule alkaloid in caulis sinomenii, these alkaloids are soluble in alcohol, dissolve each other after the acid combination in grape, then with ethanol, acidic materials is obtained polymerization protection in alcohol, reduce the acidity of whole system;Another feature of the present invention is to be cultivated by elder generation in the environment of dried orange peel, Grape Skin for the yeast mixed liquor added; yeast is obtained after being stimulated afterwards with benzoic acid; with very strong antiacid; therefore can obtain that a kind of preparation method is simply controllable by the present invention, suitable for the wild grape wine preparation method of industrialization and scale.

Description

A kind of preparation method of wild grape wine
Technical field
The present invention relates to a kind of preparation method of wild grape wine, belong to field of food.
Background technology
V. amurensis is also referred to as northeast V. amurensis(Vitis amurensis Rupr.), it is that Vitaceae Vitis fallen leaves liana is planted Thing, belongs to the more characteristic germ plasm resource of East Asia population together with Vitis davidii Foex, downy grape etc., originates in Northeast China, North China and Korea, Russia sieve This Far East Area, is distributed mainly on the ground such as China Heilungkiang, Jilin, Liaoning, the Inner Mongol.V. amurensis is most cold-resistant in Vitis One kind, branches and tendrils are resistant to -40 DEG C of low temperature, and root system is resistant to -15 DEG C of low temperature to the main Portugal such as white rot, anthrachose of grape, anthracnose Grape disease shows certain premunition, is the precious resources of Cold-resistant Grape, breeding for disease resistance.
V. amurensis is sweet in flavor sour, puckery flat;There is clearing heat and detoxicating, dispelling wind and eliminating dampness etc.;Also promoting the circulation of qi, anti-inflammatory, diuresis, hemostasis Deng effect.It is among the people to be used to its water decoction treat chronic hepatitis, ephritis, chornic arthritis, traumatic injury, difficulty and pain in micturition, stomach energy Vomiting, sore, traumatic hemorrhage etc., curative effect is preferable.According to《Compendium of Materia Medica》Recording V. amurensis can quench the thirst, please color QI invigorating;With clearing damp Numbness, strengthening the bones and muscles, the strong will of QI invigorating times power, make us fertile key, resistance to flesh bears the functions such as chill.Food long, not old macrobiosis of making light of one's life by commiting suicide, can cook wine.According to Foreign literature report is Egyptian just to be made wine with it a long time ago, and uses it as disinfectant and anatrophic.
There is the report of exploitation wild grape wine very early at home, although V. amurensis has growth or the kind of large area at home Plant, but have no large-scale production or market sale always, preparation process is there are technical difficulty, mainly due to mountain The organic acid contained in grape is far above general grape, in obtained grape wine wine flavour largely by taste masks, If excessive acid fermentation can cause nutritional ingredient to reduce again.
The content of the invention
To solve the above-mentioned problems of the prior art, the present invention provides a kind of preparation method of wild grape wine, the present invention Using simple conventional preparation techniques, it can obtain that a kind of acidity is low, stable quality, the wild grape wine of sweet-smelling.
In order to realize foregoing invention, embodiment is as follows:
A kind of wild grape wine, its preparation method are as follows:
(One)Fresh V. amurensis is chosen, crushes, takes part Grape Skin spare, remaining grape and skin are put into closed container, are put Put 5-15 days, temperature is 5-15 DEG C;Caulis Sinomenii extract is added, is stirred and evenly mixed, when constant temperature 2 is small at 40-60 DEG C.
Preferably, the V. amurensis is the ripe grape picked back, and standing time is no more than 5 days.
Preferably, described take out that part Grape Skin weight is whole fresh grape quality 0.05-0.15 times.
Preferably, the Caulis Sinomenii extract addition be whole V. amurensis quality 0.5-1.5%, the blue or green wind Boisiana extract preparation method is as follows:
(1)Take caulis sinomenii appropriate, add equivalent to 2-4 times of saturated common salt aqueous solution measured of caulis sinomenii, be heated to reflux 2 it is small when, mistake Filter, it is 1.15-1.25 to be concentrated into relative density(50-60 DEG C of detection).
The caulis sinomenii is the rattan of menispermaceous plants sinomenium acutum or hair sinomenium acutum etc., the entitled Caulis of Latin Sinomenii。
(2)Ethanol solution is added in filtrate, the concentration of alcohol of whole solution is reached 60-80%, when static 12-24 is small, mistake Filter, concentration filtrate to relative density is 1.15-1.25(50-60 DEG C of detection).
(Two)Above-mentioned mixed liquor is cooled down to 6-10 DEG C, adds saccharomycete mixed liquor, 20-30 DEG C ferments 4-8 days.
Preferably, the yeast mixed liquor addition is the 0.05-0.1% of whole mixed liquor quality.
Further, the preparation method of the yeast mixed liquor is as follows:
Appropriate dried orange peel is taken, water and the above-mentioned Grape Skin added equivalent to 2 times of amounts of Quality of Pericarpium is smashed to pieces, is uniformly mixed, adds phase When in 0.1-0.5 times of active dry yeast of Quality of Pericarpium, 20 DEG C keep the temperature 1-3 days, filtering, addition is dry equivalent to activity in filtrate The benzoic acid of the 0.01-0.05% of yeast quality, continues 20 DEG C and keeps the temperature 1-2 days after mixing, you can.
Further, the active dry yeast meets the requirement in national standard QB 2074-1995.
(Three)Lactic fermentation:Lactobacillus suspension is added, is fermented 6-12 days, it is 15-25 DEG C to keep temperature, filtering.
Preferably, the lactobacillus suspension addition is the 0.001-0.01% of whole zymotic fluid.
(Four)Ageing:Filtrate is closed to place 60-120 days, keeps 10-15 DEG C of environment temperature, filtering.
The method have the characteristics that:
1. the present invention obtains the alkaline matter in caulis sinomenii, and its alkaline matter is mainly small molecule by being separated to caulis sinomenii Alkaloid, easily through cell membrane, enters grapes tissue, is combined with acidic materials therein, and permeate after being mixed with must Out, the alcohol-soluble of the small molecule alkali in alcohol fermentation processes, caulis sinomenii is good, and after dissolving each other with ethanol, acidic materials are polymerize In ethanol, decline the acidity of whole system, increase this product alcohol taste, while avoid acidic materials influence fermentation process, into After entering in vivo, in the environment of hydrochloric acid in gastric juice, the acid of polymerization can be separated again, play original effect of acidic materials.
2. saccharomycete mixed liquor of the present invention carries out initial fermentation using active dry yeast in dried orange peel and Grape Skin, due to old Contain a large amount of alcohol components in skin, resistance of the saccharomycete to alcohol can be stimulated, and then improve its resistance to alcohol, deposited in Grape Skin Under effect, due to the substantial amounts of saccharomycete of Grape Skin itself also implication, after being mixed with above-mentioned saccharomycete, by adding benzoic acid, Electrophilic reaction easily occurs for its phenyl ring, can change the distribution of charges in saccharomycete, stimulates its variation.Since benzoic acid has weak acid Property, whole environment is claimed acidity, therefore the antiacid strong and saccharomycete suitable for being grown in grape environment can be obtained, make alcohol fermentation It is more complete.
The beneficial effects of the present invention are:
1. the present invention provides a kind of preparation method of V. amurensis, using simple preparation process, it is low to obtain a kind of acidity, and quality Stable wild grape wine.
2. preparation process of the present invention is simple, cost is low, and is suitable for industrialization and large-scale production, to the further of V. amurensis It is very big using having the function that.
Embodiment
In order to be better understood from main points of the present invention, now foregoing invention is described in further detail by specific embodiment, but under Embodiment is stated it is not intended that limiting the further of the present invention.
Embodiment 1
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.1 times of amount;Remaining grape and skin are put into closed container, are placed 10 days, and temperature is 10 DEG C;Add Caulis Sinomenii extract, Caulis Sinomenii extract addition is the 1.0% of whole V. amurensis quality, is stirred and evenly mixed, when constant temperature 2 is small at 50 DEG C.
The Caulis Sinomenii extract preparation method is as follows:
(1)Take caulis sinomenii appropriate, add the saturated common salt aqueous solutions equivalent to 3 times of caulis sinomenii amount, be heated to reflux 2 it is small when, filtering, Relative density is concentrated into as 1.19(50-60 DEG C of detection);
(2)Ethanol solution is added in filtrate, the concentration of alcohol of whole solution is reached 70%, it is static 20 it is small when, filtering, concentration filter Liquid to relative density is 1.19(50-60 DEG C of detection).
2. the above-mentioned mixed liquor of cooling adds saccharomycete mixed liquor to 8 DEG C, ferment 6 days.Yeast mixed liquor addition is whole The 0.08% of mixed liquor quality.The preparation method of the yeast mixed liquor is as follows:
Appropriate dried orange peel is taken, is smashed to pieces, the water equivalent to 2 times of amounts of Quality of Pericarpium and above-mentioned Grape Skin is added, is uniformly mixed, adds phase When in 0.3 times of active dry yeast of Quality of Pericarpium, 20 DEG C keep the temperature 2 days, filtering, addition is equivalent to active dry yeast matter in filtrate 0.03% benzoic acid of amount, continues 20 DEG C and keeps the temperature 1 day after mixing, you can.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.005% of whole zymotic fluid, ferments 9 days, protects Temperature is held as 20 DEG C, filtering.
4. ageing:Filtrate is closed to place 90 days, keeps 10-15 DEG C of environment temperature, filtering.
Embodiment 2
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.05 times of amount;Remaining grape and skin are put into closed container, are placed 5 days, and temperature is 5 DEG C;Caulis Sinomenii extract is added, it is blue or green Wind boisiana extract addition is the 0.5% of whole V. amurensis quality, is stirred and evenly mixed, when constant temperature 2 is small at 40 DEG C.
The Caulis Sinomenii extract preparation method is as follows:
(1)Take caulis sinomenii appropriate, add the saturated common salt aqueous solutions equivalent to 3.5 times of caulis sinomenii amount, be heated to reflux 2 it is small when, mistake Filter, is concentrated into relative density as 1.24(50-60 DEG C of detection);
(2)Ethanol solution is added in filtrate, the concentration of alcohol of whole solution is reached 78%, it is static 14 it is small when, filtering, concentration filter Liquid to relative density is 1.24(50-60 DEG C of detection).
2. the above-mentioned mixed liquor of cooling adds saccharomycete mixed liquor to 6 DEG C, ferment 4 days.Yeast mixed liquor addition is whole The 0.05% of mixed liquor quality.The preparation method of the yeast mixed liquor is as follows:
Appropriate dried orange peel is taken, is smashed to pieces, the water equivalent to 2 times of amounts of Quality of Pericarpium and above-mentioned Grape Skin is added, is uniformly mixed, adds phase When in 0.4 times of active dry yeast of Quality of Pericarpium, 20 DEG C keep the temperature 3 days, filtering, addition is equivalent to active dry yeast matter in filtrate 0.025% benzoic acid of amount, continues 20 DEG C and keeps the temperature 2 days after mixing, you can.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.001% of whole zymotic fluid, ferments 6 days, protects Temperature is held as 15 DEG C, filtering.
4. ageing:Filtrate is closed to place 60 days, keeps 10-15 DEG C of environment temperature, filtering.
Embodiment 3
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.15 times of amount;Remaining grape and skin are put into closed container, are placed 15 days, and temperature is 15 DEG C;Add Caulis Sinomenii extract, Caulis Sinomenii extract addition is the 1.5% of whole V. amurensis quality, is stirred and evenly mixed, when constant temperature 2 is small at 60 DEG C.The blue or green wind Boisiana extract preparation method is as follows:
(1)Take caulis sinomenii appropriate, add equivalent to 2-4 times of saturated common salt aqueous solution measured of caulis sinomenii, be heated to reflux 2 it is small when, mistake Filter, is concentrated into relative density as 1.23(50-60 DEG C of detection);
(2)Ethanol solution is added in filtrate, the concentration of alcohol of whole solution is reached 65%, it is static 13 it is small when, filtering, concentration filter Liquid to relative density is 1.22(50-60 DEG C of detection).
2. the above-mentioned mixed liquor of cooling adds saccharomycete mixed liquor to 10 DEG C, ferment 8 days.Yeast mixed liquor addition is whole The 0.1% of a mixed liquor quality.The preparation method of the yeast mixed liquor is as follows:
Appropriate dried orange peel is taken, is smashed to pieces, the water equivalent to 2 times of amounts of Quality of Pericarpium and above-mentioned Grape Skin is added, is uniformly mixed, adds phase When in 0.4 times of active dry yeast of Quality of Pericarpium, 20 DEG C keep the temperature 1 day, filtering, addition is equivalent to active dry yeast matter in filtrate 0.02% benzoic acid of amount, continues 20 DEG C and keeps the temperature 2 days after mixing, you can.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.01% of whole zymotic fluid, ferments 12 days, protects Temperature is held as 25 DEG C, filtering.
4. ageing:Filtrate is closed to place 120 days, keeps 10-15 DEG C of environment temperature, filtering.
Comparative example 1
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.06 times of amount;Remaining grape and skin are put into closed container, are placed 7 days, and temperature is 6 DEG C.
2. the above-mentioned mixed liquor of cooling adds saccharomycete to 8 DEG C, ferment 7 days.Saccharomycete addition is whole mixed liquor quality 0.08%.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.007% of whole zymotic fluid, ferments 9 days, protects Temperature is held as 20 DEG C, filtering.
4. ageing:Filtrate is closed to place 100 days, keeps 10-15 DEG C of environment temperature, filtering.
Comparative example 2
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.1 times of amount;Remaining grape and skin are put into closed container, are placed 10 days, and temperature is 10 DEG C.
2. the above-mentioned mixed liquor of cooling adds saccharomycete to 8 DEG C, ferment 6 days.Saccharomycete addition is whole mixed liquor quality 0.08%.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.005% of whole zymotic fluid, ferments 9 days, protects Temperature is held as 22 DEG C, filtering.
4. ageing:Filtrate is closed to place 75 days, keeps 10-15 DEG C of environment temperature, filtering.
Comparative example 3
1. choosing fresh V. amurensis, crush, take part Grape Skin spare, take out part Grape Skin weight as whole new fresh grape matter 0.13 times of amount;Remaining grape and skin are put into closed container, are placed 10 days, and temperature is 12 DEG C.
2. the above-mentioned mixed liquor of cooling adds saccharomycete to 8 DEG C, ferment 6 days.Yeast juice addition is whole mixed liquor quality 0.09%.
3. lactic fermentation:Lactobacillus suspension is added, lactobacillus suspension addition is the 0.006% of whole zymotic fluid, ferments 9 days, protects Temperature is held as 20 DEG C, filtering.
4. ageing:Filtrate is closed to place 90 days, keeps 10-15 DEG C of environment temperature, filtering.
Wild grape wine obtained by embodiment 1-3 is detected, according to standard GB/T/T 15037-2006, carries out complete detection, respectively Item index meets the requirements
The taste of embodiment 1 to embodiment 3 and comparative example 1-3 is judged
20 normal adults are chosen, product are carried out to above-described embodiment 1 to 3 and the gained of comparative example 1 to 3 grape wine successively Taste, with reference to standard GB/T/T 15037-2006, evaluation marking is carried out to its sense organ, mouthfeel is better, records the average mark of ten people Number, it is as a result as follows:
Embodiment 1 2 3 P- 1 P- 2 P- 3
Score 96.2 95.8 96.7 68.4 71.2 66.8
* " p- 1 " refers to 1 gained grape wine of comparative example, other and so on
* sensory judgments' standard is as follows(Source GB/T 15037-2006):
It was found from above-mentioned experimental result, the wild grape wine of present invention gained has significant advantage in terms of sense organ.
The acidity of embodiment 1 to embodiment 3 and comparative example 1-3 is detected, colleague investigates it in placement process The change of middle acidity and mouthfeel change
Wild grape wine obtained by Example 1-3 and comparative example 1-3, using standard caustic soda solution, with reference to GB/T Method in 15037-2006, detects the total acid angle value in gained grape wine, as a result as follows:
Embodiment 1 2 3 P- 1 P- 2 P- 3
Acidity(g/L) 3.12 3.18 3.24 9.15 7.63 10.41
Wild grape wine obtained by Example 1-3 and comparative example 1-3, is poured into the graduated cylinder of 100ml, at 40 DEG C, humidity 75% Placed under part, 0/3/6 month respectively, choose ten professional mouthfeel criticism personages, to above-mentioned Taste of Wine, while observed outer See, it is as a result as follows:
Embodiment 1 2 3 P- 1 P- 2 P- 3
0 month The transparent clarification of solution, it is pure Positive bouquent The transparent clarification of solution, pure Portugal Grape wine flavour The transparent clarification of solution, pure Portugal Grape wine flavour The transparent clarification of solution, There is acerbity The transparent clarification of solution, There is acerbity The transparent clarification of solution, There is acerbity
March The transparent clarification of solution, it is pure Positive bouquent The transparent clarification of solution, pure Portugal Grape wine flavour The transparent clarification of solution, pure Portugal Grape wine flavour Solution is muddy, sour and astringent Taste aggravates Solution is muddy, sour and astringent Taste aggravates Solution is muddy, sour and astringent Taste aggravates
June The transparent clarification of solution, it is pure Positive bouquent The transparent clarification of solution, pure Portugal Grape wine flavour The transparent clarification of solution, pure Portugal Grape wine flavour Solution has precipitation Solution has precipitation Solution has precipitation
From above-mentioned analysis of experimental results, the wild grape wine obtained by the present invention is respectively provided with aobvious in terms of acidity is reduced and in terms of mouthfeel Write effect.

Claims (7)

1. a kind of preparation method of wild grape wine, it is characterised in that including following steps:
(1)Fresh V. amurensis is chosen, crushes, takes part Grape Skin spare, remaining grape and skin are put into closed container, are placed 5-15 days, temperature was 5-15 DEG C;Caulis Sinomenii extract is added, is stirred and evenly mixed, when constant temperature 2 is small at 40-60 DEG C;
(2)Above-mentioned mixed liquor is cooled down to 6-10 DEG C, adds saccharomycete mixed liquor, 20-30 DEG C ferments 4-8 days;
(3)Lactic fermentation:Lactobacillus suspension is added, is fermented 6-12 days, it is 15-25 DEG C to keep temperature, filtering;
(4)Ageing:Filtrate is closed to place 60-120 days, keeps 10-15 DEG C of environment temperature, filtering.
2. wild grape wine preparation method according to claim 1, it is characterised in that:The V. amurensis be pick back into Ripe grape, standing time are no more than 5 days.
3. wild grape wine preparation method according to claim 2, it is characterised in that:The taking-up part Grape Skin weight For 0.05-0.15 times of whole fresh grape quality.
4. wild grape wine preparation method according to claim 3, it is characterised in that:The Caulis Sinomenii extract addition For the 0.5-1.5% of whole V. amurensis quality.
5. wild grape wine preparation method according to claim 4, it is characterised in that:The Caulis Sinomenii extract preparation side Method is as follows:
(1)Take caulis sinomenii appropriate, add equivalent to 2-4 times of saturated common salt aqueous solution measured of caulis sinomenii, be heated to reflux 2 it is small when, mistake Filter, it is 1.15-1.25 to be concentrated into relative density(50-60 DEG C of detection);
(2)Ethanol solution is added in filtrate, the concentration of alcohol of whole solution is reached 60-80%, when static 12-24 is small, filtering, It is 1.15-1.25 to concentrate filtrate to relative density(50-60 DEG C of detection).
6. wild grape wine preparation method according to claim 5, it is characterised in that:The yeast mixed liquor addition is The 0.05-0.1% of whole mixed liquor quality.
7. wild grape wine preparation method according to claim 6, it is characterised in that:The preparation side of the yeast mixed liquor Method is as follows:
Appropriate dried orange peel is taken, is smashed to pieces, the water equivalent to 2 times of amounts of Quality of Pericarpium and above-mentioned Grape Skin is added, is uniformly mixed, adds phase When in 0.1-0.5 times of active dry yeast of Quality of Pericarpium, 20 DEG C keep the temperature 1-3 days, filtering, addition is dry equivalent to activity in filtrate The benzoic acid of the 0.01-0.05% of yeast quality, continues 20 DEG C and keeps the temperature 1-2 days after mixing, you can.
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CN113528282A (en) * 2021-08-10 2021-10-22 赵为兴 Formula and preparation method of red butter liqueur

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