CN104738446A - Preparing methods of red raspberry seed extract product and red raspberry polymerization fruit juice and applications thereof - Google Patents
Preparing methods of red raspberry seed extract product and red raspberry polymerization fruit juice and applications thereof Download PDFInfo
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- CN104738446A CN104738446A CN201310737325.3A CN201310737325A CN104738446A CN 104738446 A CN104738446 A CN 104738446A CN 201310737325 A CN201310737325 A CN 201310737325A CN 104738446 A CN104738446 A CN 104738446A
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- raspberry
- seed extract
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Abstract
The invention relates to preparing methods of a red raspberry seed extract product and red raspberry polymerization fruit juice, and belongs to the field of fruit juice type drinks. Red raspberry fruits and red raspberry seeds are adopted as main raw materials. The red raspberry polymerization fruit juice with a special flavor is obtained by juicing the red raspberry fruits to obtain red raspberry fruit juice; extracting the red raspberry seeds by an edible ethanol solvent to obtain the red raspberry seed extract product; purifying the red raspberry seed extract product with AB-8 macroporous adsorption resin; and adding the purified red raspberry seed extract product into the red raspberry fruit juice. The obtained polymerization fruit juice has a light red color, and drinking value and nutrition value of the red raspberry fruit juice are improved. The methods are simple in operation. The obtained products have high health care functions and a wide market prospect.
Description
Technical field
The present invention relates to the preparation method of a Plant Extracts and plant juices beverage, particularly the preparation method of a kind of raspberry seed extract and raspberry polymerization fruit juice.
Background technology
Raspberry is divided into the red certain kind of berries, blackberry, blueberry, the yellow certain kind of berries, it is the economic fruit tree plant of berries of rose family rubus, the Origin of cultivation of this Plants is in Europe, and form industry gradually, there is the history of centuries, current countries in the world start to cultivate raspberry crop all gradually, and to late 1990s, world's raspberry yield has reached more than 35640 ton.Fruit of raspberry is aggregate fruit, is erythrocarpus time ripe.Containing abundant sugar, organic acid, vitamin C, vitamin E, citrin, FA and hematopoiesis compound in raspberry berry, become the medical foods being conducive to diseases prevention, curing the disease, and containing tanning acid (content is up to 1.5-2.0mg/100g fresh fruit) and in a large number natural plants SOD (superoxide dismutase), raspberry ketone, salicylic acids (natural aspirin) etc. in a large number.Wherein raspberry contains abundant Flavonoid substances, flavone compound has multiple beneficial in the physiologically active of health, comprise antioxidation activity, antitumor activity, to the effect of inflammation and immunocyte, regulates fragility and the permeability of capillary, protect cardiovascular and permeability, protection cardiovascular system, on the impact of enzyme system in body, antibiosis and antiviral functions etc.; And raspberry has special curative effect to colon cancer, cervical carcinoma, breast cancer and cancer of pancreas, having skin maintenance, anticancer, anti-ageing, step-down, the effect such as lipopenicillinase and prevention anaemia, enterogastritis, cardiovascular and cerebrovascular disease, is a kind of natural health care with important biomolecule function and nutritive value.
In the industrialization application process of raspberry, the thin succulence of sarcotesta due to raspberry, easily touch brokenly pericarp during harvesting to occur to go rotten, normal temperature is preserved and is generally difficult to reach 24 hours, not storage tolerance and transport, therefore the area of establishing in large scale raspberry, set up processing factory more, ensure that the fresh fruit plucked the same day can process process, so annual harvesting still stays a large amount of raspberry seeds to be underutilized after producing, reduce the enthusiasm of farmers' income and peasant planting raspberry, also waste natural resources and be included in the nutritional labeling in raspberry seed simultaneously.Therefore, carry out further deeply research and development to the fruit juice product of raspberry, to environmental protect, the added value improving fruit juice product is significant.
Patent of invention CN03134577.8 adopts and once adds RC212 active dry yeast list bacterium zymotechnique, its acid adjustment simultaneously utilizes D380 ion-exchange resin acid reduction method after fermentation, and result fully can not keep distinctive nutritional labeling and biological function in red raspberry fruits.Patent of invention CN102018252A discloses a kind of red raspberry beverage, mass fraction in product shared by each raw material is: raspberry pulp is 15% ~ 45%, table sugar is 5% ~ 10%, food acids is 0.05% ~ 0.2%, gellan gum is 0.01% ~ 0.02%, pectin is 0.02% ~ 0.04%, and essence is the water of 0.1% ~ 0.5% and surplus; The product that this invention is is main material with raspberry pulp, farthest remain red raspberry fruits pulp fraction, in product, dietary fiber content significantly improves, and its local flavor is more mellow.Patent of invention CN101375705 discloses a kind of raspberry health-care beverage and preparation method thereof.Concrete count 1.00-2.00 part by weight raspberry, the white granulated sugar of 0.25-0.5 part, the honey of 0.20-0.25 part, the date of 0.10-0.20 part, the matrimony vine of 0.10-0.20 part and 1.20-1.50 part water.The present invention obtains drink sour and sweet palatability, aromatic flavour, unique flavor.Its preparation technology is simple, easy to operate, efficiently convenient.And drink of the present invention contains abundant natural polyphenol class material and SOD enzyme isoreactivity composition.
Above prior art is all unresolved to be made full use of raspberry seed and increases the problem of natural nutrient component in raspberry fruit juice.
Summary of the invention
The present invention is directed to the defect existed in prior art, the invention provides a kind of method preparing raspberry seed extract and raspberry polymerization fruit juice, described raspberry polymerization fruit juice, effectively make use of the natural nutrient component of raspberry seed, improve consumption value and the nutritive value of raspberry polymerization fruit juice, and preparation method is simple, the product obtained has very strong health care, wide market.
The invention provides a kind of preparation method of raspberry seed extract, comprise the following steps:
1) raspberry seed is ground into powder, by the alcohol solution dipping 12-24h of the raspberry seed 65-75% of pulverizing;
2) after step 1) process, then carry out refluxing extraction, by extracting liquid filtering, adopt rotary evaporator to evaporate the extract after filtration, namely recycling design obtains described raspberry seed extract.
Preferably, the quality of the raspberry seed pulverized in described step 1) and the interpolation volume of ethanol are 1:10.
Preferably, described step 2) in reflux temperature be 75-85 DEG C, reflux extracting time is 3h ~ 5h.
Preferably, also comprise described step 2) in preparation-obtained raspberry seed extract carry out purifying.
Preferably, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity not higher than 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the raspberry seed extract of 75% ~ 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying at least 2h, namely obtain raspberry seed extract.
Preferably, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, clean impurity with distilled water by resin column, till rinse water is not muddy, finally elute with the raspberry seed extract of 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying 2h, namely obtain raspberry seed extract.
The preparation method that the invention provides a kind of raspberry seed polymerization fruit juice is that the raspberry seed extract described method prepared joins in raspberry fruit juice.
Preferably, the V that raspberry polymerization fruit juice adds 0.1% is also included in
c.
The invention provides a kind of food comprising raspberry seed extract prepared by described method.
Preferably, described food is beverage, is more preferably raspberry fruit juice.
Great advantage of the present invention is exactly in actual production, effectively be extracted the nutritional labeling in raspberry seed, take full advantage of the natural nutrient component of raspberry seed, and be aggregated in raspberry juice, substantially increase consumption value and the nutritive value of the raspberry polymerization fruit juice of preparation.
Detailed description of the invention
" scope " disclosed herein is with the form of lower limit and the upper limit.One or more lower limit can be respectively, and one or more upper limit.Given range is limited by a selected lower limit and a upper limit.Selected lower limit and the upper limit define the border of special scope.All scopes that can carry out by this way limiting comprise and may be combined with, and namely any lower limit can be combined to form a scope with any upper limit.Such as, list the scope of 2000-6000 and 50-200 for special parameter, be interpreted as that the scope of 2000-5000 and 50-210 also expects.In addition, if the minimum zone value listed 1 and 2, and if list maximum magnitude value 3,4 and 5, then the scope below can all expect: 1-3,1-4,1-5,2-3,2-4 and 2-5.In the present invention, unless otherwise indicated, new technical scheme can be mutually combined to form between the content range of each component of composition and its preferable range.In the present invention, unless otherwise indicated, all " part " and percentage (%) all refer to percetage by weight.In the present invention, unless otherwise indicated, in all compositions, the percentage sum of each component is 100%.In the present invention, unless otherwise indicated, the breviary of any real combinings that number range " a-b " represents between a to b represents, wherein a and b is real number.Such as number range " 0-5 " represents the whole real numbers all listed between " 0-5 " herein, and the breviary of " 0-5 " just these combinations of values represents.If do not particularly not pointed out, the benchmark of percentage of the present invention (comprising percetage by weight) is all the gross weight of described composition.In the present invention, if do not illustrated especially, all embodiments mentioned in this article and preferred embodiment can be combined to form new technical scheme mutually.In the present invention, if do not illustrated especially, all technical characteristics mentioned in this article and preferred feature can be combined to form new technical scheme mutually.In the present invention, if do not illustrated especially, mentioned in this article sequentially can to carry out in steps, also can carry out at random, but preferably order is carried out.Such as, described method comprises step (a) and (b), represents that described method can comprise the step (a) and (b) of sequentially carrying out, also can comprise the step (b) and (a) of sequentially carrying out.Such as, describedly mention described method and also can comprise step (c), represent that step (c) random order can join described method, such as, described method can comprise step (a) and (b) and (c), also step (a), (c) and (b) be can comprise, step (c), (a) and (b) etc. also can be comprised.
In the present invention, if do not illustrated especially, " comprising " mentioned in this article represents open, also can be closed.Such as, described " comprising " can represent other elements that can also comprise and not list, and also can only comprise the element listed.As used herein, include " containing ", " having " or " comprising " " comprising ", " primarily of ... form ", " substantially by ... form " and " by ... form "; " primarily of ... form ", " substantially by ... form " and " by ... formation " belong to the subordinate concept of " containing ", " having " or " comprising ".
The feature that the feature can mentioned the present invention or embodiment are mentioned combines.All features disclosed in the present specification can with any composition forms and use, each feature disclosed in description, anyly can provide identical, alternative characteristics that is impartial or similar object replaces.Therefore apart from special instruction, the feature disclosed is only general example that is impartial or similar features.As no specific instructions, various raw material of the present invention all can be obtained by commercially available; Or prepare according to the conventional method of this area.Unless otherwise defined or described herein, all specialties used herein and scientific words and those skilled in the art the meaning be familiar with identical.In addition any method similar or impartial to described content and material all can be applicable in the inventive method.
The invention provides a kind of preparation method of raspberry seed extract, comprise the following steps:
1) raspberry seed is ground into powder, by the alcohol solution dipping 12-24h of the raspberry seed 65-75% of pulverizing;
2) after step 1) process, then carry out refluxing extraction, by extracting liquid filtering, adopt rotary evaporator to evaporate the extract after filtration, namely recycling design obtains described raspberry seed extract.
In a preferred embodiment, the quality of the raspberry seed pulverized in described step 1) and the interpolation volume of ethanol are 1:10.
In a preferred embodiment, described step 2) in reflux temperature be 75-85 DEG C, reflux extracting time is 3h ~ 5h.
In a preferred embodiment, also comprise described step 2) in preparation-obtained raspberry seed extract carry out purifying.
In a preferred embodiment, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity not higher than 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the raspberry seed extract of 75% ~ 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying at least 2h, namely obtain raspberry seed extract.
In a preferred embodiment, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the raspberry seed extract of 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying 2h, namely obtain raspberry seed extract.
The invention provides a kind of preparation method of raspberry seed extract, said method comprising the steps of:
A) select without the raspberry fresh fruit of worm without corruption, squeeze, by the fruit juice sterilization treatment obtained; Fruit juice after sterilizing is cooled to less than 40 degree;
B) fruit juice cooled in step a) is filtered;
C) pomace squeezed in step a) is blunged evenly, seed, skin, slag are separated, dry after being separated the raspberry seed water cleaning obtained;
D) powder is ground into the raspberry seed obtained after step c) process;
E) the raspberry seed powder smashed step d) obtained, in 1:10(m/V) the ratio ethanolic solution that adds 70% invades bubble 12h, then after refluxing extraction 3h, extract filtered through filter under the condition of 80 DEG C;
F) extract after the filtration obtained in step e) is adopted rotary evaporator, evaporate, recycling design, obtain raspberry seed extract;
G) solution of the thick extraction obtained in step f) is passed through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, clean impurity with distilled water by resin column, till rinse water is not muddy, finally elute with the flavonoid substance of 95% ethanol by absorption, collect eluent; Rotary evaporation, recycling design, less than 70 DEG C vacuum drying 2h, obtain the raspberry seed extract of purifying.
The invention provides the preparation method of a kind of raspberry polymerization fruit juice, will join according to the raspberry seed extract obtained in described method in raspberry fruit juice prepared by described method.
In a preferred embodiment, the V adding 0.1% is also comprised in fruit juice after polymerisation
c.
The invention provides a kind of food comprising raspberry seed extract prepared by described method.
In a preferred embodiment, described food is beverage, is more preferably raspberry fruit juice.
Describe the present invention in detail below in conjunction with embodiment, but scope of the present invention is not limited thereto.
Embodiment 1:
The preparation method of raspberry seed extract:
1. with beating crusher, raspberry seed is broken into pulverulence;
2. in extractor, by the raspberry seed smashed with 70% ethanolic solution invade bubble 12h after (by 1:10(g:ml) add extractant), under the condition of 80 DEG C after refluxing extraction 3h, extract is filtered through filter;
3., with rotary evaporator, evaporated by the extract after filtering, namely recycling design obtains raspberry seed and slightly carries mixed liquor;
4. the purifying of raspberry seed extract: raspberry seed is slightly carried mixed liquor and pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the raspberry seed extract of 95% ethanol by absorption, collect eluent.Rotary evaporation, recycling design, less than 70 DEG C vacuum drying 2h, the dry thing of gained is raspberry seed extract.
Embodiment 2:
The preparation method of raspberry seed extract:
1. with beating crusher, raspberry seed is broken into pulverulence;
2. in extractor, by the raspberry seed smashed with 65% ethanolic solution invade bubble 24h after (by 1:10(g:ml) add extractant), under the condition of 85 DEG C after refluxing extraction 3h, extract is filtered through filter;
3., with rotary evaporator, evaporated by the extract after filtering, namely recycling design obtains raspberry seed and slightly carries mixed liquor;
4. raspberry seed extract: raspberry seed is slightly carried mixed liquor and pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the flavonoid substance of 95% ethanol by absorption, collect eluent.Rotary evaporation, recycling design, less than 70 DEG C vacuum drying 2h, the dry thing of gained is raspberry seed extract.
Embodiment 3:
The preparation method of raspberry seed extract:
1. with beating crusher, raspberry seed is broken into pulverulence;
2. in extractor, by the raspberry seed smashed with 75% ethanolic solution invade bubble 12h after (by 1:10(g:ml) add extractant), under the condition of 75 DEG C after refluxing extraction 5h, extract is filtered through filter;
3., with rotary evaporator, evaporated by the extract after filtering, namely recycling design obtains raspberry seed and slightly carries mixed liquor;
4. the purifying of raspberry seed extract: raspberry seed is slightly carried mixed liquor and pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, impurity is cleaned by resin column with distilled water, till rinse water is not muddy, finally elute with the flavonoid substance of 95% ethanol by absorption, collect eluent.Rotary evaporation, recycling design, less than 70 DEG C vacuum drying 2h, the dry thing of gained is raspberry seed extract.
Embodiment 4:
The preparation method of raspberry fruit juice:
Select without worm without rot raspberry fresh fruit, raspberry pulp is squeezed, obtains red raspberry fruit juice raw material liquid, and sterilization treatment is carried out to red raspberry fruit juice raw material liquid, the red raspberry fruit juice raw material liquid after sterilizing is cooled to less than 40 degree; Then by cooled red raspberry fruit juice raw material liquid, filter with diatomite filter, raspberry fruit juice can be obtained.
Embodiment 5:
The preparation method of raspberry polymerization fruit juice:
1. raspberry seed extract any embodiment in embodiment 1 ~ 3 prepared, be added in the raspberry fruit juice of preparation in embodiment 4, then stir, mixing time is 0.5h-12h, ensures that raspberry seed extract is at the abundant solvent polymerization of fruit juice;
2. allocate: in fruit juice after polymerisation, add the V of 0.1%
ccarry out protecting tone joint;
3. canned, sealing: carry out automatic canning, sealing under the vacuum condition of 0.05mpa;
4. sterilizing, cooling: sterilization temperature 90 DEG C, sterilizing time 15min, packs after being cooled to room temperature, stores, dispatches from the factory.
The raspberry polymerization fruit juice shelf-life of gained: 12 months;
The raspberry polymerization fruit juice condition of storage of gained: avoid direct sunlight, normal temperature is preserved;
The raspberry polymerization fruit juice outward appearance of gained: in light red liquid;
The raspberry polymerization fruit juice main performance index of gained: raw juice content >=100%, soluble solid >=10%, solid content: allowed a small amount of precipitation.
The foregoing is only preferred embodiment of the present invention, and be not used to limit substantial technological context of the present invention, substantial technological content of the present invention is broadly defined in the right of application, any technology entities that other people complete or method, if with application right define identical, also or a kind of change of equivalence, be all covered by being regarded as among this right.
Claims (10)
1. a preparation method for raspberry seed extract, is characterized in that, said method comprising the steps of:
1) raspberry seed is ground into powder, by the alcohol solution dipping 12-24h of the raspberry seed 65-75% of pulverizing;
2) after step 1) process, then carry out refluxing extraction, by extracting liquid filtering, adopt rotary evaporator to evaporate the extract after filtration, namely recycling design obtains described raspberry seed extract.
2. the preparation method of a kind of raspberry seed extract as claimed in claim 1, is characterized in that, the quality of the raspberry seed pulverized in described step 1) and the interpolation volume of ethanol are 1:10.
3. the preparation method of a kind of raspberry seed extract as claimed in claim 2, is characterized in that, described step 2) in refluxing extraction temperature be 75-85 DEG C, reflux extracting time is 3h ~ 5h.
4. the preparation method of a kind of raspberry seed extract as claimed in claim 3, is characterized in that, also comprise described step 2) in preparation-obtained raspberry seed extract carry out purifying.
5. the preparation method of a kind of raspberry seed extract as claimed in claim 4, it is characterized in that, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity not higher than 2BV.h, when macroporous resin adsorption is complete, clean impurity with distilled water by resin column, till rinse water is not muddy, finally elute with the raspberry seed extract of 75% ~ 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying at least 2h, namely obtain raspberry seed extract.
6. the preparation method of a kind of raspberry seed extract as claimed in claim 4, it is characterized in that, described purification condition is, step 2 by described) in the solution that obtains pass through resin column with the flow velocity of 2BV.h, when macroporous resin adsorption is complete, clean impurity with distilled water by resin column, till rinse water is not muddy, finally elute with the raspberry seed extract of 95% ethanol by absorption, collect eluent; Rotary evaporation eluent, recycling design, less than 70 DEG C vacuum drying 2h, namely obtain raspberry seed extract.
7. a preparation method for raspberry polymerization fruit juice, it is characterized in that, raspberry seed extract method described in claim 6 prepared joins in raspberry fruit juice.
8. the preparation method of a kind of raspberry polymerization fruit juice as claimed in claim 7, is characterized in that, is also included in the V that raspberry polymerization fruit juice adds 0.1%
c.
9. the raspberry seed extract prepared by method described in the arbitrary claim of claim 1 ~ 6.
10. one kind comprises the food of raspberry seed extract prepared by method described in arbitrary claim in claim 4 ~ 6.
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| CN106387539A (en) * | 2016-08-31 | 2017-02-15 | 生命果有机食品股份有限公司 | Raspberry beverage containing pulp and preparation method thereof |
| CN115568507A (en) * | 2022-10-18 | 2023-01-06 | 新疆石河子花园乳业有限公司 | Fermented dairy product with auxiliary antioxidant and lipid-lowering functions and preparation method and application thereof |
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