CN102815912B - Artificial texture stone and production method thereof - Google Patents
Artificial texture stone and production method thereof Download PDFInfo
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- CN102815912B CN102815912B CN201210341929.1A CN201210341929A CN102815912B CN 102815912 B CN102815912 B CN 102815912B CN 201210341929 A CN201210341929 A CN 201210341929A CN 102815912 B CN102815912 B CN 102815912B
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Abstract
The invention provides an artificial texture stone and a production method of the artificial texture stone. The method comprises the following steps of: preparing main color slurry and auxiliary color slurry; pouring the main color slurry and the auxiliary color slurry onto a material guide rail, and forming a pre-mixed colorful slurry body with different colors and different textures through helical push; making the pre-mixed colorful slurry body naturally flow into a die to form naturally flowing color textures; and forming. According to a formula and the production method for the artificial texture stone which is scientific in component proportion and rational in process, the process is unique, and the cost is low; the produced product is outstanding in surface texture, and the textures are vivid; and the decoration effect of the product is enhanced.
Description
Technical field
The present invention relates to a kind of artificial stone-like material, relate in particular to a kind of artificial stone-like material with lines nature, sharply marginated multicolored entire body texture, and described artificial stone-like material's production method.
Background technology
In recent years, along with the fast development of real estate industry, lithotome is simply subject to people's common concern with its decorative effect attractive in appearance and technique, and development rapidly.But lithotome belongs to Nonrenewable resources after all now, and work program is comparatively loaded down with trivial details, and density is larger, transport inconvenience, and price is relatively high.
Artificial stone-like material also obtains certain promotion and application with the simple and unsophisticated decorative effect attractive in appearance of its natural-like stone and cheap feature.Rostone as disclosed in patent CN100348540C, taking inorganicss such as silicon-dioxide, aluminum oxide, sodium oxide, ferric oxide, magnesium oxide as raw material, after adding pigment, make stone material, can be used for the decoration panel in furniture, toilet, kitchen, also can be used as building and ornament materials.
But in industry the artificial stone-like material that produces mostly simple without texture, moulding, color and luster and granular sensation are outstanding, its decorative effect and lithotome and abundant texture moulding thereof differ very large.Especially along with the raising of people's living standard, as the artificially prepd of finishing material in buildings or household, people wish that it has natural appearance, to increase the top grade sense of product.
Patent CN101190546A discloses a kind of preparation method of artificial stone plate graphic pattern, by pattern by being transferred to rostone surface, then carry out press mold, can obtain required pattern, the method can be carried out selection and the transfer printing of pattern as required easily, but pattern is only needed on stone surface, easily impaired and come off.
Patent CN101486218A discloses a kind of preparation method of natural stone-imitating pattern artificial stone product, first carving fixture has the bushing of natural marbling, the artificial stone-like material's raw material that adds mill base is poured on bushing, curing molding obtains taking off bushing after imitation natural stone pattern, and then cast artificial stone raw materials, curing molding, the method can obtain having the goods of the imitation natural stone patterns such as agate red jade decorative pattern.But the method has very high requirement to the carving fixture of bushing decorative pattern shape, once carving is made existing error and can cause decorative pattern natural not, and decorative pattern is subject to the restriction of bushing, can not easily adjust; In mass simultaneous production process, need a large amount of bushings, to the high request of bushing decorative pattern quality, make the method be unfavorable for scale operation.
Therefore, still need a kind of the have artificial stone-like material of natural texture and the production method of described stone material.
Summary of the invention
For the poor problem of existing artificial stone-like material's decorative effect, the invention provides the production method of a kind of artificial texture stone material and described artificial texture stone material.
First object of the present invention is to provide a kind of artificial texture stone material, comprises mass-tone slurry and auxiliary mill base material, and described mass-tone slurry and auxiliary mill base material be respectively independently selected from being made up of composition A or composition B, wherein,
Composition A comprises:
Silicate cement 30 ~ 70 weight parts;
Adulterant 5 ~ 50 weight parts;
Aggregate 25 ~ 55 weight parts;
Pigment 1 ~ 25 weight part;
Fluidizer 0.5 ~ 2 weight part;
Thixotropic agent 0.01 ~ 5 weight part;
Retardant 0.01 ~ 1 weight part;
Defoamer 0.05 ~ 0.5 weight part.
Composition B comprises:
Special cement 30 ~ 70 weight parts;
Adulterant 5 ~ 50 weight parts;
Aggregate 25 ~ 55 weight parts;
Pigment 1 ~ 25 weight part;
Fluidizer 0.5 ~ 2 weight part;
Tackifier 0.01 ~ 0.5 weight part;
Thixotropic agent 0.01 ~ 5 weight part;
Flocculation agent 0.01 ~ 0.5 weight part;
Setting accelerator 0.05 ~ 1 weight part;
Water repellent agent 0.05 ~ 2 weight part;
Defoamer 0.05 ~ 0.5 weight part
Wherein, described special cement is that condensation cure is than silicate cement special cement or complex cement faster.As aluminate cement, aluminosulfate cement or its combination.
In artificial texture stone material shown in the present, mass-tone slurry is preferably by composition A to be prepared, and auxiliary mill base material is preferably by composition B to be prepared.
In artificial texture stone material of the present invention, described mass-tone slurry and auxiliary mill base material weight ratio are 50 ~ 95:5 ~ 50.Be preferably mass-tone slurry and account for 50 ~ 95% of described artificial texture stone material weight, auxiliary mill base material accounts for 5 ~ 50% of described artificial texture stone material weight.
Aggregate of the present invention can be any one or a few in natural colour sand, artificial color sand, colored stone, sliver, shell, river sand.
Pigment of the present invention can be selected the conventional various pigment of the art, as the carbon black of selling on market, ferric oxide, cobalt oxide, titanium dioxide, pigment red 122, (main component is 2,9 dimethylquinacridone), organic light yellow, phthalocyanine blue, Victoria Green WPB, lemon yellow, copper sulfate, acrylic paints etc., can be wherein any one or a few.
Fluidizer of the present invention (being called again softening agent) is preferably polycarboxylic acid high-performance superplasticizer, and described polycarboxylic acid high-performance superplasticizer synthon can be containing polyoxy alkane alkenyl monomer such as polyoxyethylene groups, polyoxypropylene bases; And salt or ester or other derivative of methacrylic acid, vinylformic acid, toxilic acid (or maleic anhydride), allyl group (or methacrylic) sulfonic acid, styryl sulfonic acid or above-mentioned acid, as allyl (or methyl allyl) alcohol, propylene (or methacrylic) acid amides etc.; Can be sulfonated melamine compound condenses, sulfonated naphthalene formaldehyde condensation products, modification ligninsulfonate etc. in addition, can be wherein any one or a few.
Thixotropic agent of the present invention can be starch ethers, smectites, swelling great soil group, attapulgite class and kaolin families and the organically-modified above-mentioned substance of process thereof, can be wherein any one or a few.
Retardant of the present invention can be sulfonated lignin and derivative, hydroxycarboxylic acid and its esters, carbohydrate, zinc oxide, and weak acid and its esters etc. such as boric acid, phosphoric acid can be wherein any one or a few.
Tackifier of the present invention can be ether of cellulose, welan gum, xanthan gum, polyacrylate(s) tackifier, polyurethanes tackifier etc., can be wherein any one or a few.
Flocculation agent of the present invention can be the high molecular polymers such as polyacrylamide, polyvinyl alcohol, polyvinylpyrrolidone, polyoxyethylene, carbomer, polyacrylic acid, sodium polyacrylate, Polyacrylate Emulsion etc., can be wherein any one or a few.
Setting accelerator of the present invention can be water glass, potassium silicate, Tai-Ace S 150, villaumite (as sodium-chlor, calcium chloride), nitrate (as SODIUMNITRATE, nitrocalcite), nitrite (as Sodium Nitrite, calcium nitrite), vitriol (as sodium sulfate), carbonate (as sodium carbonate, sodium bicarbonate) etc., can be wherein any one or a few.
Water repellent agent of the present invention can be aminoresin class water repellent agent, PAPU class water repellent agent, PPE resene water repellent agent, silicone based hydrophober and fluorine-containing hydrophober etc., can be wherein any one or a few.
Adulterant of the present invention can be the conventional adulterant of concrete, as flyash, slag, silicon ash, soil.
Second object of the present invention is to provide a kind of method of producing artificial texture stone material, and step comprises:
Step 1, preparation mass-tone slurry and auxiliary mill base material, mass-tone slurry and auxiliary mill base material are respectively independently selected from being made up of above-mentioned composition A or composition B;
Step 2, mass-tone slurry and auxiliary mill base material are poured into and draw on material track, and form the colored slurry of pre-mixing with different colours texture by spiral pushing;
Step 3, the colored slurry natural flow of pre-mixing is cast in mould, forms the color and vein of natural flow;
Step 4, moulding.
In method of the present invention, the mobility of described mass-tone slurry and auxiliary mill base material and/or time of coagulation and/or wetting ability are different.Can be: 1) mass-tone slurry be there is large fluidity low viscosity wetting ability colored cement slurry, the corresponding with it auxiliary mill base material of collocation is low flow high viscosity and has certain floccular repellency colored cement slurry; Or 2) auxiliary mill base material be there is large fluidity low viscosity wetting ability colored cement slurry, corresponding with it collocation mass-tone slurry is low flow high viscosity and has certain floccular repellency colored cement slurry.Preferably, described mass-tone slurry degree of mobilization is less than auxiliary mill base material.
The degree of mobilization scope of the above-mentioned mass-tone slurry of the present invention and auxiliary mill base material is preferably 100 ~ 340mm, more preferably 140 ~ 260mm.Be preferably >=5mm of the difference of degree of mobilization, more preferably >=10mm, most preferably is >=20mm.
The difference of the time of coagulation of the above-mentioned mass-tone slurry of the present invention and the time of coagulation of auxiliary mill base material is preferably >=and 15 minutes, more preferably 0.5 ~ 6 hour, but can be also >=6 hours.
The water cement ratio of the above-mentioned mass-tone slurry of the present invention and auxiliary mill base material is preferably 0.2-0.5, and more preferably 0.25 ~ 0.45.
In the above-mentioned method of the present invention, after forming step, can also comprise maintenance and/or surface treatment step, wherein: described maintenance working method is: the product of moulding 40 ~ 100 DEG C, be preferably under 40 ~ 70 DEG C of conditions steam-cured; Described surface treatment is selected from any one or a few in sandblast, polishing, polishing, ball blast.
In the above-mentioned method of the present invention, described moulding preferred method of operation is that the mould of filling slurry is passed through to vibrating forming.Vibration amplitude is unsuitable excessive, is preferably slight vibrations.
Artificial texture stone material of the present invention can adopt any methods availalbe preparation, but is preferably the method preparation adopting described in second object of the present invention.
The present invention is by adjusting the major-minor mill base body of artificial stone-like material material prescription, prepare the major-minor mill base body that degree of mobilization differs greatly, and build by simple mixing, make its self-assembling formation multicolour, make it form the slurry of various natural textured patterns by building Self-leveling mode, filled in mould, by slight vibrating forming, prepared surface and have the artificial stone-like material of texture moulding.
The present invention is creationary utilization slurry degree of mobilization difference principle and Self-leveling technique also, configure mass-tone slurry and auxiliary mill base body that color is different with degree of mobilization, carried out naturally mixing and building, in mould, form the slurry with texture and color by Self-leveling technique, prepare the artificial stone-like material with superficial makings moulding.
Formula and the production method of component proportion science provided by the invention, the rational artificial texture stone material of technique, the artificial stone-like material of made has the features such as technique uniqueness, material are easily got, with low cost, texture outstanding, texture is true to nature, good decorating effect, can be used as a kind of external wall decorative material of higher gears, or furniture, upholstery panel.
Embodiment
The invention provides the production method of a kind of artificial texture stone material and described artificial texture stone material, described artificial texture stone material comprises mass-tone slurry and auxiliary mill base material, mass-tone slurry and auxiliary mill base material can be identical or different, but are preferably respectively independently selected from being prepared by composition A or composition B.
The method that the present invention produces described artificial texture stone material comprises the steps: 1) preparation of mould; 2) preparation of mass-tone and auxiliary look material; 3) add respectively in high speed dispersion stirrer after the mass-tone material of preparation and auxiliary look material are added water, stir 3-5 minute, form there is mobility, viscosity, wetting ability and time of coagulation difference mass-tone, auxiliary mill base material; 4) mass-tone slurry and auxiliary mill base material are cast in to draw on material track and by drawing the screw rod spiral pushing rotating on material track by sprue by a certain percentage and form the colored slurry of pre-mixing with different colours texture; 5) the colored slurry natural flow of pre-mixing is cast in the color and vein that forms natural flow in mould; 6) mould of filling slurry is passed through to slight vibrating forming, after maintenance, the demoulding, surperficial aftertreatment, obtain the natural artificial texture stone material of clean mark.
In the production method of the artificial texture stone of the present invention, the mass-tone slurry of preparation (or auxiliary look) slurry be there is large fluidity low viscosity wetting ability colored cement slurry, the corresponding with it auxiliary mill base material of collocation (or mass-tone) slurry is low flow high viscosity and has certain floccular repellency colored cement slurry.Two kinds of colored cement slurries preparing exist adjustable mobility, viscosity, wetting ability and time of coagulation difference, thereby there is adjustable repellency, by they flow be simultaneously cast in the process of mould inside distinct colors can not merge rapidly and can form lines from however sharply marginated multicolored entire body texture.
embodiment 1
Step 1, is used stone material model natural or preprocessing to turn over molding jig according to market and client's demand.Preparation mass-tone slurry and auxiliary mill base material, mass-tone pulp components comprises:
Silicate cement 40kg;
Slag 5 kg;
50 ~ 100 order quartz sand 51 kg;
Pigment 3 kg;
High-performance polycarboxylic acid super-plasticizer 0.5 kg;
Organobentonite 0.5 kg;
Citric acid 0.1 kg;
Defoamer 0.2 kg;
The weight ratio of the corresponding each component of the auxiliary mill base material of collocation is with it:
High-alumina cement 50 kg;
Silicon ash 5kg;
Color sand 37kg;
Pigment 5kg;
High-performance polycarboxylic acid super-plasticizer 0.5kg;
Ether of cellulose 0.2kg;
Organobentonite 0.5kg;
Polyacrylamide 0.1kg;
Self-control setting accelerator 1kg;
Compound water repellent agent 1kg;
Defoamer 0.2kg;
The auxiliary mill base material that the mass-tone slurry that is 160mm by the degree of mobilization of preparation and degree of mobilization are 230mm carries out pre-mixing by drawing material track.
Slurry after pre-mixing is cast in to mould inside, makes it in flow process, form natural texture.
By the slight vibrating forming of the mixture slurry with texture color in mould.
The demoulding after high-temperature steam curing 20h under 50 DEG C of conditions, carries out surface finish processing after the demoulding, make the veined artificial stone-like material of tool.
embodiment 2
Flow process 1, is used stone material model natural or preprocessing to turn over molding jig according to market and client's demand.Preparation mass-tone slurry and auxiliary mill base material, wherein, mass-tone pulp components comprises:
White portland cement 50kg;
Slag 8kg;
Sliver 5kg;
Color sand cream colour 15kg;
The steel gray 18kg of color sand;
Pigment iron oxide yellow 3kg;
High-performance polycarboxylic acid super-plasticizer 0.5kg;
Starch ethers 0.05kg;
Tartrate 0.02kg;
Defoamer 0.1kg;
Auxiliary look pulp components comprises:
White high-alumina cement 45kg;
Silicon ash 14kg;
Sliver 5kg;
Color sand cream colour 15kg;
The steel gray 18kg of color sand;
The orange 5kg of pigment;
High-performance polycarboxylic acid super-plasticizer 0.5kg;
Xanthan gum 0.4kg;
Attapulgite clay 5kg;
Polyoxyethylene 0.2kg;
Self-control setting accelerator 1kg;
Compound water repellent agent 1kg;
Defoamer 0.1kg;
The auxiliary mill base body of yellow that the orange mass-tone slurry that is 170mm by the degree of mobilization of preparation and degree of mobilization are 210mm carries out pre-mixing by drawing material track.
Slurry after pre-mixing is cast in to mould inside, makes it in flow process, form natural texture.
By the slight vibrating forming of the mixture slurry with texture color in mould.
The demoulding after high-temperature steam curing 20h under 60 DEG C of conditions, carries out shotblasting processing after the demoulding, make the veined artificial stone-like material of tool.
embodiment 3
Use stone material model natural or preprocessing to turn over molding jig according to market and client's demand.Preparation mass-tone slurry and auxiliary mill base material, wherein, mass-tone pulp components comprises:
White portland cement 50kg;
Flyash 10kg;
Color sand violet 5kg;
Color sand cream colour 15kg;
The color sand red 15kg in red top;
Pigment iron oxide yellow 3kg;
High-performance polycarboxylic acid super-plasticizer 0.5kg;
Starch ethers 0.05kg;
Tartrate 0.02kg;
Defoamer 0.1kg;
Auxiliary look pulp components comprises:
Aluminosulfate cement 50kg;
Slag 13kg;
Color sand violet 4kg;
Color sand cream colour 15kg;
The color sand red 15kg in red top;
The reddish brown 5kg of pigment;
High-performance polycarboxylic acid super-plasticizer 0.5kg;
Xanthan gum 0.4kg;
Attapulgite clay 5kg;
Polyoxyethylene 0.2kg;
Self-control setting accelerator 1kg;
Compound water repellent agent 1kg;
Defoamer 0.1kg;
The auxiliary mill base material of red-brown that the yellow mass-tone slurry that is 180mm by the degree of mobilization of preparation and degree of mobilization are 200mm carries out pre-mixing by drawing material track.
Slurry after pre-mixing is cast in to mould inside, makes it in flow process, form natural texture.
By the slight vibrating forming of the mixture slurry with texture color in mould.
The demoulding after high-temperature steam curing 20h under 50 DEG C of conditions, carries out surface finish processing after the demoulding, make the veined artificial stone-like material of tool.
In foregoing of the present invention, described degree of mobilization is all according to GB/T2419-2005 standard test.
Artificial texture stone material in the above embodiment of the present invention, mass-tone slurry and auxiliary mill base material degree of mobilization and setting time are reasonable, and two kinds of slurry good dispersions, can produce good sticking power, should not ftracture; Simultaneously method provided by the invention can produce nature, level and smooth striped, and takes into account production efficiency, can be used for large-scale industrialized production.In the above embodiment of the present invention, stone material inside and outside surface all form the texture that nature is level and smooth, and size is cut as required, can both guarantee all the time level and smooth naturally texture on cut surface.
Above specific embodiments of the invention be have been described in detail, but it is just as example, the present invention is not restricted to specific embodiment described above.To those skilled in the art, any equivalent modifications that the present invention is carried out and alternative also all among category of the present invention.Therefore, equalization conversion and the amendment done without departing from the spirit and scope of the invention, all should contain within the scope of the invention.
Claims (9)
1. an artificial texture stone material, is characterized in that, comprises mass-tone slurry and auxiliary mill base material, and described mass-tone slurry is made up of composition A, and auxiliary mill base material is made up of composition B:
Composition A comprises:
Composition B comprises:
Wherein, described special cement is aluminate cement, aluminosulfate cement or its combination.
2. artificial texture stone material according to claim 1, is characterized in that, described mass-tone slurry and auxiliary mill base material weight ratio are 50～95:5～50.
3. artificial texture stone material according to claim 1, is characterized in that, described aggregate is selected from any one or a few in natural colour sand, artificial color sand, colored stone, sliver, shell, river sand.
4. a method of producing artificial texture stone material according to claim 1, is characterized in that, step comprises:
Step 1, preparation mass-tone slurry and auxiliary mill base material, described mass-tone slurry is made up of composition A, and auxiliary mill base material is made up of composition B;
Step 2, mass-tone slurry and auxiliary mill base material are poured into and draw on material track, and form the colored slurry of pre-mixing with different colours texture by spiral pushing;
Step 3, the colored slurry natural flow of pre-mixing is cast in mould, forms the color and vein of natural flow;
Step 4, moulding.
5. method according to claim 4, is characterized in that, the mobility of mass-tone slurry and auxiliary mill base material and/or time of coagulation and/or wetting ability are different.
6. method according to claim 5, is characterized in that, auxiliary mill base material degree of mobilization is greater than or less than mass-tone slurry degree of mobilization.
7. method according to claim 4, is characterized in that, auxiliary mill base material time of coagulation and mass-tone slurry time of coagulation poor >=15 minutes.
8. according to the method described in any one in claim 4～7, it is characterized in that, described auxiliary mill base material and mass-tone slurry degree of mobilization are within the scope of 100～340mm.
9. method according to claim 4, is characterized in that, also comprises maintenance and/or surface treatment step, wherein:
Described maintenance working method is: the product of moulding is steam-cured under 40～100 DEG C of conditions;
Described surface treatment is selected from any one or a few in sandblast, polishing, polishing, ball blast.
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| CN104140227B (en) * | 2013-05-10 | 2016-04-27 | 上海德石建材有限公司 | Natural-like stone is cast in the production technique of stone |
| CN104441820B (en) * | 2014-11-18 | 2016-09-07 | 上海古猿人石材有限公司 | The artificial hole stone slab of a kind of MULTILAYER COMPOSITE and combinations thereof thing and preparation method thereof |
| CN104446243B (en) * | 2014-11-18 | 2017-11-14 | 上海古猿人石材有限公司 | A kind of cement base imitation sandstone product and preparation method thereof and for the tool in its preparation method |
| CN104402492B (en) * | 2014-11-18 | 2016-11-09 | 上海古猿人石材有限公司 | A kind of natural cavity stone imitation and combinations thereof thing and preparation method thereof |
| CN105086698B (en) * | 2015-07-31 | 2017-07-25 | 上海古猿人石材有限公司 | A kind of production method of flexible finishing material |
| CN106082879B (en) * | 2016-06-27 | 2018-06-19 | 中建商品混凝土西安有限公司 | A kind of cement base colour craftwork prepares material and preparation method thereof |
| CN110950593A (en) * | 2019-04-11 | 2020-04-03 | 武汉来道建材科技有限公司 | High-impact-resistance UHPC (ultra high Performance polycarbonate) plate imitating stone and preparation method thereof |
| CN113929360A (en) * | 2021-10-28 | 2022-01-14 | 云浮市新丽新岗石发展有限公司 | Water-ripple beige artificial granite and production process thereof |
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| CN102343619A (en) * | 2011-07-17 | 2012-02-08 | 烟台大学 | Production process and device of natural-like inorganic artificial marble feedstock |
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| WO2012007057A1 (en) * | 2010-07-16 | 2012-01-19 | Parexlanko | Redispersible dry composition of polymer finish |
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| CN102617084A (en) * | 2011-01-30 | 2012-08-01 | 汪峻峰 | Inorganic colorized decoration mortar and preparation method thereof |
| CN102343619A (en) * | 2011-07-17 | 2012-02-08 | 烟台大学 | Production process and device of natural-like inorganic artificial marble feedstock |
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