CN102805337B - Auricularia polytricha compound nutrition tablet and preparation method thereof - Google Patents
Auricularia polytricha compound nutrition tablet and preparation method thereof Download PDFInfo
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- CN102805337B CN102805337B CN2012102908619A CN201210290861A CN102805337B CN 102805337 B CN102805337 B CN 102805337B CN 2012102908619 A CN2012102908619 A CN 2012102908619A CN 201210290861 A CN201210290861 A CN 201210290861A CN 102805337 B CN102805337 B CN 102805337B
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Abstract
The invention relates to an auricularia polytricha compound nutrition tablet. A preparation method of the auricularia polytricha compound nutrition tablet comprises the following steps: taking auricularia polytricha superfine powder, cordyceps sinensis superfine powder, red jujube superfine powder and hawthorn superfine powder as main raw materials, uniformly mixing with microcrystalline cellulose, lactose, mannitol, hydroxypropyl cellulose, hydroxypropyl methyl cellulose and magnesium stearate accessories and tabletting. The auricularia polytricha composite nutrition tablet has the beneficial effects that by utilizing a variable-temperature differential puffed technology and in combination with superfine grinding, the cell wall of auricularia polytricha is broken to a maximum extent, and functional components are dissolved out to a maximum limit; and the quality is stable, and the efficacy is remarkable, and a good effect of preventing cardiovascular and cerebrovascular diseases is achieved. The auricularia polytricha compound nutrition tablet is suitable for crowds with different physiques.
Description
Technical field
The present invention relates to a kind of Uricularia polytricha compound nutritional lozenge, belong to health care product technical field.
Background technology
At present, because human living standard's raising, bad eating habit, the quickening of work rhythm, the factors such as environmental pollution, cause multiple common disease or difficult and complicated illness, to perplex for a long time people's normal life and work, in order addressing the above problem, to release targetedly various medicines and diversified health products on the market, to regulating the human endocrine system, the immunocompetence that strengthens human body has positive effect.
Uricularia polytricha [
Auricularia polytricha (Mont.) Sacc.], belong to the Auriculariaceae Auricularia, have another name called structure ear, thick auricularia auriculajudae, claim again Yellow-back fungus, white back fungus, the south China area claims yellow back of the body ear, carries on the back ear in vain.Be born in tropical and subtropical region, at warm, wet season, grow thickly in deadwood, dried-up on.Uricularia polytricha fructification colloid, shallow disc, ear form irregular shape, the back side has than the long wool hair, colourless, base portion brown only, 400-1100 * 4.5-6.5 μ m, contain in its fine hair and enrich polysaccharide, being one of six kinds of the strongest medicinal fungus of antitumor activity, being the dietotherapeutic Jelly fungi of China's preciousness, is the health food of generally acknowledging in the world.The famous physician's Li Shizhen (1518-1593 A.D.) of the Ming Dynasty is write in Compendium of Material Medica: " auricularia auriculajudae is born on the rotten wood, and property is sweet flat, and it is not hungry to cure mainly beneficial gas, and the strong will of making light of one's life by commiting suicide also has under the treatment hemorrhoid bloody flux effect such as blood ".Modern Chinese medicine is thought, Uricularia polytricha has using tonifying Qi reinforcing lungs, blood circulation promoting and enriching function, can be used for the treatment of the diseases such as Qi and blood deficiency, cough due to deficiency of the lung, hypertension and vascular sclerosis, its contained ferment and vegetable soda can promote alimentary canal and the urinary tract glandular secretion simultaneously, and collaborative secretion catalysis calculus, gall stone, kidney stone etc. had significantly dissolve effect.Auricularia auriculajudae strengthens the antineoplastic immunologic function of body in addition, can prevent kinds cancer.
The Uricularia polytricha quality is slightly thicker than black fungus, and crude fiber content is higher, and cellulose plays good effect to digestion, absorption and the metabolism of many nutriments in the human body.Be a kind of delicious flavour, nutritious edible mushroom, contain rich in protein, iron, calcium, vitamin, crude fibre, wherein protein content and meat are suitable, and iron is higher 10 times than meat, and calcium is 20 times of meat, Cobastab
2Be more than 10 times of vegetables, Uricularia polytricha also contains multiple beneficial amino acid and trace element.Contain nutritional labeling in the dried Uricularia polytricha of 100 grams: moisture 11.2 grams, protein 11.4 grams, fat 0.3 gram, carbohydrate 61.2 grams, 306 kilocalories of heats, crude fibre 7.5 grams, ash content 5.4 grams, 357 milligrams of calcium, 201 milligrams in phosphorus, 185 milligrams of iron, 0.03 milligram of carrotene, 0.15 milligram of thiamine, 0.55 milligram in riboflavin, 2.7 milligrams of niacins.All must amino acid to contain simultaneously human body.
The Uricularia polytricha product of selling on the market mainly forms such as, auricularia auriculajudae drink salted with dried fungus, auricularia auriculajudae can, auricularia auriculajudae fruit tea, auricularia auriculajudae, auricularia auriculajudae capsule occurs, although mouthfeel is good, but there are the defectives such as composition is single, performance is single in most of auricularia auriculajudae product, can not satisfy different consumers' edible demand, adding Uricularia polytricha cell membrane main component is chitin and glucan, strong but pliable in texture, should not chew, contained nutriment is difficult to see through cell membrane and enters digested utilization in the human body in the cell.
Chinese patent CN102274248A discloses a kind of Uricularia polytricha lozenge, be with Uricularia polytricha after soaking, cleaning the removal of impurity, boiling makes it well-done under 115 ℃ of conditions, again fully oven dry under 60 ℃ of conditions, be ground into powder, adding the auxiliary materials such as xylitol, sweet mellow wine, lactose in the Uricularia polytricha powder mixes, granulation, dry, be pressed into the Uricularia polytricha lozenge, have lightweight, volume is little, be easy to carry, be fit to chew clothes or containing, the advantage such as suit the taste of both old and young, but this Uricularia polytricha lozenge nutrition is single, auxiliary material adds too much, has had a strong impact on mouthfeel and the effect of Uricularia polytricha.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of Uricularia polytricha composite nutritional tablet, this nutrition sheet is nutritious, and products taste is good.The present invention also provides a kind of preparation method of Uricularia polytricha composite nutritional tablet.
Technical scheme of the present invention is as follows:
A kind of Uricularia polytricha composite nutritional tablet, weight portion is composed as follows:
100 ~ 150 parts of Uricularia polytricha Ultramicro-powders,
35 ~ 50 parts of Cordyceps sinensis Ultramicro-powders,
20 ~ 30 parts of red date Ultramicro-powders,
20 ~ 30 parts of hawthorn Ultramicro-powders,
40 ~ 50 parts of microcrystalline celluloses,
20 ~ 35 parts of lactose,
80 ~ 150 parts in sweet mellow wine,
15 ~ 30 parts of hydroxypropyl celluloses,
10 ~ 20 parts of HPMCs,
5 ~ 10 parts of dolomols;
Described Uricularia polytricha Ultramicro-powder be by Uricularia polytricha behind alternating temperature, pressure-difference and puffing broken wall, ultramicro grinding makes again;
Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder be by Cordyceps sinensis, red date, hawthorn respectively ultramicro grinding make; With said components mix in proportion, granulation, compressing tablet and get final product.
The present invention is preferred, and described Uricularia polytricha composite nutritional tablet is comprised of following weight portion component:
120 ~ 130 parts of Uricularia polytricha Ultramicro-powders,
35 ~ 40 parts of Cordyceps sinensis Ultramicro-powders,
15 ~ 20 parts of red date Ultramicro-powders,
25 ~ 30 parts of hawthorn Ultramicro-powders,
40 ~ 45 parts of microcrystalline celluloses,
30 ~ 35 parts of lactose,
130 ~ 140 parts in sweet mellow wine,
10 ~ 15 parts of hydroxypropyl celluloses,
10 ~ 15 parts of HPMCs,
5 ~ 10 parts of dolomols.
According to the present invention, being formed by following weight portion component of described Uricularia polytricha composite nutritional tablet optimum:
130 parts of Uricularia polytricha Ultramicro-powders,
35 parts of Cordyceps sinensis Ultramicro-powders,
20 parts of red date Ultramicro-powders,
30 parts of hawthorn Ultramicro-powders,
40 parts of microcrystalline celluloses,
32 parts of lactose,
140 parts in sweet mellow wine,
25 parts of hydroxypropyl celluloses,
12 parts of HPMCs,
10 parts of dolomols.
The preparation method of above-mentioned Uricularia polytricha composite nutritional tablet comprises the steps:
(1) choosing the Uricularia polytricha fructification is raw material, cleans, is dried to water content 30～50wt%, puts into the Bulking tank of bulking equipment, and the amount of putting into of Uricularia polytricha is 15～35% of Bulking tank volume in volume ratio, the sealing Bulking tank;
(2) Uricularia polytricha in the Bulking tank is heated pressurized treatment 10～30min, temperature is 70～100 ℃ in the described Bulking tank, and pressure is 0.10～0.30 MPa in the Bulking tank;
(3) open vavuum pump, vacuum tank to bulking equipment vacuumizes, and the vacuum of vacuum tank is 0～-0.1MPa, open the valve between Bulking tank and the vacuum tank, temperature in the Bulking tank, pressure moment reduces, and utilizes the alternating temperature of moment, pressure differential that Uricularia polytricha is expanded;
(4) dehumidifier: temperature rises to 70～90 ℃ in the Bulking tank, open vavuum pump, valve is in open mode all the time between maintenance Bulking tank and the vacuum tank, to the Uricularia polytricha vacuum drying 1～1.5h in the Bulking tank, be cooled to 25～30 ℃, return to and open Bulking tank behind the normal pressure and take out Uricularia polytricha;
(5) get the coarse crushing of expanded, dried Uricularia polytricha machinery, cross 40～50 mesh sieves, then ultramicro grinding is crossed 200～300 mesh sieves, and the Uricularia polytricha Ultramicro-powder of getting under the sieve is for subsequent use,
Cordyceps sinensis, red date, hawthorn, respectively coarse crushing, cross 40 mesh sieves, then ultramicro grinding, cross 300 mesh sieves, make Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder, take by weighing by weight Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder and Uricularia polytricha Ultramicro-powder and mix to get the mixed material powder;
(6) add mass fraction 80%wt～90wt% ethanol in the mixed material powder, then softwood processed drops into granulation in the mixer, crosses 20 ~ 25 mesh sieves and granulates, and 50 ℃～80 ℃ lower dry;
(7) the dried particle of step (6) and microcrystalline cellulose, lactose, sweet mellow wine, hydroxypropyl cellulose, HPMC, dolomol mixes, and crosses 16 ~ 18 mesh sieves, and compressing tablet makes the Uricularia polytricha composite nutritional tablet.
Preferred according to the present invention, Uricularia polytricha is dried to water content 40 wt% in the described step (1), and the amount of putting into of Uricularia polytricha is 25% of Bulking tank volume in volume ratio.
Preferred according to the present invention, in the described step (2), making the Bulking tank temperature in the Bulking tank is 80 ℃, and pressure is 0.30MPa, keeps 20min that Uricularia polytricha is heated pressurized treatment.Described heating pressurized treatment is by pass into steam in the interlayer of Bulking tank the Uricularia polytricha in the Bulking tank to be heated, along with the increase of temperature, and the pressure rise in the Bulking tank.
Preferred according to the present invention, in the described step (3), the vacuum of vacuum tank is-0.1MPa.
Preferred according to the present invention, in the described step (4) temperature in the Bulking tank is risen to 80 ℃, to the Uricularia polytricha vacuum drying 1.5h in the Bulking tank.
Preferred according to the present invention, ultramicro grinding utilizes vibration superfine disintegrator to carry out described in the step (5), and the Uricularia polytricha ultramicro grinding time is 30min, Cordyceps sinensis ultramicro grinding 15min, red date ultramicro grinding 10min, hawthorn ultramicro grinding 10min.The abrasive media of some is housed in the pulverizing chamber of micronizer, ball, rod or post such as hard material, pulverizing chamber produces circular vibration under the effect that adds exciting force, the judder of pulverizing chamber makes medium generation sling movement in the pulverizing chamber, under the effect of this sling movement, make each medium produce the motion same with pulverizing chamber, material is subject to medium in pulverizing chamber high acceleration clashes into, learns from each other by exchanging views, pulverized by porphyrize, broken wall under the extruding, dissection.
The Uricularia polytricha raw material is take the Jining of Shandong Province Uricularia polytricha as preferred in the above-mentioned steps (1).
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha water-soluble polysaccharide content (with glucose) after expanded wall-breaking method of the present invention is processed to pulverize more than the high 50wt% of Uricularia polytricha water-soluble polysaccharide content than standard machinery.
Excellent results of the present invention is:
1
,The present invention prepares the Uricularia polytricha composite nutritional tablet that is fit to different crowd take Uricularia polytricha, Cordyceps sinensis, red date, hawthorn as primary raw material, and its function value has obtained fully playing, and effect is remarkable, has the effect of good prevention cardiovascular and cerebrovascular disease.
2
,Uricularia polytricha has using tonifying Qi reinforcing lungs, blood circulation promoting and enriching function, can be used for the treatment of the diseases such as Qi and blood deficiency, cough due to deficiency of the lung, hypertension and vascular sclerosis, strengthens the antineoplastic immunologic function of body, can prevent kinds cancer.Cordyceps sinensis have invigorate the lung and the kidney, the effect of hemostasis and phlegm.Being used for chronic cough void breathes heavily; the labor spitting of blood of coughing; impotence and seminal emission, soreness of waist and knee joint is regulated body's immunity, is relievingd asthma, protect renal function, the enhancing hematopoiesis function, the effect such as delay senility; Uricularia polytricha compound nutritional lozenge of the present invention with the compatibility of Uricularia polytricha, Cordyceps sinensis science together; not only keep the effect of Uricularia polytricha, the original single composition of Cordyceps sinensis, according to traditional Chinese medical science compatibility theory, and strengthened resultant effect; strengthen the health care of product, improved the mouthfeel of product.
3
,The hawthorn nature and flavor are sour, sweet, tepor, enter the taste Liver Channel, and the energy promoting digestion and removing indigestion is hypotensive; The red date flavor is sweet, warm in nature, the energy strengthening the spleen and stomach, and adding red date, hawthorn have increased the nutrition of composite nutritional tablet, improve mouthfeel, and effect is comprehensive.
4
,The present invention is take Uricularia polytricha as raw material, and mutually compound with the red date with important nourishing value, its blood tonification effect is better, and it is edible to be fit to female group.
5
,Uricularia polytricha Ultramicro-powder of the present invention is through alternating temperature by Uricularia polytricha, behind the pressure-difference and puffing broken wall, ultramicro grinding makes again, adopt high steam that the Bulking tank that Uricularia polytricha is housed is carried out indirect, avoid high steam directly to contact with Uricularia polytricha, guarantee original quality of Uricularia polytricha, by the moment alternating temperature, transformation realizes carrying out expanded to Uricularia polytricha, the Uricularia polytricha cell wall structure is destroyed, unite again superfine communication technique, destroy to greatest extent the spongiocyte wall construction of Uricularia polytricha, make that functional component farthest discharges in the raw material from cell, improved the nutritional labeling of Uricularia polytricha and absorption and the utilization rate of medicinal efficacy composition.Measure by the phenolsulfuric acid method, the Uricularia polytricha water-soluble polysaccharide content that the Uricularia polytricha after processing through expanded wall-breaking method of the present invention is pulverized than standard machinery increases more than 50%.
6
,The present invention expanded end afterwards directly at Bulking tank with the Uricularia polytricha vacuum drying after expanded, open vavuum pump, valve is in open mode all the time between maintenance Bulking tank and the vacuum tank, can realize the dehumidifier of Uricularia polytricha dry, save and carry out separately drying steps, saved energy consumption.
Description of drawings
Fig. 1 is the schematic diagram of bulking equipment used in the present invention, wherein: 1, Bulking tank; 2, Bulking tank interlayer; 3, steam generator; 4, vacuum tank; 5, valve.
The specific embodiment
Below in conjunction with embodiment and Figure of description the present invention is described in detail, but is not limited to this.
Employed bulking equipment comprises Bulking tank 1, steam generator 3 and vacuum tank 4 among the embodiment, be provided with interlayer 2 on the outer wall of described Bulking tank 1, described steam generator 3 is connected with Bulking tank interlayer 2 by valve 5, and described vacuum tank 4 is connected by valve 5 with Bulking tank 1.Bulking equipment market is on sale, and the bulking equipment that uses among the embodiment is available from the fruit and vegetable dilated drying machine of changing temperature-pressure-difference of the diligent moral new material in Tianjin Science and Technology Ltd., model: QDPH1000-4.Vibration superfine disintegrator adopts the oscillatory type medicine micronizer of Jinan Billionpowder Tech﹠ Eng Co., Ltd.
The Uricularia polytricha fructification that adopts among the embodiment is take Jining of Shandong Province Uricularia polytricha fructification as raw material.
Embodiment 1
A kind of Uricularia polytricha composite nutritional tablet, weight portion is composed as follows:
Uricularia polytricha Ultramicro-powder 100g,
Cordyceps sinensis Ultramicro-powder 35g,
Red date Ultramicro-powder 20g,
Hawthorn Ultramicro-powder 20g,
Microcrystalline cellulose 40g,
Lactose 20g,
Sweet mellow wine 80g,
Hydroxypropyl cellulose 15g,
HPMC 10g,
Dolomol 5g.
The preparation method of Uricularia polytricha composite nutritional tablet:
1, choosing the Uricularia polytricha fructification is raw material, through cleaning, being dried to water content 40wt%, puts into the Bulking tank of changing temperature-pressure-difference and puffing equipment, and the amount of putting into of Uricularia polytricha is 15% of Bulking tank volume in volume ratio, the sealing Bulking tank;
2, start electric heating steam generator, the Uricularia polytricha in the Bulking tank is heated pressurized treatment, the pressure that temperature in the Bulking tank is reached in 80 ℃ and the tank reaches 0.30 MPa, keeps 20min;
3, open vavuum pump, the vacuum tank of bulking equipment is vacuumized, the vacuum-0.10MPa of vacuum tank opens the valve between Bulking tank and the vacuum tank, and the temperature in the Bulking tank, pressure moment reduces, and utilizes the alternating temperature of moment, pressure differential that Uricularia polytricha is expanded;
4, temperature rises to 80 ℃ in the Bulking tank, open vavuum pump, keep that valve is in open mode all the time between Bulking tank and the vacuum tank, under this temperature to the Uricularia polytricha vacuum drying 1.5h in the Bulking tank, then be cooled to 25 ℃, return to and open Bulking tank behind the normal pressure and take out Uricularia polytricha;
5, get the coarse crushing of expanded, dried Uricularia polytricha machinery, cross 40 mesh sieves, then put into vibration superfine disintegrator and carry out ultramicro grinding, cross 300 mesh sieves, the Uricularia polytricha Ultramicro-powder of getting under the sieve is for subsequent use, Cordyceps sinensis, red date, hawthorn, respectively coarse crushing, cross 40 mesh sieves, successively behind ultramicro grinding 15min, 10min, the 10min, cross 300 mesh sieves, make Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder, take by weighing by weight Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder and the Uricularia polytricha Ultramicro-powder that makes mixes to get the mixed material powder;
6, granulate with dry: the mixed material powder that step 5 makes adds mass fraction 90wt% ethanol and makees wetting agent, drops in the mixer and granulates, and crosses 25 mesh sieves, will wet to be placed on the stainless steel pallet, puts into baking oven, carries out drying under 60 ℃ of conditions;
7, whole grain and compressing tablet: get step 6 dry good particle and microcrystalline cellulose, lactose, sweet mellow wine, hydroxypropyl cellulose, HPMC, dolomol mixes, and crosses 18 mesh sieves, and compressing tablet makes the Uricularia polytricha composite nutritional tablet.
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha water-soluble polysaccharide content (take glucose meter) after the described expanded wall-breaking method of present embodiment is processed to be 14.22wt%.
A kind of Uricularia polytricha composite nutritional tablet, weight portion is composed as follows:
Uricularia polytricha Ultramicro-powder 150g,
Cordyceps sinensis Ultramicro-powder 50g,
Red date Ultramicro-powder 30g,
Hawthorn Ultramicro-powder 30g,
Microcrystalline cellulose 50g,
Lactose 35g,
Sweet mellow wine 150g,
Hydroxypropyl cellulose 30g,
HPMC 20g,
Dolomol 10g.
1, choosing the Uricularia polytricha fructification is raw material, through cleaning, being dried to water content 40wt%, puts into the Bulking tank of changing temperature-pressure-difference and puffing equipment, and the amount of putting into of Uricularia polytricha is 15% of Bulking tank volume in volume ratio, the sealing Bulking tank;
2, start electric heating steam generator, the Uricularia polytricha in the Bulking tank is heated pressurized treatment, the pressure that temperature in the Bulking tank is reached in 80 ℃ and the tank reaches 0.20 MPa, keeps 20min;
3, open vavuum pump, the vacuum tank of bulking equipment is vacuumized, the vacuum-0.10MPa of vacuum tank opens the valve between Bulking tank and the vacuum tank, and the temperature in the Bulking tank, pressure moment reduces, and utilizes the alternating temperature of moment, pressure differential that Uricularia polytricha is expanded;
4, temperature rises to 70 ℃ in the Bulking tank, open vavuum pump, keep that valve is in open mode all the time between Bulking tank and the vacuum tank, under this temperature to the Uricularia polytricha vacuum drying 1.5h in the Bulking tank, then be cooled to 25 ℃, return to and open Bulking tank behind the normal pressure and take out Uricularia polytricha;
5, get the coarse crushing of expanded, dried Uricularia polytricha machinery, cross 40 mesh sieves, then put into vibration superfine disintegrator and carry out ultramicro grinding, cross 300 mesh sieves, the Uricularia polytricha Ultramicro-powder of getting under the sieve is for subsequent use, Cordyceps sinensis, red date, hawthorn, respectively coarse crushing, cross 40 mesh sieves, successively behind ultramicro grinding 15min, 10min, the 10min, cross 300 mesh sieves, make Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder, take by weighing by weight Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder and the Uricularia polytricha Ultramicro-powder that makes mixes to get the mixed material powder;
6, granulate with dry: the mixed material powder that step 5 makes adds mass fraction 90wt% ethanol and makees wetting agent, drops in the mixer and granulates, and crosses 20 mesh sieves, will wet to be placed on the stainless steel pallet, puts into baking oven, carries out drying under 60 ℃ of conditions;
7, whole grain and compressing tablet: get step 6 dry good particle and microcrystalline cellulose, lactose, sweet mellow wine, hydroxypropyl cellulose, HPMC, dolomol mixes, and crosses 16 mesh sieves, and compressing tablet makes the Uricularia polytricha composite nutritional tablet.
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha water-soluble polysaccharide content (take glucose meter) after the described expanded wall-breaking method of present embodiment is processed to be 13.81wt%.
A kind of Uricularia polytricha composite nutritional tablet, composed as follows:
Uricularia polytricha Ultramicro-powder 130g,
Cordyceps sinensis Ultramicro-powder 35g,
Red date Ultramicro-powder 20g,
Hawthorn Ultramicro-powder 30g,
Microcrystalline cellulose 40g,
Lactose 32g,
Sweet mellow wine 140g,
Hydroxypropyl cellulose 25g,
HPMC 12g,
Dolomol 10g.
1, choosing the Uricularia polytricha fructification is raw material, through cleaning, being dried to water content 40wt%, puts into the Bulking tank of changing temperature-pressure-difference and puffing equipment, and the amount of putting into of Uricularia polytricha is 15% of Bulking tank volume in volume ratio, the sealing Bulking tank;
2, start electric heating steam generator, the Uricularia polytricha in the Bulking tank is heated pressurized treatment, the pressure that temperature in the Bulking tank is reached in 80 ℃ and the tank reaches 0.20 MPa, keeps 20min;
3, open vavuum pump, the vacuum tank of bulking equipment is vacuumized, the vacuum of vacuum tank-0.05 MPa opens the valve between Bulking tank and the vacuum tank, and the temperature in the Bulking tank, pressure moment reduces, and utilizes the alternating temperature of moment, pressure differential that Uricularia polytricha is expanded;
4, temperature rises to 70 ℃ in the Bulking tank, open vavuum pump, keep that valve is in open mode all the time between Bulking tank and the vacuum tank, under this temperature to the Uricularia polytricha vacuum drying 1.5h in the Bulking tank, then be cooled to 25 ℃, return to and open Bulking tank behind the normal pressure and take out Uricularia polytricha;
5, get the coarse crushing of expanded, dried Uricularia polytricha machinery, cross 40 mesh sieves, then put into vibration superfine disintegrator and carry out ultramicro grinding, cross 300 mesh sieves, the Uricularia polytricha Ultramicro-powder of getting under the sieve is for subsequent use, Cordyceps sinensis, red date, hawthorn, respectively coarse crushing, cross 40 mesh sieves, successively behind ultramicro grinding 15min, 10min, the 10min, cross 300 mesh sieves, make Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder, take by weighing by weight Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder and the Uricularia polytricha Ultramicro-powder that makes mixes to get the mixed material powder;
6, granulate with dry: the mixed material powder that step 5 makes adds mass fraction 80wt% ethanol and makees wetting agent, drops in the mixer and granulates, and crosses 20 mesh sieves, will wet to be placed on the stainless steel pallet, puts into baking oven, carries out drying under 60 ℃ of conditions;
7, whole grain and compressing tablet: get step 6 dry good particle and microcrystalline cellulose, lactose, sweet mellow wine, hydroxypropyl cellulose, HPMC, dolomol mixes, and crosses 16 mesh sieves, and compressing tablet makes the Uricularia polytricha composite nutritional tablet.
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha water-soluble polysaccharide content (take glucose meter) after the described expanded wall-breaking method of present embodiment is processed to be 13.79wt%.
Comparative Examples 1
Uricularia polytricha is carried out alternating temperature, pressure-difference and puffing, dry method as described in the embodiment 1, and difference is:
In the step 2, start electric heating steam generator, the Uricularia polytricha in the Bulking tank is heated pressurized treatment, make in the Bulking tank
The pressure that temperature reaches in 80 ℃ and the tank reaches 0.05 MPa, keeps 20min;
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha after the described expanded wall-breaking method of this Comparative Examples is processed water-soluble
Property polyoses content (take glucose meter) is 4.52wt%.
Comparative Examples 2
Uricularia polytricha is carried out alternating temperature, pressure-difference and puffing, dry method as described in the embodiment 1, and difference is:
In the step 2, start electric heating steam generator, the Uricularia polytricha in the Bulking tank is heated pressurized treatment, make in the Bulking tank
The pressure that temperature reaches in 80 ℃ and the tank reaches 0.60 MPa, keeps 20min;
Measure contrast by the phenolsulfuric acid method and find, adopt the Uricularia polytricha water after the described expanded wall-breaking method of this Comparative Examples is processed
Soluble polysaccharide content (take glucose meter) is 8.28wt%.
Changing temperature-pressure-difference technique is carried out broken wall to the cell membrane of Uricularia polytricha, and embodiment 1 and Comparative Examples 1-2 be totally 3 processing, each processing
Temperature all keeps 20min at 80 ℃ in the Bulking tank, and the vacuum of vacuum tank be-0.10MPa, carries out changing temperature-pressure-difference the cell membrane of Uricularia polytricha is carried out broken wall, adopts phenolsulfuric acid method detection Uricularia polytricha water-soluble polysaccharide (with glucose meter), and testing result sees Table 1.
The different changing temperature-pressure-difference and puffing pressure parameters of table 1 are on the experimental result of the water-soluble thick polyoses content impact of Uricularia polytricha
Interpretation of result: the expanded time is identical, vacuum tank vacuum is identical, and when the Bulking tank internal pressure was 0.05 Mpa, the pressure differential between Bulking tank and the vacuum tank was 0.15 MPa, Uricularia polytricha water-soluble polysaccharide (with glucose meter) content is less, and the Uricularia polytricha shell-broken effect is not good; When the Bulking tank internal pressure was 0.60 MPa, the pressure differential between Bulking tank and the vacuum tank was 0.70 MPa, and Uricularia polytricha water-soluble polysaccharide (with glucose meter) content is less, and the Uricularia polytricha shell-broken effect is not good; As Bulking tank internal pressure 0.30 MPa, the pressure differential between Bulking tank and the vacuum tank is 0.40 MPa, and Uricularia polytricha water-soluble polysaccharide (with glucose meter) content is higher, and the Uricularia polytricha shell-broken effect is best.Experiment finds, when changing temperature-pressure-difference carried out broken wall to the cell membrane of Uricularia polytricha, the pressure differential between the pressure of Bulking tank and Bulking tank and the vacuum tank had larger impact to the Uricularia polytricha broken wall.
Claims (8)
1. Uricularia polytricha composite nutritional tablet is characterized in that weight portion is composed as follows:
Described Uricularia polytricha Ultramicro-powder be by Uricularia polytricha behind alternating temperature, pressure-difference and puffing broken wall, ultramicro grinding makes again;
Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder be by Cordyceps sinensis, red date, hawthorn respectively ultramicro grinding make;
With said components mix in proportion, granulation, compressing tablet and get final product.
2. Uricularia polytricha composite nutritional tablet according to claim 1 is characterized in that, is comprised of the component of following weight portion proportioning:
3. the preparation method of each described Uricularia polytricha composite nutritional tablet of claim 1～2 comprises the steps:
(1) choosing the Uricularia polytricha fructification is raw material, cleans, is dried to water content 30～50wt%, puts into the Bulking tank of bulking equipment, and the amount of putting into of Uricularia polytricha is 15～35% of Bulking tank volume in volume ratio, the sealing Bulking tank;
(2) Uricularia polytricha in the Bulking tank is heated pressurized treatment 10～30min, temperature is 70～100 ℃ in the described Bulking tank, and pressure is 0.10～0.30MPa in the Bulking tank;
(3) open vavuum pump, vacuum tank to bulking equipment vacuumizes, and the vacuum of vacuum tank is 0～-0.1MPa, open the valve between Bulking tank and the vacuum tank, temperature in the Bulking tank, pressure moment reduces, and utilizes the alternating temperature of moment, pressure differential that Uricularia polytricha is expanded;
(4) temperature rises to 70～90 ℃ in the Bulking tank, open vavuum pump, valve is in open mode all the time between maintenance Bulking tank and the vacuum tank, to the Uricularia polytricha vacuum drying 1～1.5h in the Bulking tank, be cooled to 25～30 ℃, return to and open Bulking tank behind the normal pressure and take out Uricularia polytricha;
(5) get the coarse crushing of expanded, dried Uricularia polytricha machinery, cross 40～50 mesh sieves, then ultramicro grinding is crossed 200～300 mesh sieves, and the Uricularia polytricha Ultramicro-powder of getting under the sieve is for subsequent use,
Cordyceps sinensis, red date, hawthorn, respectively coarse crushing, cross 40 mesh sieves, then ultramicro grinding, cross 300 mesh sieves, make Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder, take by weighing by weight Cordyceps sinensis Ultramicro-powder, red date Ultramicro-powder, hawthorn Ultramicro-powder and Uricularia polytricha Ultramicro-powder and mix to get the mixed material powder;
(6) ethanol of adding mass fraction 80%～90% in the mixed material powder, 20～25 mesh sieves are crossed in granulation, and 50 ℃～80 ℃ are lower dry;
(7) the dried particle of step (6) and microcrystalline cellulose, lactose, sweet mellow wine, hydroxypropyl cellulose, HPMC, dolomol mixes, and crosses 16～18 mesh sieves, and compressing tablet makes the Uricularia polytricha composite nutritional tablet.
4. the preparation method of Uricularia polytricha composite nutritional tablet according to claim 3 is characterized in that, Uricularia polytricha is dried to water content 40wt% in the described step (1), and the amount of putting into of Uricularia polytricha is 25% of Bulking tank volume in volume ratio.
5. the preparation method of Uricularia polytricha composite nutritional tablet according to claim 3 is characterized in that, in the described step (2), making the Bulking tank temperature in the Bulking tank is 80 ℃, and pressure is 0.30MPa, keeps 20min that Uricularia polytricha is heated pressurized treatment.
6. the preparation method of Uricularia polytricha composite nutritional tablet according to claim 3 is characterized in that, in the described step (3), the vacuum of vacuum tank is-0.1MPa.
7. the preparation method of Uricularia polytricha composite nutritional tablet according to claim 3 is characterized in that, in the described step (4) temperature in the Bulking tank is risen to 80 ℃, to the Uricularia polytricha vacuum drying 1.5h in the Bulking tank.
8. the preparation method of Uricularia polytricha composite nutritional tablet according to claim 3, it is characterized in that, ultramicro grinding utilizes vibration superfine disintegrator to carry out described in the step (5), the Uricularia polytricha ultramicro grinding time is 30min, Cordyceps sinensis ultramicro grinding 15min, red date ultramicro grinding 10min, hawthorn ultramicro grinding 10min.
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| CN104082706A (en) * | 2014-06-11 | 2014-10-08 | 十堰伏龙山绿色食品开发有限公司 | Black fungus chewing tablets and preparation method thereof |
| CN104431850B (en) * | 2014-12-09 | 2017-07-28 | 中国农业科学院农产品加工研究所 | A kind of method that utilization pressure difference explosion preconditioning technique prepares mulberries Ultramicro-powder |
| CN104957596B (en) * | 2015-07-07 | 2017-06-16 | 青岛农业大学 | A kind of instant Uricularia polytricha cake and preparation method thereof |
| CN108435384A (en) * | 2018-02-10 | 2018-08-24 | 黄太海 | A kind of super-micro wall-broken breaking method of the black feed particles of tradition system |
| CN108477602B (en) * | 2018-02-26 | 2022-02-01 | 浙江中医药大学 | High-quality dendrobium officinale and variable-temperature differential pressure puffing drying method thereof |
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| CN101889620A (en) * | 2010-02-05 | 2010-11-24 | 吕春晓 | Health care tea drink prepared from agaric |
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| CN101889620A (en) * | 2010-02-05 | 2010-11-24 | 吕春晓 | Health care tea drink prepared from agaric |
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