CN102733183B - Fiber fabric with heating function, and preparation method thereof - Google Patents
Fiber fabric with heating function, and preparation method thereof Download PDFInfo
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Abstract
The invention provides a fiber fabric with a heating function, and a preparation method thereof. The invention belongs to the technical field of dyeing and finishing. The fiber fabric contains a capsicum tincture extract and nano-grade ceramic powder, such that the fabric can provide a warm feeling for human skin, and can provide a health-caring function. The fabric can irradiate infrared rays to human bodies. The capsicum tincture extract can hardly run off during a washing process. The method for preparing the fiber fabric comprises the steps that: a fiber fabric is subjected to fabric post-finishing by using a working solution containing a capsicum tincture extract finishing agent, a nonionic organosilicon softening agent, and a nano-grade ceramic powder dispersion liquid, such that the fiber fabric is obtained. The capsicum tincture extract and the nano-grade ceramic powder can be applied to the fabric fiber in a same process, such that the process is simple and feasible.
Description
Technical field
The present invention relates to a kind of textiles, relate in particular to a kind of fabric lining with heating function and preparation method thereof, belong to dyeing and finishing technique field.
Background technology
Enter after 21 century, the fast development of the science such as material science, information technology, bioengineering and nanometer technology, has produced far-reaching influence to the mankind's production, life.The textiles consisting of different textile fabrics has different style characteristics, in performance fiber self function, is aided with rear arrangement process technology, and strengthening a certain or some application performance is the basic characteristics of function textile.In China, the quickening of rhythm of life and the increasing of operating pressure, generally decline Chinese sleep quality.As bedding indispensable in people's sleep procedure, its assisting sleep that can carry, improve the various functions such as function and will more and more be subject to consumers in general's attention and favor, but to the comfortableness of bed necessaries with to the safety of human body, be also consumers in general's important indicator simultaneously.In addition, because modern's rhythm of life is nervous, pressure is large, health is often in sub-health state, and many people also belong to cold physique, and on the clothing of dress, adding warming, the function such as generate heat, stimulate circulation is good mode.
Far infrared is a kind of invisible ray, verified closely bound up with Human Physiology reflection at present, particularly 5.6-15 mu m waveband light beam, produces physiological activation phenomenon to human body, contribute to improve the capacity of self-regulation of human body, caused thus the great attention of medical circle.Human body surface is accepted far infrared, and from outward appearance to inner essence conduction infiltration, is absorbed generation thermogenetic effect, produces resonance, sympathetic response with in-vivo tissue cell, has promoted activity.The infrared spectrum of common ceramic is very similar to human body, all in far-infrared band, has strong absorption, and significantly absworption peak occurs in 2.5～5 μ m and more than 12 μ m, and this and the typical absworption peak of human body are very identical.Can meet the feature that should have as human body insulation material.(Shen Lanping, Li Yiling, Fan Lihong etc. the development of far infrared multifunctional health care textiles, 2000,8 (2): 6-8).The far-infrared radiation material that exploitation far-infrared fabric is used, is mainly ceramic masses, before use this far-infrared ceramic is crushed to the nano ceramic powder below 1 μ m, then it is combined with textiles.
Patent CN200910042087 provides a kind of far infrared heating shell fabric, and it comprises a far IR fibre shell fabric internal layer and near-infrared fibrage fabric skin.The far IR fibre layer of its internal layer is by mixing the polyacrylonitrile of ceramic powders and far IR fibre material and the wool of cotton blending, spandex blending forms, outer field near-infrared fibrage is by near-infrared fibrous material and wool blended the forming of mixing the warm and fine cotton blending of polypropylene of zirconium carbide, but this fabric has the polyacrylonitrile that good heat insulation effect this face weave are had relatively high expectations and need to be mixed ceramic powders or zirconium carbide, cost cost is larger, and owing to being that knit fabric DIMENSIONAL STABILITY is poor, adding of the warm and fine wool of polypropylene also makes fabric skin-friendly poor, be not suitable for using at bed necessaries.
Capsicum tincture extract (Capsicum tincture), be normally used for treating in the ointment of joint pain, the finishing agent combining by profit is applied to dyeing and finishing and processes, and object is to stimulate circulation and metabolism by capsicum tincture, produces heat accumulation thermal effect.(Li Jun, Zhou Yongjun. the skin-care finish of textiles and application thereof [J]. dyeing and finishing technique, 2006,28 (4): 1-5).But capsicum tincture extract is for after fabric, along with the washing process of fabric can be taken away by water, the effect of its spontaneous heating can reduce gradually, and consumer need to buy again, has caused unnecessary waste.So be necessary to develop and a kind ofly can make it act on lasting product.
Summary of the invention
For above problem, the invention provides a kind of fabric lining with heating function, by containing capsicum tincture extract finishing agent, the working solution of the silicone based softener of nonionic and nano-ceramic powder dispersion liquid carries out fabric post-treatment to fabric lining and obtains, it has to human body radiation far infrared, warm up, heating, health care, and capsicum tincture extract is better fixing on fabric, effect is difficult for reducing with washing.
Another object of the present invention has been to provide a kind of above-mentioned method with the fabric lining of heating function of preparing.
For achieving the above object, the present invention adopts following technical scheme:
A kind of method of preparing the fabric lining with heating function, it is characterized in that working solution by containing capsicum tincture extract finishing agent, the silicone based softener of nonionic and nano-ceramic powder dispersion liquid carries out fabric post-treatment to fabric lining and obtains, described working solution is the aqueous systems that contains 10～50g/L capsicum tincture extract finishing agent, the silicone based softener of 5～20g/L nonionic, 10～50g/L nano-ceramic powder dispersion liquid.
Above-mentioned fabric post-treatment is padding method or infusion process.
The technique of above-mentioned padding method is: configuration effort liquid, pad, and pick-up is 70%～100%, at 100～130 ℃, dries.
The technique of above-mentioned infusion process is: configuration effort liquid, with vinegar acid for adjusting pH to 4～5, dipping floods 10～30 minutes at 30～60 ℃, dries.
A kind of fabric lining with heating function, it is characterized in that the described fabric lining with heating function is by containing capsicum tincture extract finishing agent, the working solution of the silicone based softener of nonionic and nano-ceramic powder dispersion liquid carries out fabric post-treatment to fabric lining and obtains, and described working solution is the aqueous systems that contains 10～50g/L capsicum tincture extract finishing agent, the silicone based softener of 5～20g/L nonionic, 10～50g/L nano-ceramic powder dispersion liquid.
Above-mentioned fabric lining is one or more in cotton, day silk LF, day silk G100, wool, cashmere, bamboo charcoal, kapok, vegetable protein regenerated celulose fibre, model.
The capsicum tincture extract finishing agent adopting can be the capsicum tincture extract finishing agent TASTEXHOT2 that Bayer Japanese firm produces, and it take Capsicum Extract and camomile extract is main material, is equipped with the compositions such as undecenoic acid monoglyceride.Owing to take capsicum tincture as Main Ingredients and Appearance in this class extract, capsicum tincture is normally used for treating the ointment of joint pain, the finishing agent combining by profit is applied to dyeing and finishing and processes, object is to stimulate circulation and metabolism by capsicum tincture, produce heat accumulation thermal effect (Li Jun, Zhou Yongjun. the skin-care finish of textiles and application thereof [J]. dyeing and finishing technique, 2006,28 (4): 1-5).
Above-mentioned nano-ceramic powder dispersion liquid can contain one or more in silica, chromium oxide, magnesia, zirconia, zinc oxide, titanium oxide; the technology that can use prior art to disclose is prepared (Zhang Qi; ox is built; Wang Jinmei; granularity prepared by nano zircite is controlled and application [J]; Zhongyuan Technical Faculty journal, 2010,21 (6): 20-23; Deng Hua, Zhang Jimei, Li Xiuming etc., the preparation of nano titanium oxide multifunctional fabric finishing agent and performance [J], textile journal, 2006,27 (3): 92-94) or use commercially available nano-ceramic powder dispersion liquid, the nano ceramics far infrared aqueous dispersions JR-YHL01 that for example Xuancheng Jingrui New Material Co., Ltd. provides.
After above-mentioned fabrics afterfinish method is applied to face weave and completes, concrete treatment process is: grey cloth → singing → boiling-off → bleaching → HEAT SETTING → sanding → dyeing → warm sense arrangement → soft finish, each step can adopt conventional manufacturing parameter to carry out production and processing.
The fabric lining of processing through the method, harmless, can make the various goods of direct contact skin, as sheet, quilt cover, coverlet, multi-functional coverlet, underwear, mouth mask, knee-pad etc.
The present invention's beneficial effect is compared with prior art:
(1) in fabric lining provided by the invention, include capsicum tincture extract, can make human body skin produce hotness, and with health role.In addition, in fabric lining, also include nano-ceramic powder, there is the heat of accumulating and to the ultrared effect of human body radiation, further strengthened the effect warming up.
(2) method with the fabric lining of heating function of the present invention can be applied to capsicum tincture extract and nano-ceramic powder in fabric fibre in same operation.Flow process is simple.
(3) fabric lining provided by the invention, includes nano-ceramic powder, because nano-ceramic powder has small particle diameter, has higher specific area, can adsorb macromolecular organic matter.After being put in fabric, can adsorb the effect that produces capsicum tincture extract, delay the loss of capsicum tincture extract in water-washing process, after repeatedly washing, it still has heating function.
The specific embodiment
The nonionic silicone softening agent using in embodiment obtains by commercially available approach, below adopts the ultratexFSA of Ciba-Geigy.
Embodiment 1
Select yarn: select the blended yarn 30 English Zhi Zuowei warp thread of the soft silk-fibroin regenerated fiber of 30% bombax cotton and 70%, select the blended yarn 21 English Zhi Zuowei weft yarns of the soft silk-fibroin regenerated fiber of 30% bombax cotton and 70%.The density of bombax cotton is little, there is good hygroscopicity and lead moist, soft, the warm cunning of sense of touch is glutinous, but the length of bombax cotton is partially short, the lower cohesive force of brute force is poor.Soft wire protein fiber not only has the advantages such as beautiful soft, the absorb-discharge humid of gloss is good, fiber softening is good, fabric fall is good, also has the health-care functions such as the ultraviolet ray of absorption, far infrared, negative oxygen ion.Soft silk fiber length is long, regularity is good and bombax cotton blending can be learnt from other's strong points to offset one's weaknesses, and is environmental protection fiber yarn.
Weave: the blended yarn to bombax cotton and soft wire protein fiber, adopt twill-weave once on three, 133 * 60/ inches of longitude and latitude interlace densities obtain grey cloth on Rapier looms.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 4 grams per liters, 80 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 2 grams per liter hydrogen peroxide (35%), 2 grams per liter NaOH, 1 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1 ℃/min of the rate of heat addition, is heated to 80 ℃, is incubated 60 minutes, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 160 ℃ of time 30s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 10 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 5 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 50 grams per liters
Fabric post-treatment: adopt padding method to carry out.Padding method finishing technique is: configure according to the above ratio hotness finishing agent 30L, after fabric is infiltrated, two enter two rolls, and pick-up is 70%, then at 130 ℃, dries sizing.
Soft finish: the super soft amino silicon oil emulsion TF-455 of 30 grams per liter, bath raio: 1:30, after 100 ℃ of oven dry, bakes 45s at 160 ℃.
Embodiment 2
Select yarn: select sky silk G1001 that 40 English prop up as warp thread, the blended yarn 40 English Zhi Zuowei weft yarns of 70% wool and 30% sky silk G100.It has the comfortableness of natural fabric, and intensity approaches terylene, is that in all regenerated fibers, intensity is the highest.It silk is learnt from other's strong points to offset one's weaknesses mutually with wool fibre, can improve spinnability, product high resilience, and feel is sliding glutinous, has body bone.Weave: filling yarn adopts on three twill-weave once, and 133 * 72/ inches of longitude and latitude interlace densities obtain grey cloth on Rapier looms.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 8g/L, 95 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 6g/L hydrogen peroxide (35%), 3g/L NaOH, 0.5 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1.5 ℃/min of the rate of heat addition, is heated to 90 ℃, is incubated 70 minutes, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 180 ℃ of time 30s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 30 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 15 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 20 grams per liters
Fabric post-treatment: adopt padding method to carry out.Padding method finishing technique is: prepare according to the above ratio hotness finishing agent 60L, after fabric is infiltrated, two enter two rolls, and pick-up is 100%, then at 100 ℃, dries sizing.
The super soft amino silicon oil emulsion TF-455 of soft finish: 40g/L, bath raio: 1:30, after 100 ℃ of oven dry, bakes 45s at 170 ℃.
Embodiment 3
Select yarn: select sky silk G1001 that 40 English prop up as warp thread, the blended yarn 40 English Zhi Zuowei weft yarns of 70% wool and 30% sky silk G100.It has the comfortableness of natural fabric, and intensity approaches terylene, is that in all regenerated fibers, intensity is the highest.It silk is learnt from other's strong points to offset one's weaknesses mutually with wool fibre, can improve spinnability, product high resilience, and feel is sliding glutinous, has body bone.Weave: filling yarn adopts on three twill-weave once, and 133 * 72/ inches of longitude and latitude interlace densities obtain grey cloth on Rapier looms.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 8g/L, 95 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 6g/L hydrogen peroxide (35%), 3g/L NaOH, 0.5 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1.5 ℃/min of the rate of heat addition, is heated to 90 ℃, is incubated 70 minutes, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 180 ℃ of time 30s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 30 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 12 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 30 grams per liters
Fabric post-treatment: adopt padding method to carry out.Padding method finishing technique is: prepare according to the above ratio hotness finishing agent 60L, after fabric is infiltrated, two enter two rolls, and pick-up is 85%, then at 115 ℃, dries sizing.
The super soft amino silicon oil emulsion TF-455 of soft finish: 40g/L, bath raio: 1:30, after 100 ℃ of oven dry, bakes 45s at 170 ℃.
Embodiment 4
Select yarn: select the pure 60 English Zhi Zuowei warp thread that spin of 100% cotton fiber, the blended yarn 40 English Zhi Zuowei weft yarns of 40% bamboo-carbon fibre and 60% cotton fiber.Bamboo charcoal has stronger adsorption-decomposition function ability, capable of releasing negative ion, emitting far-infrared, and through repeatedly washing and still can keep above-mentioned functions, and there is soft feel and good drapability with the fabric that cotton blending is made into.
Weave: fabric tissue employing flies Warp Satin for 5 piece 2 and organizes as ground, the part that rockets is for other fabric tissues, and longitude and latitude interlace densities is 173 * 120/ inches, on electronic jacquard loom, obtains grey cloth.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 8g/L, 90 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 4g/L hydrogen peroxide (35%), 2g/L NaOH, 1 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1.5 ℃/min of the rate of heat addition, is heated to 90 ℃, insulation 80min, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 180 ℃; Time: 20s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 50 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 20 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 10 grams per liters
Fabric post-treatment: adopt infusion process to carry out.Infusion process finishing technique is: prepare according to the above ratio hotness finishing agent 40L, with vinegar acid for adjusting pH value to 5, flood 30 minutes at 30 ℃, take out fabric drying, sizing.
Soft finish: the super soft amino silicon oil emulsion TF-455 of 35 grams per liter, bath raio: 1:30, after 100 ℃ of oven dry, bakes 40s at 170 ℃.
Embodiment 5
Select yarn: select the pure 60 English Zhi Zuowei warp thread that spin of 100% cotton fiber, the blended yarn 40 English Zhi Zuowei weft yarns of 40% bamboo-carbon fibre and 60% cotton fiber.Bamboo charcoal has stronger adsorption-decomposition function ability, capable of releasing negative ion, emitting far-infrared, and through repeatedly washing and still can keep above-mentioned functions, and there is soft feel and good drapability with the fabric that cotton blending is made into.
Weave: fabric tissue employing flies Warp Satin for 5 piece 2 and organizes as ground, the part that rockets is for other fabric tissues, and longitude and latitude interlace densities is 173 * 120/ inches, on electronic jacquard loom, obtains grey cloth.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 8g/L, 90 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 4g/L hydrogen peroxide (35%), 2g/L NaOH, 1 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1.5 ℃/min of the rate of heat addition, is heated to 90 ℃, insulation 80min, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 180 ℃; Time: 20s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 30 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 15 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 20 grams per liters
Fabric post-treatment: adopt infusion process to carry out.Infusion process finishing technique is: prepare according to the above ratio hotness finishing agent 40L, with vinegar acid for adjusting pH value to 5, flood 20 minutes at 40 ℃, take out fabric drying, sizing.
Soft finish: the super soft amino silicon oil emulsion TF-455 of 35 grams per liter, bath raio: 1:30, after 100 ℃ of oven dry, bakes 40s at 170 ℃.
Embodiment 6
Select yarn: select the pure 60 English Zhi Zuowei warp thread that spin of 100% cotton fiber, the blended yarn 40 English Zhi Zuowei weft yarns of 40% bamboo-carbon fibre and 60% cotton fiber.Bamboo charcoal has stronger adsorption-decomposition function ability, capable of releasing negative ion, emitting far-infrared, and through repeatedly washing and still can keep above-mentioned functions, and there is soft feel and good drapability with the fabric that cotton blending is made into.
Weave: fabric tissue employing flies Warp Satin for 5 piece 2 and organizes as ground, the part that rockets is for other fabric tissues, and longitude and latitude interlace densities is 173 * 120/ inches, on electronic jacquard loom, obtains grey cloth.
Kiering: high-efficiency refining agent TF-1884(development of evil in febrile disease chemical industry) 8g/L, 90 ℃ for the treatment of temperatures, temperature retention time 60min, then wash.
Bleaching: 4g/L hydrogen peroxide (35%), 2g/L NaOH, 1 grams per liter hydrogen peroxide bleaching stabilizer (development of evil in febrile disease chemical industry), 50 ℃ of initial settings, 1.5 ℃/min of the rate of heat addition, is heated to 90 ℃, insulation 80min, hot water wash, adds the cold neutralization of 0.5ml/L acetic acid (30%) again, then cold wash.
HEAT SETTING: temperature: 180 ℃; Time: 20s.
Sanding: take carbon fiber sanding technology, this technique belongs to known technology field.
Preparation hotness finishing agent:
TASTEX HOT2 capsicum tincture class micellization compound (Bayer Japanese firm) 40 grams per liters
The silicone based softener of nonionic (the ultratex FSA of Ciba-Geigy) 20 grams per liters
Nano-ceramic powder dispersion liquid (JR-YHL01, Xuancheng Jingrui New Material Co., Ltd.) 20 grams per liters
Fabric post-treatment: adopt infusion process to carry out.Infusion process finishing technique is: prepare according to the above ratio hotness finishing agent 40L, with vinegar acid for adjusting pH value to 4, flood 10 minutes at 60 ℃, take out fabric drying, sizing.
Soft finish: the super soft amino silicon oil emulsion TF-455 of 35 grams per liter, bath raio: 1:30, after 100 ℃ of oven dry, bakes 40s at 170 ℃.
Claims (1)
1. a method of preparing the fabric lining with heating function, it is characterized in that working solution by containing capsicum tincture extract finishing agent, the silicone based softener of nonionic and nano-ceramic powder dispersion liquid carries out fabric post-treatment to fabric lining and obtains, described working solution is the aqueous systems that contains 10～50 g/L capsicum tincture extract finishing agents, the silicone based softener of 5～20 g/L nonionic, 10～50 g/L nano-ceramic powder dispersion liquids; Described fabric post-treatment is padding method or infusion process; The technique of described padding method is: configuration effort liquid, pad, and pick-up is 70%～100%, at 100～130 ℃, dries; The technique of described infusion process is: configuration effort liquid, and with vinegar acid for adjusting pH to 4～5, dipping floods 10～30 minutes at 30～60 ℃, dries; Described fabric lining is one or more in cotton, day silk LF, day silk G100, wool, cashmere, bamboo charcoal, kapok, vegetable protein regenerated celulose fibre, model.
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|---|
| "纺织品的护肤整理加工及其应用";李俊等;《染整技术》;20060430;第28卷(第4期);第1-5页 * |
| "远红外多功能保健纺织品的研制开发";沈兰萍等;《现代纺织技术》;20001231;第8卷(第2期);第6-8页 * |
| "远红外纺织品及其开发与应用";薛少林等;《山东纺织科技》;20011231(第1期);第48-51页 * |
| 李俊等."纺织品的护肤整理加工及其应用".《染整技术》.2006,第28卷(第4期),第1-5页. |
| 沈兰萍等."远红外多功能保健纺织品的研制开发".《现代纺织技术》.2000,第8卷(第2期),第6-8页. |
| 薛少林等."远红外纺织品及其开发与应用".《山东纺织科技》.2001,(第1期),第48-51页. |
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|---|---|
| CN102733183A (en) | 2012-10-17 |
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Address after: 226300 Jiangsu city of Nantong province Tongzhou District Industrial Park building sun Zhihao Patentee after: JIANGSU GOLDSUN TEXTILE TECHNOLOGY CO., LTD. Address before: 226300 Jiangsu city of Nantong province Tongzhou District Industrial Park building sun Zhihao Patentee before: Goldsun Holding Group Co., Ltd. |