CN102670666A - Preparation method of finest traditional Chinese medicine powder - Google Patents
Preparation method of finest traditional Chinese medicine powder Download PDFInfo
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- CN102670666A CN102670666A CN2011100634944A CN201110063494A CN102670666A CN 102670666 A CN102670666 A CN 102670666A CN 2011100634944 A CN2011100634944 A CN 2011100634944A CN 201110063494 A CN201110063494 A CN 201110063494A CN 102670666 A CN102670666 A CN 102670666A
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Abstract
The invention belongs to the medicine field, and particularly relats to a preparation method of finest traditional Chinese medicine powder. The technical problem solved by the invention is providing the preparation method of finest traditional Chinese medicine powder, belonging to an improved processing method of traditional Chinese medicines, and the preparation method of finest traditional Chinese medicine powder can crush medicines to a cell stage and process medicines more drastically so as to be good for effective ingredients fast dissolving, digesting and absorbing. The preparation method comprises the following steps: step A of coarsely crushing cleanly-prepared traditional Chinese medicine powder to pass through 80-100 mesh sieve at first; step B of processing according to a routine method (such as processing with wine, processing with vinegar, processing with sweet, steaming, stir-frying, processing with medicine juice and so on); further crushing the processed traditional Chinese medicine powder to the powder with powder size of 400-1200 meshes so as to be good for clinical application. Medicines are processed by the method, so that traditional Chinese medicines are furthest processed evenly and drastically; active ingredients are furthest dissolved out on an outer surface of a cell body, flavor and channel tropism of traditional Chinese medicines meet a clinical demand, and effectively matters are absorbed more fast, so that curative effects are played well.
Description
Technical field
The invention belongs to field of medicaments, be specifically related to the method for preparing of the fine powder of Chinese medicine.
Background technology
The prepared slices of Chinese crude drugs are Chinese crude drugs through by Chinese medical theory, Chinese medicine processing method, after concocting through processing, can directly be used for the Chinese medicine of tcm clinical practice.The prepared slices of Chinese crude drugs have comprised the Chinese medicine section (comprising cutting, piece, lobe) of part processing through the place of production, original shape pharmaceutical decocting piece and the decoction pieces of processing through cutting (at source on the basis of processing), big gun.For preceding two types, management is gone up and should be regarded as Chinese crude drug, just does decoction pieces understanding when prescription, the preparation according to Chinese medical theory.And the decoction pieces notion on the management meaning is interpreted as: " according to the needs of allotment or preparation, the further cutting of clean medical material, the big gun processed through the place of production are processed the finished product that forms be called the prepared slices of Chinese crude drugs ".
Since ancient times, Chinese medicine processing all is at primary crude drug, or under the states such as its lamellar, fourth shape, according to " regulations such as " Chinese crude drug concocted specifications " of Chinese pharmacopoeia, ministry standard, each province, autonomous region, municipality directly under the Central Government's promulgation is concocted in accordance with the law.
Because primary crude drug, lamellar or fourth shape medical material have certain thickness, can be when then concocting because of the shape of medical material, process of preparing Chinese medicine degree weakens gradually, i.e. and medical material or the decoction pieces surface process of preparing Chinese medicine is comparatively thorough, and (center) process of preparing Chinese medicine degree becomes to weaken gradually situation to medical material inside.Since cause concocting inhomogeneous and not thorough, to the medical material nature and flavor and return through change also be inhomogeneous, halfway, and then influenced the medicine certainty of curative effect clinically.Especially be that the prepared slices of Chinese crude drugs that the similar single selling in the market, use is directly taken all adopt technology circuits such as the process of preparing Chinese medicine, pulverizing, packing and produce; Generally all under states such as crude drug in whole, lamellar, fourth shape, concoct, also ubiquity is concocted not thorough, uneven phenomenon.
Invention human desires of the present invention provides a kind of and concocts more thoroughly, even, helps the method for the process of preparing Chinese medicine Chinese crude drug of effective ingredient stripping.
Summary of the invention
The technical problem that the present invention solved provides the method for preparing of the fine powder of a kind of Chinese medicine, and it belongs to the concocting method of improved Chinese crude drug, can make medical material reach cell grade and pulverize, concocts more thorough, helps the quick stripping of effective ingredient and digests and assimilates.
The method for preparing of the fine powder decoction pieces of Chinese medicine of the present invention is to adopt following technical scheme to realize:
A, Chinese crude drug was crushed to the 80-100 mesh sieve;
B, concoct according to conventional method.
Conventional concocting method has parch, steams, processed with wine, vinegar system, processed with honey, medicine juice system etc.
Further, can also be after the process of preparing Chinese medicine, being crushed to the Chinese drugs powder granularity is the 400-1200 order.
The committed step of method for preparing of the present invention is, concocts according to conventional method after Chinese crude drug is processed powder again; Like " " Chinese crude drug concocted specification " standard of Chinese pharmacopoeia, ministry standard and each province, autonomous region, municipality directly under the Central Government's promulgation.Adopt aforesaid way to handle medical material, adopt aforesaid way to handle medical material, can concoct Chinese crude drug to greatest extent uniformly, completely; Sporoderm-broken rate also helps effective ingredient and separates out cell to greatest extent more than 99%, and the meridian distribution of property and flavor that is beneficial to Chinese crude drug more meets clinical requirement, is beneficial to quicker that active substance absorbs, thereby better brings into play curative effect.And the bacteria inactivation rate rate is 100%, guaranteed clinical drug safety.
The specific embodiment
Below through to the description of specific embodiment of the invention explanation but do not limit the present invention.
At present, Chinese crude drug is normally at primary crude drug, or under the big state such as its lamellar, fourth shape, and according to existing concocting method, or processing standard handles medical material, to meet the clinical application requirement.
The present invention is in the key improvements part of prior art, and Chinese crude drug is crushed to less granularity earlier, concocts according to existing method again, and is more thorough, even so that medicinal material processing gets, and more helps the effective ingredient stripping.The method for preparing of the fine powder decoction pieces of Chinese medicine provided by the present invention is made up of following step:
A, Chinese crude drug was crushed to the 80-100 mesh sieve;
B, concoct according to conventional method.
The method that above-mentioned A, B step constitute is called for short " method one ".
Further, after can concocting according to conventional method, again Chinese crude drug being crushed to powder size is the 400-1200 order, is beneficial to clinical practice.After promptly pulverizing, the method for preparing of the fine powder decoction pieces of Chinese medicine of the present invention is made up of following steps:
A, Chinese crude drug was crushed to the 80-100 mesh sieve;
B, concoct according to conventional method;
C, to be crushed to powder size be the 400-1200 order, promptly gets.
The method that above-mentioned A, B, C step constitute is called for short " method two ".
As can use the present invention's " method one " and the following medical material of " method two " process of preparing Chinese medicine: animal medicinal material, ratio of rhizome medicinal material, leaf class medical material, fruit crude drugs etc.Like Endothelium Corneum Gigeriae Galli; Bungarus Parvus; Hippocampus; Solenognathus; Periostachum bombycis; Cornu Cervi Pantotrichum; Gecko; Zaocys; Agkistrodon; Scorpio; Scolopendra; Hirudo; Placenta Hominis; Squama Manis; Pheretima; Testis et Pentis Canis; Nidus Vespae; Spirulina; Pseudobulbus Bletillae (Rhizoma Bletillae); Fructus Ligustri Lucidi; Folium Apocyni Veneti; Herba Cistanches; Radix Isatidis; Radix Salviae Miltiorrhizae; Flower of Radix Notoginseng; Radix Ginseng; Radix Panacis Quinquefolii; Radix Notoginseng; Rhizoma Gastrodiae; Radix Lamiophlomidis Rotatae; Ganoderma; Radix Rhodiolae; Radix Polygoni Multiflori Preparata; Cordyceps mycelia powder; The Radix Astragali; Rhizoma Corydalis; Rhizoma Corydalis Decumbentis; Bulbus Fritillariae Cirrhosae; Bulbus Fritillariae Ussuriensis; Bulbus Fritillariae Thunbergii Herba Siegesbeckiae; Herba Epimedii; Semen Allii Tuberosi; Folium Ginkgo; Brassica campestris L pollen; Folium Eucommiae; Monas cuspurpureus Went; Herba Erigerontis; Fructus Schisandrae Chinensis; Rhizoma Paridis; Ganoderma spore; Lignum Aquilariae Resinatum; Cortex Cinnamomi; Radix Aristolochiae Kaempferi; Pollen Pini; Radix Isatidis; Sanguis Draxonis; Sanguis Draxonis; Gecko; Cornu Saigae Tataricae; Cornu Bubali; Margarita; Succinum; Carapax Trionycis; Fructus Gardeniae; The Radix Angelicae Dahuricae; Cortex Moutan; Flos Lonicerae; Indigo Naturalis; Calculus Bovis; Rhizoma Belamcandae; Rhizoma Smilacis Glabrae; Fel Ursi powder; Cortex Magnoliae Officinalis; Fructus Amomi; Spora Lygodii; Rhizoma Chuanxiong; Flos Carthami; Radix Curcumae; Semen Ziziphi Spinosae; Moschus; Radix Glycyrrhizae; Herba Cynomorii; Colla Corii Asini; Radix Rehmanniae; The Radix Paeoniae Alba; Rhizoma Polygonati; Fructus Lycii; Carapax et Plastrum Testudinis; Radix Ophiopogonis; Fructus Corni; Os Sepiae; Semen Strychni; In Catechu or the Concha Arcae any one.
Below through the preparation instance to prove beneficial effect of the present invention, used medical material is same batch.
Embodiment 1 Hippocampus
One, existing method:
1, processed with wine (1): outwash ash bits, put in the iron wire sieve, with the crisp system of slow fire, treat roasting heat after, crisp again from the fire-fighting proper amount of white spirit, repeatedly for several times, crisply be degree to buff, cool promptly and get (or levigation is used); Every Hippocampus 10kg uses Chinese liquor 2kg.Or
2, processed with wine (2): get clean Hippocampus and pass through, put the stove side and dry or dry with steeping in wine.
Two, method one:
1, processed with wine (1):
A, get Hippocampus, be crushed to the 80-100 mesh sieve;
B, put in the iron plate, with the crisp system of slow fire, treat roasting heat after, crisp again from the fire-fighting proper amount of white spirit, repeatedly for several times, crisply be degree to buff, cool and promptly get; Every Hippocampus 10kg uses Chinese liquor 2kg.
2, processed with wine (2):
A, get Hippocampus, be crushed to the 80-100 mesh sieve;
B, get clean Hippocampus and pass through, put that stove is other to be dried or dry with steeping in wine.
Three, method two:
1, processed with wine (1):
A, get Hippocampus, be crushed to the 80-100 mesh sieve;
B, put in the electronic rotation frying pan, the spray proper amount of white spirit was rotated 1-2 hour, placed 24 hours; With slow fire parch to water content below 5%; Every Hippocampus 10kg uses Chinese liquor 2kg;
C, be crushed to powder size in the 400-1200 order, promptly get.
2, processed with wine (2):
A, get Hippocampus, be crushed to the 80-100 mesh sieve;
B, get clean Hippocampus and pass through, put that stove is other to be dried or dry with steeping in wine;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Hippocampus appearance characters of contrast and decoction liquor color contrast are seen table 1:
Table 1 Hippocampus appearance character and decoction liquor color contrast
Indicate:
1, six groups of Hippocampus consumptions are identical.
2, decoction liquor is for pressing 8 times of amounts for the first time, and the 2-3 time 6 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and the decoction liquor color of method one and existing method is close.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
Embodiment 2 Radix Notoginseng
One, existing method:
Clean silt with cold water, medicine per jin adds 3 liang in water, puts into the steel pot and boils, and often stirs, and treats that water exhausts the back and takes out, and do to eighty per cant at the stand, in the input cylinder, adds a cover wet cloth, runs through taking-up, is cut into the thick top of half point sheet and dries.
Two, method one:
A, get Radix Notoginseng, be crushed to the 80-100 mesh sieve;
B, clean silt with cold water, medicine per jin adds 3 liang in water, puts into the steel pot and boils, and often stirs, and treats that water exhausts the back and takes out, and do to eighty per cant at the stand, in the input cylinder, adds a cover wet cloth, runs through taking-up, is cut into the thick top of half point sheet and dries.
Three, method two:
A, get Radix Notoginseng, be crushed to the 80-100 mesh sieve;
B, clean silt with cold water, medicine per jin adds 3 liang in water, puts into the steel pot and boils, and often stirs, and treats that water exhausts the back and takes out, and do to eighty per cant at the stand, in the input cylinder, adds a cover wet cloth, runs through taking-up, is cut into the thick top of half point sheet and dries;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Radix Notoginseng appearance characters of contrast and decoction liquor color contrast are seen table 2:
Table 2 Radix Notoginseng appearance character and decoction liquor color contrast
Indicate:
1, three groups of Radix Notoginseng consumptions are identical.
2, decoction liquor is for pressing 10 times of amounts for the first time, and the 2-3 time 8 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
Embodiment 3 Fructus Ligustri Lucidi
One, existing method:
1, vinegar system: if get its astriction, medicinal red vinegar per jin is mixed thoroughly for 2 liang to inhale and is passed through, and drops in the food steamer and steams, and steams to take out to dry promptly to Shanghai Automobile Factory to get.
2, processed with wine: if get the effectiveness that it strengthens the invigorating middle warmer yin nourishing, medicinal Chinese liquor per jin is mixed thoroughly for 1 liang to inhale and is passed through, and drops in the food steamer, steams to take out to Shanghai Automobile Factory and dries.
Two, method one:
1, vinegar system:
A, get Fructus Ligustri Lucidi, be crushed to the 80-100 mesh sieve;
B, medicinal red vinegar per jin mix thoroughly for 2 liang to inhale and pass through, and drop in the food steamer and steam, and steam to take out to dry promptly to Shanghai Automobile Factory to get.
2, processed with wine:
A, get Fructus Ligustri Lucidi, be crushed to the 80-100 mesh sieve;
B, medicinal Chinese liquor per jin are mixed thoroughly for 1 liang to inhale and are passed through, and drop in the food steamer, steam to Shanghai Automobile Factory's taking-up and dry, and promptly get.
Three, method two:
1, vinegar system:
A, get Fructus Ligustri Lucidi, be crushed to the 80-100 mesh sieve;
B, medicinal red vinegar per jin mix thoroughly for 2 liang to inhale and pass through, and drop in the food steamer and steam, and steam to take out to Shanghai Automobile Factory and dry;
C, be crushed to powder size in the 400-1200 order, promptly get.
2, processed with wine:
A, get Fructus Ligustri Lucidi, be crushed to the 80-100 mesh sieve;
B, medicinal Chinese liquor per jin mix thoroughly for 1 liang to inhale and pass through, and drop in the food steamer, steam to take out to Shanghai Automobile Factory and dry;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Fructus Ligustri Lucidi appearance characters of contrast and decoction liquor color contrast are seen table 3:
Table 3 Fructus Ligustri Lucidi appearance character and decoction liquor color contrast
Indicate:
1, six groups of Fructus Ligustri Lucidi consumptions are identical.
2, decoction liquor is for pressing 10 times of amounts for the first time, and the 2-3 time 8 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
Embodiment 4 Radixs Astragali
One, existing method:
1, processed with honey: if get its invigorating middle warmer effect, medicinal sweet 4 liang per jin, drop into to refine in the pot and open, descend tablet to stir again with slow fire, to golden yellow, spread out cold tack-free for good to evacuate.
2, rice is fried: if get its increase with in the effect of being good for the stomach, 3 liang in medicinal rice per jin burns heat with pot, the rice medicine is with frying, and is degree to coke yellow.
3, wine is fried: can reach the table tonify deficiency, add wine while frying, be faint yellow.
Two, method one:
1, processed with honey:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
B, medicinal sweet 4 liang per jin drop in the pot refining and open, and descend tablet to stir with slow fire again, and to golden yellow, spreading out cold is good to evacuate tack-free.
2, rice is fried:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
3 liang in B, medicinal rice per jin, the pot burning is hot, and the rice medicine is to spend with frying to coke yellow.
3, wine is fried:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
B, add wine, be faint yellow while frying.
Three, method two:
1, processed with honey:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
B, medicinal sweet 4 liang per jin drop in the pot refining and open, and descend tablet to stir with slow fire again, and to golden yellow, spreading out cold is good to evacuate tack-free;
C, be crushed to powder size in the 400-1200 order, promptly get.
2, rice is fried:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
3 liang in B, medicinal rice per jin, the pot burning is hot, and the rice medicine is to spend with frying to coke yellow;
C, be crushed to powder size in the 400-1200 order, promptly get.
3, wine is fried:
A, get the Radix Astragali, be crushed to the 80-100 mesh sieve;
B, add wine, be faint yellow while frying;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Radix Astragali appearance characters of contrast and decoction liquor color contrast are seen table 4:
Table 4 Radix Astragali appearance character and decoction liquor color contrast
Indicate:
1, nine groups of Radix Astragali consumptions are identical.
2, decoction liquor is for pressing 10 times of amounts for the first time, and the 2-3 time 8 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
Embodiment 5 Fructus Schisandrae Chinensis
One, existing method:
1, steam: drop into and steam Shanghai Automobile Factory in the food steamer, taking-up is dried.
2, red vinegar system: if get the astringent effect, per jinly mix thoroughly for 2 liang, it is inhaled pass through, drop in the food steamer, steam Shanghai Automobile Factory's taking-up and dries with red vinegar.
3, processed with honey: if get the effect of its invigorating middle warmer yin nourishing, 3 liang of medicinal Mel per jin are admixed and are inhaled even the input in the food steamer, and steaming Shanghai Automobile Factory is degree of being with black.
4, yellow wine system: if get the effect of its nourishing kidney, medicinal 2 liang of yellow wine per jin are mixed thoroughly, drop in the food steamer, steam to take out to dry promptly to Shanghai Automobile Factory to get.
Two, method one:
1, steam:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
Steam Shanghai Automobile Factory in B, the input food steamer, taking-up is dried.
2, red vinegar system:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
B, per jinly mix thoroughly for 2 liang, it is inhaled pass through, drop in the food steamer, steam Shanghai Automobile Factory and take out and dries with red vinegar.
3, processed with honey:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
3 liang of B, medicinal Mel per jin are admixed and are inhaled even the input in the food steamer, and steaming Shanghai Automobile Factory is degree of being with black.
4, yellow wine system:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
B, medicinal 2 liang of yellow wine per jin are mixed thoroughly, drop in the food steamer, steam to take out to dry promptly to Shanghai Automobile Factory to get.
Three, method two:
1, steam:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
Steam Shanghai Automobile Factory in B, the input food steamer, taking-up is dried;
C, be crushed to powder size in the 400-1200 order, promptly get.
2, red vinegar system:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
B, per jinly mix thoroughly for 2 liang, it is inhaled pass through, drop in the food steamer, steam Shanghai Automobile Factory and take out and dries with red vinegar;
C, be crushed to powder size in the 400-1200 order, promptly get.
3, processed with honey:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
3 liang of B, medicinal Mel per jin are admixed and are inhaled even the input in the food steamer, and steaming Shanghai Automobile Factory is degree of being with black, and taking-up is dried;
C, be crushed to powder size in the 400-1200 order, promptly get.
4, yellow wine system:
A, get Fructus Schisandrae Chinensis, be crushed to the 80-100 mesh sieve;
B, medicinal 2 liang of yellow wine per jin are mixed thoroughly, drop in the food steamer, steam to take out to Shanghai Automobile Factory and dry;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Fructus Schisandrae Chinensis appearance characters of contrast and decoction liquor color contrast are seen table 5:
Table 5 Fructus Schisandrae Chinensis appearance character and decoction liquor color contrast
Indicate:
1,12 groups of Fructus Schisandrae Chinensis consumptions are identical.
2, decoction liquor is for pressing 10 times of amounts for the first time, and the 2-3 time 8 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark, or color is close.
Embodiment 6 Radix Salviae Miltiorrhizaes
One, existing method:
1, fries: get its temperature compensation effect, tablet is dropped in the pot, use slow fire to fry little Jiao and be degree.
Two, method one:
1, fry:
A, get Radix Salviae Miltiorrhizae, be crushed to the 80-100 mesh sieve;
B, tablet is dropped in the pot, using slow fire to fry little Jiao is degree.
Three, method two:
1, fry:
A, get Radix Salviae Miltiorrhizae, be crushed to the 80-100 mesh sieve;
B, tablet is dropped in the pot, using slow fire to fry little Jiao is degree;
C, be crushed to powder size in the 400-1200 order, promptly get.
Four, three kinds of method gained Radix Salviae Miltiorrhizae appearance characters of contrast and decoction liquor color contrast are seen table 6:
Table 6 Radix Salviae Miltiorrhizae appearance character and decoction liquor color contrast
Indicate:
1, three groups of Radix Salviae Miltiorrhizae consumptions are identical.
2, decoction liquor is for pressing 10 times of amounts for the first time, and the 2-3 time 8 times of water gagings decoct, and filter the back gained, the numbering of the identical or similar color of correspondence in the numeral colour system table in the decoction liquor color.
Inventor's perusal filtrating color:
The 1st decoction liquor: the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 2nd decoction liquor: (1) decoction liquor color is all of light color than the 1st decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
The 3rd decoction liquor: (1) decoction liquor color is all of light color than the 2nd decoction liquor.(2) the decoction liquor color of method two is dark than the decoction liquor color of method one and existing method, and method one decoction liquor color than existing methods is dark.
Embodiment 7 Endothelium Corneum Gigeriae Galli
One, existing method:
1, parch: get Endothelium Corneum Gigeriae Galli, photograph is fried or stir-baking in sand method (an appendix II of Chinese Pharmacopoeia version in 2005 D) is fried to heaving.
2, vinegar system: get Endothelium Corneum Gigeriae Galli, fry to heaving according to the method for frying, spray vinegar takes out drying; Every 100kg Endothelium Corneum Gigeriae Galli is used vinegar 15kg.
3, processed with salt: get Endothelium Corneum Gigeriae Galli, fry to heaving, take out drying according to method of stir-baking medicine with salt solu-tion (an appendix II of Chinese Pharmacopoeia version in 2005 D); Every 100kg Endothelium Corneum Gigeriae Galli is used salt 2kg.
Two, method one:
1, parch:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, photograph are fried or the stir-baking in sand method is fried to heaving.
2, vinegar system:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, the photograph method of frying is fried to heaving, and spray vinegar takes out drying; Every 100kg Endothelium Corneum Gigeriae Galli is used vinegar 15kg.
3, processed with salt:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, photograph method of stir-baking medicine with salt solu-tion are fried to heaving, and take out drying; Every 100kg Endothelium Corneum Gigeriae Galli is used salt 2kg.
Three, method two:
1, parch:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, photograph are fried or the stir-baking in sand method is fried to heaving;
C, be crushed to powder size in the 400-1200 order, promptly get.
2, vinegar system:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, the photograph method of frying is fried to heaving, and spray vinegar takes out drying;
C, be crushed to powder size in the 400-1200 order, promptly get.
Wherein, every 100kg Endothelium Corneum Gigeriae Galli is used vinegar 15kg.
3, processed with salt:
A, get Endothelium Corneum Gigeriae Galli, be crushed to the 80-100 mesh sieve;
B, photograph method of stir-baking medicine with salt solu-tion are fried to heaving, and take out;
C, be crushed to powder size in the 400-1200 order, promptly get.
Wherein, every 100kg Endothelium Corneum Gigeriae Galli is used salt 2kg
Four, table 7 is seen in three kinds of method gained Endothelium Corneum Gigeriae Galli appearance characters of contrast and extractum contrast:
Table 7 Endothelium Corneum Gigeriae Galli appearance character and extractum contrast
| Concocting method | Appearance character | Extract content |
| Existing method (parch) | Irregular roll film | 7.6％ |
| Existing method (vinegar system) | Irregular roll film | 7.8％ |
| Existing method (processed with salt) | Irregular roll film | 7.8％ |
| Method one (parch) | Powder: granularity 80-100 order | 8.2％ |
| Method one (vinegar system) | Powder: granularity 80-100 order | 8.4％ |
| Method one (processed with salt) | Powder: granularity 80-100 order | 8.3％ |
| Method two (parch) | Powder: granularity is less than 50 microns | 8.3％ |
| Method two (vinegar system) | Powder: granularity is less than 50 microns | 8.6％ |
| Method two (processed with salt) | Powder: granularity is less than 50 microns | 8.5％ |
Indicate:
1,9 groups of Endothelium Corneum Gigeriae Galli consumptions are identical.
2, extractum detects: the hot dipping (an appendix X of Chinese Pharmacopoeia version in 2005 A) according under the ethanol-soluble extractives algoscopy item is measured, and makes solvent with Diluted Alcohol, detects extract content.
The inventor has also investigated by existing method to Bungarus Parvus, Solenognathus, Periostachum bombycis, Cornu Cervi Pantotrichum, Gecko, Zaocys, Agkistrodon, Scorpio, Scolopendra, Hirudo, Placenta Hominis, Squama Manis, Pheretima, Testis et Pentis Canis, Nidus Vespae, spirulina, Pseudobulbus Bletillae (Rhizoma Bletillae), Folium Apocyni Veneti, Herba Cistanches, Radix Isatidis, flower of Radix Notoginseng, Radix Ginseng, Radix Panacis Quinquefolii, Rhizoma Gastrodiae, Radix Lamiophlomidis Rotatae, Ganoderma, Radix Rhodiolae, Radix Polygoni Multiflori Preparata, Cordyceps mycelia powder, Rhizoma Corydalis, Rhizoma Corydalis Decumbentis, Bulbus Fritillariae Cirrhosae, Bulbus Fritillariae Ussuriensis, Bulbus Fritillariae Thunbergii 、 Herba Siegesbeckiae, Herba Epimedii, Semen Allii Tuberosi, Folium Ginkgo, Brassica campestris L pollen, Folium Eucommiae, Monas cuspurpureus Went, Herba Erigerontis, Rhizoma Paridis, Ganoderma spore, Lignum Aquilariae Resinatum, Cortex Cinnamomi, Radix Aristolochiae Kaempferi, Pollen Pini, Radix Isatidis, Sanguis Draxonis, Sanguis Draxonis, Gecko, Cornu Saigae Tataricae, Cornu Bubali, Margarita, succinum, Carapax Trionycis, Fructus Gardeniae, the Radix Angelicae Dahuricae, Cortex Moutan, Flos Lonicerae, Indigo Naturalis, Calculus Bovis, Rhizoma Belamcandae, Rhizoma Smilacis Glabrae, Fel Ursi powder, Cortex Magnoliae Officinalis, Fructus Amomi, Spora Lygodii, Rhizoma Chuanxiong, Flos Carthami, Radix Curcumae, Semen Ziziphi Spinosae, Moschus, Radix Glycyrrhizae, Herba Cynomorii, Colla Corii Asini, Radix Rehmanniae, the Radix Paeoniae Alba, Rhizoma Polygonati, Fructus Lycii, Carapax et Plastrum Testudinis, Radix Ophiopogonis, Fructus Corni, Os Sepiae, Semen Strychni, Catechu, Concha Arcae; The decoction liquor of each medical material of method one and method two preparations or extractum contrast; From the content of the color of decoction liquor or extractum can find out method one and method two all than existing methods the Chinese crude drug of preparation at shade or extract content obviously because existing method; It is more thorough, even that concocting method after result's demonstration improves through the present invention can make that medicinal material processing gets, and helps the effective ingredient stripping; Owing to be crushed to the 400-1200 order, sporoderm-broken rate is more than 99%, and the bacteria inactivation rate rate is more than 90%.
Claims (4)
1. the method for preparing of the fine powder of Chinese medicine, it is characterized in that: it is made up of following step:
A, Chinese crude drug was crushed to the 80-100 mesh sieve;
B, concoct according to conventional method.
2. the method for preparing of the fine powder of Chinese medicine, it is characterized in that: it is made up of following step:
A, Chinese crude drug was crushed to the 80-100 mesh sieve;
B, according to conventional method concoct, drying;
C, to be crushed to powder size again be the 400-1200 order, promptly gets.
3. the method for preparing of the fine powder of Chinese medicine according to claim 1 and 2, it is characterized in that: said Chinese crude drug is animal medicinal material, ratio of rhizome medicinal material, leaf class medical material, fruit crude drugs.
4. the method for preparing of the fine powder of Chinese medicine according to claim 1 and 2 is characterized in that: said Chinese crude drug be in Endothelium Corneum Gigeriae Galli, Bungarus Parvus, Hippocampus, Solenognathus, Periostachum bombycis, Cornu Cervi Pantotrichum, Gecko, Zaocys, Agkistrodon, Scorpio, Scolopendra, Hirudo, Placenta Hominis, Squama Manis, Pheretima, Testis et Pentis Canis, Nidus Vespae, spirulina, Pseudobulbus Bletillae (Rhizoma Bletillae), Fructus Ligustri Lucidi, Folium Apocyni Veneti, Herba Cistanches, Radix Isatidis, Radix Salviae Miltiorrhizae, flower of Radix Notoginseng, Radix Ginseng, Radix Panacis Quinquefolii, Radix Notoginseng, Rhizoma Gastrodiae, Radix Lamiophlomidis Rotatae, Ganoderma, Radix Rhodiolae, Radix Polygoni Multiflori Preparata, Cordyceps mycelia powder, the Radix Astragali, Rhizoma Corydalis, Rhizoma Corydalis Decumbentis, Bulbus Fritillariae Cirrhosae, Bulbus Fritillariae Ussuriensis, Bulbus Fritillariae Thunbergii 、 Herba Siegesbeckiae, Herba Epimedii, Semen Allii Tuberosi, Folium Ginkgo, Brassica campestris L pollen, Folium Eucommiae, Monas cuspurpureus Went, Herba Erigerontis, Fructus Schisandrae Chinensis, Rhizoma Paridis, Ganoderma spore, Lignum Aquilariae Resinatum, Cortex Cinnamomi, Radix Aristolochiae Kaempferi, Pollen Pini, Radix Isatidis, Sanguis Draxonis, Sanguis Draxonis, Gecko, Cornu Saigae Tataricae, Cornu Bubali, Margarita, succinum, Carapax Trionycis, Fructus Gardeniae, the Radix Angelicae Dahuricae, Cortex Moutan, Flos Lonicerae, Indigo Naturalis, Calculus Bovis, Rhizoma Belamcandae, Rhizoma Smilacis Glabrae, Fel Ursi powder, Cortex Magnoliae Officinalis, Fructus Amomi, Spora Lygodii, Rhizoma Chuanxiong, Flos Carthami, Radix Curcumae, Semen Ziziphi Spinosae, Moschus, Radix Glycyrrhizae, Herba Cynomorii, Colla Corii Asini, Radix Rehmanniae, the Radix Paeoniae Alba, Rhizoma Polygonati, Fructus Lycii, Carapax et Plastrum Testudinis, Radix Ophiopogonis, Fructus Corni, Os Sepiae, Semen Strychni, Catechu or the Concha Arcae any one.
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| CN103083374A (en) * | 2013-01-31 | 2013-05-08 | 孟令刚 | Tea cynomorium songaricum and preparation method thereof |
| CN103393599A (en) * | 2013-08-05 | 2013-11-20 | 四川金岁方药业有限公司 | Preparation method of traditional Chinese medicine fine powder |
| CN103471970A (en) * | 2013-09-18 | 2013-12-25 | 泸州百草堂中药饮片有限公司 | Identification method of superfine powder of traditional Chinese medicinal material |
| CN104055818A (en) * | 2013-03-20 | 2014-09-24 | 中山市中智药业集团有限公司 | Wall-broken Erigeron breviscapus preparation |
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| CN104055818A (en) * | 2013-03-20 | 2014-09-24 | 中山市中智药业集团有限公司 | Wall-broken Erigeron breviscapus preparation |
| CN104055818B (en) * | 2013-03-20 | 2018-08-21 | 中山市中智药业集团有限公司 | A kind of erigeron breviscapus broken wall preparation |
| CN103393599A (en) * | 2013-08-05 | 2013-11-20 | 四川金岁方药业有限公司 | Preparation method of traditional Chinese medicine fine powder |
| CN103393599B (en) * | 2013-08-05 | 2014-09-10 | 四川金岁方药业有限公司 | Preparation method of traditional Chinese medicine fine powder |
| CN103471970A (en) * | 2013-09-18 | 2013-12-25 | 泸州百草堂中药饮片有限公司 | Identification method of superfine powder of traditional Chinese medicinal material |
| CN105311351A (en) * | 2014-07-13 | 2016-02-10 | 胡培芹 | Chinese patent medicine for treating rhinitis |
| CN104367809A (en) * | 2014-11-17 | 2015-02-25 | 徐畅 | Nine-steamed-dried product as well as preparation method and application |
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