CN102639432B - 官能化的氧化锆纳米粒子及由其制备的高折射率膜 - Google Patents

官能化的氧化锆纳米粒子及由其制备的高折射率膜 Download PDF

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Publication number
CN102639432B
CN102639432B CN201080054586.XA CN201080054586A CN102639432B CN 102639432 B CN102639432 B CN 102639432B CN 201080054586 A CN201080054586 A CN 201080054586A CN 102639432 B CN102639432 B CN 102639432B
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nanoparticles
zirconia
modified
combinations
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Chinese (zh)
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CN102639432A (zh
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盖伊·D·乔利
内森·E·舒尔茨
郝恩才
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3M Innovative Properties Co
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3M Innovative Properties Co
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/006—Anti-reflective coatings
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/64—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups singly-bound to oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2244—Oxides; Hydroxides of metals of zirconium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CN201080054586.XA 2009-12-02 2010-11-19 官能化的氧化锆纳米粒子及由其制备的高折射率膜 Expired - Fee Related CN102639432B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410643765.7A CN104495921B (zh) 2009-12-02 2010-11-19 官能化的氧化锆纳米粒子及由其制备的高折射率膜

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US26596809P 2009-12-02 2009-12-02
US61/265,968 2009-12-02
PCT/US2010/057435 WO2011068697A2 (en) 2009-12-02 2010-11-19 Functionalized zirconia nanoparticles and high index films made therefrom

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CN102639432A CN102639432A (zh) 2012-08-15
CN102639432B true CN102639432B (zh) 2014-12-10

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CN201080054586.XA Expired - Fee Related CN102639432B (zh) 2009-12-02 2010-11-19 官能化的氧化锆纳米粒子及由其制备的高折射率膜

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US (2) US8512464B2 (enExample)
EP (1) EP2507161B1 (enExample)
JP (1) JP5698760B2 (enExample)
CN (2) CN104495921B (enExample)
WO (1) WO2011068697A2 (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2389342B1 (en) * 2009-01-22 2020-11-04 3M Innovative Properties Company Surface-modified zirconia nanoparticles
KR101898746B1 (ko) * 2010-12-22 2018-09-13 쓰리엠 이노베이티브 프로퍼티즈 컴파니 표면-개질된 지르코니아 나노입자
US11133118B2 (en) 2012-05-22 2021-09-28 University Of Massachusetts Patterned nanoparticle structures
US9477354B2 (en) * 2012-11-16 2016-10-25 3M Innovative Properties Company Conductive trace hiding materials, articles, and methods
US20150023643A1 (en) * 2013-07-17 2015-01-22 State of Oregon acting by and through the State Board of Higher Education on behalf of the Univers Gradient optical polymer nanocomposites
TWI543938B (zh) 2014-05-13 2016-08-01 國立中央大學 金屬氧化物奈米顆粒材料
EP3189107B1 (en) * 2014-09-04 2018-11-28 3M Innovative Properties Company Hardcoat and method of making the same
TW201741766A (zh) * 2015-12-17 2017-12-01 陶氏全球科技責任有限公司 具有高介電常數之光可成像薄膜
TW201800860A (zh) * 2015-12-17 2018-01-01 陶氏全球科技責任有限公司 具有高介電常數之光可成像薄膜
JP6389839B2 (ja) 2016-03-23 2018-09-12 株式会社先端ナノプロセス基盤開発センター 感光性組成物およびパターン形成方法
TW201802587A (zh) * 2016-03-24 2018-01-16 陶氏全球科技責任有限公司 具有高介電常數之光可成像薄膜
DE102017106647B4 (de) * 2017-03-28 2022-04-28 Lisa Dräxlmaier GmbH Verwendung eines keramischen Pulvers auf der Basis von Seltenerdmetalloxid-stabilisiertem Zirconium(di)oxid als Haftverbesserer für Polymerformkörper, klebstoffbeschichteter Polymerformkörper, Verfahren zur Herstellung eines haftungsverbesserten Polymerformkörpers und dessen Verwendung
JP2019019232A (ja) * 2017-07-18 2019-02-07 第一工業製薬株式会社 酸化ジルコニウム粒子分散体組成物およびその硬化物
CN111377735A (zh) * 2018-12-27 2020-07-07 上海元颉新材料科技有限公司 一种经表面修饰的纳米氧化锆陶瓷粉及其制备方法和应用
US10570063B1 (en) * 2019-02-05 2020-02-25 Magnesium Elektron Limited Zirconia dispersion for use in forming nano ceramics
US20230286824A1 (en) * 2020-08-27 2023-09-14 3M Innovative Properties Company Surface-Modified Transition Metal Oxide Nanoparticles, Method of Making the Same, and Curable Composition and Article Including the Same
CN115368776A (zh) * 2021-09-30 2022-11-22 广东聚华印刷显示技术有限公司 墨水、光折射率调节膜及其制备方法、应用
CN114735749A (zh) * 2022-05-06 2022-07-12 山东国瓷功能材料股份有限公司 表面处理的氧化锆纳米粉体、氧化锆分散液及应用

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1191531A (zh) * 1995-06-07 1998-08-26 美国辉瑞有限公司 作为抗发炎剂的n－羟基脲

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE600278A (fr) 1960-02-18 1961-08-16 Basf Ag Procédé pour la production de N-aryl-N'-hydroxy-urées.
US3893863A (en) 1972-05-10 1975-07-08 Eastman Kodak Co Photographic elements, compositions and processes
JP2620630B2 (ja) * 1987-12-25 1997-06-18 日本写真印刷株式会社 粘度の安定化した水性ゾル
US5013770A (en) * 1989-07-27 1991-05-07 Basf Corporation Cross-linkable surface-modified micaceous particulates and coating compositions containing the same
IE910980A1 (en) 1990-03-27 1991-10-09 Smithkline Beecham Corp 5-lipoxygenase inhibitors
KR900016822A (ko) 1990-04-20 1990-11-14 하라 레이노스께 슬라이드 프로젝터
TW448144B (en) * 1993-08-19 2001-08-01 Pfizer Phenoxyphenyl cyclopentenyl hydroxyureas
JP3322885B2 (ja) * 1995-02-02 2002-09-09 日研化学株式会社 Ｎ−ヒドロキシウレア誘導体
DE19715426A1 (de) * 1997-04-14 1998-10-15 Bayer Ag Blockierte Isocyanatgruppen aufweisende kolloidale Metalloxide
US6365185B1 (en) * 1998-03-26 2002-04-02 University Of Cincinnati Self-destructing, controlled release peroral drug delivery system
US20030008914A1 (en) * 1998-10-16 2003-01-09 C. Grace Yeh Pharmaceutical formulations useful to treat inflammatory and immune disorders
JP4392781B2 (ja) * 2000-08-15 2010-01-06 富士フイルム株式会社 光電変換素子の作成方法及び光電変換素子
JP2002362012A (ja) * 2001-06-08 2002-12-18 Mitsubishi Paper Mills Ltd インクジェット記録材料
KR100556158B1 (ko) * 2002-10-17 2006-03-06 (주) 디지탈바이오텍 신규 엔-하이드록시 티오우레아, 우레아 및 아미드계화합물 및 이를 함유하는 약제학적 조성물
US7289202B2 (en) 2004-09-10 2007-10-30 3M Innovative Properties Company Methods for testing durable optical elements
US7282272B2 (en) 2003-09-12 2007-10-16 3M Innovative Properties Company Polymerizable compositions comprising nanoparticles
US7074463B2 (en) 2003-09-12 2006-07-11 3M Innovative Properties Company Durable optical element
US7238440B2 (en) 2003-10-03 2007-07-03 E. I. Du Pont De Nemours And Company Membrane free fuel cell
EP1758959A1 (en) 2004-05-07 2007-03-07 3M Innovative Properties Company Stain repellent optical hard coating
US20050249940A1 (en) 2004-05-07 2005-11-10 3M Innovative Properties Company Fluoropolyether poly(meth)acryl compounds
US20050249956A1 (en) 2004-05-07 2005-11-10 Naiyong Jing Stain repellent optical hard coating
US7101618B2 (en) 2004-05-07 2006-09-05 3M Innovative Properties Company Article comprising fluorochemical surface layer
US7649029B2 (en) * 2004-05-17 2010-01-19 3M Innovative Properties Company Dental compositions containing nanozirconia fillers
KR101166942B1 (ko) * 2004-05-17 2012-07-19 쓰리엠 이노베이티브 프로퍼티즈 컴파니 나노지르코니아 충전재를 함유하는 치과용 조성물
US7491441B2 (en) * 2004-12-30 2009-02-17 3M Innovative Properties Company High refractive index, durable hard coats
US7264872B2 (en) 2004-12-30 2007-09-04 3M Innovative Properties Company Durable high index nanocomposites for AR coatings
US7241437B2 (en) * 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
US20070014018A1 (en) 2004-12-30 2007-01-18 Wheatley John A Internal components of optical device comprising hardcoat
MX325549B (es) * 2006-06-14 2014-11-24 Du Pont Sustrato recubierto que tiene resistencia mejorada contra ralladuras y desgaste.
JP2008077048A (ja) * 2006-08-23 2008-04-03 Fujifilm Corp 熱現像感光材料
JP2008090262A (ja) * 2006-09-04 2008-04-17 Fujifilm Corp 熱現像感光材料および画像形成方法
JP2009096842A (ja) * 2007-10-15 2009-05-07 Konica Minolta Holdings Inc 半導体膜形成用塗布液、それを用いた半導体膜及び色素増感型太陽電池
US8647510B2 (en) 2007-12-28 2014-02-11 3M Innovative Properties Company Method of making zirconia-containing nanoparticles

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1191531A (zh) * 1995-06-07 1998-08-26 美国辉瑞有限公司 作为抗发炎剂的n－羟基脲

Also Published As

Publication number Publication date
US20130046107A1 (en) 2013-02-21
US8512464B2 (en) 2013-08-20
CN104495921B (zh) 2016-09-07
EP2507161A2 (en) 2012-10-10
CN102639432A (zh) 2012-08-15
US8569537B2 (en) 2013-10-29
JP5698760B2 (ja) 2015-04-08
EP2507161B1 (en) 2015-05-06
WO2011068697A2 (en) 2011-06-09
US20110126734A1 (en) 2011-06-02
WO2011068697A3 (en) 2011-10-27
JP2013512850A (ja) 2013-04-18
CN104495921A (zh) 2015-04-08
EP2507161A4 (en) 2014-01-01

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