CN102599194B - Insecticidal composition containing tea saponin - Google Patents
Insecticidal composition containing tea saponin Download PDFInfo
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- CN102599194B CN102599194B CN201210054685.9A CN201210054685A CN102599194B CN 102599194 B CN102599194 B CN 102599194B CN 201210054685 A CN201210054685 A CN 201210054685A CN 102599194 B CN102599194 B CN 102599194B
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- tea saponin
- alkyl glycoside
- sodium alginate
- composition containing
- insecticidal composition
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- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 67
- 229930182490 saponin Natural products 0.000 title claims abstract description 67
- 150000007949 saponins Chemical class 0.000 title claims abstract description 67
- 239000000203 mixture Substances 0.000 title claims abstract description 26
- 230000000749 insecticidal effect Effects 0.000 title abstract description 11
- 241001122767 Theaceae Species 0.000 title abstract 9
- -1 alkyl glycoside Chemical class 0.000 claims abstract description 24
- 229930182470 glycoside Natural products 0.000 claims abstract description 20
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 18
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 18
- 239000000661 sodium alginate Substances 0.000 claims abstract description 18
- 230000000361 pesticidal effect Effects 0.000 claims abstract description 16
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 claims description 16
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 claims description 16
- 229940095100 fulvic acid Drugs 0.000 claims description 16
- 239000002509 fulvic acid Substances 0.000 claims description 16
- 241000907661 Pieris rapae Species 0.000 claims description 4
- 230000002147 killing effect Effects 0.000 claims description 4
- 241000238631 Hexapoda Species 0.000 claims description 3
- 239000000575 pesticide Substances 0.000 abstract description 9
- 239000000839 emulsion Substances 0.000 description 18
- 239000002917 insecticide Substances 0.000 description 15
- 239000005906 Imidacloprid Substances 0.000 description 13
- YWTYJOPNNQFBPC-UHFFFAOYSA-N imidacloprid Chemical compound [O-][N+](=O)\N=C1/NCCN1CC1=CC=C(Cl)N=C1 YWTYJOPNNQFBPC-UHFFFAOYSA-N 0.000 description 13
- 229940056881 imidacloprid Drugs 0.000 description 13
- 238000002156 mixing Methods 0.000 description 13
- 230000000857 drug effect Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 230000001804 emulsifying effect Effects 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000003905 agrochemical Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
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- 238000000034 method Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 235000010149 Brassica rapa subsp chinensis Nutrition 0.000 description 2
- 235000000536 Brassica rapa subsp pekinensis Nutrition 0.000 description 2
- 241000499436 Brassica rapa subsp. pekinensis Species 0.000 description 2
- 241000500437 Plutella xylostella Species 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- 150000001409 amidines Chemical class 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Natural products O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- ZCVAOQKBXKSDMS-PVAVHDDUSA-N (+)-trans-(S)-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-PVAVHDDUSA-N 0.000 description 1
- CXBMCYHAMVGWJQ-CABCVRRESA-N (1,3-dioxo-4,5,6,7-tetrahydroisoindol-2-yl)methyl (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OCN1C(=O)C(CCCC2)=C2C1=O CXBMCYHAMVGWJQ-CABCVRRESA-N 0.000 description 1
- YATDSXRLIUJOQN-SVRRBLITSA-N (2,3,4,5,6-pentafluorophenyl)methyl (1r,3s)-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(Cl)Cl)[C@H]1C(=O)OCC1=C(F)C(F)=C(F)C(F)=C1F YATDSXRLIUJOQN-SVRRBLITSA-N 0.000 description 1
- HOKKPVIRMVDYPB-UVTDQMKNSA-N (Z)-thiacloprid Chemical compound C1=NC(Cl)=CC=C1CN1C(=N/C#N)/SCC1 HOKKPVIRMVDYPB-UVTDQMKNSA-N 0.000 description 1
- STUSTWKEFDQFFZ-UHFFFAOYSA-N Chlordimeform Chemical compound CN(C)C=NC1=CC=C(Cl)C=C1C STUSTWKEFDQFFZ-UHFFFAOYSA-N 0.000 description 1
- 239000005940 Thiacloprid Substances 0.000 description 1
- VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical class CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000035 biogenic effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- VEMKTZHHVJILDY-UXHICEINSA-N bioresmethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OCC1=COC(CC=2C=CC=CC=2)=C1 VEMKTZHHVJILDY-UXHICEINSA-N 0.000 description 1
- 150000004657 carbamic acid derivatives Chemical class 0.000 description 1
- DUEPRVBVGDRKAG-UHFFFAOYSA-N carbofuran Chemical compound CNC(=O)OC1=CC=CC2=C1OC(C)(C)C2 DUEPRVBVGDRKAG-UHFFFAOYSA-N 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229950006668 fenfluthrin Drugs 0.000 description 1
- HAWJXYBZNNRMNO-UHFFFAOYSA-N furathiocarb Chemical compound CCCCOC(=O)N(C)SN(C)C(=O)OC1=CC=CC2=C1OC(C)(C)C2 HAWJXYBZNNRMNO-UHFFFAOYSA-N 0.000 description 1
- JLYXXMFPNIAWKQ-GNIYUCBRSA-N gamma-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@@H](Cl)[C@H](Cl)[C@H]1Cl JLYXXMFPNIAWKQ-GNIYUCBRSA-N 0.000 description 1
- JLYXXMFPNIAWKQ-UHFFFAOYSA-N gamma-hexachlorocyclohexane Natural products ClC1C(Cl)C(Cl)C(Cl)C(Cl)C1Cl JLYXXMFPNIAWKQ-UHFFFAOYSA-N 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 229960002809 lindane Drugs 0.000 description 1
- 239000003120 macrolide antibiotic agent Substances 0.000 description 1
- 239000004530 micro-emulsion Substances 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 150000004045 organic chlorine compounds Chemical class 0.000 description 1
- 235000012771 pancakes Nutrition 0.000 description 1
- 150000002966 pentacyclic triterpenoids Chemical class 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- SMKRKQBMYOFFMU-UHFFFAOYSA-N prallethrin Chemical compound CC1(C)C(C=C(C)C)C1C(=O)OC1C(C)=C(CC#C)C(=O)C1 SMKRKQBMYOFFMU-UHFFFAOYSA-N 0.000 description 1
- FITIWKDOCAUBQD-UHFFFAOYSA-N prothiofos Chemical compound CCCSP(=S)(OCC)OC1=CC=C(Cl)C=C1Cl FITIWKDOCAUBQD-UHFFFAOYSA-N 0.000 description 1
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 1
- 229940070846 pyrethrins Drugs 0.000 description 1
- 239000002728 pyrethroid Substances 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000006273 synthetic pesticide Substances 0.000 description 1
- 229960005199 tetramethrin Drugs 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000004562 water dispersible granule Substances 0.000 description 1
- 239000004549 water soluble granule Substances 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to an insecticidal composition containing tea saponin, in particular to an insecticidal composition containing the tea saponin, which can improve the insecticidal speed. The insecticidal composition comprises the tea saponin, alkyl glycoside and sodium alginate, wherein the weight ratio of the tea saponin to the alkyl glycoside to the sodium alginate is (5-15):(1-5):(1-5). The insecticidal composition containing the tea saponin can enhance the pesticide effect of the pesticide tea saponin and increase the insecticidal speed of the tea saponin. The insecticidal composition containing the tea saponin also can improve the pesticide effect of other pesticides and accelerate the acting speed of the pesticide.
Description
Technical field
The present invention relates to a kind of Pesticidal combination containing Tea Saponin, particularly, relate to a kind of Tea Saponin Pesticidal combination that improves desinsection speed.
Background technology
Tea Saponin (Teasaponia) is a kind of pentacyclic triterpenoid extracting in tea-seed pancake.It is a kind of natural nonionic surface active agent of function admirable.Along with the application study work of Tea Saponin deepens continuously, the application of Tea Saponin in daily-use chemical industry, light textile, medicine and pesticide industry is also more and more extensive.Bibliographical information Tea Saponin is mainly used in wettable powder as fields such as wetting agent, vegetable insecticide and bactericide, plant growth regulations on pesticide industry
Tea Saponin joins after synthetic pesticide or biogenic pesticide, itself can reach the toxic effect to insect, can also reduce the consumption of pesticide original medicine simultaneously, for example add 1000 and 2000mg/L Tea Saponin after can reduce respectively Rogor consumption 18.13% and 53.70%.This can reduce use cost largely for expensive pesticide species, also can be therefore and reduce the harmful effects such as residual contamination to environment, improve agricultural chemicals safety in utilization.That is to say, Tea Saponin can play synergistic effect to a lot of agricultural chemicals.
Because Tea Saponin itself is exactly good insecticide, but its drug effect performance is slow, the drug effect phase is long, insecticidal effect is not obvious in a short time, rarely have at present report can improve the auxiliary agent of Tea Saponin to pest controling effect, the composition of the control efficiency that can strengthen Tea Saponin and other insecticides is not provided yet.
For solving the problems of the technologies described above, the invention provides a kind of insecticides adjuvant, this pesticidal preparations can effectively solve the problem of residue of pesticide.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of Tea Saponin Pesticidal combination that improves desinsection speed, said composition comprises Tea Saponin, alkyl glycoside and sodium alginate, and wherein the weight ratio of Tea Saponin, alkyl glycoside and sodium alginate is 5-15: 1-5: 1-5.
In above-mentioned composition, can also comprise fulvic acid, wherein the weight of fulvic acid and the weight ratio of Tea Saponin are 0.5-1: 1.
In above-mentioned composition, can also comprise other insecticides, other insecticides can be pyrethroids, natural pyrethrins, tetramethrin, S-bioallethrin, fenfluthrin, prallethrin etc.; Organophosphorus ester, as first Toyodan; Carbamates, as carbofuran, furathiocarb etc.; Macrolide, as Olivomitecidin, the close mycin that compares; Organochlorine compound, as 5a,6,9,9a-hexahydro-6,9-methano-2,4, lindane etc.; Amidine class, as galecron, two worm amidines etc.; Chlorine nicotinyl compounds, as Imidacloprid, thiacloprid, pyridine worm miaow etc.Preferably, can comprise Imidacloprid.
Preferably, other insecticides account for 10% of Tea Saponin weight in above-mentioned composition.
In above-mentioned Tea Saponin Pesticidal combination, preferred, alkyl glycoside is alkyl glycoside class material arbitrarily.
Preferably, above-mentioned Tea Saponin Pesticidal combination can be prepared into wetting powder, sustained release agent, pulvis, micro-capsule suspension, dispersible dense dose, seed treatment emulsion, aqueous emulsion, large granula, granule, microemulsion, oil-suspending agent, finish, any one in seed with coated pesticidal, suspension emulsion, water-soluble granule, soluble thick agent, water-dispersible granules, preferably, above-mentioned Tea Saponin Pesticidal combination is prepared into aqueous emulsion.
Above-mentioned Tea Saponin Pesticidal combination of the present invention can, by the insecticides adjuvant preparation method preparation of this area routine, for example, by being uniformly mixed, or by methods such as high speed shear mixing, not have special restriction.
The present invention also provides above-mentioned Tea Saponin Pesticidal combination for improving the desinsection speed of insecticide and strengthening the purposes of pest controling effect, and wherein said insecticide is preferably Imidacloprid.
Tea Saponin used, alkyl glycoside, sodium alginate, fulvic acid in the present invention, be the conventional substances that can buy on market, is not particularly limited.
The present invention also provides a kind of composition that can be used in the control efficiency that improves Tea Saponin and other insecticide compositions, said composition comprises alkyl glycoside, sodium alginate and fulvic acid, wherein the weight ratio of alkyl glycoside, sodium alginate and fulvic acid is 2: 1: 5, or 3: 1: 8,2: 3: 10, other insecticides were Imidacloprid.
The beneficial effect of technique scheme of the present invention is that the Tea Saponin Pesticidal combination of the application of the invention, can strengthen the drug effect of agricultural chemicals Tea Saponin, and the desinsection speed of Tea Saponin is provided.Tea Saponin Pesticidal combination of the present invention can also improve the drug effect of other agricultural chemicals and accelerate drug effect speed.
Embodiment
In order to understand the present invention, further illustrate the present invention with embodiment below, but do not limit the present invention.
Embodiment 1 10% Tea Saponin aqueous emulsion
Get Tea Saponin 5kg, alkyl glycoside 2kg, sodium alginate 1kg, fulvic acid 5kg, 37kg water, fully mixes, and said mixture is extracted into high shear mixing still, starts high-shear emulsifying homogenizer, and material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, obtain 10% Tea Saponin aqueous emulsion.
Embodiment 2 20% Tea Saponin aqueous emulsions
Get Tea Saponin 10kg, alkyl glycoside 3kg, sodium alginate 1kg, fulvic acid 8kg, 28kg water, fully mixes, and said mixture is extracted into high shear mixing still, starts high-shear emulsifying homogenizer, and material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, obtain 20% Tea Saponin aqueous emulsion.
Embodiment 3 30% Tea Saponin aqueous emulsions
Get Tea Saponin 15kg, alkyl glycoside 2kg, sodium alginate 3kg, fulvic acid 10kg, 20kg water, fully mixes, and said mixture is extracted into high shear mixing still, starts high-shear emulsifying homogenizer, and material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, obtain 30% Tea Saponin aqueous emulsion.
Embodiment 4 blank liquid
Alkyl glycoside 7kg, sodium alginate 8kg, fulvic acid 15kg, 20kg water, fully mixes, and said mixture is extracted into high shear mixing still, starts high-shear emulsifying homogenizer, and material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, obtain blank liquid.
Embodiment 5 insecticide effect embodiment
By the 10% Tea Saponin aqueous emulsion of embodiment 1-3,, 20% Tea Saponin aqueous emulsion and 30% Tea Saponin aqueous emulsion, and the blank of embodiment 4, the former powder of 60% Tea Saponin (Tea Inst., Chinese Academy of Agricultural Sciences's purchase), be diluted to respectively low age imported cabbageworm on finite concentration spraying control Chinese cabbage, then observe control efficiency, 1-3 days statistics control efficiency after spray medicine, control efficiency accounts for the percentage calculation of diamond-back moth total amount with the quantity of dead low age imported cabbageworm.Valid density refers to and sprays the concentration that contains Tea Saponin in liquid, sprays blank and sprays according to the extension rate of the aqueous emulsion of embodiment 1.
Concrete outcome is as following table:
Found through experiments, the Tea Saponin aqueous emulsion that comprises alkyl glycoside, fulvic acid and sodium alginate, due to the effect of three kinds of auxiliary components, makes Tea Saponin aqueous emulsion increase the speed of killing of imported cabbageworm, and has increased insect killing effect.Because auxiliary agent does not have insecticidal activity, so by making the combination of used additives, actual listing provides the insecticide efficiency of Tea Saponin.
The effect that embodiment 6 mixes other insecticides
Get Tea Saponin 10kg, alkyl glycoside 3kg, sodium alginate 1kg, fulvic acid 8kg, 1kg Imidacloprid, 27kg water, fully mixes, and said mixture is extracted into high shear mixing still, starts high-shear emulsifying homogenizer, and material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, obtain 22% Tea Saponin Imidacloprid aqueous emulsion.
Control sample is prepared as follows:
Get Tea Saponin 10kg, alkylaryl formaldehyde resin APEO 4kg, sodium lignin sulfonate 3kg, 1kg Imidacloprid, 32kg water, fully mixes, and said mixture is extracted into high shear mixing still, start high-shear emulsifying homogenizer, material is carried out to high speed shear mixing; After reaching particle diameter 5-15nm, just can stop high shear, must contrast 22% Tea Saponin Imidacloprid aqueous emulsion.
According to the insecticidal effect of diamond-back moth on the method test Chinese cabbage of embodiment 5, valid density refers to Tea Saponin and the concentration of Imidacloprid gross weight in solution.
Experimental result is as follows:
Can find out from experimental result, by the composition of Tea Saponin and Imidacloprid, add after alkyl glycoside, sodium alginate and fulvic acid, strengthened the desinsection effect of Tea Saponin and imidacloprid composition, and desinsection speed also be accelerated.Alkyl glycoside, sodium alginate and fulvic acid can strengthen the drug effect of Tea Saponin and imidacloprid composition thus, and the composition of Tea Saponin, alkyl glycoside, sodium alginate and fulvic acid can strengthen the drug effect of Imidacloprid in other words.
Claims (2)
1. one kind is improved the Tea Saponin Pesticidal combination of desinsection speed, said composition is made up of Tea Saponin, alkyl glycoside, fulvic acid and sodium alginate, and wherein the weight ratio of Tea Saponin, alkyl glycoside, fulvic acid and sodium alginate is 5: 2: 5: 1 or 10: 3: 8: 1 or 15: 2: 10: 3.
2. composition claimed in claim 1 is for the purposes of the speed of killing to imported cabbageworm and insect killing effect increase.
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| CN104419559A (en) * | 2013-08-22 | 2015-03-18 | 南通恒鼎重型机床有限公司 | Detergent specially used for removing acarids |
| CN103609558B (en) * | 2013-11-11 | 2016-06-08 | 李文斌 | A kind of environmental protection bactericide synergist and preparation method thereof |
| CN103651358B (en) * | 2013-11-22 | 2015-07-01 | 光景生物科技(苏州)有限公司 | Tea saponin granule, as well as preparation method and use thereof |
| CN103621558A (en) * | 2013-11-28 | 2014-03-12 | 山西省农业科学院棉花研究所 | Imidacloprid wettable powder seed-dressing agent for preventing and controlling Aphis gossypii Glover and preparation method and application thereof |
| CN105104434A (en) * | 2015-08-18 | 2015-12-02 | 崔明华 | Green efficient seed dressing agent and preparation method therefor |
| CN107494596A (en) * | 2017-08-10 | 2017-12-22 | 黑龙江九穗谷农业科技发展有限公司 | Antimicrobial protection agent is used in one kind plantation |
| CN109336707A (en) * | 2018-11-13 | 2019-02-15 | 崔焰普 | A kind of foliar fertilizer with prevention and treatment vegetable aphid |
| CN110214731A (en) * | 2019-07-18 | 2019-09-10 | 安徽众渔生物科技有限公司 | One seed shrimp crab culture pond trash fish scavenger |
| CN111567550B (en) * | 2020-06-22 | 2021-11-09 | 江苏艾津作物科技集团有限公司 | Imidacloprid composition, preparation method thereof and application thereof in pesticide |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101810188A (en) * | 2010-04-20 | 2010-08-25 | 浙江大学 | Compound imidacloprid aqueous suspension prepared by using tea saponin as synergist and surface active agent |
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