CN102585591A - Method for making blue offset printing ink - Google Patents
Method for making blue offset printing ink Download PDFInfo
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- CN102585591A CN102585591A CN2012100632939A CN201210063293A CN102585591A CN 102585591 A CN102585591 A CN 102585591A CN 2012100632939 A CN2012100632939 A CN 2012100632939A CN 201210063293 A CN201210063293 A CN 201210063293A CN 102585591 A CN102585591 A CN 102585591A
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Abstract
The invention discloses a method for making blue offset printing ink and belongs to the field of printing ink making. The method comprises the following steps: (1) DM Direct Milled blue pigment, connection material and calcium carbonate are fed into a kneader to be stirred uniformly; (2) stirring and heating are performed to fully disperse the DM blue pigment until the mixture has the same color as a standard sample, and then the rest connection material and dispersant are added to obtain primary ink; (3) the primary ink is rolled on a three-roll machine until the fineness of the primary ink is less than or equal to 15 Mum; and (4), printing ink oil, antioxidant and drying agent are added into the rolled primary ink. The blue printing ink made by adopting the method has the advantages as follows: the production method is simple, the production efficiency is higher, and the ink properties are better; water draining is not required in a production process, and the yield is higher; the DM blue pigment takes the resin for printing ink as pigment treating-agent, so as to avoid troubles in water draining and reduce environmental pollution to the maximum extent; the dispersivity of the pigment is good, so that the printing ink has high gloss, high color density and good transparency; and the production cost of the DM blue pigment is relatively lower, and the production efficiency of the DM blue pigment is high.
Description
Technical field
The present invention relates to a kind of offset printing blue oil China ink production technique, belong to printing ink and make the field.
Background technology
Flexographic ink has two kinds of working methods, dry method and wet methods at present.The distributes ink property that dry method makes is poor, and the gloss of finished product, transparency and depth of shade are not good; Wet processing adopts the pigment of filter cake formula; Though finished product printing ink is better than dry production at fermentation such as gloss, transparency and depth of shade; But, both limited to Wastewater Recovery and to handle required expense more also very high to some extent owing to need draining in the production process for the space.
Summary of the invention
The technical problem that the present invention will solve provides a kind of method of manufacture of offset printing blue oil China ink, and the working method of blue oil China ink of the present invention is easy, and production efficiency is higher, and China ink property is better.Production process need not draining, and output is higher.The resin that the blue pigment use of DM printing ink is used has been avoided the trouble of draining as the treatment agent of pigment, has farthest reduced the pollution to environment, and pigment-dispersing ink good, that make is high, depth of shade is high, transparency good.The cost of manufacture of the blue pigment of DM is also relatively low, and production efficiency is high.
The technical scheme that the present invention taked is: a kind of offset printing blue oil China ink method of manufacture may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 25～40 weight parts, 10～30 weight parts and 1～15 weight part is put in the kneader stirred;
(2) stir and be warming up to 110～120 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 10～20 weight parts and the dispersion agent of 0.1～3 weight part and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller;
(4) add the ink oil of 1～15 weight part, the inhibitor of 0.1～2 weight part and the siccative of 0.1～3 weight part in the basic China ink after rolling.
Each material temperature is 50～70 ℃ in the middle kneader of step (1).
The friction resistant auxiliary agent that also adds 1～5 weight part in the step (2).
Basic black rolling temperature is 50～70 ℃ in the step (3), and pressure is 30～60MPa.
Lime carbonate plays the effect of filling in printing ink.
Connect material and add in two steps, in step (1) and step (2), add respectively, because step (2) need at first be warmed up to 110～120 ℃; If the connection material that step (1) adds is too much, printing ink is rare excessively, influences the dispersed with stirring effect; After temperature lowers; Remaining connection material is added in the printing ink retrogradation again, and it is easier to grind in the back step.
Connect material: rosin modified phenolic resin is the sylvic oil or the gummy oil of staple, and other conventional material that connects of this area.
The friction resistant auxiliary agent: staple is a polyethylene wax, and other conventional friction resistant auxiliary agent of this area.
Siccative: 2-ethylhexoate siccative, and other conventional drying agent of this area, accelerate the rate of drying of printing ink on printing sheets.
Dispersion agent: the verivate of Ammonia or phthalocyanine blue.
Inhibitor: be TPV series inhibitor, prevent printing ink in printing process at ink fountain and roll surface skinning.
Ink oil is 270～315 ℃ MO for the boiling range scope.
DM is the abbreviation of Direct Milled, and DM pigment is to name with the making method of this kind pigment.
DM method: Direct Milled Production Method.
DM pigment: Direct Milled pigment is the commercially available prod.
Adopt the beneficial effect that technique scheme produced to be: the working method of blue oil China ink of the present invention is easy, and production efficiency is higher, and China ink property is better.Production process need not draining, and output is higher.The resin that the blue pigment use of DM printing ink is used is as the treatment agent of pigment; Resin demand generally accounts for 1/3rd of pigment total amount, and its configuration of surface of blue pigment that makes in this way is Powdered, has avoided the trouble of draining; Farthest reduced pollution to environment; And since pigment through plastic resin treatment, so DM pigment possesses the characteristic same with filter cake, good dispersivity, the ink that makes is high, depth of shade is high, transparency good.The cost of manufacture of the blue pigment of DM is also relatively low, and production efficiency is high.
The middle stirring of step (2) also is warming up to 110～120 ℃, can keep the color of ink vividness, if the too high color excessive variation of temperature can influence the vividness of ink colors.
Embodiment
Embodiment 1
A kind of offset printing blue oil China ink method of manufacture may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 30 weight parts, 20 weight parts and 10 weight parts is put in the kneader stirred, temperature is 60 ℃;
(2) stir and be warming up to 120 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 15 weight parts, the dispersion agent of 2 weight parts and the friction resistant auxiliary agent of 3 weight parts and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller, basic black rolling temperature is 60 ℃, and pressure is 50MPa;
(4) ink oil, the inhibitor of 1 weight part and the siccative of 2 weight parts of adding 10 weight parts in the basic China ink after rolling.
The blue pigment of DM is that sky, Tianjin wing printing material ltd produces.
Embodiment 2
A kind of offset printing blue oil China ink method of manufacture may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 25 weight parts, 30 weight parts and 1 weight part is put in the kneader stirred, temperature is 70 ℃;
(2) stir and be warming up to 110 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 10 weight parts, the dispersion agent of 3 weight parts and the friction resistant auxiliary agent of 1 weight part and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller, basic black rolling temperature is 70 ℃, and pressure is 30MPa;
(4) ink oil, the inhibitor of 0.1 weight part and the siccative of 0.1 weight part of adding 1 weight part in the basic China ink after rolling.
The blue pigment of DM is that sky, Tianjin wing printing material ltd produces.
Embodiment 3
A kind of offset printing blue oil China ink method of manufacture may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 40 weight parts, 10 weight parts and 15 weight parts is put in the kneader stirred, temperature is 50 ℃;
(2) stir and be warming up to 115 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 20 weight parts, the dispersion agent of 0.1 weight part and the friction resistant auxiliary agent of 5 weight parts and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller, basic black rolling temperature is 50 ℃, and pressure is 60MPa;
(4) ink oil, the inhibitor of 2 weight parts and the siccative of 3 weight parts of adding 15 weight parts in the basic China ink after rolling.
The blue pigment of DM is that sky, Tianjin wing printing material ltd produces.
Embodiment 4
A kind of offset printing blue oil China ink method of manufacture may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 35 weight parts, 25 weight parts and 10 weight parts is put in the kneader stirred, temperature is 65 ℃;
(2) stir and be warming up to 120 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 15 weight parts and the dispersion agent of 2.5 weight parts and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller, basic black rolling temperature is 65 ℃, and pressure is 55MPa;
(4) ink oil, the inhibitor of 1.5 weight parts and the siccative of 2.5 weight parts of adding 12 weight parts in the basic China ink after rolling.
The blue pigment of DM is that sky, Tianjin wing printing material ltd produces.
Blue oil China ink working method of the present invention and dry method and wet type method for producing correlation data such as following table 1:
Table 1
| The parameter project | Blue oil China ink working method of the present invention | Dry method | Wet method |
| Dispersed | Good | Difference | Good |
| Whether need draining | Do not need | Do not need | Need |
| Produce man-hour | 1～2 hour/100 kilograms | 2～3 hours/100 kilograms | 1～2 hour/100 kilograms |
| Manufacturing cost | Low | High | Low |
Claims (4)
1. an offset printing blue oil China ink method of manufacture is characterized in that, may further comprise the steps:
(1) lime carbonate of the connection material of the blue pigment of the DM of 25～40 weight parts, 10～30 weight parts and 1～15 weight part is put in the kneader stirred;
(2) stir and be warming up to 110～120 ℃, it is identical with the standard specimen color that the blue pigment of DM fully is dispersed to, and adds the connection material of 10～20 weight parts and the dispersion agent of 0.1～3 weight part and obtain Ji Mo;
(3) said base China ink is rolling to fineness≤15 μ m on three-roller;
(4) add the ink oil of 1～15 weight part, the inhibitor of 0.1～2 weight part and the siccative of 0.1～3 weight part in the basic China ink after rolling.
2. a kind of according to claim 1 offset printing blue oil China ink method of manufacture is characterized in that each material temperature is 50～70 ℃ in the middle kneader of step (1).
3. a kind of according to claim 1 offset printing blue oil China ink method of manufacture is characterized in that, also adds the friction resistant auxiliary agent of 1～5 weight part in the step (2).
4. a kind of according to claim 1 offset printing blue oil China ink method of manufacture is characterized in that basic black rolling temperature is 50～70 ℃ in the step (3), and pressure is 30～60MPa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210063293.9A CN102585591B (en) | 2012-03-12 | 2012-03-12 | Method for making blue offset printing ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210063293.9A CN102585591B (en) | 2012-03-12 | 2012-03-12 | Method for making blue offset printing ink |
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| CN102585591A true CN102585591A (en) | 2012-07-18 |
| CN102585591B CN102585591B (en) | 2014-06-04 |
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| CN201210063293.9A Expired - Fee Related CN102585591B (en) | 2012-03-12 | 2012-03-12 | Method for making blue offset printing ink |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103013227A (en) * | 2012-12-27 | 2013-04-03 | 茂名阪田油墨有限公司 | Planographic printing ink containing high-concentration calcium carbonate and preparation method thereof |
| CN103045004A (en) * | 2012-12-27 | 2013-04-17 | 茂名阪田油墨有限公司 | Preparation method for producing basic ink of printing ink through staged kneading |
| CN103087587A (en) * | 2013-02-06 | 2013-05-08 | 茂名阪田油墨有限公司 | Preparation method for producing calcium-carbonate-containing lithographic ink through one-step kneading method |
| CN106590147A (en) * | 2016-12-06 | 2017-04-26 | 韦保祥 | Modified ink containing zirconium 2-ethylhexanoate assistant and preparation technology thereof |
| CN106752312A (en) * | 2016-12-07 | 2017-05-31 | 韦保祥 | A kind of modified plant oil-based ink composition |
| CN106752305A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of modified ink composite and its technique |
| CN106752311A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of ink composite for adding 2 ethyl hexanoic acid bismuth |
| CN106752304A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of ink for adding 2 ethyl hexanoic acid aluminium and preparation method thereof |
| CN113773696A (en) * | 2021-10-09 | 2021-12-10 | 龙港市鑫鑫印刷机械有限公司 | Printing ink and preparation method thereof |
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| SU1708821A1 (en) * | 1988-12-26 | 1992-01-30 | Всесоюзный Научно-Исследовательский Институт Комплексных Проблем Полиграфии | Dye for offset and relief printing |
| JP2001293889A (en) * | 2000-04-11 | 2001-10-23 | Seiko Epson Corp | Print by combination of pigment ink and dye ink |
| CN101284963A (en) * | 2007-12-17 | 2008-10-15 | 上海牡丹油墨有限公司 | Water-expelling production process for offset printing magenta printing ink |
| CN101319106A (en) * | 2007-06-07 | 2008-12-10 | 鹤壁百运佳大豆油墨科技有限公司 | Hot-set soybean oil resin lithographic plate offset printing ink for rotary machine |
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2012
- 2012-03-12 CN CN201210063293.9A patent/CN102585591B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1708821A1 (en) * | 1988-12-26 | 1992-01-30 | Всесоюзный Научно-Исследовательский Институт Комплексных Проблем Полиграфии | Dye for offset and relief printing |
| JP2001293889A (en) * | 2000-04-11 | 2001-10-23 | Seiko Epson Corp | Print by combination of pigment ink and dye ink |
| CN101319106A (en) * | 2007-06-07 | 2008-12-10 | 鹤壁百运佳大豆油墨科技有限公司 | Hot-set soybean oil resin lithographic plate offset printing ink for rotary machine |
| CN101284963A (en) * | 2007-12-17 | 2008-10-15 | 上海牡丹油墨有限公司 | Water-expelling production process for offset printing magenta printing ink |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103013227A (en) * | 2012-12-27 | 2013-04-03 | 茂名阪田油墨有限公司 | Planographic printing ink containing high-concentration calcium carbonate and preparation method thereof |
| CN103045004A (en) * | 2012-12-27 | 2013-04-17 | 茂名阪田油墨有限公司 | Preparation method for producing basic ink of printing ink through staged kneading |
| CN103013227B (en) * | 2012-12-27 | 2014-06-18 | 茂名阪田油墨有限公司 | Planographic printing ink containing high-concentration calcium carbonate and preparation method thereof |
| CN103045004B (en) * | 2012-12-27 | 2014-06-18 | 茂名阪田油墨有限公司 | Preparation method for producing basic ink of printing ink through staged kneading |
| CN103087587A (en) * | 2013-02-06 | 2013-05-08 | 茂名阪田油墨有限公司 | Preparation method for producing calcium-carbonate-containing lithographic ink through one-step kneading method |
| CN103087587B (en) * | 2013-02-06 | 2014-10-15 | 茂名阪田油墨有限公司 | Preparation method for producing calcium-carbonate-containing lithographic ink through one-step kneading method |
| CN106590147A (en) * | 2016-12-06 | 2017-04-26 | 韦保祥 | Modified ink containing zirconium 2-ethylhexanoate assistant and preparation technology thereof |
| CN106752305A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of modified ink composite and its technique |
| CN106752311A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of ink composite for adding 2 ethyl hexanoic acid bismuth |
| CN106752304A (en) * | 2016-12-06 | 2017-05-31 | 韦保祥 | A kind of ink for adding 2 ethyl hexanoic acid aluminium and preparation method thereof |
| CN106752312A (en) * | 2016-12-07 | 2017-05-31 | 韦保祥 | A kind of modified plant oil-based ink composition |
| CN113773696A (en) * | 2021-10-09 | 2021-12-10 | 龙港市鑫鑫印刷机械有限公司 | Printing ink and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN102585591B (en) | 2014-06-04 |
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Granted publication date: 20140604 Termination date: 20160312 |