CN102585222B - 一种热塑性聚酰亚胺材料及用此材料制备挠性覆铜板的方法 - Google Patents
一种热塑性聚酰亚胺材料及用此材料制备挠性覆铜板的方法 Download PDFInfo
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- CN102585222B CN102585222B CN201210050178.8A CN201210050178A CN102585222B CN 102585222 B CN102585222 B CN 102585222B CN 201210050178 A CN201210050178 A CN 201210050178A CN 102585222 B CN102585222 B CN 102585222B
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- tpi
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- thermoplastic polyimide
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- monomer
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- 229920006259 thermoplastic polyimide Polymers 0.000 title claims abstract description 54
- 239000000463 material Substances 0.000 title claims abstract description 22
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title abstract description 31
- 238000000034 method Methods 0.000 title abstract description 19
- 229910052802 copper Inorganic materials 0.000 title abstract description 18
- 239000010949 copper Substances 0.000 title abstract description 18
- 150000004985 diamines Chemical class 0.000 claims abstract description 8
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 20
- 239000000178 monomer Substances 0.000 claims description 20
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 18
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 13
- GTDPSWPPOUPBNX-UHFFFAOYSA-N ac1mqpva Chemical compound CC12C(=O)OC(=O)C1(C)C1(C)C2(C)C(=O)OC1=O GTDPSWPPOUPBNX-UHFFFAOYSA-N 0.000 claims description 12
- 229920005575 poly(amic acid) Polymers 0.000 claims description 12
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 9
- NSGXIBWMJZWTPY-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropane Chemical compound FC(F)(F)CC(F)(F)F NSGXIBWMJZWTPY-UHFFFAOYSA-N 0.000 claims description 8
- UKJLNMAFNRKWGR-UHFFFAOYSA-N cyclohexatrienamine Chemical group NC1=CC=C=C[CH]1 UKJLNMAFNRKWGR-UHFFFAOYSA-N 0.000 claims description 8
- QRYTXFUBAZNNBP-UHFFFAOYSA-N 1-ethoxy-4-phenylbenzene Chemical group C1=CC(OCC)=CC=C1C1=CC=CC=C1 QRYTXFUBAZNNBP-UHFFFAOYSA-N 0.000 claims description 7
- YVNRUPSDZZZUQJ-UHFFFAOYSA-N [O].NC1=CC=CC=C1 Chemical compound [O].NC1=CC=CC=C1 YVNRUPSDZZZUQJ-UHFFFAOYSA-N 0.000 claims description 6
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 5
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 4
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 4
- 239000001273 butane Substances 0.000 claims description 4
- ANSXAPJVJOKRDJ-UHFFFAOYSA-N furo[3,4-f][2]benzofuran-1,3,5,7-tetrone Chemical compound C1=C2C(=O)OC(=O)C2=CC2=C1C(=O)OC2=O ANSXAPJVJOKRDJ-UHFFFAOYSA-N 0.000 claims description 4
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 4
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims description 3
- 125000003983 fluorenyl group Chemical class C1(=CC=CC=2C3=CC=CC=C3CC12)* 0.000 claims description 3
- 239000012943 hotmelt Substances 0.000 claims description 3
- HLBLWEWZXPIGSM-UHFFFAOYSA-N 4-Aminophenyl ether Chemical compound C1=CC(N)=CC=C1OC1=CC=C(N)C=C1 HLBLWEWZXPIGSM-UHFFFAOYSA-N 0.000 claims description 2
- VQVIHDPBMFABCQ-UHFFFAOYSA-N 5-(1,3-dioxo-2-benzofuran-5-carbonyl)-2-benzofuran-1,3-dione Chemical compound C1=C2C(=O)OC(=O)C2=CC(C(C=2C=C3C(=O)OC(=O)C3=CC=2)=O)=C1 VQVIHDPBMFABCQ-UHFFFAOYSA-N 0.000 claims 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 claims 1
- 238000010128 melt processing Methods 0.000 claims 1
- 229920001721 polyimide Polymers 0.000 abstract description 27
- 239000000843 powder Substances 0.000 abstract description 17
- 238000006243 chemical reaction Methods 0.000 abstract description 16
- 239000011889 copper foil Substances 0.000 abstract description 15
- 238000012545 processing Methods 0.000 abstract description 6
- 229920001577 copolymer Polymers 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 150000008065 acid anhydrides Chemical class 0.000 abstract description 2
- 229920001187 thermosetting polymer Polymers 0.000 abstract description 2
- BEKFRNOZJSYWKZ-UHFFFAOYSA-N 4-[2-(4-aminophenyl)-1,1,1,3,3,3-hexafluoropropan-2-yl]aniline Chemical compound C1=CC(N)=CC=C1C(C(F)(F)F)(C(F)(F)F)C1=CC=C(N)C=C1 BEKFRNOZJSYWKZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000004952 Polyamide Substances 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- 238000005476 soldering Methods 0.000 abstract 1
- 239000004642 Polyimide Substances 0.000 description 22
- 239000012528 membrane Substances 0.000 description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 14
- 239000005357 flat glass Substances 0.000 description 14
- 238000003756 stirring Methods 0.000 description 14
- 238000001291 vacuum drying Methods 0.000 description 14
- 238000000576 coating method Methods 0.000 description 12
- 150000001875 compounds Chemical class 0.000 description 9
- 239000012046 mixed solvent Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 7
- 239000008367 deionised water Substances 0.000 description 7
- 229910021641 deionized water Inorganic materials 0.000 description 7
- 238000011010 flushing procedure Methods 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- 239000011521 glass Substances 0.000 description 6
- 238000011161 development Methods 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000010030 laminating Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 230000009977 dual effect Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000003825 pressing Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011810 insulating material Substances 0.000 description 2
- 229920003223 poly(pyromellitimide-1,4-diphenyl ether) Polymers 0.000 description 2
- 229910000679 solder Inorganic materials 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- CMQUQOHNANGDOR-UHFFFAOYSA-N 2,3-dibromo-4-(2,4-dibromo-5-hydroxyphenyl)phenol Chemical compound BrC1=C(Br)C(O)=CC=C1C1=CC(O)=C(Br)C=C1Br CMQUQOHNANGDOR-UHFFFAOYSA-N 0.000 description 1
- -1 4-ethoxybiphenyl phenol-3, 5-diaminobenzoic acid ester Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 150000003949 imides Chemical class 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920006267 polyester film Polymers 0.000 description 1
- 239000009719 polyimide resin Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Laminated Bodies (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Abstract
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CN201210050178.8A CN102585222B (zh) | 2012-02-25 | 2012-02-25 | 一种热塑性聚酰亚胺材料及用此材料制备挠性覆铜板的方法 |
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CN102585222B true CN102585222B (zh) | 2014-05-07 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP7048020B2 (ja) | 2017-01-31 | 2022-04-05 | エルジー・ケム・リミテッド | ポリイミド及びこれより製造されたフレキシブルディスプレイ用ポリイミドフィルム |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102993748B (zh) * | 2012-10-19 | 2014-10-08 | 南京理工大学 | 聚酰亚胺薄膜及利用该薄膜制备两层柔性覆铜板的方法 |
CN103192563A (zh) * | 2013-04-24 | 2013-07-10 | 昆山翰辉电子科技有限公司 | 软性印刷电路板用复合式双面铜箔基板 |
CN103739842B (zh) * | 2013-12-20 | 2016-08-31 | 深圳瑞华泰薄膜科技有限公司 | 一种热塑性聚酰亚胺及用其制备挠性覆铜板的方法 |
CN106139936B (zh) * | 2016-06-29 | 2018-09-11 | 常州市阳光药业有限公司 | 聚酰亚胺气体分离膜及其制备方法和应用 |
EP3519504A4 (en) * | 2016-09-28 | 2020-05-20 | Dow Global Technologies LLC | SOLVENT SYSTEMS FOR THE SYNTHESIS OF POLY (AMIC ACID) AND POLYIMIDE POLYMERS |
CN106519685B (zh) * | 2016-11-08 | 2019-06-04 | 南京中鸿润宁新材料科技有限公司 | 一种聚酰亚胺材料、其制备方法和应用 |
CN109651631B (zh) * | 2018-01-18 | 2020-09-25 | 深圳瑞华泰薄膜科技股份有限公司 | 一种低介质损耗的聚酰亚胺薄膜 |
CN109438702A (zh) * | 2018-09-29 | 2019-03-08 | 苏州市新广益电子有限公司 | 一种用于fpc行业的tpi薄膜及其制备和加工方法 |
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JP7048020B2 (ja) | 2017-01-31 | 2022-04-05 | エルジー・ケム・リミテッド | ポリイミド及びこれより製造されたフレキシブルディスプレイ用ポリイミドフィルム |
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Effective date of registration: 20190306 Address after: No. 18 Yinchun Road, Qixia District, Nanjing, Jiangsu Province, 210028 Patentee after: Nanjing Hongrun Ning new Mstar Technology Ltd Address before: 316021 No. 66 Honglu Avenue, Zhoushan Economic Development Zone, Zhejiang Province (No. 1 Factory of Kechuang Center) Patentee before: Zhoushan Weite New Material Technology Co.,Ltd. |
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Effective date of registration: 20201202 Address after: 226600, Jiangsu County, Nantong province Haian corner town industrial concentration area Patentee after: Nantong Jinchao Machine Tool Co.,Ltd. Address before: The spring road in Qixia District of Nanjing City, Jiangsu Province, No. 18 210028 Patentee before: NANJING ZHONGHONG RUNNING NEW MATERIAL TECHNOLOGY Co.,Ltd. |
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Granted publication date: 20140507 Termination date: 20210225 |
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