CN102551059A - Purslane oral liquid and preparation method thereof - Google Patents
Purslane oral liquid and preparation method thereof Download PDFInfo
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- CN102551059A CN102551059A CN2012100257420A CN201210025742A CN102551059A CN 102551059 A CN102551059 A CN 102551059A CN 2012100257420 A CN2012100257420 A CN 2012100257420A CN 201210025742 A CN201210025742 A CN 201210025742A CN 102551059 A CN102551059 A CN 102551059A
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Abstract
The invention discloses purslane oral liquid and a preparation method of the oral liquid. The oral liquid comprises the following components in percentage by weight: 10% of purslane, 0.07% of cinnamon, 0.03% of clove, 0.07% of polygonatum and the balance of purified water. The method comprises the steps of adding cleaned main material purslane in clean water ten times weight of the purslane, soaking for 6h and boiling for 2h at a temperature of 80 DEG C; adding auxiliary materials comprising the cinnamon, the clove and the polygonatum into the main material, wherein the polygonatum should be soaked for 24h and peeled before being added into the main material and the cinnamon and the clove should be soaked for 30min in clear water before being added into the main material; filtering the juice prepared through boiling and removing dregs by utilizing a duplex filter to obtain clear juice, sterilizing the clear juice for 15min at a temperature of 121 DEG C, rapidly cooling to 40 DEG C, and aseptically filling to obtain the purslane oral liquid. The preparation method and the obtained product have the advantages of simplicity, wide practicality, suitability in industrial production and the like.
Description
Invention field
The present invention relates to oral liquid and preparation method thereof technical field, concrete, the present invention relates to a kind of purslane oral liquid and preparation method thereof technical field.
Background technology
Purslane (Portulaca oleracea L); Another name longevity greens/mustard green, five-element's grass, horse amaranth Lay, long life dish; Belong to annual meat herbaceous plant; It is cold in nature, flavor is sour, and richness is closed unrighted acid, vitamin C, E and carrotene, is one of 78 kinds of integration of drinking and medicinal herbs wild plants of China Ministry of Public Health regulation.And malic acid, glutamic acid and asparatate, oxalic acid etc., calcium, phosphorus, iron, and zinc, copper equal size also higher.In addition, also contain more potassium element, multiple sylvite such as potassium nitrate, potassium sulfate, potassium binoxalate are wherein arranged.Anti-inflammation, reducing blood lipid, antiatherosclerosis, enhance immunity power, the anti-ageing effect of waiting for a long time are arranged; Have clearing heat and detoxicating, clearing damp and only be with effect; Be applicable to damp invasion of lower energizer, band down look yellow, sticky flavor is smelly, oliguria with yellow urine, thirsty bitter taste, red tongue with yellowish fur, arteries and veins cunning person, also can be used for diarrhea due to damp-heat, dysentery etc.Ability expelling parasite effect is applicable to infantile ancylostomiasis.And have clearing heat and detoxicating, antidiarrheal dysentery, remove intestines dirt, beneficial gas qi-restoratives effect, be applicable to the treatment protracted dysentery.Be that a kind of the health care is worth very high herbaceous plant.Anti-inflammation, reducing blood lipid, antiatherosclerosis, enhance immunity power, the anti-ageing effect of waiting for a long time are arranged, and are that a kind of the health care is worth very high edible wild herbs.Now, people normally are made into dish through the kitchen cooking and eat, and this is cumbersome, and in gastronomical process, many active ingredients of purslane are prone to be destroyed, and influence health-care effect.
Existing bibliographical information, purslane has many drug effects and pharmacological function, concrete main the report as follows:
1, antibacterial action Qu Shuyan report purslane ethanol extract is paid the dysentery characterized by blood in the stool bacillus to will Hayes and Fo Shi has significant inhibitory effect.Water decoction all has inhibitory action to will Hayes, Song Nei Shi, Si Shi and Fei Shi shigella dysenteriae, but shigella dysenteriae can produce the tangible resistance to the action of a drug after in purslane meat soup, repeatedly going down to posterity.Alcohol leaching thing or water decoction also have inhibitory action to Escherichia coli, typhoid bacillus and staphylococcus aureus; To some pathomycete such as Microsporon audouini etc., different inhibitory action is arranged also.To tubercle bacillus unrestraint effect; To mouse peritoneal injection coli-infection, all invalid with residue decocting liquid after alcohol extract or the alcohol extracting.Ma Muying in 1992 has reported the wild purslane of selling the food market, the Shenzhen bacteriostasis to multiple common food pollution bacterium.The result shows that purslane all has stronger inhibitory action to multiple common food pollution bacterium.Still have certain bacteriostasis even be diluted to 12.5% concentration.Especially to many bacteriums; Like Escherichia coli; Bacteriostasis such as salmonella, proteus, Shigella, staphylococcus aureus, bacillus subtilis, bacillus cereus are stronger, and Sarcina lutea is not suppressed, and are not obvious to mustiness bacillus inhibitory action.Purslane also has inhibitory action to some moulds, as also stronger to inhibitory action such as Mucor racemosus, red mould, Alternaria, aspergillus flavus; And bread mold, Trichoderma viride, aspergillus niger are not had bacteriostasis, saccharomycete there is not bacteriostasis.
2, to the effect of smooth muscle Qu Shuyan report in 1985 purslane extract (water boiling concentration add alcohol remove deposition process) and the crystalline potassium chloride that separates thereof to cavy, rat and rabbit exsomatize, all there is tangible excitation in the uterus on the throne of dog.Purslane injection 2ml (being equivalent to crude drug 5-10g) be by force than using ergometrine 0.2mg, use pituitrin 10 units to be a little less than; Then similar with 4-6ml with pituitrin 10 units.The potassium chloride crystallization that from purslane, separates has tangible contraction to the isolated rat ileum, and it makes intensity and PGE1, and 200ug, neostigmine 0.25mg are similar, and 20% decoction 0.2ml has inhibitory action to the small intestine of guinea pig that exsomatizes.After this foreign scholar SunbhanichM etc. has studied water juice that the purslane fresh plant presses and extracting in boiling water thing to the atrium of exsomatizing the cavy enterocinesia and exsomatizing and the influence of tracheae contraction.The result shows that for stripped ileum, water juice and extracting in boiling water thing all make tensity, amplitude, the frequency of contraction strengthen.This effect and acetylcholine are similar, and are dose dependents.But the tensity of contraction and the increase of wriggling can be blocked by atropine slightly.Two types preparation all demonstrates the effect to heart myocardial contractive power and contraction rate of dose dependent, and to the relexation of isolated tracheal bar.These effects are similar with the effect that isoprel produces, and can be blocked fully by inderal (2.1x10 (5) mol/L).Purslane can be respectively as relaxant and cardiotonic to this medicine of exercising result prompting in isolated guinea pig ileum and atrium, and it can be used for treating bronchial astehma to bronchial dilating effect.
3, to the effect of skeletal muscle: OkwuasabaF equals report purslane water extract in 1987 has unique making to exsomatize and in the characteristic of body skeletal muscle diastole, and the skeletal muscle that this water extract part is used for due to the spinal cord injury is tetanic effectively.The author has further studied the pharmacologically active of the various extracts of purslane again, and contrasts with water extract.The result shows; With regard to regard to the inhibitory action of big white mouse nervus phrenicus one hemidiaphragm flesh (MS and NS) and frog rectus aabdominis sample; The effect of the various extracts of purslane (methyl alcohol (MEE), ether (DEE) and dialyzable (DIF) extract) is similar and also quite similar with the effect of water extract (AEE).
4, to the effect in uterus: Li Shourou equals report in 1979, and purslane has two kinds of opposite effects to animal uterus, and one is excitation, is the potassium chloride of getting in the purslane; One is inhibitory action, is the organic principle in the purslane.Sylvite mainly is present in the stem, and organic principle mainly is present in the leaf.
5, to the effect of cardiovascular system: Lanzhou medical college report, 20% water decoction 0.2ml has inhibitory action to isolated frog heart.To anesthesia dog intravenous injection 3ml/ only, breathing, blood pressure, heartbeat all do not have obvious influence.
6, short ulcer healing effect: national Chinese herbal medicine compilation report, these article contain abundant vitamin A appearance material, so can promote epithelial physiological function to be tending towards normal.
7, other effect: the water-soluble and fat-soluble extract of report purslanes such as StefanovZH can prolong the life of severe diabetes mellitus rat and rabbit due to the alloxan, but does not influence blood sugar level, and the prompting purslane extract can improve the disorder of lipid-metabolism.
The historical summary record, integration of drinking and medicinal herbs.Purslane is a good medicine, is again ticbit.China ancients claim that purslane is " longevity greens/mustard green "; Purslane also is a conventional Chinese medicine; According to the record of ancient medical book such as Northern and Southern Dynasties' " Mingyi Bielu ", the Tang Dynasty " dietetic materia medica ", Ming Dynasty's Compendium of Material Medica, purslane has " clearing heat and detoxicating, the blood detumescence of loosing, end dysentery " effect.China's fresh purslane commonly used among the people and decocting liquid are treated chordapsus, dysentery, diarrhoea etc.Purslane have the title of " natural antibiotics ".Modern medicine shows that purslane mainly contains reducing blood lipid, anti-inflammation, enhance immunity, the anti-ageing effect of waiting for a long time except that the above-mentioned medicinal function of proof purslane.It has treatment, adjusting, nutrition three big functions, and these functions make it to produce comprehensive effect in human body, eliminate disease and prolong life, and expel pathogenetic factors and reinforce antipathogenetic qi.At present the development and use mode of purslane mainly is directly edible or is processed into semi-finished product, is that the drink processed of raw material is also rare with the purslane, particularly to can effectively keep purslane effectively the property of medicine prepare oral liquid and do not appear in the newspapers.
Summary of the invention
Show that through the comprehensive comparative analysis of prior art bibliographical information has been seen in the research of domestic relevant purslane oral liquid, but do not see bibliographical information with the research that the present invention fills a prescription the purslane oral liquid identical.The present invention provides a kind of purslane oral liquid and preparation method thereof.The present invention uses orthogonal experiment to optimize the preparation technology of purslane oral liquid, and the purslane active material more is prone to stripping, has reduced Polysaccharide from Portulaca oleracea and active ingredient loss, and guarantees the quality of purslane oral liquid through high pressure steam sterilization.
Particularly, the invention provides a kind of purslane oral liquid prescription, according to weight percent meter, this oral liquid component does, purslane 10%, and Chinese cassia tree 0.7 ‰, cloves 0.3 ‰, Ou Yuzhu 0.7 ‰, and all the other are pure water.
Simultaneously, the present invention further provides a kind of preparation method of purslane oral liquid, and concrete preparation method's step is following:
(1) selecting major ingredient for use is purslane, and the clean water that the purslane of cleaning is added 10 times of weight soaked 6 hours, and back 80 degree decoct 2 hours; The employing auxiliary material is Chinese cassia tree, cloves, Ou Yuzhu, and after its Central European radix polygonati officinalis will be soaked 24 hours earlier, the decortication back added in the major ingredient; Chinese cassia tree, cloves are soaked in clear water after 30 minutes and add in the major ingredient.
(2) juice that decocts above-mentioned preparation obtains juice clearly through the duplex strainer filter cleaner.
(3) adopt 121 degree sterilizations 15 minutes, be quickly cooled to 40 degree.
(4) behind sterile filling, prepare the purslane oral liquid.
Through the concrete summary of the invention of embodiment of the present invention, can reach following effect:
The present invention adopts the mode that decocts to get juice; Juice is got in traditional fragmentation with respect to the prior art report, and active material more is prone to stripping, for reducing the loss of Polysaccharide from Portulaca oleracea; Improve to alcohol precipitation clarification process in the prior art, the present invention adopts duplex strainer to carry out filtered juice.It is big to the present invention is directed in the present research purslane active ingredient loss simultaneously; The problem that sanitary standard is difficult up to standard; The utilization orthogonal experiment has been optimized the preparation technology of purslane oral liquid, reduces active ingredient loss, and guarantees the quality of purslane oral liquid through high pressure steam sterilization.
Through existing purslane oral liquid fabricating technology contrast, aspect advantages such as purslane oral liquid provided by the invention and preparation method thereof has simply, practical, suitable suitability for industrialized production.Through orthogonal optimization preparation technology, reach and practice thrift power consumption, reduce purslane active material work in-process and lose in a large number, guarantee the effect of food safety and sanitation.
Description of drawings:
Fig. 1 is shown as the process chart of preparation purslane oral liquid.
Fig. 2 is shown as the influence of amount of water to the purslane oral liquid.
Fig. 3 is shown as the influence of the time of decocting to the purslane oral liquid.
Fig. 4 is shown as the influence of cloves addition to the purslane oral liquid.
The specific embodiment
Below, lift embodiment the present invention is described, still, the present invention is not limited to following embodiment.In addition, in following explanation, if no special instructions, % all refers to the m/m mass percent.
Purslane: the gloomy agricultural development in source, Xinjiang Co., Ltd provides; Ou Yuzhu, cloves, Chinese cassia tree: pharmacy buys; Jacketed pan; Rotary Evaporators; The sterile working platform; Autoclave.
All reagent selected for use among the present invention and instrument all are well known selecting for use, but do not limit enforcement of the present invention, and other reagent more well known in the art and equipment are all applicable to the enforcement of the following embodiment of the present invention.
Embodiment one: the preparation of purslane oral liquid
Referring to accompanying drawing 1, preparation purslane oral liquid concrete steps are following:
1, selecting major ingredient for use is purslane, and the clean water that 300g cleans 10 times of weight of purslane adding soaked 6 hours, and back 80 degree decoct 2 hours; Auxiliary material is Chinese cassia tree, cloves, Ou Yuzhu.After its Central European radix polygonati officinalis will be soaked 24 hours earlier, the decortication back added in the major ingredient.Chinese cassia tree, cloves are soaked in clear water and add in the major ingredient after 30 minutes; Adopt the major ingredient supplementary product consumption: purslane 300g, Chinese cassia tree 2g, cloves 1g, Ou Yuzhu 2g.
2, filter: the juice after decocting obtains juice clearly through the duplex strainer filter cleaner.
3, sterilization: use 121 degree sterilizations 15 minutes, be quickly cooled to 40 degree.
4, both got finished product purslane oral liquid behind the sterile filling.
Embodiment two: the preparation of purslane oral liquid
The purslane oral liquid prescription, according to weight percent meter, this oral liquid component does, purslane 10%, Chinese cassia tree 0.7 ‰, cloves 0.3 ‰, Ou Yuzhu 0.7 ‰, and all the other are pure water.
The preparation method of purslane oral liquid, concrete preparation method's step is following:
(1) selecting major ingredient for use is purslane, and the clean water that the purslane of cleaning is added 10 times of weight soaked 6 hours, and back 80 degree decoct 2 hours; The employing auxiliary material is Chinese cassia tree, cloves, Ou Yuzhu, and after its Central European radix polygonati officinalis will be soaked 24 hours earlier, the decortication back added in the major ingredient; Chinese cassia tree, cloves are soaked in clear water after 30 minutes and add in the major ingredient.
(2) juice that decocts above-mentioned preparation obtains juice clearly through the duplex strainer filter cleaner.
(3) adopt 121 degree sterilizations 15 minutes, be quickly cooled to 40 degree.
(4) behind sterile filling, prepare the purslane oral liquid.
Embodiment three: the definite and optimization of purslane oral liquid preparation technology parameter
1. experiment of single factor
Owing to the product special flavour that how much directly influences of cloves addition, so research decocts the time, amount of water, three factors of cloves addition are to the influence of purslane oral liquid
2. orthogonal experiment
Select L for use through experiment of single factor
9(3
4) orthogonal table preferred for preparation technology.
3. assay determination
The bacterium total bacteria count adopts GB/T 4789.2-2008, and the Escherichia coli counting adopts GB/T4789.38-2008
4. subjective appreciation
Form evaluation group by this area professional, respectively the purslane oral liquid is marked, every index total points each 10 minutes is calculated total points then.Aesthetic quality's standards of grading are seen table 1
Table 1 sensory evaluation scores standard
Result and analysis:
Table 2 orthogonal experiment factor level table
Table 3 quadrature is table as a result
| Factor | The A infusion time | The B amount of water | C cloves addition | Empty row | Sensory evaluation scores |
| Experiment 1 | 1 | 1 | ?1 | 1 | 28 |
| Experiment 2 | 1 | 2 | ?2 | 2 | 32 |
| Experiment 3 | 1 | 3 | ?3 | 3 | 28 |
| Experiment 4 | 2 | 1 | ?2 | 3 | 32 |
| |
2 | 2 | ?3 | 1 | 34 |
| Experiment 6 | 2 | 3 | ?1 | 2 | 30 |
| Experiment 7 | 3 | 1 | ?3 | 2 | 30 |
| Experiment 8 | 3 | 2 | ?1 | 3 | 34 |
| Experiment 9 | 3 | 3 | ?2 | 1 | 32 |
| ?k1 | 29.333 | 30 | ?30.667 | 31.333 | |
| ?k2 | 32 | 33.333 | ?32 | 30.667 | |
| ?k3 | 32 | 30 | ?30.667 | 31.333 | |
| ?R | 2.667 | 3.333 | ?1.333 | 0.666 |
Table 4 analysis of variance table
| Factor | Sum of square of deviations | The free degree | The F ratio | The F critical value | Conspicuousness |
| The infusion time | 14.222 | 2 | 15.998 | ?19 | |
| Amount of water | 22.222 | 2 | 24.997 | ?19 | * |
| The cloves addition | 3.556 | 2 | 4 | ?19 | |
| Error | 0.89 | 2 |
Annotate: * representes significant difference (p＜0.05)
5. best preparation technology's confirms
Found out that by Fig. 2 the amount of water when boiling purslane extract is the back downward trend that rises earlier to the influence of purslane oral liquid sense organ with the increase of rate of water added, when amount of water reaches 10 times of purslanes when heavy, the sensory evaluation scores of purslane oral liquid is optimum.
Find out that by Fig. 3 along with the prolongation that decocts the time, the sensory evaluation scores of purslane oral liquid is in rising trend, when greater than 120min, tends towards stability.
The increase of being found out the cloves addition by Fig. 4 result is little to the organoleptic effects variation of purslane oral liquid, and when the cloves addition reached 0.3 ‰, the sensory evaluation scores of purslane oral liquid was optimum.
By Fig. 2,3,4 sensory evaluation scores results select suitable factor level; Confirm that orthogonal array sees table 2; Can find out that by table 3 the optimal preparation technology that the orthogonal experiment theory draws is A2B2C2 or A3B2C2, promptly decocts 120min or 150min; The pure water that adds 10 times of raw material weights adds 0.3 ‰ cloves.Find out that from table 3 range analysis each factor is B＞A＞C to the primary and secondary relation of purslane oral liquid influence, amount of water is a principal element, and the infusion time, concentration of alcohol takes second place.
Find out that by table 4 The results of analysis of variance amount of water is remarkable to the influence of purslane oral liquid, and infusion time and cloves addition are not remarkable to the organoleptic effects of purslane oral liquid; Because it is not remarkable to the influence of purslane oral liquid to decoct the time, consider to decoct overlong time, can destroy the purslane active material to a certain extent; And power consumption; So optimal preparation technology is decided to be: decoct 120min, add the pure water of 10 times of raw material weights, add 0.3 ‰ cloves.
6. quality standard
The purslane oral liquid is a rufous liquid, and taste lubrication has the purslane peculiar taste, and is little bitter, and the cloves flavor is moderate.Total number of bacteria≤1000/g, Escherichia coli≤30/100g, pathogenic bacteria must not detect.
7. conclusion
Purslane oral liquid preparation technology parameter is: decoct 120min, add the pure water of 10 times of raw material weights, add 0.3 ‰ cloves.The purslane oral liquid of processing by above-mentioned prescription is rufous liquid, has the purslane peculiar taste, and is little bitter.
Claims (2)
1. a purslane oral liquid is characterized in that, according to weight percent meter, described oral liquid component does, purslane 10%, and Chinese cassia tree 0.7 ‰, cloves 0.3 ‰, Ou Yuzhu 0.7 ‰, and all the other are pure water.
2. the preparation method of a purslane oral liquid is characterized in that, the concrete preparation method's step of described oral liquid is following:
(1) selecting major ingredient for use is purslane, and the clean water that the purslane of cleaning is added 10 times of weight soaked 6 hours, and back 80 degree decoct 2 hours; The employing auxiliary material is Chinese cassia tree, cloves, Ou Yuzhu, and after its Central European radix polygonati officinalis will be soaked 24 hours earlier, the decortication back added in the major ingredient; Chinese cassia tree, cloves are soaked in clear water and add in the major ingredient after 30 minutes;
(2) juice that decocts above-mentioned preparation obtains juice clearly through the duplex strainer filter cleaner;
(3) adopt 121 degree sterilizations 15 minutes, be quickly cooled to 40 degree;
(4) behind sterile filling, prepare the purslane oral liquid.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103251003A (en) * | 2013-05-08 | 2013-08-21 | 新疆天山骄子食品有限责任公司 | Longevity vegetable nutrient oral solution and preparation process thereof |
| CN105381034A (en) * | 2015-12-24 | 2016-03-09 | 兰州古驰生物科技有限公司 | Traditional Chinese medicine health-care preparation used for conditioning leucorrhea disease |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103251003A (en) * | 2013-05-08 | 2013-08-21 | 新疆天山骄子食品有限责任公司 | Longevity vegetable nutrient oral solution and preparation process thereof |
| CN105381034A (en) * | 2015-12-24 | 2016-03-09 | 兰州古驰生物科技有限公司 | Traditional Chinese medicine health-care preparation used for conditioning leucorrhea disease |
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