CN102550544B - Dry alhagi sparsifolia alkaline essential oil and extraction and application thereof - Google Patents
Dry alhagi sparsifolia alkaline essential oil and extraction and application thereof Download PDFInfo
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- CN102550544B CN102550544B CN2011103900291A CN201110390029A CN102550544B CN 102550544 B CN102550544 B CN 102550544B CN 2011103900291 A CN2011103900291 A CN 2011103900291A CN 201110390029 A CN201110390029 A CN 201110390029A CN 102550544 B CN102550544 B CN 102550544B
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Abstract
The invention discloses dry alhagi sparsifolia alkaline essential oil. The dry alhagi sparsifolia alkaline essential oil is prepared by performing processes such as mixing, stirring, natural fermentation, natural precipitation and concentration and the like on 20 to 60 parts of dry alhagi sparsifolia powder, 2 to 5 parts of potassium hydroxide and 200 and 400 parts of water. The obtained dry alhagi sparsifolia alkaline essential oil is used for preparing crop antitranspirant. An extraction process for the dry alhagi sparsifolia alkaline essential oil has the advantages of simpleness, clearness and convenience for implementation and is extremely suitable for mass production; and the crop antitranspirant prepared from the dry alhagi sparsifolia alkaline essential oil has the advantages of obvious effects, no toxicity and no harm.
Description
Technical field
The present invention relates to a Plant Extracts, particularly, relate to dry camel thorn alkaline essential oil and its extraction process and purposes.
Background technology
Camel thorn is that pulse family, camel thorn belong to machaka, mainly is distributed in arid area, China inland, and there is distribution the whole area, Xinjiang, especially in the majority with South Sinkiang, the upper thorniness of main branch, leaf Long Circle, pollen redness, bloom June, most contain August, and every flower can be opened more than 20 days, the fruit of bearing pods, raceme, root system generally reaches 20 meters.Camel thorn can be a kind of drought-enduring plant of self-sow from desert and depths, Gobi desert groundwater absorbing part and nutrition, has the characteristic of cold-resistant, drought resisting, salt tolerant and anti-blown sand.
Current research shows, contains the nutrient component that a lot of flavonoids, alkaloids etc. are useful to biology in camel thorn, at medical domain, and the record of existing camel thorn fungistatic effect.But the utilization to camel thorn in prior art also only is confined to check winds and fix drifting sand mostly, as animals forage, and do not find the application of other deeper degrees.
In addition, in the arid area of camel thorn growth, the plant drought Journal of Sex Research is one of major issue of various countries scientist concern always.Plant corpus mainly obtains moisture by flourishing root system from soil, in these moisture, the metabolism of the water of 1% left and right for self is only arranged, remaining moisture has lost by transpiration, the most water that lose are discharged by pore, therefore, the transpiration of reduction plant has extremely important effect for drought resisting.In this field, antitranspirant is aspect reduction plant corpus transpiration, having played great role, and particularly in arid area, it has alleviated coercing that arid causes plant corpus to a certain extent.Antitranspirant commonly used as phenylmercuric acetate (PMA) be a kind of organic mercury, belong to lipophilic toxin, its residual drug effect through inhaling the people, eat, after skin absorbs, can cause huge infringement to human body, therefore, the composition of antitranspirant is needed improvement badly.
Summary of the invention
The technical problem to be solved in the present invention is to overcome existing defect, a kind of dry camel thorn alkaline essential oil is provided, and provide its extraction process, that this extraction process has advantages of is easy, clear, conveniently implement, be highly suitable for to produce in enormous quantities, and the antitranspirant of the crops that simultaneously prepare with dry camel thorn alkaline essential oil has advantages of successful, nontoxic.
In order to solve the problems of the technologies described above, the invention provides following technical scheme:
Dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 20-60 part;
Potassium hydroxide: 2-5 part;
Water: 200-400 part.
Preferably, the raw material proportioning that comprises following parts by weight:
Dry camel thorn powder: 30-50 part;
Potassium hydroxide: 3 parts;
Water: 300 parts.
Preferably, the raw material proportioning that comprises following parts by weight:
Dry camel thorn powder: 40 parts;
Potassium hydroxide: 3 parts;
Water: 300 parts.
Preferably, wherein:
The water content of described dry camel thorn powder≤5%, purity >=99%;
The purity of described potassium hydroxide >=99%, described purity is pure for analyzing.
Particularly, its content of organic matter>=30g/L, K
2O>=60g/L, PH is 7-9, water-insoluble≤5g/L.
The extraction process of dry camel thorn alkaline essential oil of the present invention comprises the following steps:
(1) by potassium hydroxide, temperature, be proportionally that the water of 25 ℃-35 ℃ adds reactor, more than stirring 30min;
(2) proportionally, dry camel thorn powder is added to reactor, more than stirring 20min;
(3) after stirring, spontaneous fermentation 60-80 hour under room temperature;
(4) after spontaneous fermentation, stir 1-3 hour, the concentrated 7-15 days of precipitation under 25 ℃-35 ℃, obtain the dry camel thorn alkaline essential oil of finished product.
The application of dry camel thorn alkaline essential oil of the present invention is the antitranspirant for the preparation of crops.
Dry camel thorn alkaline essential oil and extraction process thereof proposed by the invention have following beneficial effect:
1. dry camel thorn alkaline essential oil proposed by the invention has the effect that keeps and improve the hydrophilic and water retention capacity of plant cell, can prevent cell dehydration, make plant cell there is significant drought-resistant ability, active ingredient wherein can keep the stability of the interior hydrolase of plant corpus as RNA enzyme, protease, lipase, reduce the decomposition of large biological molecule, prevent that cytoplasma membrane is undermined.Simultaneously, it can make again cell have higher viscosity and elasticity, improves the cell water retention capacity by higher viscosity, the mechanical damage while by higher elasticity, preventing the cell dehydration.Under the protective effect of dry camel thorn alkaline essential oil, it is stable that the protoplasm structure has kept to a certain extent, avoided the disorder of cellular metabolism abnormal, makes photosynthesis and respiration still maintain normal level under drought condition.In addition, dry camel thorn alkaline essential oil can also provide sufficient potassium ion for plant.
2. the extraction process of dry camel thorn alkaline essential oil proposed by the invention is easy, clear, and convenient enforcement, be highly suitable for large batch of extraction.
3. dry camel thorn alkaline essential oil proposed by the invention is with after liquid potassium fulvate, abscisic acid mix, the transpiration that can be used for reducing crops as antitranspirant, this saving for the drought-resistant water-preserving ability that improves the arid area crops and water resource is significant.
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein, only for description and interpretation the present invention, is not intended to limit the present invention.
One, product and Preparation Example
Embodiment 1
Dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 20 parts;
Potassium hydroxide: 2 parts;
Water: 200 parts.
The extraction process of dry camel thorn alkaline essential oil comprises the following steps:
(1) water that is proportionally 25 ℃ by potassium hydroxide, temperature adds reactor, stirs 30min;
(2) proportionally, dry camel thorn powder is added to reactor, stir 20min;
(3) in reactor, spontaneous fermentation 60 hours;
(4) after spontaneous fermentation, stir 1 hour, 25 ℃ of natural sedimentations concentrate 15 days, obtain dry camel thorn alkaline essential oil.
Embodiment 2
Dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 60 parts;
Potassium hydroxide: 5 parts;
Water: 400 parts.
The extraction process of dry camel thorn alkaline essential oil comprises the following steps:
(1) water that is proportionally 35 ℃ by potassium hydroxide, temperature adds reactor, stirs 40min;
(2) proportionally, dry camel thorn powder is added to reactor, stir 30min;
(3) in reactor, spontaneous fermentation 70 hours;
(4) after spontaneous fermentation, stir 3 hours, 30 ℃ of natural sedimentations concentrate 10 days, obtain dry camel thorn alkaline essential oil.
Embodiment 3
Dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 40 parts;
Potassium hydroxide: 3 parts;
Water: 300 parts.
Wherein, the water content of dry camel thorn powder is 5%, and purity is 99%; Potassium hydroxide is for analyzing pure 99%.
The extraction process of dry camel thorn alkaline essential oil comprises the following steps:
(1) water that is proportionally 35 ℃ by potassium hydroxide, temperature adds reactor, stirs 40min;
(2) proportionally, dry camel thorn powder is added to reactor, stir 30min;
(3) in reactor, spontaneous fermentation 70 hours;
(4) after spontaneous fermentation, stir 3 hours, 30 ℃ of natural sedimentations concentrate 10 days, obtain dry camel thorn alkaline essential oil.
Dry its index of camel thorn alkaline essential oil made through above technique is as follows:
The content of organic matter is 35g/L, K
2O content 62g/L, PH is 8, water-insoluble is 3g/L.
Embodiment 4
Dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 50 parts;
Potassium hydroxide: 3 parts;
Water: 300 parts.
Wherein, the water content of dry camel thorn powder is 3%, and purity is 99%; Potassium hydroxide is for analyzing pure 99.5%.
The extraction process of dry camel thorn alkaline essential oil comprises the following steps:
(1) water that is proportionally 30 ℃ by potassium hydroxide, temperature adds reactor, stirs 50min;
(2) proportionally, dry camel thorn powder is added to reactor, stir 30min;
(3) in reactor, spontaneous fermentation 72 hours;
(4) after spontaneous fermentation, stir 2 hours, 35 ℃ of natural sedimentations concentrate 7 days, obtain dry camel thorn alkaline essential oil.
Dry its index of camel thorn alkaline essential oil made through above technique is as follows:
The content of organic matter is 38g/L, K
2O content 66g/L, PH is 7, water-insoluble is 4g/L.
Two, Application Example
Embodiment 5
By the dry camel thorn essential oil in embodiment 1 for the preparation of the crops antitranspirant, the component that its component is following parts by weight:
Liquid potassium fulvate: 496 parts;
Dry camel thorn alkaline essential oil: 496 parts;
Abscisic acid: 8 parts;
Above component fully mixes, and makes antitranspirant.
Under the normal water supply condition, the transpiration by this transpiration agent for reducing wheat, specific as follows:
Experimental group: spray the antitranspirant (400 times of dilute with waters) that the present embodiment makes;
Control group: spray phenylmercuric acetate on the market (PMA) identical with the experimental group volume, typical concentrations;
Blank group: spray the water with the experimental group equal volume.
Physiological status is in full accord before spraying for three selected wheats (every group of 40 strain wheats) of group, and under the same time identical conditions, its water-saving amount is measured, concrete numerical value is as shown in table 1: (illustrate: plant absorbs the moisture overwhelming majority of coming and is lost to external by transpiration, small part is only arranged for its vital movement, when its transpiration is suppressed, the also corresponding minimizing of moisture that plant absorbs, therefore, to three identical water of group pouring, measure its surplus water after certain hour, be scaled to the power that water-saving amount can judge transpiration).
Table 1
By table 1, can find out, the water consumption that sprays the experimental group of antitranspirant proposed by the invention is starkly lower than control group and blank group, and water-saving result is very obvious.By Observe and measure, the wheat physiological status of experimental group is all normal, and form there is no extremely.
Embodiment 6
By the dry camel thorn essential oil in embodiment 3 for the preparation of the crops antitranspirant, the component of the following parts by weight of its composition:
Liquid potassium fulvate: 500 parts;
Dry camel thorn alkaline essential oil: 500 parts;
Abscisic acid: 10 parts;
Above component fully mixes, and makes antitranspirant.
Under the normal water supply condition, the transpiration by this transpiration agent for reducing corn, specific as follows:
Experimental group: spray the antitranspirant that the present embodiment makes, 600 times of uses of dilute with water;
Control group: spray abscisic acid on the market (ABA) antitranspirant identical with the experimental group volume, typical concentrations;
Blank group: spray the water with the experimental group equal volume.
Three selected (every group of 40 strains) Maize Physiological states of group are in full accord, and under the same time identical conditions, its water-saving amount measured, and concrete numerical value is as shown in table 2:
Table 2
By table 2, can find out, the water consumption that sprays the experimental group of antitranspirant proposed by the invention is starkly lower than control group and blank group, and water-saving result is very obvious.In addition, the antitranspirant itself proposed due to the present invention contains abundant nutriment, when reducing the crops transpiration, has also promoted growing of plant, and the physiological status of experimental group is compared vigorous a lot with the physiological status of blank group with control group.
In above embodiment, abscisic acid (ABA) antitranspirant is purchased from Henan Zheng Shi chemical industry Co., Ltd; Phenylmercuric acetate (PMA) is purchased from Qingdao Golden Horse chemical industry Co., Ltd.
Finally it should be noted that: the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment, the present invention is had been described in detail, for a person skilled in the art, its technical scheme that still can put down in writing aforementioned each embodiment is modified, or part technical characterictic wherein is equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (7)
1. dry camel thorn alkaline essential oil comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 20-60 part;
Potassium hydroxide: 2-5 part;
Water: 200-400 part;
Wherein, described dry camel thorn alkaline essential oil makes by the following method:
(1) by potassium hydroxide, temperature, be proportionally that the water of 25 ℃-35 ℃ adds reactor, more than stirring 30min;
(2) proportionally, dry camel thorn powder is added to reactor, more than stirring 20min;
(3) after stirring, spontaneous fermentation 60-80 hour under room temperature;
(4) after spontaneous fermentation, stir 1-3 hour, the concentrated 7-15 days of precipitation under 25 ℃-35 ℃, obtain the dry camel thorn alkaline essential oil of finished product.
2. dry camel thorn alkaline essential oil according to claim 1 comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 30-50 part;
Potassium hydroxide: 3 parts;
Water: 300 parts.
3. dry camel thorn alkaline essential oil according to claim 1 comprises the raw material proportioning of following parts by weight:
Dry camel thorn powder: 40 parts;
Potassium hydroxide: 3 parts;
Water: 300 parts.
4. according to the described dry camel thorn alkaline essential oil of claim 1-3 any one, wherein:
The water content of described dry camel thorn powder≤5%, purity >=99%;
The purity of described potassium hydroxide >=99%, described purity is pure for analyzing.
5. dry camel thorn alkaline essential oil according to claim 4, its content of organic matter>=30g/L, K
2O>=60g/L, pH is 7-9, water-insoluble≤5g/L.
6. the extraction process of the described dry camel thorn alkaline essential oil of claim 1-5 any one comprises the following steps:
(1) by potassium hydroxide, temperature, be proportionally that the water of 25 ℃-35 ℃ adds reactor, more than stirring 30min;
(2) proportionally, dry camel thorn powder is added to reactor, more than stirring 20min;
(3) after stirring, spontaneous fermentation 60-80 hour under room temperature;
(4) after spontaneous fermentation, stir 1-3 hour, the concentrated 7-15 days of precipitation under 25 ℃-35 ℃, obtain the dry camel thorn alkaline essential oil of finished product.
7. the application of the described dry camel thorn alkaline essential oil of claim 1-5 any one in preparation crops antitranspirant.
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