CN102488076B - Safe and efficient composite mildew preventive for feed - Google Patents
Safe and efficient composite mildew preventive for feed Download PDFInfo
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- CN102488076B CN102488076B CN 201110372505 CN201110372505A CN102488076B CN 102488076 B CN102488076 B CN 102488076B CN 201110372505 CN201110372505 CN 201110372505 CN 201110372505 A CN201110372505 A CN 201110372505A CN 102488076 B CN102488076 B CN 102488076B
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- 230000003449 preventive effect Effects 0.000 title claims abstract description 26
- 239000002131 composite material Substances 0.000 title abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 27
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims abstract description 24
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims abstract description 22
- TWNIBLMWSKIRAT-RWOPYEJCSA-N (1r,2s,3s,4s,5r)-6,8-dioxabicyclo[3.2.1]octane-2,3,4-triol Chemical compound O1[C@@]2([H])OC[C@]1([H])[C@@H](O)[C@H](O)[C@@H]2O TWNIBLMWSKIRAT-RWOPYEJCSA-N 0.000 claims abstract description 13
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 claims abstract description 13
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000010081 allicin Nutrition 0.000 claims abstract description 13
- OPGYRRGJRBEUFK-UHFFFAOYSA-L disodium;diacetate Chemical compound [Na+].[Na+].CC([O-])=O.CC([O-])=O OPGYRRGJRBEUFK-UHFFFAOYSA-L 0.000 claims abstract description 12
- 235000019260 propionic acid Nutrition 0.000 claims abstract description 12
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims abstract description 12
- 239000001632 sodium acetate Substances 0.000 claims abstract description 12
- 235000017454 sodium diacetate Nutrition 0.000 claims abstract description 12
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000001530 fumaric acid Substances 0.000 claims abstract description 11
- 239000004334 sorbic acid Substances 0.000 claims abstract description 11
- 235000010199 sorbic acid Nutrition 0.000 claims abstract description 11
- 229940075582 sorbic acid Drugs 0.000 claims abstract description 11
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000002360 preparation method Methods 0.000 claims abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 150000001875 compounds Chemical class 0.000 claims description 17
- 241001081179 Litsea Species 0.000 claims description 11
- 235000012854 Litsea cubeba Nutrition 0.000 claims description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims description 10
- 238000005303 weighing Methods 0.000 claims description 10
- 240000008042 Zea mays Species 0.000 claims description 6
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 235000012054 meals Nutrition 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 241000287828 Gallus gallus Species 0.000 claims description 4
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 claims description 4
- 235000009973 maize Nutrition 0.000 claims description 4
- 235000012241 calcium silicate Nutrition 0.000 claims description 2
- 239000012467 final product Substances 0.000 claims description 2
- 239000010455 vermiculite Substances 0.000 claims description 2
- 229910052902 vermiculite Inorganic materials 0.000 claims description 2
- 235000019354 vermiculite Nutrition 0.000 claims description 2
- PFRGXCVKLLPLIP-UHFFFAOYSA-N diallyl disulfide Chemical compound C=CCSSCC=C PFRGXCVKLLPLIP-UHFFFAOYSA-N 0.000 claims 2
- 240000002234 Allium sativum Species 0.000 claims 1
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 claims 1
- 240000003731 Piper cubeba Species 0.000 claims 1
- 235000002711 Piper cubeba Nutrition 0.000 claims 1
- 241000235342 Saccharomycetes Species 0.000 claims 1
- 239000000440 bentonite Substances 0.000 claims 1
- 229910000278 bentonite Inorganic materials 0.000 claims 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical group O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims 1
- 230000003115 biocidal effect Effects 0.000 claims 1
- 229940043350 citral Drugs 0.000 claims 1
- 235000013399 edible fruits Nutrition 0.000 claims 1
- 238000000855 fermentation Methods 0.000 claims 1
- 230000004151 fermentation Effects 0.000 claims 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 235000019629 palatability Nutrition 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000000969 carrier Substances 0.000 abstract 2
- 235000011087 fumaric acid Nutrition 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000001289 litsea cubeba fruit oil Substances 0.000 abstract 2
- 239000003674 animal food additive Substances 0.000 abstract 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 description 8
- 239000003921 oil Substances 0.000 description 6
- 235000019198 oils Nutrition 0.000 description 6
- 241001465754 Metazoa Species 0.000 description 5
- 239000000498 cooling water Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000013019 agitation Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000011229 interlayer Substances 0.000 description 3
- 150000007524 organic acids Chemical class 0.000 description 3
- 238000012856 packing Methods 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000419 plant extract Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 235000019733 Fish meal Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 235000012216 bentonite Nutrition 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 1
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000004467 fishmeal Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Fodder In General (AREA)
Abstract
The invention relates to a feed additive and specially, relates to a safe and efficient composite mildew preventive for feed and a preparation method thereof. The safe and efficient composite feed mildew preventive comprises: by weight, 15 to 30% of litseacubeba oil, 5 to 15% of allicin, 2 to 8% of propionic acid, 2 to 10% of sorbic acid, 1 to 10% of fumaric acid, 5 to 15% of sodium diacetate, 1 to 5% of mannosan and 30 to 65% of carriers. The preparation method comprises the following steps of adding litseacubeba oil, propionic acid, sorbic acid and fumaric acid into a reactor according to the ratios, heating the mixture in the reactor to a temperature of 45 to 60 DEG C with stirring to obtain a liquid mixture after uniform mixing, well mixing allicin, sodium diacetate, mannosan, the carriers and the liquid mixture in a mixer, cooling, taking out the cooled mixture from the mixer, crushing, sieving, and carrying out examination and packaging to obtain the safe and efficient composite feed mildew preventive. Compared with the prior art, the safe and efficient composite feed mildew preventive has less irritation, greatly improved safety, good mildew-proof effects and antibacterial effects, and strong palatability and satisfies environmental protection requirements.
Description
Technical field
The present invention relates to a kind of feed addictive, be specially the safety high efficient compound Midew preventive for feed; The invention still further relates to the preparation method of this mould inhibitor.
Background technology
Feed is easy to be subject to mould contamination in the process of circulation of producing, store, selling and causes and go mouldy, and feed mold causes huge economic loss to feed industry and animal husbandry.Therefore, how to prevent feed mold that whole animal husbandry is had important using value, adding mould inhibitor in feed is the important measures that guarantee feed quality and animal health.Midew preventive for feed mainly contains three major types in the market: the first kind is pure organic acid type, and primary raw material has propionic acid, acetic acid, benzoic acid etc.; Equations of The Second Kind is pure acylate type, such as propionate, acetate, Sodium Benzoate etc.; The 3rd class is the composite composite mildew inhibitor that forms of organic acid and salt thereof.These mould inhibitors are not good to the anti-mold effect of feed, have strong impulse, cause animal feed intake to descend, and the rear medicine of searching for food is residual in vivo, and animal body is produced certain side effect.
Although at present existing above-mentioned dissimilar mildew-resistant raw material is carried out the composite mildew inhibitor for feed that obtains, this mould inhibitor is with the shortcoming that can partly improve the one-component mould inhibitor, and it is Shortcomings part also at aspects such as palatability, security and validity.
Summary of the invention
The technical problem to be solved in the present invention provides that a kind of palatability with plant extracts, organic acid and the combination of its esters compatibility is strong, excitant is little, safer, efficient, the mildew inhibitor for feed of good antimicrobial effect and preparation method thereof.
Safety high efficient compound Midew preventive for feed of the present invention, its component and weight proportion are as follows:
Litsea citrate oil 15-30%
Allicin 5-15%
Propionic acid 2-8%
Sorbic acid 2-10%
Fumaric acid 1-10%
Sodium Diacetate 5-15%
Mannosan 1%-5%
Carrier 30 as one kind-65%
Preferred weight proportion is:
Litsea citrate oil 20%
Allicin 10%
Propionic acid 2.5%
Sorbic acid 2.5%
Fumaric acid 5%
Sodium Diacetate 5%
Mannosan 2.5%
Carrier 52.5%
In above-mentioned prescription, each component can directly be bought also voluntarily manufacture from market, and each component all reaches the feed grade standard.
Safety high efficient compound Midew preventive for feed of the present invention is prepared with following methods:
1) takes by weighing the litsea citrate oil of 15-30 weight portion, the propionic acid of 2-8 weight portion and the sorbic acid of 2-10 weight portion and the fumaric acid of 1-10 weight portion and drop in the reactor, stir, be heated to simultaneously 45-60 ℃, obtain liquefied mixture after mixing;
2) taking by weighing the allicin of 5-15 weight portion, the sodium Diacetate of 5-15 weight portion, the mannosan of 5-10 weight portion and carrier and the above-mentioned liquefied mixture of 30-65 weight portion mixes in mixer, take out material after the cooling through pulverizing, sieve, check, pack, and get final product.
Above-mentioned steps 1) in, mixing speed is 50-90r/min, and the heating-up time is controlled at 15-35min; Step 2) in, liquefied mixture is preferably under the condition that mixing speed is 20-60r/min with allicin, sodium Diacetate, mannosan and carrier and mixes, and the cooling water of opening simultaneously the mixer chuck cools off.
The present invention more finally selects mentioned component through long-felt and determines the best proportioning of each composition, thereby obtains safety high efficient compound Midew preventive for feed of the present invention; Mutually work in coordination with, mutually promote between each composition of the present invention, it is compared with existing unitary class chemical anti mildew agent, and anti-mold effect increases, and bacteriostasis strengthens, and security increases; Compare with existing other composite type mouldproof agents, in prescription, reduced the consumption of chemical anti mildew agent, add plant extracts active component and microbial fermenters, the excitant of this product is reduced greatly, palatability, security and validity are greatly improved, more meet the requirement of green, environmental protection, safety, therefore should fill a prescription more scientific reasonable.Safety high efficient compound Midew preventive for feed preparation method of the present invention is simple, processing ease.
Effect assessment
The experiment feed: the chicken feed that adopts our company to develop voluntarily is that experimental subjects is carried out the mildew-resistant experiment, and concrete feed formula is: corn 55.5%, dregs of beans 20.9%, peanut meal 7%, expanded soybean 2%, corn protein powder 5.2%, fish meal 3.2%, corn oil 2.2%, stone flour 1.3%, calcium bicarbonate 1.4%, salt 0.3, micro-compound premix 1%; Water content is 14%.
Experimentation: choose 100 parts in above-mentioned chicken feed, add 0.2 part of safety high efficient compound Midew preventive for feed of the present invention, use plastic bag sealing, not add any mildew-resistant material as blank, the situation of going mouldy of routine observation feed.
Experimental result: the chicken feed that adds safety high efficient compound Midew preventive for feed of the present invention can not produce caking and mildew phenomena in three months, produced by four month and slightly go mouldy, and control group will produce caking and slightly go mouldy in two weeks.
The specific embodiment
The invention will be further described below in conjunction with embodiment, but the present invention is not limited to these embodiment.Below umber described in each embodiment all refer to weight portion.
Embodiment 1
1) takes by weighing 20 parts litsea citrate oil, 2.5 parts propionic acid, 2.5 parts sorbic acid and 5 parts
Fumaric acid drops in the reactor, and 70r/min stirs, and is heated to 50 ℃ in the 15min, behind the mixing
To liquefied mixture;
2) taking by weighing 10 parts allicin, 5 parts sodium Diacetate, 2.5 parts mannosan, 22.5 parts of bentonites and 30 parts of maize cob meals drops in the mixer, open and stir and transfer to 30r/min, under agitation with above-mentioned steps 1) the gained liquefied mixture adds mixer and inhales and carry, mix, the cooling water of opening simultaneously the mixer interlayer cools off, after liquefied mixture all drops into mixer, continue to mix 20min, after the cooling mixture is discharged mixer, through pulverizing, sieve, check, packing, namely obtain Midew preventive for feed of the present invention.
Embodiment 2
1) take by weighing 18 parts litsea citrate oil, 2 parts propionic acid, 2 parts sorbic acid and 3 parts fumaric acid and drop in the reactor, 60r/min stirs, and is heated to 55 ℃ in the 15min, obtains liquefied mixture behind the mixing;
2) taking by weighing 15 parts allicin, 7.5 parts sodium Diacetate, 2.5 parts mannosan, 25 parts of vermiculite powers and 25 parts of maize cob meals drops in the mixer, open and stir and transfer to 25r/min, under agitation with above-mentioned steps 1) the gained liquefied mixture adds mixer and inhales and carry, mix, the cooling water of opening simultaneously the mixer interlayer cools off, after liquefied mixture all drops into mixer, continue to mix 25min, after the cooling mixture is discharged mixer, through pulverizing, sieve, check, packing, namely obtain Midew preventive for feed of the present invention.
Embodiment 3
1) take by weighing 25 parts litsea citrate oil, 3 parts propionic acid, 5 parts sorbic acid and 2 parts fumaric acid and drop in the reactor, 80r/min stirs, and is heated to 50 ℃ in the 20min, obtains liquefied mixture behind the mixing;
2) taking by weighing 10 parts allicin, 10 parts sodium Diacetate, 5 parts mannosan, 25 parts of calcium silicates and 15 parts of maize cob meals drops in the mixer, open and stir and transfer to 35r/min, under agitation with above-mentioned steps 1) the gained liquefied mixture adds mixer and inhales and carry, mix, the cooling water of opening simultaneously the mixer interlayer cools off, after liquefied mixture all drops into mixer, continue to mix 25min, after the cooling mixture is discharged mixer, through pulverizing, sieve, check, packing, namely obtain Midew preventive for feed of the present invention.
Claims (9)
1. a safety high efficient compound Midew preventive for feed is characterized in that, its component and heavy
The amount proportioning is:
Litsea citrate oil 15-30%
Allicin 5-15%
Propionic acid 2-8%
Sorbic acid 2-10%
Fumaric acid 1-10%
Sodium Diacetate 5-15%
Mannosan 1%-5%
Carrier 30 as one kind-65%.
2. safety high efficient compound Midew preventive for feed according to claim 1, its component
And weight proportion is preferably:
Litsea citrate oil 20%
Allicin 10%
Propionic acid 2.5%
Sorbic acid 2.5%
Fumaric acid 5%
Sodium Diacetate 5%
Mannosan 2.5%
Carrier 52.5%.
3. safety high efficient compound Midew preventive for feed according to claim 1 and 2, it is characterized in that: described litsea citrate oil is the extract of the plant fruit of a cubeb litsea tree, wherein the content of citral 〉=80%.
4. safety high efficient compound Midew preventive for feed according to claim 1 and 2, it is characterized in that: the material with broad spectrum antibiotic activity of described allicin for from the plant garlic, extracting, wherein diallyl disulphide and Diallytrisin content summation 〉=80%.
5. safety high efficient compound Midew preventive for feed according to claim 1 and 2, it is characterized in that: described mannosan is made by saccharomycetes to make fermentation, wherein is mainly beta-mannase.
6. safety high efficient compound Midew preventive for feed according to claim 1 and 2, it is characterized in that: described carrier is bentonite, calcium silicates, the mixture of any one or more material in vermiculite power and the maize cob meal.
7. the preparation method of a safety high efficient compound Midew preventive for feed, its step is as follows:
1) takes by weighing the litsea citrate oil of 15-30 weight portion, the propionic acid of 2-10 weight portion, the sorbic acid of 2-10 weight portion and the fumaric acid of 1-10 weight portion and drop in the reactor, be heated to 45-60 ℃ under the stirring condition, obtain liquefied mixture after mixing;
2) taking by weighing the allicin of 5-15 weight portion, the sodium Diacetate of 5-15 weight portion, the mannosan of 5-10 weight portion and carrier and the above-mentioned liquefied mixture of 30-65 weight portion mixes in mixer, take out material after the cooling through pulverizing, sieve, check, pack, and get final product.
8. the preparation method of safety high efficient compound Midew preventive for feed according to claim 7 is characterized in that: step 1) in, mixing speed is 50-90r/min, the heating-up time is controlled at 15-35min.
9. such as each described safety high efficient compound Midew preventive for feed application in the chicken feed among the claim 1-6.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 201110372505 CN102488076B (en) | 2011-11-07 | 2011-11-07 | Safe and efficient composite mildew preventive for feed |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110372505 CN102488076B (en) | 2011-11-07 | 2011-11-07 | Safe and efficient composite mildew preventive for feed |
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| CN102488076A CN102488076A (en) | 2012-06-13 |
| CN102488076B true CN102488076B (en) | 2013-04-03 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1141732A (en) * | 1995-07-28 | 1997-02-05 | 丁时东 | Midew preventive for feed |
| CN1372814A (en) * | 2002-03-18 | 2002-10-09 | 浙江大学 | Process for preparing feed nano additive to adsorb fungal toxin from feed |
| CN1843151A (en) * | 2006-03-16 | 2006-10-11 | 上海交通大学 | Composite mold toxin sorbent |
| CN101849609A (en) * | 2010-05-20 | 2010-10-06 | 南京奥迈科技有限公司 | Novel adsorbing and treating agent for mycotoxins in feed and application thereof |
| CN101953430A (en) * | 2010-07-15 | 2011-01-26 | 北京龙科方舟生物工程技术中心 | Feed, preparation method and use thereof in improvement in reproductive performance of sows |
-
2011
- 2011-11-07 CN CN 201110372505 patent/CN102488076B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1141732A (en) * | 1995-07-28 | 1997-02-05 | 丁时东 | Midew preventive for feed |
| CN1372814A (en) * | 2002-03-18 | 2002-10-09 | 浙江大学 | Process for preparing feed nano additive to adsorb fungal toxin from feed |
| CN1843151A (en) * | 2006-03-16 | 2006-10-11 | 上海交通大学 | Composite mold toxin sorbent |
| CN101849609A (en) * | 2010-05-20 | 2010-10-06 | 南京奥迈科技有限公司 | Novel adsorbing and treating agent for mycotoxins in feed and application thereof |
| CN101953430A (en) * | 2010-07-15 | 2011-01-26 | 北京龙科方舟生物工程技术中心 | Feed, preparation method and use thereof in improvement in reproductive performance of sows |
Non-Patent Citations (6)
| Title |
|---|
| 几种可做为饲料防霉剂的中草药提取物;白雪;《饲料饲草》;20091231(第3期);第48页 * |
| 常顺华等.霉变饲料中添加酯化葡甘露聚糖对肉仔鸡生产性能和抗氧化指标的影响.《饲料广角》.2010,(第6期),第38-40页. |
| 彭小芳等.酵母细胞壁多糖的生理功能及其应用研究进展.《湖南饲料》.2011,(第5期),第13-14页. |
| 白雪.几种可做为饲料防霉剂的中草药提取物.《饲料饲草》.2009,(第3期),第48页. |
| 酵母细胞壁多糖的生理功能及其应用研究进展;彭小芳等;《湖南饲料》;20110928(第5期);第13-14页 * |
| 霉变饲料中添加酯化葡甘露聚糖对肉仔鸡生产性能和抗氧化指标的影响;常顺华等;《饲料广角》;20101231(第6期);第38-40页 * |
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| CN102488076A (en) | 2012-06-13 |
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