CN102424776A - Red monas rice and pine needle wine and preparation method thereof - Google Patents
Red monas rice and pine needle wine and preparation method thereof Download PDFInfo
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Abstract
The present invention discloses a red monas rice and pine needle wine. The wine is prepared by the following raw materials, wherein the raw materials comprise, by weight, 20-80 g of pine needle, 6-12 g of mongolian milkvetch root, 15-25 g of red monas rice, 7-10% of mixed yeast, edible ethanol, citric acid and honey, wherein the alcohol content of the red monas rice and pine needle wine is 13-15% with the edible ethanol, the acid content of the red monas rice and pine needle wine is 0.45-0.55% with the citric acid, the sugar content of the red monas rice and pine needle wine is 5.5-6.5% with the honey, the mixed yeast is prepared by mixing grape wine active dry yeast, single roxburgh rose fruit wine yeast and yellow wine yeast according to a ratio of the grape wine active dry yeast to the single roxburgh rose fruit wine yeast to the yellow wine yeast of 1:0.8-1.2:0.8-1.2, the pine needle and the mongolian milkvetch root are prepared into the pine needle extract and the mongolian milkvetch root extract during the red monas rice and pine needle wine preparation process. The produced red monas rice and pine needle wine of the present invention has characteristics of soft and red color, unique taste, unique flavor, strong palatability, and high active ingredients of the pine needle, has originality and advancement in the field of the new wine development, and is suitable for popularization.
Description
Technical field
The present invention relates to health promoting wine and preparation method thereof, exactly is a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine and preparation method thereof.
Background technology
Pine needle almost whole body all is precious, and medicine food scope is very extensive, is that our valuable material not to the utmost inexhaustible, that use is rich.Confirm according to traditional medicine and modern medicine study achievement: pine needle rich in proteins, microbiotic, chlorophyll, vegetable fibre, plant ferment, 8 seed amino acids and multiple micro-ore deposit element, multivitamin isoreactivity material.The Compendium of Material Medica record, " the feelings temperature is bitter, and is nontoxic for pine needle, pine tag by name, goes into liver, kidney, lung, all warps of spleen, controls each dirty pyogenic infections, cold and dampness ".Add " pine is the length of hundred wood, and its leaf, skin, cream cure mainly rheumatism, piliation, and five viscera settling, strong positive bowl spares, not hungry prolonging life obeyed permanent tooth for a long time and preserved youthful looks, and skin is pure as jade, and it is not old to make light of one's life by commiting suicide ... ".In China's first Chinese materia medica ancient books and records Shennong's Herbal, medicine is fallen into three classes, what can only cure the disease is " prescribe medicine "; Not only can cure the disease but also can strengthen be called " Chinese medicine " of energy; When the treatment disease is arranged again, can play and safeguard life, help be only " medicine-feeding " of " longevity ".What in " medicine-feeding ", mentioned at first is exactly " pine ".Legendary god of farming Yan Di, also known as Shen Nong, a legendary ruler classifies ten kinds of things the thing of long-lived indispensability as, is respectively: day, mountain, water, stone, pine, go, wood, grass, crane, tortoise.This is contained pine by wood, but goes to be listed separately at this, it serves to show that the effect of pine is more important.
The Radix Astragali is a traditional Chinese medicines material simply, i.e. medicine food dual purpose plant, and its major function is (1) tonifying Qi and lifting yang, strengthening superficial resistance to stop perspiration; Give birth to the ability strengthening superficial resistance to stop perspiration, control asthenic symptoms spontaneous perspiration, night sweat.(2) diuresis holder poison, apocenosis, expelling pus and promoting granulation; Be used for not closing up for a long time and edema due to deficiency of the spleen after the carbuncle sore is not burst or burst.The modern study result shows that the Radix Astragali has the enhancing body immunologic function, protects the liver, diuresis, anti-ageing, anti-stress, step-down and anti-microbial effect more widely.Can eliminate experimental nephritic proteinuria, strengthen myocardial contraction, blood sugar regulation content.
Existing thousands of years of the history of honey wine brewing, how on the books the Ancient Times in China document is.Honey be crude substance nutritious, be rich in the various active material, have the effect of nutritious tonifying and disease preventing and treating, and safe and reliable, have no side effect.
Red colouring agent for food, also used as a Chinese medicine is the song that utilizes monascus to produce, and because of taking on a red color, and generates red pigments, so promptly be referred to as red colouring agent for food, also used as a Chinese medicine since ancient times, is thought the extremely healthcare products of preciousness by the world of medicine.In Ming Dynasty's Exploitation of the Works of Nature, being referred to as red song, is Chinese medicine, is again food.Ming Dynasty's LI Shi-Zhen is estimated it in Compendium of Material Medica and is said: " this be the people peep good fortune skilful person also "; " strange medicine also "; Pharmacopeia is concentrated the mountain range to carry these article to have effects such as promoting blood circulation and removing blood stasis, strengthening the spleen to promote digestion in many ancient times, is used to treat that dyspepsia is glutted, post partum longtime lochia, trace stagnate diseases such as stomachache and wound
The application of now red colouring agent for food, also used as a Chinese medicine not only extensively but also extremely eyeball look at, the research of red colouring agent for food, also used as a Chinese medicine has more obtained the concern in the world.The biologist of Peking University filters out a strain Monascus anka Nakazawa et sato from numerous Monascus anka Nakazawa et sato kinds, in its meta-bolites, found to reduce the natural statin substance of serum cholesterol.Passed through a large amount of work the wild-type strain variation has been the production bacterial classification; Make it to produce high-content, human body synthetic cholesterol key enzyme (HMG---CoA reductase enzyme) specific inhibitor one natural statin substance stable, that be fit to pharmacy; Simultaneously can also produce many compositions, close lipid acid or the like like indispensable amino acid, insatiable hunger to the human body beneficial.At this moment red colouring agent for food, also used as a Chinese medicine only as the existing very big difference of the red colouring agent for food, also used as a Chinese medicine of pigment, therefore is called purpose-made monascus with general.Purpose-made monascus has been used for pharmacy now; Discover in a large number it have very powerful reducing total cholesterol, reduce low density lipoprotein cholesterol, reduce serum triglyceride, reduce the remarkable comprehensive therapeutic effect of AI, high density lipoprotein increasing SUV and take safe, spinoff is little; And can efficacious therapy cardiovascular and cerebrovascular diseases and the diseases relevant such as coronary heart disease, Stroke with hyperlipidemia, like mellitus, nephrotic syndrome and fatty liver.Be considered to the most promising current lipopenicillinase material.
The pharmacologist finds in recent years, and red colouring agent for food, also used as a Chinese medicine is used as medicine, and is a kind of outstanding reducing blood-fat, hypotensive natural drug.In LI Shi-Zhen chief editor's monumental work " herbal guiding principle monascus Zoopagales " book, promptly record the good recipe of curing the disease that several contain the red colouring agent for food, also used as a Chinese medicine composition.The researchist of China Chinese Academy of Sciences exploitation be the lipopenicillinase new drug " olbetam " of raw material with the red colouring agent for food, also used as a Chinese medicine, curative effect can match in excellence or beauty with the stanin fat-reducing medicament of u s company exploitation, abroad is referred to as " China he spit of fland ".In addition, the monascus verivate also has very the strong anti-oxidation antitumous effect of holding concurrently.Along with scientist deepens continuously to the physiology of monascus and the understanding of pharmacological action, ancient red colouring agent for food, also used as a Chinese medicine is expected to become important new drug source.
Summary of the invention
The purpose of this invention is to provide and a kind ofly utilize its health promoting wine that makes to contain multiple natural nutrient component, have red colouring agent for food, also used as a Chinese medicine pine needle wine of unique local flavor and very high healthy nutritive value and preparation method thereof.
Above-mentioned purpose realizes through following scheme:
A kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: be to process: pine needle 20-80 gram by the following weight proportion raw material; Radix Astragali 6-12 gram, red colouring agent for food, also used as a Chinese medicine 15-25 gram, mixed yeast bacterial classification 7-10%; Make the red colouring agent for food, also used as a Chinese medicine pine needle wine contain the edible ethanol that the alcohol amount reaches 13-15%, make red colouring agent for food, also used as a Chinese medicine pine needle wine acid content reach the Hydrocerol A of 0.45-0.55%; Make red colouring agent for food, also used as a Chinese medicine pine needle wine sugar content reach the honey of 5.5-6.5%; Described mixed yeast bacterial classification is that wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification mix with 1: 0.8～1.2: 0.8～1.2; The described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract when preparation red colouring agent for food, also used as a Chinese medicine pine needle wine.
The preparation method of described red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: the described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract by weight ratio, get pine needle extract and Radix Astragali extractive solution; Pine needle extract, step Radix Astragali extractive solution are mixed by weight ratio; And then add honey and mix, after stirring, the red colouring agent for food, also used as a Chinese medicine liquid that will add suitable quantity of water more also adds wherein and stirs; Transfer pH value 3.8-4.0 with Hydrocerol A, promptly as mother liquor; Be to be inoculated in the above-mentioned mother liquor behind the mixed yeast liquid to ferment with the activation of described mixed yeast bacterial classification again, separate get liquid after, put about 10～15 ℃ of following ageing 40d after; It is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
The preparation method of described red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: may further comprise the steps:
(1) preparation of pine needle extract
After the fresh pine needle of the weighing by weight ratio after 1. will cleaning is cut into broken section of 3-6cm, with the common salt aqueous solution dipping of 3-5% 12-24 hour;
2. with step 1. the pine needle behind common salt aqueous solution dipping drain away the water; Use pH value 4.0-4.5, concentration to soak 10-12 hour as the 20-40% aqueous ethanolic solution; Wherein the feed liquid weight proportion of pine needle and aqueous ethanolic solution is 1: 5.5～6.5; Use power 200-250W then, the ultrasonication 30-60 of frequency 33-50khz minute, get extracting solution behind the recovery ethanol;
3. step gained extracting solution be will go up and instantaneous 115-120 ℃ of High Temperature Sterilization 5-10 second, fast cooling or C taked
060 radurizations, radiation dose are 3-6kgy, and it is subsequent use to get pine needle extract;
(2) preparation of Radix Astragali extractive solution
1. extract and concentrate
The weighing Radix Astragali adds water extraction 2-3 time that 3-4 doubly measures by weight ratio, and the time was respectively 1-2 hour,, merge three times decoction extracting solution, filter, specific density is 1.10～1.15 when being concentrated into 80 ℃ of heat and surveying, concentrated extract;
2. alcohol precipitation, reclaim ethanol
To go up step gained medicinal extract places in the Alcohol-settling tank; Chuck feeds and to add the ethanol adjustment after the tap water cooling and contain the alcohol amount and be 45-55%, stirs, and is airtight; Left standstill 22-26 hour; Get supernatant screen cloth filtration back and reclaim ethanol, specific density was 1.20～1.26 when liquid concentrator was concentrated into 80 ℃ of heat surveys, and it is subsequent use to get Radix Astragali extractive solution;
(3) preparation of honey solution: the honey that weighing is an amount of, heat-treat, temperature 100-110 ℃, after 18-22 minute, cooling, subsequent use;
(4) preparation of red colouring agent for food, also used as a Chinese medicine solution: weighing red colouring agent for food, also used as a Chinese medicine by weight ratio, add an amount of purified water and soaked 5～6 hours, red colouring agent for food, also used as a Chinese medicine liquid is subsequent use;
(5) activation of bacterial classification: after selecting for use wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification to mix with 1: 0.8～1.2: 0.8～1.2; In 35-40 ℃ about 5% sugar aqueous solution, adding the mixed yeast bacterial classification immediately makes its concentration reach 7-10%; After careful the mixing, insulation is left standstill, and whenever at a distance from about 10 minutes, stirs once; Through 20-30 minute, the mixed yeast liquid after the activation;
(6) pine needle extract of step (1) gained, the Radix Astragali extractive solution of step (2) gained are mixed by weight ratio; Then with step (3) honey after treatment set by step 22～26% consumption of the total mixed solution quality of (1), step (2) add wherein; Stir, step (4) gained red colouring agent for food, also used as a Chinese medicine liquid is also added wherein stir again, transfer pH value 3.8-4.0 with Hydrocerol A; Promptly as mother liquor; The consumption of the mixed yeast liquid about 0.5% with step (5) after activated is inoculated in the above-mentioned mother liquor and ferments, and the primary fermentation time is 4-5d days, 25～28 ℃ of leavening temperatures; Separation is carried out secondary fermentation with residue mixed yeast liquid after getting liquid again, and the secondary fermentation time is 25-30d, 18～22 ℃ of leavening temperatures; Separate get liquid after, put about 10～15 ℃ of following ageing 40d after, it is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: described pine needle first-selected vegetative period more than 3 meters, more than 6 years; Bright pine needle apart from the city beyond 5 kilometers, no disease and pest and pollution, every pine tree pine needle harvesting amount must not exceed it and set 1/3rd of total leaf amount.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: the described Alcohol-settling tank of step (2) is 1.5m
3Alcohol-settling tank, step (2) add ethanol adjustment gained and contain the preferred 20-40% of alcohol amount, and the described screen cloth of step (2) is 200 eye mesh screens.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: step (2) uses the WZ-500 haplo-effect concentrator to reclaim ethanol; Using LH-500 scraper plate vacuum concentration pot to carry out liquid concentrator concentrates; The Diluted Alcohol that reclaims is recycled into the ethanol of high density, the dense alcohol jar of blowback 3T with the LH-300 alcohol distillation column.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: described red colouring agent for food, also used as a Chinese medicine is to utilize monascus to pass through microbe in solid state or the resulting product of liquid state fermentation.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: the described fermentation of step (6) is temperature controlled fermentation in the vat of stainless steel or ceramic; Described clarification filter for gelatin or casein food grade and JA finings as compound clarifier; Under 10-15 ℃ of condition, clarify, filter with ultrafiltration apparatus.
Beneficial effect of the present invention is:
1, the red colouring agent for food, also used as a Chinese medicine pine needle wine produced of this technology have color and luster soft ruddy, give off a strong fragrance, mouthfeel, unique flavor, palatability is strong, effective constituent is higher in the pine needle, has originality, advance aspect the exploitation of beverage new product, is fit to extensively promote.Not, only use ethanol and water as extraction solvent in production process, therefore no organic solution service recorder can not introduce other impurity in whole leaching process, and this has just simplified the step of separation and purification greatly, has reduced the cost of separation and purification; Moreover used extraction solvent is aqueous ethanolic solution, capable of circulationly utilizes again, so do not have the waste liquid eliminating in the production process, is beneficial to environment protection.
2, pine needle is used saline soak, with the wax in effective removal pine needle with alleviate its sour and astringent taste, drink mouthfeel thereby improve it.
3, raw material extracts used solvent to adopt pH value is the 20-40% aqueous ethanolic solution of 4.0-4.5, is beneficial to the leaching of effective constituent and the color and luster of gained extracting solution; Adopt ultrasound assisted extraction technique, improved efficient, practiced thrift the extraction time and the energy greatly, reduced cost.We adopt sterilising method is the method for TRANSIENT HIGH TEMPERATURE sterilization, guarantee that the pine needle drink reaches the effect of sterilization, guarantee that simultaneously the pine needle composition is not damaged, and can avoid adding sanitas again, thereby improve product quality, mouthfeel and local flavor.Simultaneously, employed red colouring agent for food, also used as a Chinese medicine composition, monascus ruber excretory meta-bolites has antibacterial and germicidal action, though the wine of rice fermented with red yeast number of degrees of making lower, need not add any sanitas, thereby realize that really pure natural does not have the interpolation drink.Honey is heat-treated the safety that helps to ferment carry out, also can help the stability of honey finished wine.But heat treated temperature and time must not be crossed and exceed for a long time, otherwise unfavorable to the alcohol generation.Adopting the method for mixed yeast bacterial classification fermentation, is that especially the local flavor to wine is useful because of mixed yeast fermentation is better than single yeast.Employed raw and auxiliary material, vessel all meet the requirement or the standard code of national relevant laws and regulations in the production process.
4, the present invention has the health-care effect that improves immunizing power to human body.
Embodiment
A kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: be to process: pine needle 20-80 gram by the following weight proportion raw material; Radix Astragali 6-12 gram, red colouring agent for food, also used as a Chinese medicine 15-25 gram, mixed yeast bacterial classification 7-10%; Make the red colouring agent for food, also used as a Chinese medicine pine needle wine contain the edible ethanol that the alcohol amount reaches 13-15%, make red colouring agent for food, also used as a Chinese medicine pine needle wine acid content reach the Hydrocerol A of 0.45-0.55%; Make red colouring agent for food, also used as a Chinese medicine pine needle wine sugar content reach the honey of 5.5-6.5%; Described mixed yeast bacterial classification is that wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification mix with 1: 0.8～1.2: 0.8～1.2; The described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract when preparation red colouring agent for food, also used as a Chinese medicine pine needle wine.
The preparation method of described red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: the described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract by weight ratio, get pine needle extract and Radix Astragali extractive solution; Pine needle extract, step Radix Astragali extractive solution are mixed by weight ratio; And then add honey and mix, after stirring, the red colouring agent for food, also used as a Chinese medicine liquid that will add suitable quantity of water more also adds wherein and stirs; Transfer pH value 3.8-4.0 with Hydrocerol A, promptly as mother liquor; Be to be inoculated in the above-mentioned mother liquor behind the mixed yeast liquid to ferment with the activation of described mixed yeast bacterial classification again, separate get liquid after, put about 10～15 ℃ of following ageing 40d after; It is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
The preparation method of described red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: may further comprise the steps:
(1) preparation of pine needle extract
After the fresh pine needle of the weighing by weight ratio after 1. will cleaning is cut into broken section of 3-6cm, with the common salt aqueous solution dipping of 3-5% 12-24 hour;
2. with step 1. the pine needle behind common salt aqueous solution dipping drain away the water; Use pH value 4.0-4.5, concentration to soak 10-12 hour as the 20-40% aqueous ethanolic solution; Wherein the feed liquid weight proportion of pine needle and aqueous ethanolic solution is 1: 5.5～6.5; Use power 200-250W then, the ultrasonication 30-60 of frequency 33-50khz minute, get extracting solution behind the recovery ethanol;
3. step gained extracting solution be will go up and instantaneous 115-120 ℃ of High Temperature Sterilization 5-10 second, fast cooling or C taked
060 radurizations, radiation dose are 3-6kgy, and it is subsequent use to get pine needle extract;
(2) preparation of Radix Astragali extractive solution
1. extract and concentrate
The weighing Radix Astragali adds water extraction 2-3 time that 3-4 doubly measures by weight ratio, and the time was respectively 1-2 hour,, merge three times decoction extracting solution, filter, specific density is 1.10～1.15 when being concentrated into 80 ℃ of heat and surveying, concentrated extract;
2. alcohol precipitation, reclaim ethanol
To go up step gained medicinal extract places in the Alcohol-settling tank; Chuck feeds and to add the ethanol adjustment after the tap water cooling and contain the alcohol amount and be 45-55%, stirs, and is airtight; Left standstill 22-26 hour; Get supernatant screen cloth filtration back and reclaim ethanol, specific density was 1.20～1.26 when liquid concentrator was concentrated into 80 ℃ of heat surveys, and it is subsequent use to get Radix Astragali extractive solution;
(3) preparation of honey solution: the honey that weighing is an amount of, heat-treat, temperature 100-110 ℃, after 18-22 minute, cooling, subsequent use;
(4) preparation of red colouring agent for food, also used as a Chinese medicine solution: weighing red colouring agent for food, also used as a Chinese medicine by weight ratio, add an amount of purified water and soaked 5～6 hours, red colouring agent for food, also used as a Chinese medicine liquid is subsequent use;
(5) activation of bacterial classification: after selecting for use wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification to mix with 1: 0.8～1.2: 0.8～1.2; In 35-40 ℃ about 5% sugar aqueous solution, adding the mixed yeast bacterial classification immediately makes its concentration reach 7-10%; After careful the mixing, insulation is left standstill, and whenever at a distance from about 10 minutes, stirs once; Through 20-30 minute, the mixed yeast liquid after the activation;
(6) pine needle extract of step (1) gained, the Radix Astragali extractive solution of step (2) gained are mixed by weight ratio; Then with step (3) honey after treatment set by step 22～26% consumption of the total mixed solution quality of (1), step (2) add wherein; Stir, step (4) gained red colouring agent for food, also used as a Chinese medicine liquid is also added wherein stir again, transfer pH value 3.8-4.0 with Hydrocerol A; Promptly as mother liquor; The consumption of the mixed yeast liquid about 0.5% with step (5) after activated is inoculated in the above-mentioned mother liquor and ferments, and the primary fermentation time is 4-5d days, 25～28 ℃ of leavening temperatures; Separation is carried out secondary fermentation with residue mixed yeast liquid after getting liquid again, and the secondary fermentation time is 25-30d, 18～22 ℃ of leavening temperatures; Separate get liquid after, put about 10～15 ℃ of following ageing 40d after, it is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: described pine needle first-selected vegetative period more than 3 meters, more than 6 years; Bright pine needle apart from the city beyond 5 kilometers, no disease and pest and pollution, every pine tree pine needle harvesting amount must not exceed it and set 1/3rd of total leaf amount.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: the described Alcohol-settling tank of step (2) is 1.5m
3Alcohol-settling tank, step (2) add ethanol adjustment gained and contain the preferred 20-40% of alcohol amount, and the described screen cloth of step (2) is 200 eye mesh screens.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: step (2) uses the WZ-500 haplo-effect concentrator to reclaim ethanol; Using LH-500 scraper plate vacuum concentration pot to carry out liquid concentrator concentrates; The Diluted Alcohol that reclaims is recycled into the ethanol of high density, the dense alcohol jar of blowback 3T with the LH-300 alcohol distillation column.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine is characterized in that: described red colouring agent for food, also used as a Chinese medicine is to utilize monascus to pass through microbe in solid state or the resulting product of liquid state fermentation.
The preparation method of described a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: the described fermentation of step (6) is temperature controlled fermentation in the vat of stainless steel or ceramic; Described clarification filter for gelatin or casein food grade and JA finings as compound clarifier; Under 10-15 ℃ of condition, clarify, filter with ultrafiltration apparatus.
With monokaryon-macrophage phagocytic function experiment embodiment is carried out pharmacological experiment study below.Select 20 mouse, be divided into two groups at random by body weight, one group is control group; One group is the treatment group, and 10 every group, control group uses saline water to irritate stomach; The treatment group gives embodiment pine needle wine 5ml/kg and irritates stomach, surveys monokaryon-macrophage phagocytic percentage and phagocytic index value behind the continuous irrigation stomach 30d.The result sees table 1.
The monokaryon of table 1 embodiment-macrophage phagocytic function experimental result
The result shows that control group is compared with the treatment group, and difference is all remarkable, and therefore p proves that less than 0.01 the present invention has the nourishing function that improves immunizing power.
Claims (8)
1. red colouring agent for food, also used as a Chinese medicine pine needle wine; It is characterized in that: be to process: pine needle 20-80 by the following weight proportion raw material; Radix Astragali 6-12, red colouring agent for food, also used as a Chinese medicine 15-25, mixed yeast bacterial classification 7-10%; Make the red colouring agent for food, also used as a Chinese medicine pine needle wine contain the edible ethanol that the alcohol amount reaches 13-15%, make red colouring agent for food, also used as a Chinese medicine pine needle wine acid content reach the Hydrocerol A of 0.45-0.55%; Make red colouring agent for food, also used as a Chinese medicine pine needle wine sugar content reach the honey of 5.5-6.5%; Described mixed yeast bacterial classification is that wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification mix with 1:0.8～1.2:0.8～1.2; The described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract when preparation red colouring agent for food, also used as a Chinese medicine pine needle wine.
2. the preparation method of a red colouring agent for food, also used as a Chinese medicine pine needle wine as claimed in claim 1 is characterized in that: the described pine needle and the Radix Astragali are processed extract from pine needles and Radix Astragali extract by weight ratio, get pine needle extract and Radix Astragali extractive solution; Pine needle extract, step Radix Astragali extractive solution are mixed by weight ratio; And then add honey and mix, after stirring, the red colouring agent for food, also used as a Chinese medicine liquid that will add suitable quantity of water more also adds wherein and stirs; Transfer pH value 3.8-4.0 with Hydrocerol A, promptly as mother liquor; Be to be inoculated in the above-mentioned mother liquor behind the mixed yeast liquid to ferment with the activation of described mixed yeast bacterial classification again, separate get liquid after, put about 10～15 ℃ of following ageing 40d after; It is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
3. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 2 is characterized in that:
May further comprise the steps:
(1) preparation of pine needle extract
After the fresh pine needle of the weighing by weight ratio after 1. will cleaning is cut into broken section of 3-6cm, with the common salt aqueous solution dipping of 3-5% 12-24 hour;
2. with step 1. the pine needle behind common salt aqueous solution dipping drain away the water; Use pH value 4.0-4.5, concentration to soak 10-12 hour as the 20-40% aqueous ethanolic solution; Wherein the feed liquid weight proportion of pine needle and aqueous ethanolic solution is 1:5.5～6.5; Use power 200-250W then, the ultrasonication 30-60 of frequency 33-50khz minute, get extracting solution behind the recovery ethanol;
3. step gained extracting solution be will go up and instantaneous 115-120 ℃ of High Temperature Sterilization 5-10 second, fast cooling or C taked
O60 radurizations, radiation dose are 3-6kgy, and it is subsequent use to get pine needle extract;
(2) preparation of Radix Astragali extractive solution
1. extract and concentrate
The weighing Radix Astragali adds water extraction 2-3 time that 3-4 doubly measures by weight ratio, and the time was respectively 1-2 hour,, merge three times decoction extracting solution, filter, specific density is 1.10～1.15 when being concentrated into 80 ℃ of heat and surveying, concentrated extract;
2. alcohol precipitation, reclaim ethanol
To go up step gained medicinal extract places in the Alcohol-settling tank; Chuck feeds and to add the ethanol adjustment after the tap water cooling and contain the alcohol amount and be 45-55%, stirs, and is airtight; Left standstill 22-26 hour; Get supernatant screen cloth filtration back and reclaim ethanol, specific density was 1.20～1.26 when liquid concentrator was concentrated into 80 ℃ of heat surveys, and it is subsequent use to get Radix Astragali extractive solution;
(3) preparation of honey solution: the honey that weighing is an amount of, heat-treat, temperature 100-110 ℃, after 18-22 minute, cooling, subsequent use;
(4) preparation of red colouring agent for food, also used as a Chinese medicine solution: weighing red colouring agent for food, also used as a Chinese medicine by weight ratio, add an amount of purified water and soaked 5～6 hours, red colouring agent for food, also used as a Chinese medicine liquid is subsequent use;
(5) activation of bacterial classification: after selecting for use wine active dry yeast bacterial classification, Single Roxburgh Rose Fruit brewer yeast bacterial classification and yellow wine yeast bacterial classification to mix with 1:0.8～1.2:0.8～1.2; In 35-40 ℃ about 5% sugar aqueous solution, adding the mixed yeast bacterial classification immediately makes its concentration reach 7-10%; After careful the mixing, insulation is left standstill, and whenever at a distance from about 10 minutes, stirs once; Through 20-30 minute, the mixed yeast liquid after the activation;
(6) pine needle extract of step (1) gained, the Radix Astragali extractive solution of step (2) gained are mixed by weight ratio; Then with step (3) honey after treatment set by step 22～26% consumption of the total mixed solution quality of (1), step (2) add wherein; Stir, step (4) gained red colouring agent for food, also used as a Chinese medicine liquid is also added wherein stir again, transfer pH value 3.8-4.0 with Hydrocerol A; Promptly as mother liquor; The consumption of the mixed yeast liquid about 0.5% with step (5) after activated is inoculated in and carries out primary fermentation in the above-mentioned mother liquor, and the primary fermentation time is 4-5d days, 25～28 ℃ of leavening temperatures; Separation is carried out secondary fermentation with residue mixed yeast liquid after getting liquid again, and the secondary fermentation time is 25-30d, 18～22 ℃ of leavening temperatures; Separate get liquid after, put about 10～15 ℃ of following ageing 40d after, it is clarified, filters; Carry out flavor mixing again, promptly add edible ethanol and make the alcohol amount of containing reach 13-15%, after adding honey and Hydrocerol A and making sugar, acid content reach 5.5-6.5% and 0.45-0.55% respectively; Smart filter, can, packing, finished product promptly get product.
4. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 3; It is characterized in that: described pine needle first-selected vegetative period more than 3 meters, more than 6 years; Bright pine needle apart from the city beyond 5 kilometers, no disease and pest and pollution, every pine tree pine needle harvesting amount must not exceed it and set 1/3rd of total leaf amount.
5. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 3 is characterized in that: the described Alcohol-settling tank of step (2) is 1.5 m
3Alcohol-settling tank, step (2) add ethanol adjustment gained and contain the preferred 20-40% of alcohol amount, and the described screen cloth of step (2) is 200 eye mesh screens.
6. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 3; It is characterized in that: step (2) uses the WZ-500 haplo-effect concentrator to reclaim ethanol; Using LH-500 scraper plate vacuum concentration pot to carry out liquid concentrator concentrates; The Diluted Alcohol that reclaims is recycled into the ethanol of high density, the dense alcohol jar of blowback 3T with the LH-300 alcohol distillation column.
7. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 3 is characterized in that: described red colouring agent for food, also used as a Chinese medicine is to utilize monascus to pass through microbe in solid state or the resulting product of liquid state fermentation.
8. the preparation method of a kind of red colouring agent for food, also used as a Chinese medicine pine needle wine according to claim 3; It is characterized in that: the described fermentation of step (6) is temperature controlled fermentation in the vat of stainless steel or ceramic; Described clarification filter for gelatin or casein food grade and JA finings as compound clarifier; Under 10-15 ℃ of condition, clarify, filter with ultrafiltration apparatus.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102894355A (en) * | 2012-08-15 | 2013-01-30 | 苏州谷力生物科技有限公司 | Composition with blood circulation activating and qi benefiting functions |
| CN103215165A (en) * | 2013-03-16 | 2013-07-24 | 陆开云 | Mulberry and pine needle rice wine and preparation method thereof |
| CN105495613A (en) * | 2015-12-03 | 2016-04-20 | 张文俊 | Pine needle enzyme with immunity boosting function and preparation technology of pine needle enzyme |
| CN111876298A (en) * | 2020-07-27 | 2020-11-03 | 曾鑫 | Pine needle wine and preparation method thereof |
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| CN1492035A (en) * | 2002-09-18 | 2004-04-28 | 赵京洙 | Pine mushroom and pine needle wine |
| CN102220207A (en) * | 2011-05-09 | 2011-10-19 | 王水生 | Process and method for making pine needle black tea yellow wine by using microorganism fermentation technique |
| CN102220208A (en) * | 2011-05-09 | 2011-10-19 | 王鹿鹿 | Technology and method for preparing pine needle corn wine by microbial fermentation |
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| CN1078259A (en) * | 1993-02-23 | 1993-11-10 | 雷邦华 | Working method of a kind of pine needle health-care wine and products thereof |
| CN1309173A (en) * | 2001-01-12 | 2001-08-22 | 贵州省平塘县龙宇食品饮料果酒厂 | Pine needle wine |
| CN1492035A (en) * | 2002-09-18 | 2004-04-28 | 赵京洙 | Pine mushroom and pine needle wine |
| CN102220207A (en) * | 2011-05-09 | 2011-10-19 | 王水生 | Process and method for making pine needle black tea yellow wine by using microorganism fermentation technique |
| CN102220208A (en) * | 2011-05-09 | 2011-10-19 | 王鹿鹿 | Technology and method for preparing pine needle corn wine by microbial fermentation |
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| CN102894355A (en) * | 2012-08-15 | 2013-01-30 | 苏州谷力生物科技有限公司 | Composition with blood circulation activating and qi benefiting functions |
| CN103215165A (en) * | 2013-03-16 | 2013-07-24 | 陆开云 | Mulberry and pine needle rice wine and preparation method thereof |
| CN103215165B (en) * | 2013-03-16 | 2014-02-19 | 陆开云 | Mulberry and pine needle rice wine and preparation method thereof |
| CN105495613A (en) * | 2015-12-03 | 2016-04-20 | 张文俊 | Pine needle enzyme with immunity boosting function and preparation technology of pine needle enzyme |
| CN111876298A (en) * | 2020-07-27 | 2020-11-03 | 曾鑫 | Pine needle wine and preparation method thereof |
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| CN102424776B (en) | 2013-01-02 |
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