CN104068302A - Enteromorpha polysaccharide oral liquid and preparation method thereof - Google Patents
Enteromorpha polysaccharide oral liquid and preparation method thereof Download PDFInfo
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- CN104068302A CN104068302A CN201310122512.0A CN201310122512A CN104068302A CN 104068302 A CN104068302 A CN 104068302A CN 201310122512 A CN201310122512 A CN 201310122512A CN 104068302 A CN104068302 A CN 104068302A
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- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 60
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- 239000007788 liquid Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 15
- 239000003765 sweetening agent Substances 0.000 claims abstract description 15
- 238000001291 vacuum drying Methods 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 238000010298 pulverizing process Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 108090000790 Enzymes Proteins 0.000 claims abstract description 5
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- 241000544058 Halophila Species 0.000 claims description 54
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 9
- 235000002722 Dioscorea batatas Nutrition 0.000 claims description 9
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- 240000001811 Dioscorea oppositifolia Species 0.000 claims description 9
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- 244000241838 Lycium barbarum Species 0.000 claims description 9
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 7
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- 238000001914 filtration Methods 0.000 claims description 4
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- 241000512259 Ascophyllum nodosum Species 0.000 abstract 1
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- 239000003814 drug Substances 0.000 description 2
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- 238000004519 manufacturing process Methods 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
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- 239000003963 antioxidant agent Substances 0.000 description 1
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- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to an enteromorpha polysaccharide oral liquid and a preparation method thereof. The invention is characterized by adopting the following technical scheme: 1, obtaining enteromorpha polysaccharide by using enteromorpha as a raw material through purification, drying, pulverizing, extracting with hot water, enzymolysis, enzyme deactivation, centrifuging purification, ethanol precipitation and vacuum drying in sequence; 2, weighing 30-40% of lentinula edodes, 10-30% of kelp, 10-30% of yams and 10-30% of Chinese wolfberries in percentage by weight, and preparing a Chinese medicinal herb extract for later use through procedures of mixing, pulverizing, extracting in hot water, centrifuging, concentration, vacuum drying and the like; and 3, mixing 5-15% of enteromorpha polysaccharide, 5-15% of Chinese medicinal herb extract, 5-10% of sweetening agents and the balance of water in percentage by weight, and sterilizing, bottling, sealing, inspecting and packing the mixed liquid to obtain a finished product. The enteromorpha polysaccharide oral liquid is rich in nutrition and high in safety, and has multiple health-care functions of reducing blood sugar, reducing blood fat, enhancing the immunity, resisting tumors and the like.
Description
Technical field
The invention belongs to functional food manufacture field, more particularly, relate to a kind of sea grass polysaccharide oral liquid and preparation method thereof.
Background technology
Enteromorpha (Enteromorpha) is a kind of large-scale green alga, is commonly called as tongue bar, green laver etc., is the algae of Chlorophyta Ulvales Ulvaceae Enteromorpha, is grown in intertidal zone.In China, Enteromorpha output is very high, especially East Coastal.In recent years, the Fast-propagation of Enteromorpha pollutes China coast, and the pollution causing for administering Enteromorpha excessive multiplication, need to expend a large amount of manpower and materials, therefore if Enteromorpha is used, not only can administers Enteromorpha and pollute, and can also turn waste into wealth simultaneously.Enteromorpha is edible and medicinal algae since ancient times, studies confirm that: the main component water-soluble polysaccharide of Enteromorpha is the composition that pharmacologically active is very strong, there is reducing blood lipid, anti-oxidant, antitumor and strengthen the BAs such as immunity, can effectively prevent and treat various diseases.
But up to the present, the sea grass polysaccharide of take is few as main functional food, and its medicinal health value is not also excavated fully.The tonifying Qi of the Traditional Chinese Medicine principle of enriching blood can be had complementary advantages, bring out the best in each other with the effect of sea grass polysaccharide.Through patent retrieval and data consultation, for the exploitation of sea grass polysaccharide, there is not yet the report that utilizes Chinese Traditional Medicine technology and biotechnology to combine to manufacture oral liquid.
Summary of the invention
The present invention is exactly for the problems referred to above, and a kind of sea grass polysaccharide oral liquid and preparation method thereof is provided, and product prepared by this technique is not only nutritious, safe, and has hypoglycemic, reducing blood lipid, enhancing immunity, the plurality of health care functions such as antitumor.
For solving the problems of the technologies described above, the component that a technical scheme of the present invention is described oral liquid and weight content are sea grass polysaccharide 5～15%, Chinese medical extract 5～15%, sweetener 5～10%, and surplus is water.Described sea grass polysaccharide is to adopt hot water lixiviate, enzyme process except step acquisitions such as albumen, alcohol precipitations; Described Chinese medical extract dry powder is to adopt hot water extraction to obtain.
Described sweetener is one or both in white granulated sugar, xylitol, FOS, honey.
The raw material of described acquisition Chinese medical extract is mushroom, sea-tangle, Chinese yam, matrimony vine.Percentage by weight during its compatibility is mushroom 30～40%, sea-tangle 10～30%, Chinese yam 10～30%, matrimony vine 10～30%.
A preparation method for sea grass polysaccharide oral liquid, comprises following preparation steps:
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to after 60～80 ℃ of oven dry, pulverize, sieve (20～60 order).
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 20～60 (w/v, g/ml), add distilled water, fully stir, 90～100 ℃ are soaked 4～6h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 1%～3%, regulating pH value is 5.0～6.0, at 50～60 ℃ of enzymolysis 1～2h of temperature, obtains sea grass polysaccharide the second leaching liquor.
4. Enteromorpha the second leaching liquor is heated to 90～100 ℃, residual enzyme is carried out to deactivation, fully stir and soak, process 30～60min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by sea grass polysaccharide the 3rd leaching liquor at the centrifugal 10～15min of 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 2～3 times of volumes of concentrate, after 4 ℃ of standing 3～4h, the centrifugal 10～15min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30～40%, sea-tangle 10～30%, Chinese yam 10～30%, matrimony vine 10～30%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying.
(3) choose one or both in xylitol, FOS, honey as sweetener
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 5～15%, Chinese medical extract 5～15%, sweetener 5～10% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Beneficial effect of the present invention:
The main component containing in the present invention formula is sea grass polysaccharide, and sea grass polysaccharide has significant reducing blood lipid, antifatigue, antibacterial, antitumor and to strengthen the various biological such as immunity active.The compatibility raw material mushroom of its Chinese medical extract can have step-down, norcholesterol, reducing blood lipid, anticancer, improve immunity, can prevention of arterial sclerosis, the disease such as cirrhosis, cancer; Sea-tangle has hypoglycemic, fat-reducing, beauty treatment, inhibition tumour, step-down, lipopenicillinase, delaying sanility prevention cardiovascular and cerebrovascular diseases, improves immunity.Chinese yam can increase T lymphocytes in human body, strengthens immunologic function, and delaying cell aging reduces cholesterol and triglycerides, and the illnesss such as hypertension and high fat of blood are improved to effect.The adjustable body's immunity of matrimony vine, can effectively suppress tumor growth and cell mutation, have delay senility, the effect of AFL, adjusting blood fat and the aspect such as blood sugar, promotion hematopoiesis function,
Rich raw material sources used of the present invention, makes its more easily large-scale batch production.
The present invention's raw material used are all natural product, and safety has no side effect, and can eat for a long time.
The specific embodiment
Embodiment 1
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to 40 orders of pulverizing, sieve after 80 ℃ of oven dry.
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 60 (w/v, g/ml), add distilled water, fully stir, 90 ℃ of lixiviate 4h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 3%, regulating pH value is 5.0, at temperature 50 enzymolysis 1h, obtains sea grass polysaccharide the second leaching liquor.
4. sea grass polysaccharide the second leaching liquor is heated to 100 ℃, fully stirs and soak, process 30min, obtain sea grass polysaccharide the 3rd leaching liquor
5. by the centrifugal 10min of sea grass polysaccharide the 3rd leaching liquor 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 3 times of volumes of concentrate, after 4 ℃ of standing 3h, the centrifugal 10min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30%, sea-tangle 30%, Chinese yam 20%, matrimony vine 20%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose FOS as sweetener, standby.
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener (FOS) and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 10%, Chinese medical extract 10%, FOS 5% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Embodiment 2
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to 40 orders of pulverizing, sieve after 80 ℃ of oven dry.
2. take gained Enteromorpha powder, by solid-liquid ratio 1: 60 (w/v, g/ml), add distilled water, fully stir, 90 ℃ of lixiviate 4h, obtain sea grass polysaccharide the first leaching liquor.
3. in described sea grass polysaccharide the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 3%, regulating pH value is 5.0, at temperature 50 C enzymolysis 1h, obtains sea grass polysaccharide the second leaching liquor.
4. sea grass polysaccharide the second leaching liquor is heated to 100 ℃, fully stirs and soak, process 30min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by the centrifugal 10min of sea grass polysaccharide the 3rd leaching liquor 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 3 times of volumes of concentrate, after 4 ℃ of standing 3h, the centrifugal 10min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30%, sea-tangle 20%, Chinese yam 30%, matrimony vine 20%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose xylitol as sweetener, standby.
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener (xylitol) and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 10%, Chinese medical extract 15%, xylitol 5% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
Claims (4)
1. a sea grass polysaccharide oral liquid, is characterized in that, the component of described oral liquid and weight content are sea grass polysaccharide 5～15%, Chinese medical extract 5～15%, sweetener 5～10%, and surplus is water.Described sea grass polysaccharide is to adopt hot water lixiviate, enzyme process except step acquisitions such as albumen, alcohol precipitations; Described Chinese medical extract is to adopt hot water extraction to obtain.
2. a kind of sea grass polysaccharide oral liquid according to claim 1, is characterized in that described sweetener is one or both in white granulated sugar, xylitol, FOS, honey.
3. a kind of sea grass polysaccharide oral liquid according to claim 1 and 2, the raw material that it is characterized in that obtaining Chinese medical extract is mushroom, sea-tangle, the red sage root, ginkgo leaf, Chinese yam, matrimony vine.Percentage by weight during its compatibility is mushroom 30～40%, sea-tangle 10～30%, Chinese yam 10～30%, matrimony vine 10～30%.
4. the preparation method of a kind of sea grass polysaccharide oral liquid according to claim 1, is characterized in that through following preparation technology:
(1) sea grass polysaccharide preparation
1. Enteromorpha is cleaned up to after 60～80 ℃ of oven dry, pulverize, sieve (20～60 order).
2. take gained Enteromorpha powder, by solid-liquid ratio l: 20～60 (w/v, g/ml) add distilled water, fully stir, 90～100 ℃ are soaked 4～6h, obtain sea grass polysaccharide the first leaching liquor.
3. in described Enteromorpha the first leaching liquor, add the papain that is equivalent to Enteromorpha powder weight volume 1%～3%, regulating pH value is 5.0～6.0, at 50～60 ℃ of enzymolysis 1～2h of temperature, obtains sea grass polysaccharide the second leaching liquor.
4. Enteromorpha the second leaching liquor is heated to 90～100 ℃, residual enzyme is carried out to deactivation, fully stir and soak, process 30～60min, obtain sea grass polysaccharide the 3rd leaching liquor.
5. by sea grass polysaccharide the 3rd leaching liquor at the centrifugal 10～15min of 10000rpm, supernatant liquid filtering final vacuum is concentrated; The ethanol that adds 2～3 times of volumes of concentrate, after 4 ℃ of standing 3～4h, the centrifugal 10～15min of 4000rpm, sediment vacuum drying, obtains sea grass polysaccharide.
(2) preparation of Chinese medical extract
Weigh by weight percentage mushroom 30～40%, sea-tangle 10～30%, Chinese yam 10～30%, matrimony vine 10～30%, through being mixed, pulverizing, hot water lixiviate, centrifugal, concentrated, vacuum drying obtain Chinese medical extract.
(3) choose one or both in white granulated sugar, xylitol, FOS, honey as sweetener
(4) allotment weighs the middle sea grass polysaccharide of preparing of step (1), sweetener and the water chosen in the Chinese medical extract of preparation, step (3) in step (2) mix.It is sea grass polysaccharide 5～15%, Chinese medical extract 5～15%, sweetener 5～10% that weighing makes the weight content of each component, and surplus is water.
(5) mixed liquor step (4) being obtained carries out sterilizing, bottling, sealing, check, packing and gets product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310122512.0A CN104068302A (en) | 2013-03-29 | 2013-03-29 | Enteromorpha polysaccharide oral liquid and preparation method thereof |
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| CN201310122512.0A CN104068302A (en) | 2013-03-29 | 2013-03-29 | Enteromorpha polysaccharide oral liquid and preparation method thereof |
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| CN104068302A true CN104068302A (en) | 2014-10-01 |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105011150A (en) * | 2015-08-26 | 2015-11-04 | 缪雪峰 | Preparation technology of seaweed healthcare oral liquid |
| CN105055616A (en) * | 2015-08-12 | 2015-11-18 | 蔡婷婷 | Seaweed-containing healthcare oral liquid |
| CN106819704A (en) * | 2017-03-07 | 2017-06-13 | 桂林理工大学 | Pyrus nivalis local flavor sea grass polysaccharide reducing blood lipid and function of blood sugar reduction beverage and preparation method |
| CN108003199A (en) * | 2017-07-12 | 2018-05-08 | 中国科学院过程工程研究所 | A kind of Enteromorpha oligosaccharide with function of blood sugar reduction and its preparation method and application |
| CN108409877A (en) * | 2017-07-12 | 2018-08-17 | 中国科学院过程工程研究所 | Sea grass polysaccharide, enteromorpha oligosaccharide, medical composition and its use |
| CN109393451A (en) * | 2017-08-18 | 2019-03-01 | 青岛瑞思德生物科技有限公司 | A kind of health food that immunity can be improved containing Enteromorpha |
| WO2019100843A1 (en) * | 2017-08-17 | 2019-05-31 | 福建海兴保健食品有限公司 | Enteromorpha prolifera polysaccharide composite blood lipid-lowering health care product and preparation method therefor |
| WO2021078297A1 (en) * | 2019-10-25 | 2021-04-29 | 运鸿集团股份有限公司 | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
| CN114376233A (en) * | 2022-03-23 | 2022-04-22 | 青岛海大生物集团股份有限公司 | Enteromorpha polysaccharide health food with immunity enhancing function and preparation method thereof |
| CN114672235A (en) * | 2022-04-25 | 2022-06-28 | 山东中胜涂料有限公司 | High-wear-resistance quick-drying water-based acrylic polyurethane finish paint and preparation method thereof |
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| CN102100322A (en) * | 2011-01-11 | 2011-06-22 | 福建农林大学 | Composite food glue containing enteromorpha gel polysaccharide and preparation method thereof |
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- 2013-03-29 CN CN201310122512.0A patent/CN104068302A/en active Pending
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| CN108003199A (en) * | 2017-07-12 | 2018-05-08 | 中国科学院过程工程研究所 | A kind of Enteromorpha oligosaccharide with function of blood sugar reduction and its preparation method and application |
| CN108409877A (en) * | 2017-07-12 | 2018-08-17 | 中国科学院过程工程研究所 | Sea grass polysaccharide, enteromorpha oligosaccharide, medical composition and its use |
| CN108409877B (en) * | 2017-07-12 | 2020-02-18 | 中国科学院过程工程研究所 | Enteromorpha polysaccharide, enteromorpha oligosaccharide, pharmaceutical composition and application thereof |
| WO2019100843A1 (en) * | 2017-08-17 | 2019-05-31 | 福建海兴保健食品有限公司 | Enteromorpha prolifera polysaccharide composite blood lipid-lowering health care product and preparation method therefor |
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| WO2021078297A1 (en) * | 2019-10-25 | 2021-04-29 | 运鸿集团股份有限公司 | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
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| GB2605893B (en) * | 2019-10-25 | 2023-12-06 | China Yunhong Holdings Co Ltd | Active polysaccharide compound nutrient capable of enhancing immunity and resisting fatigue and preparation method therefor |
| CN114376233A (en) * | 2022-03-23 | 2022-04-22 | 青岛海大生物集团股份有限公司 | Enteromorpha polysaccharide health food with immunity enhancing function and preparation method thereof |
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