CN102416068A - Cleaning and skin-care composition and preparation method thereof - Google Patents

Cleaning and skin-care composition and preparation method thereof Download PDF

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Publication number
CN102416068A
CN102416068A CN201110414422XA CN201110414422A CN102416068A CN 102416068 A CN102416068 A CN 102416068A CN 201110414422X A CN201110414422X A CN 201110414422XA CN 201110414422 A CN201110414422 A CN 201110414422A CN 102416068 A CN102416068 A CN 102416068A
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semen sojae
sojae atricolor
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parts
fructus sapindi
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CN102416068B (en
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杨敏忠
吴莉
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Sichuan Pharmaceutical Co China Masein
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Chengdu Mosun Pharmaceutical Dev Co ltd
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Abstract

The invention discloses a cleaning and skin-care composition which comprises the following raw materials in parts by weight: 1-28 parts of soybean and 50-320 parts of Chinese soapberry. The invention also discloses a preparation method of the composition, which comprises the steps of preparing the soybean and the soapberry into extracting solutions and then mixing the extracting solutions. The invention has the advantages of environment-friendly raw materials, simple process, strong bacteriostatic action, mild action and no stimulation to skin and mucosa, and the bacteriostatic rate is up to more than 90%.

Description

A kind of cleaning skin care compositions and method for preparing
Technical field
The invention belongs to the Chinese medicine for external application field, be specifically related to a kind of natural composition that cleans maintenance nursing skin, mucosa and preparation method thereof.
Background technology
Along with the deterioration of environment, the outburst of various diseases, people require increasingly highly to health, and it is clean that all article that require environment of living in and use are not only wanted, and especially pathogenic bacterium can not be arranged.Except environmental health, Personal hygiene requires higher, and various antibacterial fancy soap bath gel collutorys and so on are tinkling of jades already to meet the eye on every side, and various privates care products are also come out one after another simultaneously.
Make a general survey of all external preparation for skin products; All have claim the bacteriostasis antibiosis person; Its main component is nothing more than chemical drugs and Chinese and western drugses such as chlorhexidine (being hibitane), triclosan (i.e. 2,4,4 '-three chloro-2 '-dihydroxy diphenyl ethers), benzalkonium bromide, metronidazole, Radix Sophorae Flavescentis, Fructus Cnidiis.As everyone knows, " being three fens poison of medicine ", society all advocates environmental protection now, and people are uphold nature, and are natural pollution-free, promptly mean health.
Summary of the invention
The weak point that exists to the existing composition of medicine similar with the present invention; The object of the invention aims to provide the natural composition of a kind of cleaning-nursing skin, mucosa; Compositions through this pure natural; To people a kind of safe antibacterial cleaning product is provided; The antibiotic cleaning that can be used for body surface skin and mucosa like hair washing, clean, gargle, take a shower, bathe foot, all has dandruff, acne, oral ulcer, halitosis, pudendal pruritus/abnormal flavour, tinea manus and pedis and other various dermatopathies and alleviates and preventive effect.
Another object of the present invention is to provide the method for preparing of the natural composition of this cleaning-nursing skin mucosa.
In order to achieve the above object, the present invention has adopted following technical scheme:
The natural composition of a kind of cleaning-nursing skin, mucosa is formed by following feedstock production by weight:
Semen sojae atricolor 1-28 part, Fructus Sapindi Mukouossi 50-320 part.
Above-mentioned two kinds of raw materials add following ingredients after extracting:
Plants essential oil 1-10 part, Oleum Cocois 50-230 part, glycerol 20-300 part.
Optimum, above-mentioned cleaning-nursing skin, the natural composition of mucosa, each composition weight proportioning is:
10 parts of Semen sojae atricolor, 80 parts of Fructus Sapindi Mukouossis, 3 parts of plants essential oils, 120 parts of Oleum Cocois, 50 parts of glycerol.
Said components of the present invention and pharmaceutically acceptable carrier are processed gel, lotion, spray, suppository, effervescent tablet, liniment.
The present invention also can be applicable to prepare shampoo, cleansing milk, bath gel etc.
The method of the natural composition of preparation cleaning-nursing skin, mucosa, its preparation methods steps is following:
1. the preparation of soybean extraction liquid:
A. Semen sojae atricolor after 20-30 hour, is broken into the mud shape with the pure water of 2-3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add volume ratio 0.1%-0.5% chitosan then, isolated by filtration obtains transparent soybean extraction liquid after concentrating;
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the peel of Fructus Sapindi Mukouossi pulverizing, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. press said formula ratio with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. press formula ratio plants essential oil is mixed with non-ionic surfactant polyoxyethylene castor oil hydrogenated, polyoxyethylene castor oil, TX10 or tween 1-30 part, stir, slowly add then in the mixed liquor I, get the mixture II;
5. by formula ratio Oleum Cocois, glycerol are mixed to evenly, add in the mixture II, add water stir compositions.
In the prescription of the present invention:
Soybean extraction liquid is a colourless transparent liquid, can be directly water-soluble, and overcome hibitane and triclosan etc. and must be dissolved in just water-soluble shortcoming after the ethanol earlier, reduced the zest of product to skin and mucosa.Soybean extraction liquid all has good inactivating efficacy to bacterial strains such as Candida albicans, coliform, pneumobacillus, legionella, mycete, tinea alba bacterium, green pus bacterium.Soybean extraction liquid is as medical material, be widely used in gynaecologic washing lotion, medical supplies, sanitary towel, wet tissue, cosmetics, oral hygiene, anthelmintic, medicated napkin, home-use gas defence articles for use, water purification, vegetable (eating usefulness raw) disinfectant solution etc. various antibiotic, smelly, sterilization field disappears.Its high-quality of nationality, safety efficiently, has the characteristics of cost performance, is just extensively paid close attention to, and progressively replaces hibitane, and traditional antibiosis and sterilization agent such as triclosan belongs to the top standard in the world, domestic like product.
Fructus Sapindi Mukouossi, peel contain saponin (Saponin), vitamin C, tyrosine (Tyrosine), glycine (Glycine), alanine (Alanine), Folium Symplocoris Caudatae, fructose, glucose, pentose, methylpentose, arabic gum, rhamnose.Environmental protection, nuisanceless.Its extracting solution foam is abundant, effectively takes out stains, and antibiotic beauty treatment, tender skin, brightens speckle, acne removing, prevents and treats dermatosis.The pure natural product, 100% high-fall separating, life-time service can not produce any to human body and the deleterious residue of environment.Help health, help environmental conservation.
Plants essential oil is an extraction plant specific aromatic substance, is taken from herbal flower, leaf, root, bark, fruit, seed, resin etc. and extract with distillation, squeezing mode.Plants essential oil is called liquid golden again, and it has following effect: one, purify air and antibacterial: because quintessence oil has antibiotic antiseptical composition, so that it has is antibiotic, antimicrobial and antiviral characteristic.Two, cytotrophy is provided: because quintessence oil contains hormone, vitamin, antibiotic, so can furnish us with soma nutrition.Three, balance body and mind spirit: the most important speciality of quintessence oil is an abnormal smells from the patient, and it can influence the limbic system of brain, acts in the olfactory sensation, and small aromatic molecules more can cause the reaction of psychology and physiology different levels on nervus centralis.Four, immunologic function: wherein most important characteristic is the immune system that volatile oil helps to strengthen health, helps the attack of the various pathogenic bacterias of opposing, virus.Five, has natural anticorrosion speciality.
Oleum Cocois is the endosperm of Petiolus Trachycarpi kind of plant Cortex cocois radicis, through pulverizing the oil that is squeezed after baking is steamed, is white in color or faint yellow fat.Contain free fatty in the oil, caproic acid, Palmic acid, caprylic acid, Stearic Acid, capric acid, oleic acid, lauric acid contains stigmastatrienol in the sterol of Oleum Cocois, stigmasterol and 24-ethylidenecholest-5-en-3.beta.-ol., hitodesterol and sterol, cupreol.Tool is controlled scabies, chilblain, the effect of skin or hair care.
Raw material environmental protection of the present invention, technology is simple, bacteriostasis is powerful (bacteriostasis rate is up to more than 90%), but action temperature with, non-stimulated to skin and mucosa.
Test Example
(1) fungistatic effect
1, according to GB15979-2002, this sample is under experimental condition, and stock solution acts on 2min to escherichia coli, and average bacteriostasis rate is 100%.
To colibacillary fungistatic effect
Figure 322871DEST_PATH_IMAGE001
Average clump count of positive controls and scope: 6.47 * 104 (4.90 * 104～7.70 * 104) cfu/ml
The negative control asepsis growth.
Conclusion: this sample stock solution has strong bacteriostasis to escherichia coli.
2, according to GB15979-2002, this sample stock solution under experimental condition acts on 2min to staphylococcus aureus, and average bacteriostasis rate is 100%.
The fungistatic effect of staphylococcus aureus
Figure 584088DEST_PATH_IMAGE002
Average clump count of positive controls and scope: 6.47 * 104 (4.90 * 104～7.70 * 104) cfu/ml
The negative control asepsis growth.
Conclusion: this sample stock solution has strong bacteriostasis to staphylococcus aureus.
3, according to GB15979-2002, this sample is under experimental condition, and stock solution is to Candida albicans effect 10min, and average bacteriostasis rate is 93.14%.
Fungistatic effect to Candida albicans
Figure 66016DEST_PATH_IMAGE003
Average clump count of positive controls and scope: 6.47 * 104 (4.90 * 104～7.70 * 104) cfu/ml
The negative control asepsis growth.
Conclusion: this sample stock solution has strong bacteriostasis to Candida albicans.
(2) irritant experiment
Sample is to rabbit vagina mucosa irritation result of the test
Figure 121697DEST_PATH_IMAGE004
Remarks: every section integration=epithelium+leukocyte infiltration+congestion of blood vessel+edema; Every average integral=(A section integration+B section integration+C section integration)/3; Scoring=(No. 2 animal average integral+, No. 1 animal average integral+No. 3 animal average integral)/3; SI=experimental group average integral-matched group average integral.
Conclusion: this sample is a nonirritant to rabbit vagina mucosa irritation result of the test.
The specific embodiment
Embodiment 1
1. the preparation of soybean extraction liquid:
A. the 10g Semen sojae atricolor after 25 hours, is broken into the mud shape with the pure water of 2.5 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add the chitosan of volume ratio 0.5% then, isolated by filtration obtains transparent soybean extraction liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 80g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 3g is mixed with polyoxyethylene hydrogenated Oleum Ricini 1g, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 120g, glycerol 50 are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 2
1. the preparation of soybean extraction liquid:
A. Semen sojae atricolor 1g after 20 hours, is broken into the mud shape with the pure water of 2 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add the chitosan of volume ratio 0.1% then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 50g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 1g is mixed with TX10 3g, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 50g, glycerol 20g are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 3
1. the preparation of soybean extraction liquid:
A. the 28g Semen sojae atricolor after 30 hours, is broken into the mud shape with the pure water of 3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add volume ratio 0.3% chitosan then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 320g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 10g is mixed with polyoxyethylene castor oil 10g, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 230g, glycerol 300g are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 4
1. the preparation of soybean extraction liquid:
A. the 20g Semen sojae atricolor after 20 hours, is broken into the mud shape with the pure water of 2 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add the chitosan of volume ratio 0.2% then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 120g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 8g is mixed with tween 10g, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 170g, glycerol 150g are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 5
1. the preparation of soybean extraction liquid:
A. the 15g Semen sojae atricolor after 30 hours, is broken into the mud shape with the pure water of 3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add the chitosan of volume ratio 0.4% then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 60g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 2g is mixed with non-ionic surface active agent, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 55g, glycerol 75g are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 6
1. the preparation of soybean extraction liquid:
A. the 25g Semen sojae atricolor after 30 hours, is broken into the mud shape with the pure water of 3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add volume ratio 0.25% chitosan then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 90g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 5g is mixed with non-ionic surface active agent, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 90g, glycerol 120g are mixed to evenly, add in the mixture II, add water stir compositions.
Embodiment 7
1. the preparation of soybean extraction liquid:
A. the 3g Semen sojae atricolor after 30 hours, is broken into the mud shape with the pure water of 3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add the chitosan of volume ratio 0.3% then, isolated by filtration obtains transparent Semen sojae atricolor and extracts thick liquid after concentrating.
2. the preparation of Fructus Sapindi Mukouossi extracting solution:
Get the pulverizing of 65g peel of Fructus Sapindi Mukouossi, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
3. with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
4. plants essential oil 5g is mixed with polyoxyethylene hydrogenated Oleum Ricini 5g, stir, slowly add then in the mixed liquor I, get the mixture II;
5. Oleum Cocois 58g, glycerol 50 are mixed to evenly, add in the mixture II, add water stir compositions.

Claims (6)

1. one kind is cleaned skin care compositions, comprises the raw material of following weight portion: Semen sojae atricolor 1-28 part, Fructus Sapindi Mukouossi 50-320 part.
2. compositions according to claim 1 is characterized in that, the weight ratio of described component is: 10 parts of Semen sojae atricolor, 80 parts of Fructus Sapindi Mukouossis.
3. compositions according to claim 1 is characterized in that, also comprises in the described component:
Plants essential oil 1-10 part, Oleum Cocois 50-230 part, glycerol 20-300 part.
4. compositions according to claim 3 is characterized in that, described composition weight proportioning is: 10 parts of Semen sojae atricolor, 80 parts of Fructus Sapindi Mukouossis, 3 parts of plants essential oils, 120 parts of Oleum Cocois, 50 parts of glycerol.
5. the described preparation of compositions method of the arbitrary claim of claim 1-4 comprises the steps:
(1) preparation of soybean extraction liquid:
A. Semen sojae atricolor after 20-30 hour, is broken into the mud shape with the pure water of 2-3 times of weight dipping;
The Semen sojae atricolor that b. will be broken into the mud shape obtains white emulsion through extraction tower mixing, isolated by filtration;
C. add 4 times of pure water of Semen sojae atricolor weight in the white emulsion, add volume ratio 0.1%-0.5% chitosan then, isolated by filtration obtains transparent soybean extraction liquid after concentrating;
(2) preparation of Fructus Sapindi Mukouossi extracting solution:
Get the peel of Fructus Sapindi Mukouossi pulverizing, soaked 2 hours, boiled 2 hours, filter, get filtrate for later use with its 3 times amount purified water;
(3) press said formula ratio with soybean extraction liquid and Fructus Sapindi Mukouossi extract mixing, get the mixed liquor I;
(4) press formula ratio plants essential oil is mixed with non-ionic surface active agent 1-30 part, stir, slowly add then in the mixed liquor I, get the mixture II;
(5) by formula ratio Oleum Cocois, glycerol are mixed to evenly, add in the mixture II, add water stir compositions.
6. method for preparing according to claim 5 is characterized in that, described non-ionic surface active agent is polyoxyethylene hydrogenated Oleum Ricini, polyoxyethylene castor oil, TX10 or tween.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106389198A (en) * 2016-10-06 2017-02-15 刘艺鹏 Soap nut skin beautifying skin care product
CN109674701A (en) * 2019-01-14 2019-04-26 澳宝化妆品（惠州）有限公司 One kind scalp cleaning compositions of extract containing soapberry fruit and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101411682A (en) * 2008-11-27 2009-04-22 天台县满园春农林开发有限公司 Soapberry complete natural plant facial lotion

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101411682A (en) * 2008-11-27 2009-04-22 天台县满园春农林开发有限公司 Soapberry complete natural plant facial lotion

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
台秀梅: "个人护肤品中的天然组分", 《日用化学品科学》 *
吴小红等: "用于化妆品中的植物", 《国际中医中药杂志》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106389198A (en) * 2016-10-06 2017-02-15 刘艺鹏 Soap nut skin beautifying skin care product
CN109674701A (en) * 2019-01-14 2019-04-26 澳宝化妆品（惠州）有限公司 One kind scalp cleaning compositions of extract containing soapberry fruit and preparation method thereof

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