CN102370670A - Efficient processing method of Chinese caterpillar fungus - Google Patents
Efficient processing method of Chinese caterpillar fungus Download PDFInfo
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- CN102370670A CN102370670A CN2011101689709A CN201110168970A CN102370670A CN 102370670 A CN102370670 A CN 102370670A CN 2011101689709 A CN2011101689709 A CN 2011101689709A CN 201110168970 A CN201110168970 A CN 201110168970A CN 102370670 A CN102370670 A CN 102370670A
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- cordyceps
- caterpillar fungus
- chinese caterpillar
- minutes
- normal saline
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- 238000003672 processing method Methods 0.000 title abstract description 7
- 241000233866 Fungi Species 0.000 title abstract 11
- 240000001307 Myosotis scorpioides Species 0.000 title abstract 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000000034 method Methods 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 16
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 7
- 241000190633 Cordyceps Species 0.000 claims description 80
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
- 238000003754 machining Methods 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 7
- 230000001105 regulatory effect Effects 0.000 claims description 5
- 235000016709 nutrition Nutrition 0.000 abstract description 5
- 230000005714 functional activity Effects 0.000 abstract description 4
- 230000035764 nutrition Effects 0.000 abstract description 4
- 238000002791 soaking Methods 0.000 abstract description 2
- 244000005700 microbiome Species 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- OIRDTQYFTABQOQ-KQYNXXCUSA-N adenosine Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1O OIRDTQYFTABQOQ-KQYNXXCUSA-N 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 5
- 235000017491 Bambusa tulda Nutrition 0.000 description 5
- 241001330002 Bambuseae Species 0.000 description 5
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 5
- 239000011425 bamboo Substances 0.000 description 5
- 239000005030 aluminium foil Substances 0.000 description 4
- 239000000428 dust Substances 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 229910052573 porcelain Inorganic materials 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000002126 C01EB10 - Adenosine Substances 0.000 description 3
- KQLDDLUWUFBQHP-UHFFFAOYSA-N Cordycepin Natural products C1=NC=2C(N)=NC=NC=2N1C1OCC(CO)C1O KQLDDLUWUFBQHP-UHFFFAOYSA-N 0.000 description 3
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 3
- 229960005305 adenosine Drugs 0.000 description 3
- 238000003556 assay Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- OFEZSBMBBKLLBJ-BAJZRUMYSA-N cordycepin Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)C[C@H]1O OFEZSBMBBKLLBJ-BAJZRUMYSA-N 0.000 description 3
- OFEZSBMBBKLLBJ-UHFFFAOYSA-N cordycepine Natural products C1=NC=2C(N)=NC=NC=2N1C1OC(CO)CC1O OFEZSBMBBKLLBJ-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- 208000013116 chronic cough Diseases 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 210000003734 kidney Anatomy 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241001480006 Clavicipitaceae Species 0.000 description 1
- 208000000059 Dyspnea Diseases 0.000 description 1
- 206010013975 Dyspnoeas Diseases 0.000 description 1
- 241000222336 Ganoderma Species 0.000 description 1
- 241000130660 Hepialidae Species 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 208000034189 Sclerosis Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000023597 hemostasis Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 201000001881 impotence Diseases 0.000 description 1
- 210000000629 knee joint Anatomy 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 239000006101 laboratory sample Substances 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229960002668 sodium chloride Drugs 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
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Abstract
The invention discloses an efficient processing method of Chinese caterpillar fungus. The method comprises the following steps of: putting fresh Chinese caterpillar fungus into acid normal saline of which the pH value is 2-4 for soaking in a way that the Chinese caterpillar fungus is fully submerged below the liquid surface; slightly overturning once every 10-20 minutes; washing the Chinese caterpillar fungus till surface-attached impurities are removed; taking the washed Chinese caterpillar fungus out; standing at the room temperature for 25-35 minutes; transferring wet Chinese caterpillar fungus into liquid nitrogen; taking the Chinese caterpillar fungus out 25-35 seconds later; smashing; and quickly packaging in vacuum. By adopting the processing method, the nutrition and functional activity losses of the picked Chinese caterpillar fungus can be prevented in the processing process, browning of the Chinese caterpillar fungus is avoided, and the Chinese caterpillar fungus is hardly polluted by harmful microorganisms when stored for a long time.
Description
Technical field
The invention belongs to technical field of Chinese medicines, be specifically related to a kind of high-efficiency machining method of Cordyceps.
Background technology
Cordyceps plantworms; Entomophyte claims " Cordyceps ", " Cordyceps " again, is to originate in the geographic rare medicinal herbs simply in Yunnan Province of China, Sichuan, Tibet and Qinghai.For Clavicipitaceae fungus Cordyceps colonizes in Stroma and the dry composite body of larva corpse on the Hepialidae insect larvae; This property of medicine is sweet equals, returns lung, kidney channel; And the effect that kidney-supplementing liver-boosting, hemostasis and phlegm are arranged is used for deficiency of kidney essence, impotence and seminal emission, soreness of waist and knee joint, chronic cough dyspnea due to deficiency, chronic cough spitting of blood.
The output of Cordyceps is lower, and demand is very vigorous, and the bright Cordyceps after plucking is difficult to storage and transport, and the medicinal herb grower adopts the sunshine method that Cordyceps is at source dried after harvesting usually at present, and this also is the way that for many years numerous medicinal herb growers extensively taked.This method efficient is low, water content is not easy control; And receive weather effect bigger, Cordyceps volume-diminished in the dry run, the obvious brown stain of color and luster meeting; Influence outward appearance; Also receive harmful microbial contamination easily, nutrition and the functional activity of Cordyceps also have bigger loss in the process of drying simultaneously, also do not have a kind of desirable effective method to solve this technical problem at present.
Summary of the invention
The purpose of this invention is to provide a kind of high-efficiency machining method that prevents Cordyceps nutrition and Cordyceps of functional activity loss in plucking the post-treatment process.
The objective of the invention is to realize in the following manner:
A kind of high-efficiency machining method of Cordyceps, this method may further comprise the steps: get fresh Cordyceps, put into pH value and be 2～4 acid normal saline and soak; The complete submergence Cordyceps of liquid level was overturn once in per 10～20 minutes gently, Cordyceps is washed till the surface nothing adheres to impurity; Take out washed Cordyceps, room temperature was placed 25～35 minutes, changed in the liquid nitrogen when keeping Cordyceps moistening; Take out after 25～35 seconds, pulverize, vacuum-packed rapidly.
Described pH value is that 2～4 acid normal saline is for regulating the normal saline of pH value through citric acid.Compare with other acidic materials, citric acid is easy to be easy to get, safety non-toxic, and Cordyceps can effectively maintain active component through in the normal saline of its adjusting, soaking.
Above-mentioned soak time is preferably 0.5～1.5 hour, and the upset number of times is 3～4 times.The liquid nitrogen temperature of using is-194～-198 ℃, and the preferred liquid nitrogen temperature of using is-196 ℃.The pulverizing time is 1～1.5 minute, and preferably the pulverizing time is about 1 minute, is crushed to 200 orders～400 orders.
The most preferred method of Cordyceps highly-efficient processing of the present invention is: get fresh Cordyceps, be no more than 8 hours apart from gathering, put into pH value and be 2～4 acid injection normal saline (be preferably mass percentage concentration be 0.9% sodium-chloride water solution) immersion 1 hour; The complete submergence Cordyceps of liquid level overturn in per 15 minutes gently, impurity such as the silt that adheres on the removal Cordyceps surface, dust; Take out washed Cordyceps with bamboo let, room temperature was placed in the porcelain dish about 30 minutes, kept the moistening of Cordyceps; Polypide is changed in the liquid nitrogen; Liquid nitrogen temperature is about-196 ℃, takes out after 30 seconds, puts into the spheroid mill and pulverizes 1～1.5 minute; Be crushed to 200 orders～400 orders, Cordyceps is sealed with aluminium foil bag is vacuum-packed rapidly.
In addition, the present invention has tried out the container of various material, finds to adorn Cordyceps to container with bamboo length, and it is comparatively suitable to change in the liquid nitrogen container again, and easily Cordyceps is poured out after taking out, not sticking wall.
When Cordyceps was pulverized, the time was unsuitable long, get final product in 1～1.5 minute, both can guarantee the fineness pulverized, can avoid equipment heating destruction nutritional labeling in the crushing process again.
Adopt Cordyceps that processing method of the present invention obtains and the comparison of shining the Cordyceps active constituent content that drying method obtains:
Laboratory sample: get bright Cordyceps, be no more than 8 hours apart from gathering.
Method 1, dry Cordyceps: between 4～June of collection period, dry after bright Cordyceps is removed mud in the Qinghai-Tibet Platean Cordyceps, under the sunshine sufficiency, directly to dry in 2～3 days, the Cordyceps weight after drying is 20% of bright Cordyceps, under 4 ℃ of conditions, preserves 12 months.
Method 2, Cordyceps powder:, under 4 ℃ of conditions, preserved 12 months according to the Cordyceps powder that the embodiment of the invention 1 method prepares.
Content assaying method:
1, with reference to " Chinese food journal " in June, 2007, P144～149, Gu Zhenyu etc. publish an article: the assay method of cordycepic acid, cordycepin in " content of cordycepin and cordycepic acid in the high effective liquid chromatography for measuring Cordyceps ".
2, the Cordyceps polysaccharide detection method is with reference to the assay method of polysaccharide under Ganoderma item of 2010 editions pharmacopeia.
3, the adenosine detection method is with reference to the assay method of adenosine under Cordyceps item of 2010 editions pharmacopeia.
The Cordyceps that fresh Cordyceps, processing method of the present invention are obtained compares with the active constituent content and the outward appearance of shining the Cordyceps that drying method obtains, and the result sees table 1:
Table 1
The result: under 4 ℃ of conditions, preserving 12 months effects with the Cordyceps powder of the inventive method preparation does not have destruction, the polypide invariant color, and the outward appearance abnormal smells from the patient is all good.Drying Cordyceps weight is about 20% of bright Cordyceps, so corresponding functional component content should be divided by about 5, but through active constituent content measuring, can dry adenosine in the Cordyceps, cordycepin, cordycepic acid has greater loss when drying, and the browning that darkens.
" % " of the present invention is the quality percentage composition.
With prior art beneficial effect more of the present invention: with prior art relatively, processing method of the present invention is soaked in pH value is 2～4 acid normal saline and can fully be removed silt and keep the polypide even tissue full; In liquid nitrogen, placing can be rapidly with the polypide sclerosis, the convenient pulverizing.Processing method of the present invention has prevented that Cordyceps nutrition in plucking the post-treatment process runs off with functional activity, and color and luster can brown stain, and outward appearance is good, and long-term the placement is difficult for receiving being harmful to microbial contamination.
The specific embodiment
Embodiment 1
Get apart from the bright Cordyceps about 200 that are no more than 8 hours of gathering, nearly weigh 200 grams, putting into and using mass percent concentration is that the injection normal saline (pH value is 4) that 10% citric acid solution is regulated soaked 1 hour, and liquid level surpasses the Cordyceps height.Overturn once gently in per 15 minutes, impurity such as the silt of removal Cordyceps surface attachment, dust take out washed Cordyceps with bamboo let, and room temperature was placed on porcelain dish interior 30 minutes; When keeping Cordyceps moistening, polypide is changed over to rapidly in the small-sized liquid nitrogen container, liquid nitrogen temperature is about-196 ℃; Take out after 30 seconds, put into the spheroid mill and pulverize, a charge weight is about 50 grams in the spheroid mill; About 1 minute pulverizing time, be crushed to 200 orders, Cordyceps is sealed with aluminium foil bag is vacuum-packed rapidly.
Embodiment 2
Get apart from the bright Cordyceps about 200 that are no more than 8 hours of gathering, nearly weigh 200 grams, putting into and using mass percent concentration is that the injection normal saline (pH value is 2) that 10% citric acid solution is regulated soaked 0.5 hour, and liquid level surpasses the Cordyceps height.Overturn once gently in per 10 minutes, impurity such as the silt of removal Cordyceps surface attachment, dust take out washed Cordyceps with bamboo let, and room temperature was placed on porcelain dish interior 25 minutes; When keeping Cordyceps moistening, polypide is changed over to rapidly in the small-sized liquid nitrogen container, liquid nitrogen temperature is about-194 ℃; Take out after 35 seconds, put into the spheroid mill and pulverize, a charge weight is about 50 grams in the spheroid mill; About 1 minute pulverizing time, be crushed to 200 orders, Cordyceps is sealed with aluminium foil bag is vacuum-packed rapidly.
Embodiment 3
Get apart from the bright Cordyceps about 200 that are no more than 8 hours of gathering, nearly weigh 200 grams, putting into and using mass percent concentration is that the injection normal saline (pH value is 3) that 10% citric acid solution is regulated soaked 1.5 hours, and liquid level surpasses the Cordyceps height.Overturn once gently in per 20 minutes, impurity such as the silt of removal Cordyceps surface attachment, dust take out washed Cordyceps with bamboo let, and room temperature was placed on porcelain dish interior 35 minutes; When keeping Cordyceps moistening, polypide is changed over to rapidly in the small-sized liquid nitrogen container, liquid nitrogen temperature is about-198 ℃; Take out after 25 seconds, put into the spheroid mill and pulverize, a charge weight is about 50 grams in the spheroid mill; About 1.5 minutes pulverizing time, be crushed to 400 orders, Cordyceps is sealed with aluminium foil bag is vacuum-packed rapidly.
Claims (6)
1. the high-efficiency machining method of a Cordyceps is characterized in that this method may further comprise the steps: get fresh Cordyceps, put into pH value and be 2～4 acid normal saline and soak; The complete submergence Cordyceps of liquid level overturn once in per 10～20 minutes gently, Cordyceps is washed till the surface nothing adheres to impurity; Take out washed Cordyceps, room temperature was placed 25～35 minutes, changed in the liquid nitrogen when keeping Cordyceps moistening; Take out after 25～35 seconds, pulverize, vacuum-packed rapidly.
2. the high-efficiency machining method of Cordyceps according to claim 1 is characterized in that described pH value is that 2～4 acid normal saline is for regulating the normal saline of pH value through citric acid.
3. the high-efficiency machining method of Cordyceps according to claim 1 is characterized in that soak time is 0.5～1.5 hour, and the upset number of times is 3～4 times.
4. the high-efficiency machining method of Cordyceps according to claim 1 is characterized in that the liquid nitrogen temperature that this method is used is-194～198 ℃.
5. the high-efficiency machining method of Cordyceps according to claim 1 is characterized in that this method pulverizing time is 1～1.5 minute.
6. the high-efficiency machining method of Cordyceps according to claim 1 is characterized in that being crushed to 200 orders～400 orders.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110168970 CN102370670B (en) | 2011-06-22 | 2011-06-22 | Efficient processing method of Chinese caterpillar fungus |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110168970 CN102370670B (en) | 2011-06-22 | 2011-06-22 | Efficient processing method of Chinese caterpillar fungus |
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| CN102370670A true CN102370670A (en) | 2012-03-14 |
| CN102370670B CN102370670B (en) | 2013-09-11 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103706582A (en) * | 2012-12-31 | 2014-04-09 | 陈玉龙 | Quick cleaning method for Cordyceps sinensis |
| CN106214706A (en) * | 2016-03-09 | 2016-12-14 | 西藏藏山奇藏医药保健品有限公司 | A kind of heavy metals removal method in Cordyceps |
| CN107674104A (en) * | 2017-09-05 | 2018-02-09 | 马鞍山市安康菌业有限公司 | The extracting method of cordycepin in a kind of Cordyceps militaris |
| CN108251246A (en) * | 2018-03-05 | 2018-07-06 | 安徽省霍山县福康石斛开发有限公司 | A kind of preparation method of radix polygonati officinalis dendrobium wine |
| CN108478710A (en) * | 2018-03-05 | 2018-09-04 | 安徽省霍山县福康石斛开发有限公司 | A kind of processing technology of Huoshan rice dry measure used in former times vertical bar |
| CN109717356A (en) * | 2019-03-08 | 2019-05-07 | 中国科学院西北高原生物研究所 | A kind of fresh cordyceps sinensis quick-freezing fresh-keeping method of liquid nitrogen combination with liquid carbon dioxide |
| CN109717355A (en) * | 2019-03-08 | 2019-05-07 | 中国科学院西北高原生物研究所 | A kind of preservation method of fresh cordyceps sinensis |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103706582A (en) * | 2012-12-31 | 2014-04-09 | 陈玉龙 | Quick cleaning method for Cordyceps sinensis |
| CN106214706A (en) * | 2016-03-09 | 2016-12-14 | 西藏藏山奇藏医药保健品有限公司 | A kind of heavy metals removal method in Cordyceps |
| CN107674104A (en) * | 2017-09-05 | 2018-02-09 | 马鞍山市安康菌业有限公司 | The extracting method of cordycepin in a kind of Cordyceps militaris |
| CN108251246A (en) * | 2018-03-05 | 2018-07-06 | 安徽省霍山县福康石斛开发有限公司 | A kind of preparation method of radix polygonati officinalis dendrobium wine |
| CN108478710A (en) * | 2018-03-05 | 2018-09-04 | 安徽省霍山县福康石斛开发有限公司 | A kind of processing technology of Huoshan rice dry measure used in former times vertical bar |
| CN109717356A (en) * | 2019-03-08 | 2019-05-07 | 中国科学院西北高原生物研究所 | A kind of fresh cordyceps sinensis quick-freezing fresh-keeping method of liquid nitrogen combination with liquid carbon dioxide |
| CN109717355A (en) * | 2019-03-08 | 2019-05-07 | 中国科学院西北高原生物研究所 | A kind of preservation method of fresh cordyceps sinensis |
| CN109717356B (en) * | 2019-03-08 | 2022-03-08 | 中国科学院西北高原生物研究所 | Fresh cordyceps sinensis quick-freezing preservation method combining liquid nitrogen with liquid carbon dioxide |
| CN109717355B (en) * | 2019-03-08 | 2022-04-08 | 中国科学院西北高原生物研究所 | Fresh preservation method of fresh cordyceps sinensis |
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| CN102370670B (en) | 2013-09-11 |
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