CN102365256A - 制备纯环十二酮的方法 - Google Patents

制备纯环十二酮的方法 Download PDF

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Publication number
CN102365256A
CN102365256A CN2010800147909A CN201080014790A CN102365256A CN 102365256 A CN102365256 A CN 102365256A CN 2010800147909 A CN2010800147909 A CN 2010800147909A CN 201080014790 A CN201080014790 A CN 201080014790A CN 102365256 A CN102365256 A CN 102365256A
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CN
China
Prior art keywords
carbon atoms
rings
composition
compound
cyclic
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Pending
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CN2010800147909A
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English (en)
Chinese (zh)
Inventor
J·H·特莱斯
B·罗斯勒-菲戈尔`
A·豪克
A·迈尔
C·米勒
M·舍伯尔
T·基希纳
S·塞斯什库斯
R·平科斯
G-D·特本
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BASF SE
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BASF SE
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Publication of CN102365256A publication Critical patent/CN102365256A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2010800147909A 2009-01-28 2010-01-27 制备纯环十二酮的方法 Pending CN102365256A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09151525.4 2009-01-28
EP09151525 2009-01-28
PCT/EP2010/050888 WO2010086314A1 (de) 2009-01-28 2010-01-27 Verfahren zur herstellung von reinem cyclododecanon

Publications (1)

Publication Number Publication Date
CN102365256A true CN102365256A (zh) 2012-02-29

Family

ID=42262059

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2010800147909A Pending CN102365256A (zh) 2009-01-28 2010-01-27 制备纯环十二酮的方法

Country Status (7)

Country Link
US (1) US8188320B2 (https=)
EP (1) EP2391597B1 (https=)
JP (1) JP5661647B2 (https=)
KR (1) KR20110110359A (https=)
CN (1) CN102365256A (https=)
ES (1) ES2698849T3 (https=)
WO (1) WO2010086314A1 (https=)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379547A (zh) * 2012-06-13 2015-02-25 巴斯夫欧洲公司 制备大环酮的方法
CN105315146A (zh) * 2014-08-01 2016-02-10 赢创德固赛有限公司 制备环十二酮的方法
CN106715375A (zh) * 2014-09-30 2017-05-24 巴斯夫欧洲公司 新环状醛作为芳香物质的用途
CN107001996A (zh) * 2014-10-14 2017-08-01 巴斯夫欧洲公司 十六碳‑8,15‑二烯醛作为合成香料的用途
CN108137461A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 提纯环十六碳-8-烯-1-酮的方法
CN108137460A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 (e/z)-环十五碳烯酮异构体的新型混合物的用途、其制备和作为增香剂物质的用途
CN114874085A (zh) * 2022-07-12 2022-08-09 中国天辰工程有限公司 一种环十二酮提纯工艺
CN116003254A (zh) * 2015-01-30 2023-04-25 西姆莱斯股份公司 用于制备取代的烷基环烷酮的方法

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KR20110110359A (ko) 2009-01-28 2011-10-06 바스프 에스이 순수 시클로도데칸온의 제조 방법
DE102009047196A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von 1,6-Hexandiol
WO2011115132A1 (ja) * 2010-03-15 2011-09-22 宇部興産株式会社 アミド化合物の製造方法
US9394212B2 (en) 2010-06-15 2016-07-19 Basf Se Process for the cooligomerization of olefins
DE102014212602A1 (de) 2013-07-02 2015-01-08 Basf Se Verfahren zur Herstellung eines Ketons aus einem Olefin
EP3002058A1 (de) * 2014-10-02 2016-04-06 Evonik Degussa GmbH Katalysatorsystem zur Herstellung von Ketonen aus Epoxiden
EP3938485A1 (en) * 2019-03-15 2022-01-19 Basf Se Use of 4,8,11-dodecatrienal to impart a clean aroma impression to a composition

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DE10344595A1 (de) * 2003-09-25 2005-05-12 Basf Ag Verfahren zur Herstellung eines Ketons
DE102004046167A1 (de) 2004-09-23 2006-04-06 Basf Ag Verfahren zur Reinigung und Aufkonzentrierung von Distickstoffmonoxid
DE102005048250A1 (de) * 2005-10-07 2007-04-12 Basf Ag Verfahren zur Farbzahlverbesserung
DE102005055588A1 (de) 2005-11-22 2007-05-24 Basf Ag Verfahren zur Isolierung von N2O
ATE517078T1 (de) * 2006-03-10 2011-08-15 Basf Se Verfahren zur herstellung von benzophenoniminen
KR101374007B1 (ko) * 2006-06-29 2014-03-12 바스프 에스이 시클릭 케톤의 제조 방법
JP5086342B2 (ja) * 2006-06-29 2012-11-28 ビーエーエスエフ ソシエタス・ヨーロピア 環状ケトンの製造方法
US7790930B2 (en) * 2006-06-29 2010-09-07 Basf Se Method for purifying cyclic ketones
JP5244121B2 (ja) 2006-12-11 2013-07-24 ビーエーエスエフ ソシエタス・ヨーロピア Ｎ２ｏを単離する方法
WO2009024549A2 (de) * 2007-08-21 2009-02-26 Basf Se Verfahren und vorrichtung zur oxidation organischer verbindungen
KR20100043253A (ko) * 2007-08-21 2010-04-28 바스프 에스이 유기 화합물의 산화를 위한 방법 및 장치
MY148576A (en) * 2007-12-21 2013-04-30 Basf Se Process for preparing epsilon-caprolactone
WO2009092683A2 (de) 2008-01-25 2009-07-30 Basf Se METHODE ZUR SELEKTIVEN GROßTECHNISCHEN HERSTELLUNG VON 1,5,9 CYCLODODECATRIEN
WO2009092682A2 (de) 2008-01-25 2009-07-30 Basf Se Verfahren und vorrichtung zur destillativen aufarbeitung von 1,5,9-cyclododecatrien und gewinnung von cdt mit hoher reinheit
WO2009121707A1 (de) 2008-04-02 2009-10-08 Basf Se Verfahren zur reinigung von distickstoffmonoxid
JP5372135B2 (ja) 2008-04-02 2013-12-18 ビーエーエスエフ ソシエタス・ヨーロピア Ｎ２ｏの精製方法
WO2010023211A2 (de) * 2008-08-29 2010-03-04 Basf Se Verfahren zur herstellung von zyklischen ketonen
EP2384317B1 (de) * 2008-12-30 2014-04-23 Basf Se Verfahren zur herstellung von ketonen durch umsetzung von 1,1-disubtituierten olefinen mit n2o
CN102361687B (zh) 2009-01-21 2015-05-13 巴斯夫欧洲公司 用于非催化或均相催化反应的管束反应器
WO2010086313A1 (de) * 2009-01-28 2010-08-05 Basf Se Verfahren zur isolierung von dodecatrienal und seine verwendung als aromastoff
KR20110110359A (ko) 2009-01-28 2011-10-06 바스프 에스이 순수 시클로도데칸온의 제조 방법

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379547A (zh) * 2012-06-13 2015-02-25 巴斯夫欧洲公司 制备大环酮的方法
CN105315146A (zh) * 2014-08-01 2016-02-10 赢创德固赛有限公司 制备环十二酮的方法
CN105315146B (zh) * 2014-08-01 2019-09-20 赢创德固赛有限公司 制备环十二酮的方法
CN106715375A (zh) * 2014-09-30 2017-05-24 巴斯夫欧洲公司 新环状醛作为芳香物质的用途
CN107001996A (zh) * 2014-10-14 2017-08-01 巴斯夫欧洲公司 十六碳‑8,15‑二烯醛作为合成香料的用途
CN116003254A (zh) * 2015-01-30 2023-04-25 西姆莱斯股份公司 用于制备取代的烷基环烷酮的方法
CN108137461A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 提纯环十六碳-8-烯-1-酮的方法
CN108137460A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 (e/z)-环十五碳烯酮异构体的新型混合物的用途、其制备和作为增香剂物质的用途
CN114874085A (zh) * 2022-07-12 2022-08-09 中国天辰工程有限公司 一种环十二酮提纯工艺
CN114874085B (zh) * 2022-07-12 2022-10-11 中国天辰工程有限公司 一种环十二酮提纯工艺

Also Published As

Publication number Publication date
JP5661647B2 (ja) 2015-01-28
US8188320B2 (en) 2012-05-29
EP2391597A1 (de) 2011-12-07
ES2698849T3 (es) 2019-02-06
EP2391597B1 (de) 2018-08-22
WO2010086314A1 (de) 2010-08-05
JP2012516301A (ja) 2012-07-19
US20100191018A1 (en) 2010-07-29
KR20110110359A (ko) 2011-10-06

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Application publication date: 20120229