CN102326836A - Production method for alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents - Google Patents

Production method for alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents Download PDF

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Publication number
CN102326836A
CN102326836A CN201110226701A CN201110226701A CN102326836A CN 102326836 A CN102326836 A CN 102326836A CN 201110226701 A CN201110226701 A CN 201110226701A CN 201110226701 A CN201110226701 A CN 201110226701A CN 102326836 A CN102326836 A CN 102326836A
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spicy
alcohol
fresh
sterilization
attapulgite
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吴梦舟
许庆华
蒋文兰
许盛英
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Abstract

The invention discloses a production method for alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents, which has the main technical scheme that a crushed spicy and hot mixture and edible alcohol are mixed and are added into a stainless steel container, soaking, press filtering, blending, high-speed stirring and dehydration treatment are carried out, and the materials are canned into finished products of the alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents. The alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents consist of pepper, red pepper, truestar anisetree, fennel, black pepper, cinnamon, liquorice, alcohol and high-viscosity attapulgite clay powder. The active ingredients of the lcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents are gradually released and are seeped into all spaces in a food package bag, a layer of sterilization and fresh-keeping film is formed on the surface of the food, after the alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents are in contact with the food with higher water content, the alcoholic strength of the sterilization and fresh-keeping film is higher than or equal to 70 degrees, the optimum sterilization concentration can be maintained for a longer time, the goals of full process sterilization and fresh keeping of the food in the shelf life are ensured, and the sterilization and fresh-keeping agents are applicable to the sterilization and the fresh keeping of meat products and aquatic products.

Description

The production method of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite
Technical field
The present invention relates to sterilization fresh-keeping liquid, be specifically related to the production method of the spicy antistaling disinfectant of a kind of alcohol radical cream-like attapulgite.
Background technology
The invasion and attack of microorganisms such as bacterium, mould, saccharomycete are principal elements of food spoilage; Therefore in production, processing and the storage of food; Anticorrisive agent has very, and important use is worth; But because the fabricated food additive has certain toxic and side effect, people tend to select safe antiseptics for natural food.
The change of soil water content of food in shelf life usually can cause the change of food quality, such as; Fresh fruit of vegetables is at duration of storage; Because the evaporation of moisture can cause fruits and vegetables outward appearance wilting shrinkage, freshness and tender and crisp degree all descend, and commodity value also descends thereupon even loses; And the loose goods of institutional frameworks such as cake, bread because phenomenons such as drying shrinkage is stiff can take place in the evaporation of moisture, also cause the decline of its edible quality.The evaporation of food water also may promote the activity of some enzyme in the food to increase, and makes the polymer substance degraded, shortens the shelf life of product.Therefore, the food that some water content are higher, for example food sterilizations such as fresh fish, fresh meat, fruit, vegetables, bean product, curing food and birthday cake are fresh-keeping, should not adopt deoxidation anti-mould fresh keeping agent and drier to carry out Preservation Treatment.
Adopt the alcohol radical extract to carry out sterilization, mildew-resistant and anticorrosion; In the hope of reaching fresh-keeping purpose, be not that the alcohol radical extract directly is added on inside of food, but be used for the packing of food; Because the water content of some food self is than higher; When alcohol radical extract alcoholic strength was spent less than 80, the active ingredient of alcohol radical extract alcoholic strength reduced the practical effect of sterilization fresh-keeping easily by dilution of the moisture in the food and dissolving.
Chinese patent Granted publication CN 100353871 C; December 12 2007 Granted publication day; Name is called " granular concave rod alcohol antistaling agent ", discloses that a kind of " a kind of granular concave rod alcohol antistaling agent, the main points of its technical scheme are; granular concave rod alcohol antistaling agent, are made up of the concavo-convex rod of porous particle, edible alcohol, citric acid, sodium Diacetate and water.With granular concave rod alcohol antistaling agent with being packed by fresh-keeping foodstuff; Fresh-keeping gas in the granular concave rod can slowly release, and evaporate into the various piece in the package body, around by fresh-keeping foodstuff, forms certain density protective layer; Can suppress bacterial reproduction; Kill multiple mould, bacterium and other spoilage organisms, thereby the food in preventing to pack is mouldy and putrid and deteriorated, reaches fresh-keeping effect.Be applicable to the fresh-keeping of various fruits and vegetables, food, meat and aquatic products ".
The weak point of above-mentioned patent is " granular concave rod alcohol antistaling agent " alcoholic strength less than 80 degree, and being used for the higher food of water content, to carry out the practical effect of sterilization fresh-keeping undesirable.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, the production method of the spicy antistaling disinfectant of a kind of alcohol radical cream-like attapulgite is provided.
The production method of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite: the spicy mixture after will pulverizing and edible alcohol mix the back add in the rustless steel container soak, press filtration, blend, high-speed stirred and processed, canned is the spicy antistaling disinfectant finished product of alcohol radical cream-like attapulgite.
The spicy antistaling disinfectant of alcohol radical cream-like attapulgite is made up of Chinese prickly ash, pimiento, Chinese anise, fennel seeds, pepper, cassia bark, Radix Glycyrrhizae, alcohol and high sticking Concave-convex clay rod powder.
Chinese prickly ash is to 10 kinds of gram-positive bacterias such as bacillus anthracis, hemolytic streptococcus, corynebacterium diphtheriae, Diplococcus pneumopniae, staphylococcus aureus, lemon yellow and staphylococcus albus, hay bacilluses, and pathogenic bacteria all have the obvious suppression effect in the intestines such as Escherichia coli, Song Nei Shi dysentery bar flute, proteus, typhoid fever and paratyphosum Bacterium, Pseudomonas aeruginosa, comma bacillus.
Pimiento contains capsicim, and hot fragrance is arranged, and can remove the fishy smell in the dish, and nutritive value is very high, has resisting cold, whets the appetite and the effect of sterilization, also has anti-inflammatory and antioxidation.
The aromatic odor that Chinese anise is pleasantly sweet and strong all has stronger inhibitory action to staphylococcus aureus, pneumococcus, corynebacterium diphtheriae, hay bacillus, comma bacillus, typhoid bacillus, paratyphosum Bacterium, shigella dysenteriae, Escherichia coli and common pathogenic dermatophyte.
Fennel seeds have antibacterial action, can remove peculiar smell such as the smelling of fish or mutton.
Pepper has the effect of antiseptic and inhibiting bacteria function, goes raw meat to separate and has a strong smell, and can separate the poison of foods such as fish, crab, meat or fish.
Cassia bark has inhibitory action to staphylococcus aureus, shigella dysenteriae, Escherichia coli, proteus etc.
Radix Glycyrrhizae is a kind ofly both can increase sweet seasoning, anti-oxidant, has the function of antibacterial, anti-inflammatory, detoxifcation and deodorizing again.Radix Glycyrrhizae also has detoxication, and staphylococcus aureus, hay bacillus, saccharomycete, fungi and streptococcus etc. are had inhibitory action.
Alcohol has strong lethal effect for bacterium when 70% (V), also can make anticorrisive agent, solvent etc.If alcohol concentration is lower than 70%,, can not the protein coagulating in its body can not thoroughly be killed bacterium equally though can get in the bacterial body.Have only the alcohol of 70%-75% successfully to enter in the bacterial body, again can be effectively with the protein coagulating in the bacterial body, thereby thorough killing bacteria.
The Concave-convex clay rod soil property is fine and smooth; Water imbibition is strong, tool viscosity and plasticity when wet, strong adhesion; It is a kind of natural minerals gel carrier; Help the spicy antistaling disinfectant of alcohol radical cream-like attapulgite and be adsorbed on papery, cloth matter and the solid body, make the spicy antistaling disinfectant of alcohol radical cream-like attapulgite of various different conditions, increase the purposes of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite.
High sticking Concave-convex clay rod powder is meant gets 28.0g Concave-convex clay rod powder sample; Add in the suspension cup of homogenizer, add 372g water again, the suspension cup is placed on the homogenizer; Under 11000 rev/mins of rotating speeds, stirred 20 minutes; To pass through the high-speed stirred sample suspension again and pour in the beaker of 250ml, the viscosity of using NDJ-1 type rotation viscometer to test its suspension, the Concave-convex clay rod powder of tested viscosity value >=2200 mPas is high sticking Concave-convex clay rod powder.
The present invention is achieved through following technical proposals:
1, the production method of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite: ⑴ adds spicy mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ spicy mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are spicy alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 55~70 degree; The batching of spicy alcohol mixture is made up of following component by weight percentage: spicy mixture 45~85% and alcohol 15~55%, and soak time was controlled at 2~8 days; ⑶ carry out press filtration in the spicy alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is spicy alcohol extract; ⑷ add in the spicy alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be the spicy alcohol extract of high concentration, the batching of the spicy alcohol extract of high concentration is made up of following component by weight percentage: the alcohol 25~65% of spicy alcohol extract 35~75% and alcoholic strength>=95 degree; ⑸ mix spicy alcohol extract of high concentration and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is the spicy antistaling disinfectant semi-finished product of alcohol radical cream-like attapulgite; The speed controlling of homogenizer is 4000~5000 rev/mins, and the half-finished batching of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite is made up of following component by weight percentage: spicy alcohol extract 85~95% of high concentration and high sticking Concave-convex clay rod powder 5~15%; ⑹ with carrying out processed in the spicy antistaling disinfectant semi-finished product input of the alcohol radical cream-like attapulgite alcohol radical sterilization fresh-keeping fluid dewatering device; The spicy antistaling disinfectant alcoholic strength of alcohol radical cream-like attapulgite after the processed>=99 degree, canned is the spicy antistaling disinfectant finished product of alcohol radical cream-like attapulgite;
The batching of said spicy mixture is made up of following component by weight percentage: Chinese prickly ash 20~40%, pimiento 1~20%, anise 1~20%, fennel seeds 1~15%, pepper 1~15%, cassia bark 1~10% and Radix Glycyrrhizae 1~10%;
Said alcohol radical sterilization fresh-keeping fluid dewatering device is made up of cylindrical container, cover plate, attachment bolt, charging aperture, charging valve, pressure-air import, pressure-air air intake valve, pressure-air pipeline, web plate, stainless steel basket, the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering, transparent glass tube, alcohol meter, transparent glass tube loam cake, glass tube support, discharge nozzle, discharging valve, discharging opening and support;
The separate case application of alcohol radical sterilization fresh-keeping fluid dewatering device patent of invention, number of patent application is: 201110211758.6;
The agent of said graininess alcohol radical sterilization fresh-keeping fluid dewatering is made up of red bentonite, dolomite Concave-convex clay rod, bauxite, sulfuric acid, high sticking Concave-convex clay rod powder and 3A molecular screen primary powder.The production method of graininess alcohol radical sterilization fresh-keeping fluid dewatering agent: carry out acidification after red bentonite, dolomite Concave-convex clay rod and bauxite mixed, again with the sticking Concave-convex clay rod powder of height with the 3A molecular screen primary powder mixes, the common pulverizing is the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering after compressing tablet and the roasting;
Graininess alcohol radical sterilization fresh-keeping fluid dewatering agent separate case application patent of invention, number of patent application is: 201110210542.8.
Spicy and other batching in the spicy antistaling disinfectant of alcohol radical cream-like attapulgite all has sterilization fresh-keeping effect preferably; The concentration of active ingredient and alcohol concentration are all high; Be used in the packaging for foodstuff; The active ingredient of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite slowly discharges and is penetrated into the interior institute of packaging for foodstuff has living space, and forms one deck sterilization fresh-keeping film on the surface of food; Because the alcoholic strength of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite >=99 degree; After the higher Food Contact of water content; The alcoholic strength of sterilization fresh-keeping film >=70 degree; The concentration that keeps best sterilization of long period is goed deep into the inner kill microorganisms of food or is suppressed its growth and breeding, guarantees that food whole process in shelf life reaches sterilization, prevents to go mouldy and fresh-keeping purpose.
The simple alcohol that uses is the antibacterial and sterilization at food surface; There is certain limitation in the action of microorganisms in food inside own; The spicy antistaling disinfectant of alcohol radical cream-like attapulgite has been given full play to spicy and alcohol characteristic separately; Antibacterial, sterilization in surface and inner kill microorganisms carry out simultaneously, are a kind of antistaling disinfectants efficiently.
Method for using: 1. with nonwoven the solid-state sorbing material that adsorbs behind the spicy antistaling disinfectant of alcohol radical cream-like attapulgite, be packaged as the spicy antistaling disinfectant of a kind of solid-state alcohol radical cream-like attapulgite, the nonwoven skin is packed with plastic bag sealing; 2. tear the plastic bag sealing packing; The spicy antistaling disinfectant of solid-state alcohol radical cream-like attapulgite is placed in the food container that needs sterilization fresh-keeping; Active ingredient in the spicy antistaling disinfectant of alcohol radical cream-like attapulgite constantly slowly discharges in food container; Form one deck sterilization fresh-keeping film on the surface of food, reach sterilization, prevent to go mouldy and fresh-keeping purpose.
That the spicy antistaling disinfectant of alcohol radical cream-like attapulgite has is nontoxic, noresidue, no burn into quality safety is reliable and bactericidal effect is good characteristics, can not produce harm to human body, and production method technology is simple, and is easy to operate, do not have environmental pollution.
The spicy antistaling disinfectant of alcohol radical cream-like attapulgite is applicable to produces various paperys, cloth matter and the spicy antistaling disinfectant of solid-state alcohol radical cream-like attapulgite, also is applicable to add in the food sterilization preservation device and carries out sterilization fresh-keeping.
The spicy antistaling disinfectant of alcohol radical cream-like attapulgite is applicable to the sterilization fresh-keeping of meat products and aquatic products.
The specific embodiment
Below in conjunction with embodiment the present invention is done further description:
1, the production method of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite: ⑴ adds spicy mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ spicy mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are spicy alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 60 degree; The batching of spicy alcohol mixture is made up of following component by weight percentage: spicy mixture 66% and alcohol 34%, and soak time was controlled at 5 days; ⑶ carry out press filtration in the spicy alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is spicy alcohol extract; ⑷ add in the spicy alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be the spicy alcohol extract of high concentration, the batching of the spicy alcohol extract of high concentration is made up of following component by weight percentage: the alcohol 32% of spicy alcohol extract 68% and alcoholic strength>=95 degree; ⑸ mix spicy alcohol extract of high concentration and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is the spicy antistaling disinfectant semi-finished product of alcohol radical cream-like attapulgite; The speed controlling of homogenizer is 4500~5000 rev/mins, and the half-finished batching of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite is made up of following component by weight percentage: spicy alcohol extract 92% of high concentration and high sticking Concave-convex clay rod powder 8%; ⑹ with carrying out processed in the spicy antistaling disinfectant semi-finished product input of the alcohol radical cream-like attapulgite alcohol radical sterilization fresh-keeping fluid dewatering device; The spicy antistaling disinfectant alcoholic strength of alcohol radical cream-like attapulgite after the processed>=99 degree, canned is the spicy antistaling disinfectant finished product of alcohol radical cream-like attapulgite;
The batching of said spicy mixture is made up of following component by weight percentage: Chinese prickly ash 30%, pimiento 1~20%, anise 15%, fennel seeds 12%, pepper 10%, cassia bark 8% and Radix Glycyrrhizae 5%.
The on-the-spot test result: the alcoholic strength of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite is 99.2%.

Claims (1)

1. the production method of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite is characterized in that, ⑴ adds spicy mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ spicy mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are spicy alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 55~70 degree; The batching of spicy alcohol mixture is made up of following component by weight percentage: spicy mixture 45~85% and alcohol 15~55%, and soak time was controlled at 2~8 days; ⑶ carry out press filtration in the spicy alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is spicy alcohol extract; ⑷ add in the spicy alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be the spicy alcohol extract of high concentration, the batching of the spicy alcohol extract of high concentration is made up of following component by weight percentage: the alcohol 25~65% of spicy alcohol extract 35~75% and alcoholic strength>=95 degree; ⑸ mix spicy alcohol extract of high concentration and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is the spicy antistaling disinfectant semi-finished product of alcohol radical cream-like attapulgite; The speed controlling of homogenizer is 4000~5000 rev/mins, and the half-finished batching of the spicy antistaling disinfectant of alcohol radical cream-like attapulgite is made up of following component by weight percentage: spicy alcohol extract 85~95% of high concentration and high sticking Concave-convex clay rod powder 5~15%; ⑹ with carrying out processed in the spicy antistaling disinfectant semi-finished product input of the alcohol radical cream-like attapulgite alcohol radical sterilization fresh-keeping fluid dewatering device; The spicy antistaling disinfectant alcoholic strength of alcohol radical cream-like attapulgite after the processed>=99 degree, canned is the spicy antistaling disinfectant finished product of alcohol radical cream-like attapulgite;
The batching of said spicy mixture is made up of following component by weight percentage: Chinese prickly ash 20~40%, pimiento 1~20%, anise 1~20%, fennel seeds 1~15%, pepper 1~15%, cassia bark 1~10% and Radix Glycyrrhizae 1~10%;
Said alcohol radical sterilization fresh-keeping fluid dewatering device is made up of cylindrical container, cover plate, attachment bolt, charging aperture, charging valve, pressure-air import, pressure-air air intake valve, pressure-air pipeline, web plate, stainless steel basket, the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering, transparent glass tube, alcohol meter, transparent glass tube loam cake, glass tube support, discharge nozzle, discharging valve, discharging opening and support;
The agent of said graininess alcohol radical sterilization fresh-keeping fluid dewatering is made up of red bentonite, dolomite Concave-convex clay rod, bauxite, sulfuric acid, high sticking Concave-convex clay rod powder and 3A molecular screen primary powder; The production method of graininess alcohol radical sterilization fresh-keeping fluid dewatering agent: carry out acidification after red bentonite, dolomite Concave-convex clay rod and bauxite mixed, again with the sticking Concave-convex clay rod powder of height with the 3A molecular screen primary powder mixes, the common pulverizing is the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering after compressing tablet and the roasting.
CN201110226701A 2011-08-09 2011-08-09 Production method for alcohol group paste attapulgite spicy and hot sterilization and fresh-keeping agents Pending CN102326836A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103549624A (en) * 2013-10-30 2014-02-05 湖北小胡鸭食品有限责任公司 Preparation method and application of natural plant source preservatives
CN106538928A (en) * 2016-10-25 2017-03-29 颍上县润海畜禽养殖股份有限公司 A kind of sterilized deoxygenation feed antistaling agent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103549624A (en) * 2013-10-30 2014-02-05 湖北小胡鸭食品有限责任公司 Preparation method and application of natural plant source preservatives
CN106538928A (en) * 2016-10-25 2017-03-29 颍上县润海畜禽养殖股份有限公司 A kind of sterilized deoxygenation feed antistaling agent and preparation method thereof

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Application publication date: 20120125