CN102326832A - Production method of alcohol-based pasty attapulgite fleeceflower root sterilization preservative - Google Patents
Production method of alcohol-based pasty attapulgite fleeceflower root sterilization preservative Download PDFInfo
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- CN102326832A CN102326832A CN201110225896A CN201110225896A CN102326832A CN 102326832 A CN102326832 A CN 102326832A CN 201110225896 A CN201110225896 A CN 201110225896A CN 201110225896 A CN201110225896 A CN 201110225896A CN 102326832 A CN102326832 A CN 102326832A
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Abstract
The invention discloses a production method of an alcohol-based pasty attapulgite fleeceflower root sterilization preservative. According to the technical scheme, the method comprises the following steps of: mixing the crushed fleeceflower root mixture and edible alcohol, adding the mixture into a stainless steel container, performing soaking, pressure filtration, blending, high-speed stirring and dehydrating treatments, canning, and thus obtaining a finished product of the alcohol-based pasty attapulgite fleeceflower root sterilization preservative. The alcohol-based pasty attapulgite fleeceflower root sterilization preservative consists of fleeceflower root, ephedra, cassia twig, dutchmanspipe root, asarum, peanut shell, liquorice, alcohol and high-viscosity attapulgite clay powder. The effective ingredients of the alcohol-based pasty attapulgite fleeceflower root sterilization preservative are slowly released and penetrated to all space in a food package, and a layer of sterilization fresh-keeping film is formed on the surface of the food; the alcoholic strength of the sterilization fresh-keeping film is more than or equal to 70 degrees, and relatively long-time optimal sterilization concentration is kept, so that the purposes of sterilizing and keeping the food fresh in the whole shelf life are fulfilled; and the alcohol-based pasty attapulgite fleeceflower root sterilization preservative is suitable for sterilization and fresh keeping of fruits, vegetables and food.
Description
Technical field
The present invention relates to antistaling disinfectant, be specifically related to a kind of production method of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant.
Background technology
The invasion and attack of microorganisms such as bacterium, mould, saccharomycete are principal elements of food spoilage; Therefore in production, processing and the storage of food; Anticorrisive agent has very, and important use is worth; But because the fabricated food additive has certain toxic and side effect, people tend to select safe antiseptics for natural food.
The change of soil water content of food in shelf life usually can cause the change of food quality, such as; Fresh fruit of vegetables is at duration of storage; Because the evaporation of moisture can cause fruits and vegetables outward appearance wilting shrinkage, freshness and tender and crisp degree all descend, and commodity value also descends thereupon even loses; And the loose goods of institutional frameworks such as cake, bread because phenomenons such as drying shrinkage is stiff can take place in the evaporation of moisture, also cause the decline of its edible quality.The evaporation of food water also may promote the activity of some enzyme in the food to increase, and makes the polymer substance degraded, shortens the shelf life of product.Therefore, the food that some water content are higher, for example food sterilizations such as fresh fish, fresh meat, fruit, vegetables, bean product, curing food and birthday cake are fresh-keeping, should not adopt deoxidation anti-mould fresh keeping agent and drier to carry out Preservation Treatment.
Adopt the alcohol radical extract to carry out sterilization, mildew-resistant and anticorrosion; In the hope of reaching fresh-keeping purpose, be not that the alcohol radical extract directly is added on inside of food, but be used for the packing of food; Because the water content of some food self is than higher; When alcohol radical extract alcoholic strength was spent less than 80, the active ingredient of alcohol radical extract alcoholic strength reduced the practical effect of sterilization fresh-keeping easily by dilution of the moisture in the food and dissolving.
Chinese patent Granted publication CN 100353871 C; December 12 2007 Granted publication day; Name is called " granular concave rod alcohol antistaling agent ", discloses that a kind of " a kind of granular concave rod alcohol antistaling agent, the main points of its technical scheme are; granular concave rod alcohol antistaling agent, are made up of the concavo-convex rod of porous particle, edible alcohol, citric acid, sodium Diacetate and water.With granular concave rod alcohol antistaling agent with being packed by fresh-keeping foodstuff; Fresh-keeping gas in the granular concave rod can slowly release, and evaporate into the various piece in the package body, around by fresh-keeping foodstuff, forms certain density protective layer; Can suppress bacterial reproduction; Kill multiple mould, bacterium and other spoilage organisms, thereby the food in preventing to pack is mouldy and putrid and deteriorated, reaches fresh-keeping effect.Be applicable to the fresh-keeping of various fruits and vegetables, food, meat and aquatic products ".
The weak point of above-mentioned patent is " granular concave rod alcohol antistaling agent " alcoholic strength less than 80 degree, and being used for the higher food of water content, to carry out the practical effect of sterilization fresh-keeping undesirable.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of production method of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is provided.
The production method of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant: the fleece-flower root mixture after will pulverizing and edible alcohol mix the back add in the rustless steel container soak, press filtration, blend, high-speed stirred and processed, canned is alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant finished product.
Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is made up of the fleece-flower root, Chinese ephedra, cassia twig, dutchmanspipe root, the root of Chinese wild ginger, peanut shell, Radix Glycyrrhizae, alcohol and high sticking Concave-convex clay rod powder.
The fleece-flower root all has inhibitory action in various degree to staphylococcus aureus, staphylococcus albus, shigella flexneri, sonne bacillus, typhoid bacillus, paratyphosum Bacterium, corynebacterium diphtheriae, beta hemolytic streptococcus etc.
Chinese ephedra has antibacterial action, and staphylococcus aureus, first, beta hemolysis streptococcus, haemophilus influenzae, Diplococcus pneumopniae, bacillus anthracis, corynebacterium diphtheriae, Escherichia coli and neisser's diplococcus etc. are had inhibitory action.
Cassia twig can suppress Escherichia coli, hay bacillus and staphylococcus aureus, and staphylococcus albus, shigella, typhoid fever and paratyphoid A bacillus, pneumococcus, aerobacteria, proteus, bacillus anthracis, Salmonella enteritidis, comma bacillus etc. are also had inhibitory action.
Dutchmanspipe root has inhibitory action in various degree to bacillus such as staphylococcus aureus and green pus, large intestine and distortion.
The root of Chinese wild ginger has certain inhibitory action to gram positive bacteria, hay bacillus and typhoid bacillus, and tubercle bacillus and typhoid bacillus are also had inhibitory action.Multiple fungi such as Aspergillus flavus, black-koji mould, Candida albicans etc. all there is inhibitory action.
Peanut shell is the pod shell of peanut, is a kind of assembly of complex organic compound, and peanut shell is as the discarded object of peanut, mainly is used as fuel or is used as waste residue to discard.Yet in the peanut shell except that containing a large amount of carbohydrate and crude fibre; Contain a spot of polyphenols and Flavonoid substances; Peanut shell alcohol leaching liquor can suppress the growth of staphylococcus and hay bacillus, and catarrh bacterium, Candida albicans, proteus are also had inhibitory action.
Radix Glycyrrhizae is a kind ofly both can increase sweet seasoning, anti-oxidant, has the function of antibacterial, anti-inflammatory, detoxifcation and deodorizing again.Radix Glycyrrhizae also has detoxication, and staphylococcus aureus, hay bacillus, saccharomycete, fungi and streptococcus etc. are had inhibitory action.
Alcohol has strong lethal effect for bacterium when 70% (V), also can make anticorrisive agent, solvent etc.If alcohol concentration is lower than 70%,, can not the protein coagulating in its body can not thoroughly be killed bacterium equally though can get in the bacterial body.Have only the alcohol of 70%-75% successfully to enter in the bacterial body, again can be effectively with the protein coagulating in the bacterial body, thereby thorough killing bacteria.
The Concave-convex clay rod soil property is fine and smooth; Water imbibition is strong, tool viscosity and plasticity when wet, strong adhesion; It is a kind of natural minerals gel carrier; Help alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant and be adsorbed on papery, cloth matter and the solid body, make the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant of various different conditions, increase the purposes of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant.
High sticking Concave-convex clay rod powder is meant gets 28.0g Concave-convex clay rod powder sample; Add in the suspension cup of homogenizer, add 372g water again, the suspension cup is placed on the homogenizer; Under 11000 rev/mins of rotating speeds, stirred 20 minutes; To pass through the high-speed stirred sample suspension again and pour in the beaker of 250ml, the viscosity of using NDJ-1 type rotation viscometer to test its suspension, the Concave-convex clay rod powder of tested viscosity value >=2200 mPas is high sticking Concave-convex clay rod powder.
The present invention is achieved through following technical proposals:
1, the production method of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant: ⑴ adds fleece-flower root mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ fleece-flower root mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are fleece-flower root alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 55～70 degree; The batching of fleece-flower root alcohol mixture is made up of following component by weight percentage: fleece-flower root mixture 45～85% and alcohol 15～55%, and soak time was controlled at 2～8 days; ⑶ carry out press filtration in the fleece-flower root alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is fleece-flower root alcohol extract; ⑷ add in the fleece-flower root alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be high concentration fleece-flower root alcohol extract, the batching of high concentration fleece-flower root alcohol extract is made up of following component by weight percentage: the alcohol 25～65% of fleece-flower root alcohol extract 35～75% and alcoholic strength>=95 degree; ⑸ mix high concentration fleece-flower root alcohol extract and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is an alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product; The speed controlling of homogenizer is 4000～5000 rev/mins, and the half-finished batching of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is made up of following component by weight percentage: high concentration fleece-flower root alcohol extract 85～95% and high sticking Concave-convex clay rod powder 5～15%; ⑹ with carrying out processed in the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product input alcohol radical sterilization fresh-keeping fluid dewatering device; Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant alcoholic strength after the processed>=99 degree, canned is alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant finished product;
The batching of said fleece-flower root mixture is made up of following component by weight percentage: the fleece-flower root 20～45%, Chinese ephedra 1～20%, cassia twig 1～20%, dutchmanspipe root 1～15%, the root of Chinese wild ginger 1～15%, peanut shell 1～10% and Radix Glycyrrhizae 1～10%;
Said alcohol radical sterilization fresh-keeping fluid dewatering device is made up of cylindrical container, cover plate, attachment bolt, charging aperture, charging valve, pressure-air import, pressure-air air intake valve, pressure-air pipeline, web plate, stainless steel basket, the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering, transparent glass tube, alcohol meter, transparent glass tube loam cake, glass tube support, discharge nozzle, discharging valve, discharging opening and support;
The separate case application of alcohol radical sterilization fresh-keeping fluid dewatering device patent of invention, number of patent application is: 201110211758.6;
The agent of said graininess alcohol radical sterilization fresh-keeping fluid dewatering is made up of red bentonite, dolomite Concave-convex clay rod, bauxite, sulfuric acid, high sticking Concave-convex clay rod powder and 3A molecular screen primary powder.The production method of graininess alcohol radical sterilization fresh-keeping fluid dewatering agent: carry out acidification after red bentonite, dolomite Concave-convex clay rod and bauxite mixed, again with the sticking Concave-convex clay rod powder of height with the 3A molecular screen primary powder mixes, the common pulverizing is the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering after compressing tablet and the roasting;
Graininess alcohol radical sterilization fresh-keeping fluid dewatering agent separate case application patent of invention, number of patent application is: 201110210542.8.
The fleece-flower root in the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant all has sterilization fresh-keeping effect preferably with other batching; The concentration of active ingredient and alcohol concentration are all high; Be used in the packaging for foodstuff; The active ingredient of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant slowly discharges and is penetrated into the interior institute of packaging for foodstuff has living space, and forms one deck sterilization fresh-keeping film on the surface of food; Because the alcoholic strength of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant >=99 degree; After the higher Food Contact of water content; The alcoholic strength of sterilization fresh-keeping film >=70 degree; The concentration that keeps best sterilization of long period is goed deep into the inner kill microorganisms of food or is suppressed its growth and breeding, guarantees that food whole process in shelf life reaches sterilization, prevents to go mouldy and fresh-keeping purpose.
The simple alcohol that uses is the antibacterial and sterilization at food surface; There is certain limitation in the action of microorganisms in food inside own; Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant has been given full play to the fleece-flower root and alcohol characteristic separately; Antibacterial, sterilization in surface and inner kill microorganisms carry out simultaneously, are a kind of antistaling disinfectants efficiently.
Method for using: 1. with nonwoven the solid-state sorbing material that adsorbs behind the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant, be packaged as a kind of solid-state alcohol radical fleece-flower root antistaling disinfectant, the nonwoven skin is packed with plastic bag sealing; 2. tear the plastic bag sealing packing; Solid-state alcohol radical fleece-flower root antistaling disinfectant is placed in the food container that needs sterilization fresh-keeping; Active ingredient in the alcohol radical fleece-flower root antistaling disinfectant constantly slowly discharges in food container; Form one deck sterilization fresh-keeping film on the surface of food, reach sterilization, prevent to go mouldy and fresh-keeping purpose.
That alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant has is nontoxic, noresidue, no burn into quality safety is reliable and bactericidal effect is good characteristics, can not produce harm to human body, and production method technology is simple, and is easy to operate, do not have environmental pollution.
Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is applicable to produces various paperys, cloth matter and solid-state alcohol radical fleece-flower root antistaling disinfectant, also is applicable to add in the food sterilization preservation device and carries out sterilization fresh-keeping.
Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is applicable to the sterilization fresh-keeping of fruits and vegetables and food.
The specific embodiment
Below in conjunction with embodiment the present invention is done further description:
1, the production method of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant: ⑴ adds fleece-flower root mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ fleece-flower root mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are fleece-flower root alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 60 degree; The batching of fleece-flower root alcohol mixture is made up of following component by weight percentage: fleece-flower root mixture 64% and alcohol 36%, and soak time was controlled at 6 days; ⑶ carry out press filtration in the fleece-flower root alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is fleece-flower root alcohol extract; ⑷ add in the fleece-flower root alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be high concentration fleece-flower root alcohol extract, the batching of high concentration fleece-flower root alcohol extract is made up of following component by weight percentage: the alcohol 30% of fleece-flower root alcohol extract 70 and alcoholic strength>=95 degree; ⑸ mix high concentration fleece-flower root alcohol extract and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is an alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product; The speed controlling of homogenizer is 4500～5000 rev/mins, and the half-finished batching of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is made up of following component by weight percentage: high concentration fleece-flower root alcohol extract 91% and high sticking Concave-convex clay rod powder 9%; ⑹ with carrying out processed in the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product input alcohol radical sterilization fresh-keeping fluid dewatering device; Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant alcoholic strength after the processed>=99 degree, canned is alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant finished product;
The batching of said fleece-flower root mixture is made up of following component by weight percentage: the fleece-flower root 32%, Chinese ephedra 16%, cassia twig 14%, dutchmanspipe root 12%, the root of Chinese wild ginger 12%, peanut shell 10% and Radix Glycyrrhizae 4%.
The on-the-spot test result: the alcoholic strength of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is 99.2%.
Claims (1)
1. the production method of an alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is characterized in that, ⑴ adds fleece-flower root mixture in the pulverizer and pulverizes, the grain fineness after the pulverizing≤0.2 millimeter; ⑵ fleece-flower root mixture after will pulverize and edible alcohol mix interior immersion of back adding rustless steel container and are fleece-flower root alcohol mixture; The alcoholic strength of edible alcohol is controlled to be 55～70 degree; The batching of fleece-flower root alcohol mixture is made up of following component by weight percentage: fleece-flower root mixture 45～85% and alcohol 15～55%, and soak time was controlled at 2～8 days; ⑶ carry out press filtration in the fleece-flower root alcohol mixture adding filter press after will soak, the liquid that obtains after the press filtration is fleece-flower root alcohol extract; ⑷ add in the fleece-flower root alcohol extract with the edible alcohol of alcoholic strength>=95 degree; Blend and be high concentration fleece-flower root alcohol extract, the batching of high concentration fleece-flower root alcohol extract is made up of following component by weight percentage: the alcohol 25～65% of fleece-flower root alcohol extract 35～75% and alcoholic strength>=95 degree; ⑸ mix high concentration fleece-flower root alcohol extract and high sticking Concave-convex clay rod powder in the back input homogenizer; High-speed stirred is an alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product; The speed controlling of homogenizer is 4000～5000 rev/mins, and the half-finished batching of alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant is made up of following component by weight percentage: high concentration fleece-flower root alcohol extract 85～95% and high sticking Concave-convex clay rod powder 5～15%; ⑹ with carrying out processed in the alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant semi-finished product input alcohol radical sterilization fresh-keeping fluid dewatering device; Alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant alcoholic strength after the processed>=99 degree, canned is alcohol radical cream-like attapulgite fleece-flower root antistaling disinfectant finished product;
The batching of said fleece-flower root mixture is made up of following component by weight percentage: the fleece-flower root 20～45%, Chinese ephedra 1～20%, cassia twig 1～20%, dutchmanspipe root 1～15%, the root of Chinese wild ginger 1～15%, peanut shell 1～10% and Radix Glycyrrhizae 1～10%;
Said alcohol radical sterilization fresh-keeping fluid dewatering device is made up of cylindrical container, cover plate, attachment bolt, charging aperture, charging valve, pressure-air import, pressure-air air intake valve, pressure-air pipeline, web plate, stainless steel basket, the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering, transparent glass tube, alcohol meter, transparent glass tube loam cake, glass tube support, discharge nozzle, discharging valve, discharging opening and support;
The agent of said graininess alcohol radical sterilization fresh-keeping fluid dewatering is made up of red bentonite, dolomite Concave-convex clay rod, bauxite, sulfuric acid, high sticking Concave-convex clay rod powder and 3A molecular screen primary powder; The production method of graininess alcohol radical sterilization fresh-keeping fluid dewatering agent: carry out acidification after red bentonite, dolomite Concave-convex clay rod and bauxite mixed, again with the sticking Concave-convex clay rod powder of height with the 3A molecular screen primary powder mixes, the common pulverizing is the agent of graininess alcohol radical sterilization fresh-keeping fluid dewatering after compressing tablet and the roasting.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103876052A (en) * | 2014-03-11 | 2014-06-25 | 同福碗粥股份有限公司 | Bamboo tube healthy porridge and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103876052A (en) * | 2014-03-11 | 2014-06-25 | 同福碗粥股份有限公司 | Bamboo tube healthy porridge and preparation method thereof |
| CN103876052B (en) * | 2014-03-11 | 2015-09-30 | 同福碗粥股份有限公司 | A kind of thick bamboo tube health-preserving porridge and preparation method thereof |
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Application publication date: 20120125 |