CN102321437A - Novel UV (ultraviolet)-curable decoration adhesive - Google Patents
Novel UV (ultraviolet)-curable decoration adhesive Download PDFInfo
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- CN102321437A CN102321437A CN201110208083A CN201110208083A CN102321437A CN 102321437 A CN102321437 A CN 102321437A CN 201110208083 A CN201110208083 A CN 201110208083A CN 201110208083 A CN201110208083 A CN 201110208083A CN 102321437 A CN102321437 A CN 102321437A
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Abstract
The invention discloses a novel UV (ultraviolet)-curable decoration adhesive. The formula of the decoration adhesive comprises the following components in percentage by mass: 35-60% of UV oligomer, 30-55% of UV monomer, 4-10% of photo initiator, 1-5% of rheology control additive, 0.1-0.5% of defoaming agent, 0.1-0.5% of substrate wetting agent and 0-5% of pigment. The UV-curable decoration adhesive can be coated on a substrate by an extrusion dispenser to form three-dimensional patterns and words with different heights and rich colors or profiles of patterns and words; and different pigments or spray-printing UV ink can be added, so that the patterns have various colors and special effects, such as metal texture, pearl light, fluorescence, color change and the like, thus signboards or decorative articles are move beautiful.
Description
Technical field
The present invention relates to solidify the glue field, particularly a kind of UV solidifies decorating glue.
Background technology
Present advertising signboard and decorative article kind are more and more, and making method and the effect of making are also varied, and main has following several kinds:
1, use some flexible medias, hollow out becomes pattern or literal, is attached on the another kind of base material;
2, adopt the method for spray ink Printing, directly print pattern or literal on base material are as adopting UV ink printed, Weak solvent ink printed etc.;
3, adopt engraving process, on base material, carve out pattern or literal;
4, adopt the plastic uptake method, produce solid pattern or literal;
Above certain methods cooperates lighting effects again; Can produce diversified signboard or decorative article, but there is certain deficiency in above method, 1,2 two kind of method make is plane effect; The visual impact sense is not strong; 3,4 two kinds of methods can only adopt unicolor base material basically, and color effects is bad, and the 4th kind of method is difficult to make more complicated, meticulous article.
Summary of the invention
For addressing the above problem, the purpose of this invention is to provide a kind of novel UV and solidify decorating glue, can produce existing stereoscopic sensation gorgeous abundant signboard of color or decorative article again.
The objective of the invention is to realize like this: a kind of novel UV solidifies decorating glue, it is characterized in that: calculate prescription by mass percentage and comprise following component: 35～60% UV oligomer, 30～55% UV monomer, 4～10% light trigger, 1～5% rheology control auxiliary agent, 0.1～0.5% skimmer, 0.1～0.5% base material wetting agent, 0～5% colorant.
Described UV oligomer is selected from one or more mixing in polyester acrylate oligomer or the urethane acrylate oligomer.
Described UV monomer is selected from one or more mixing among EOEOEA, THFA, IBOA, PHEA, HDDA, DPGDA, TPGDA, HEMA, TMPTA, EO3TMPTA, PO3TMPTA, EO4PETA or the DPHA.
Described light trigger is selected from HMPP, HCPK, MMMP, BDMB, ITX, 2,4,6 Three methyl Benzene methyl acyl phenylbenzene oxidations see or BAPO1 in one or more mixing.
Described rheology control auxiliary agent is selected from aerosil or wilkinite.
Described skimmer is selected from organo-siloxane.
Described base material wetting agent is selected from organo-siloxane or fluorine-carbon modified propenoate.
Described colorant is selected from one or more mixing in pigment, high-visibility pigment, sensitization discoloration pigment, heat discoloration pigment, pearlescence, metal(lic)powder, aluminium-silver slurry, luminescent powder or the dyestuff.
Described UV solidifies viscosity 120000～200000cps/25 ℃ of decorating glue, surface tension 28～35 dynes per centimeter, and minimum curing energy is 300mJ/cm
2
UV of the present invention solidifies decorating glue through extruding point gum machine; Can on base material, form highly different; 3 D stereo pattern and literal that color is abundant, the perhaps profile of pattern and literal, and can add various colorant or spray printing UV ink makes pattern have various colors and special-effect; Like metal sense, pearly-lustre, fluorescence, variable color etc., make signboard or decorative article more attractive in appearance.
Embodiment
UV of the present invention solidifies decorating glue, calculates prescription by mass percentage and comprises following component: 35～60% UV oligomer, 30～55% UV monomer, 4～10% light trigger, 1～5% rheology control auxiliary agent, 0.1～0.5% skimmer, 0.1～0.5% base material wetting agent, 0～5% colorant.
UV of the present invention solidifies decorating glue and comprises one or more UV oligomers; The UV oligomer is as main connection material; Colorant had good wetting parcel ability; Base material is had good sticking power, have good outdoor persistence, keep the vividness of color with making product behind the UV monomer curing reaction.The UV oligomer is selected from one or more mixing in polyester acrylate oligomer, the urethane acrylate oligomer, preferentially selects the polyester acrylate oligomer for use, accounts for 35～60% of gross weight, is preferably 45～55%.
UV of the present invention solidifies decorating glue and comprises one or more UV monomers; The UV monomer is as carrier, and main effect is dilution UV oligomer, dissolving light trigger and auxiliary agent, simultaneously through selecting different functionality, not isoplastic monomer; Can regulate the curing speed of product; The contraction of adjustment UV photocuring process strengthens the sticking power of product on base material, regulates the hardness and the snappiness of solidifying the back product.The UV monomer comprises: EOEOEA (ethoxy ethoxy ethyl propylene acid esters), THFA (tetrahydrofurfuryl propenoate), IBOA (iso-bornyl acrylate), PHEA (2-phenoxyethyl acrylate), HDDA (1; The 6-hexanediyl ester), one or more mixing among DPGDA (propylene glycol diacrylate), TPGDA (tripropylene glycol diacrylate), HEMA (2-hydroxyethyl methacrylic ester), TMPTA (Viscoat 295), EO3TMPTA (ethoxyquin trimethylolpropane trimethacrylate), PO3TMPTA (the third oxidation Viscoat 295), EO4PETA (ethoxyquin tetramethylol methane tetraacrylate), the DPHA (dipentaerythritol acrylate); Account for 30～55% of gross weight, be preferably 35～45%.
UV of the present invention solidifies decorating glue and comprises one or more light triggers; The effect of light trigger is under the irradiation of UV light, to produce radical, causes UV oligomer and the monomeric polyreaction of UV, according to distinct colors and concentration; Should adjust the kind and the ratio of light trigger; Light trigger comprises HMPP (2-hydroxy-2-methyl-1-phenyl-acetone-1), HCPK (1-hydroxyl-cyclohexyl benzophenone), MMMP (2-methyl isophthalic acid-[4 first sulfydryl phenyl]-2-morpholine acetone 1), BDMB (2-phenyl-2-dimethylamino-1-[4-morpholinyl phenyl]-butanone-1), ITX (isopropyl thioxanthone), TPO (2,4, the oxidation of 6-Three methyl Benzene methyl acyl phenylbenzene is seen), BAPO1 (two [2; 4; 6-Three methyl Benzene methyl acyl] the phenyl oxidation sees) in one or more mix, account for 4～10% of gross weight, be preferably 6～8%.
UV of the present invention solidifies the contained rheology control auxiliary agent of decorating glue; Give UV and solidify the decorating glue good rheological; To be applicable to the needs of extruding point gum machine, the rheology control auxiliary agent is selected from aerosil or wilkinite, preferentially selects aerosil; Account for 1～5% of gross weight, preferred 3～5%.
UV of the present invention solidifies the contained skimmer of decorating glue; Its effect is to prevent to produce bubble in the production process, needs high speed dispersion colorant and auxiliary agent in the production process, can bring air into and form bubble; The viscosity that UV solidifies decorating glue is very big; Bubble is difficult to overflow, and the UV that contains great amount of bubbles solidifies can influence the outward appearance of product after decorating glue is extruded curing, so needs to add the generation that skimmer reduces bubble; Skimmer generally adopts organo-siloxane, for example EFKA2035, EFKA2025, EFKA2040, BYI065, BYK141 or the like commercially available prod.Consumption accounts for 0.1～0.5% of gross weight, and preferred 0.1～0.3%.
UV of the present invention solidifies the contained base material wetting agent of decorating glue; Its effect is to help rapid wetting base material, strengthens UV and solidifies the sticking power of decorating glue on base material, and UV curing decorating glue viscosity is very big; Extrude the back solidifies at once; To the very short not good enough sticking power that influences of wetting effect that causes of the wetting time of base material, the base material wetting agent is selected from organo-siloxane or fluorine-carbon modified propenoate, for example BYK333, BYK306, BYK388, EFKA3033, EFKA3239, EFKA3277 or the like commercially available prod.Consumption accounts for 0.1～0.5% of gross weight, and preferred 0.2～0.4%.
UV of the present invention solidifies the contained colorant of decorating glue; Give various colors of product and special-effect, colorant comprises one or more mixing in pigment, high-visibility pigment, sensitization discoloration pigment, heat discoloration pigment, pearlescence, metal(lic)powder, aluminium-silver slurry, luminescent powder or the dyestuff.Wherein: pigment gives product various real looks, strong covering power; The high-visibility pigment color is very bright-coloured, the tool translucent effect; Sensitization discoloration pigment color after special light such as infrared rays, uviolizing can change; Heat discoloration pigment color after temperature changes can change thereupon; Pearlescence, metal(lic)powder, aluminium-silver slurry are given the special expression effect of product such as metal sense, nacreous lustre, and it is luminous evening that luminescent powder can make product absorb energy daytime; Dyestuff can be made transparent coloured product.Through the collocation of various colorants, can produce the product of rich color, the various effects of tool, the consumption of colorant accounts for 0～5% of gross weight.
For guaranteeing before curing, to keep certain shape after decorating glue is extruded, preferably, UV of the present invention solidifies the viscosity controller of decorating glue at 120000～200000cps/25 ℃.If viscosity is low excessively, decorating glue may water clock at extruder head, and the difficult control of the pressure of extruding, and causes the inhomogeneous distortion that causes figure of glue amount of extruding, and decorating glue viscosity is low simultaneously, extrudes the back and on base material, caves in easily, causes figure deformation; If viscosity is too high, extrusion ratio is difficulty, and extruding the back does not have suitable levelling on base material, cause the unsmooth decorative effect that influences of patterned surfaces.For cooperating employed base material, it is wetting preferably to make that decorating glue has on base material, guarantees that decorating glue has good sticking power on base material; Preferably; UV of the present invention solidifies surface tension control 28～35 dynes per centimeter of decorating glue, if surface tension is too high, decorating glue is nonwetting or wetting insufficient on base material; The sticking power of decorating glue on base material is bad, in use comes off easily.The minimum curing energy that the UV that the present invention makes solidifies decorating glue can be low to moderate 300mJ/cm
2
Specific embodiment
1, UV solidifies the preparation of decorating glue: prescription is seen table 1
Table 1.
2, UV solidifies the production technique of decorating glue:
Prescription by the foregoing description 1-5 is ready to each component.With UV monomer proportional mixing, add light trigger earlier, stirring and dissolving adds polyester acrylate again; Stir, add auxiliary agent again, under high-speed stirring, add aerosil, stir about 1 hour; Add colorant more in proportion, stir 30min, promptly get UV after the filtration and solidify decorating glue.
By the product that embodiment 1-5 prescription makes, performance all meets request for utilization, and promptly viscosity 120000～200000cps/25 ℃, surface tension 28～35 dynes per centimeter are solidified energy greater than 300mJ/cm
2
During use, can form pattern and literal through extruding point gum machine.Extrude point gum machine and controlled by computer, have single head or bull, extruder head temperature controllable heating UV glue is to obtain suitable extruding viscosity to adapt to different requirement; Can accurately locate, on X, Y, Z axle, accurate stepping arranged, to obtain meticulous 3 D stereo pattern; Have the UV cure system, guarantee that the UV glue of extruding in time solidifies, and prevents its distortion of caving in.
Claims (10)
1. a novel UV solidifies decorating glue, it is characterized in that: calculate prescription by mass percentage and comprise following component: 35～60% UV oligomer, 30～55% UV monomer, 4～10% light trigger, 1～5% rheology control auxiliary agent, 0.1～0.5% skimmer, 0.1～0.5% base material wetting agent, 0～5% colorant.
2. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described UV oligomer is selected from one or more mixing in polyester acrylate oligomer or the urethane acrylate oligomer.
3. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described UV monomer is selected from one or more mixing among EOEOEA, THFA, IBOA, PHEA, HDDA, DPGDA, TPGDA, HEMA, TMPTA, EO3TMPTA, PO3TMPTA, EO4PETA or the DPHA.
4. a kind of novel UV according to claim 1 solidifies decorating glue; It is characterized in that: described light trigger is selected from HMPP, HCPK, MMMP, BDMB, ITX, 2; 4,6 Three methyl Benzene methyl acyl phenylbenzene oxidations see or BAPO1 in one or more mixing.
5. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described rheology control auxiliary agent is selected from aerosil or wilkinite.
6. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described skimmer is selected from organo-siloxane.
7. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described base material wetting agent is selected from organo-siloxane or fluorine-carbon modified propenoate.
8. a kind of novel UV according to claim 1 solidifies decorating glue, and it is characterized in that: described colorant is selected from one or more mixing in pigment, high-visibility pigment, sensitization discoloration pigment, heat discoloration pigment, pearlescence, metal(lic)powder, aluminium-silver slurry, luminescent powder or the dyestuff.
9. solidify decorating glue according to the described a kind of novel UV of arbitrary claim among the claim 1-8, it is characterized in that: described UV solidifies viscosity 120000～200000cps/25 ℃ of decorating glue, surface tension 28～35 dynes per centimeter.
10. solidify decorating glue according to the described a kind of novel UV of arbitrary claim among the claim 1-8, it is characterized in that: the minimum curing energy that described UV solidifies decorating glue is 300mJ/cm
2
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| CN102637805A (en) * | 2012-04-25 | 2012-08-15 | 嘉悠国际贸易（上海）有限公司 | UV (ultraviolet) silica gel packaged LED (light-emitting diode) and packaging technology thereof |
| CN103265904A (en) * | 2013-05-07 | 2013-08-28 | 浙江大学宁波理工学院 | Luminescence gel and preparation method thereof |
| CN104894924A (en) * | 2015-06-25 | 2015-09-09 | 浙江维涅斯装饰材料股份有限公司 | Rotary screen printing wallpaper production process |
| WO2016077984A1 (en) * | 2014-11-18 | 2016-05-26 | Henkel (China) Company Limited | Photo-curable adhesive composition, preparation and use thereof |
| CN105860784A (en) * | 2016-06-06 | 2016-08-17 | 武夷学院 | UV curing coating and application method thereof |
| CN106433492A (en) * | 2016-09-18 | 2017-02-22 | 深圳市华星光电技术有限公司 | Lateral light-shading glue and frameless display device |
| CN108641620A (en) * | 2018-03-28 | 2018-10-12 | 广州慧谷工程材料有限公司 | A kind of pressure sensitive adhesive and its application process being used for imagery optical component, touch panel, display device |
| CN109762498A (en) * | 2019-01-11 | 2019-05-17 | 广东鑫凯科技实业有限公司 | A kind of true porcelain cement of luminous type high brightness and preparation method thereof |
| CN110003841A (en) * | 2019-04-16 | 2019-07-12 | 厦门韦尔通科技有限公司 | A kind of ultraviolet cured adhesive and preparation method thereof, application method and a kind of electronic product |
| CN110003840A (en) * | 2019-03-18 | 2019-07-12 | 晋江联兴反光材料有限公司 | A kind of UV glue for reflective membrane, reflective membrane and preparation method thereof |
| CN110607126A (en) * | 2019-08-15 | 2019-12-24 | 湖南梵鑫科技有限公司 | Electronic coating adhesive for protecting electronic circuit board and preparation method thereof |
| CN111231533A (en) * | 2020-03-11 | 2020-06-05 | 深圳市星坤包装制品有限公司 | UV printing process for color packaging box |
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| CN102637805A (en) * | 2012-04-25 | 2012-08-15 | 嘉悠国际贸易（上海）有限公司 | UV (ultraviolet) silica gel packaged LED (light-emitting diode) and packaging technology thereof |
| CN102637805B (en) * | 2012-04-25 | 2015-03-18 | 嘉悠国际贸易（上海）有限公司 | UV (ultraviolet) silica gel packaged LED (light-emitting diode) and packaging technology thereof |
| CN103265904A (en) * | 2013-05-07 | 2013-08-28 | 浙江大学宁波理工学院 | Luminescence gel and preparation method thereof |
| CN103265904B (en) * | 2013-05-07 | 2015-10-28 | 浙江大学宁波理工学院 | A kind of Luminescence gel and preparation method thereof |
| WO2016077984A1 (en) * | 2014-11-18 | 2016-05-26 | Henkel (China) Company Limited | Photo-curable adhesive composition, preparation and use thereof |
| US10717907B2 (en) | 2014-11-18 | 2020-07-21 | Henkel Ag & Co. Kgaa | Photo-curable adhesive composition, preparation and use thereof |
| CN104894924A (en) * | 2015-06-25 | 2015-09-09 | 浙江维涅斯装饰材料股份有限公司 | Rotary screen printing wallpaper production process |
| CN105860784B (en) * | 2016-06-06 | 2017-09-29 | 武夷学院 | A kind of UV is coating material solidified and its application process |
| CN105860784A (en) * | 2016-06-06 | 2016-08-17 | 武夷学院 | UV curing coating and application method thereof |
| CN106433492A (en) * | 2016-09-18 | 2017-02-22 | 深圳市华星光电技术有限公司 | Lateral light-shading glue and frameless display device |
| CN108641620A (en) * | 2018-03-28 | 2018-10-12 | 广州慧谷工程材料有限公司 | A kind of pressure sensitive adhesive and its application process being used for imagery optical component, touch panel, display device |
| CN109762498A (en) * | 2019-01-11 | 2019-05-17 | 广东鑫凯科技实业有限公司 | A kind of true porcelain cement of luminous type high brightness and preparation method thereof |
| CN110003840A (en) * | 2019-03-18 | 2019-07-12 | 晋江联兴反光材料有限公司 | A kind of UV glue for reflective membrane, reflective membrane and preparation method thereof |
| CN110003841A (en) * | 2019-04-16 | 2019-07-12 | 厦门韦尔通科技有限公司 | A kind of ultraviolet cured adhesive and preparation method thereof, application method and a kind of electronic product |
| CN110607126A (en) * | 2019-08-15 | 2019-12-24 | 湖南梵鑫科技有限公司 | Electronic coating adhesive for protecting electronic circuit board and preparation method thereof |
| CN111231533A (en) * | 2020-03-11 | 2020-06-05 | 深圳市星坤包装制品有限公司 | UV printing process for color packaging box |
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