CN105153926A - Solvent-free type ultraviolet (UV) photocuring texture paint and preparation and use method thereof - Google Patents
Solvent-free type ultraviolet (UV) photocuring texture paint and preparation and use method thereof Download PDFInfo
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- CN105153926A CN105153926A CN201510697937.3A CN201510697937A CN105153926A CN 105153926 A CN105153926 A CN 105153926A CN 201510697937 A CN201510697937 A CN 201510697937A CN 105153926 A CN105153926 A CN 105153926A
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Abstract
The invention discloses solvent-free type ultraviolet (UV) photocuring texture paint and a preparation and use method thereof. The solvent-free type ultraviolet (UV) photocuring texture paint is prepared from, by mass, 9-11 parts of aromatic polyurethane 3 functional group crylic acid oligomer, 28-33 parts of aliphatic polyurethane 2 functional group crylic acid oligomer, 36-44 parts of bisphenol A epoxy 2 functional group crylic acid oligomer, 7.5-8.5 parts of tripropylene glycol diacrylate (TPGDA) monomers, 6-7 parts of 1,6-high definition discrete architecture (HDDA) monomers, 4-6 parts of pentaerythritol triacrylate (PET3A) monomers, 2-3.5 parts of 2-hydroxy-2-methyl-1-phenyl-1-acetone light initiator (1173), 2-4 parts of reaction type tertiary amine promoter and 0.48-0.58 part of polyether modified polydimethylsiloxane flatting agent. According to the solvent-free type ultraviolet (UV) photocuring texture paint and the preparation and use method thereof, energy saving and environment friendliness can be achieved, operation is easy and convenient, a texture shape is formed, curing and drying are fast, the visual effect is good, and the paint is especially suitable for being used for indoor PVC coated wall slab decoration of building houses through a simple roller painting coating mode.
Description
[technical field]
The present invention relates to the technical field of chemistry painting industry, the technical field of particularly a kind of no-solvent type ultraviolet (UV) photocuring texture paint and preparation thereof, using method.
[background technology]
Civilian coating is widely used in the internal and external ornament of master builder room.Traditional coating is the smooth protective membrane forming one deck densification on coated substrate, can not be formed and have the strong texture artistic effect of stereoscopic sensation.
For meeting the vision requirement that people promote day by day to coatings decoration, arisen at the historic moment various artistry coating in market, these coating are when forming the artistry effect playing oneself, all need artificial singularity operation, as used special instrument or specific pattern mold etc., have and volatilize air-polluting VOC material in drying process, have and need long-time heating bake drying, not only consuming time but also take a lot of work.
[summary of the invention]
Object of the present invention solves the problems of the prior art exactly, propose a kind of energy-conserving and environment-protective, simple to operation, form that textured, rapid solidification are dry, the no-solvent type ultraviolet (UV) photocuring texture paint of good visual effect and preparation thereof, using method, be particularly suited for the use of PVC pad pasting body of wall flat board decoration in the room in master builder room, parlor by simple roller coat coating method.
For achieving the above object, the present invention proposes a kind of no-solvent type ultraviolet (UV) photocuring texture paint, comprise following component and the quality proportioning of each component is: aromatic urethane 3 functional group acrylated oligomer: 9 ~ 11 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 28 ~ 33 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 36 ~ 44 parts, tripropylene glycol diacrylate monomer (TPGDA): 7.5 ~ 8.5 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6 ~ 7 parts, pentaerythritol triacrylate monomer (PET3A): 4 ~ 6 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 2 ~ 3.5 parts, response type tertiary amine aided initiating: 2 ~ 4 parts, polyether-modified polydimethylsiloxane flow agent: 0.48 ~ 0.58 part.
As preferably, the quality proportioning of described each component is: aromatic urethane 3 functional group acrylated oligomer: 10 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 30 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 40 parts, tripropylene glycol diacrylate monomer (TPGDA): 8 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6.5 parts, pentaerythritol triacrylate monomer (PET3A): 5 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 3 parts, response type tertiary amine aided initiating: 3 parts, polyether-modified polydimethylsiloxane flow agent: 0.5 part.
For achieving the above object, the present invention proposes a kind of preparation method of no-solvent type ultraviolet (UV) photocuring texture paint, comprise the following steps:
A) add tripropylene glycol diacrylate monomer (TPGDA) in stirring dispersion machine in the ratio in formula, and to open stirring dispersion machine setting speed be 320 revs/min;
B) adding 1,6-hexylene glycol two acrylic ester monomer (HDDA) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
C) adding pentaerythritol triacrylate monomer (PET3A) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
D) aromatic urethane 3 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 2 ~ 3 minutes;
E) aliphatic polyurethane 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2 ~ 3 minutes, then stirring 2 ~ 3 minutes of reversing;
F) bisphenol-A epoxy 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
G) response type tertiary amine aided initiating is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
H) polyether-modified polydimethylsiloxane flow agent is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
I) 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173) is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2 ~ 3 minutes, then stirring 2 ~ 3 minutes of reversing; Improving stirring dispersion machine speed setting is again 520 ~ 620 revs/min, stir 4 ~ 5 minutes, and then to improve stirring dispersion machine speed setting be 950 ~ 1000 revs/min, control temperature is no more than 48 ~ 53 DEG C, be stirred to evenly, obtained a kind of no-solvent type ultraviolet (UV) photocuring texture paint;
J) a kind of no-solvent type ultraviolet (UV) photocuring texture paint grenadine obtained in i) step is filtered and packs.
As preferably, in described i) step, first rotate forward stirring 2.5 minutes, then stirring 2.5 minutes of reversing; Improving stirring dispersion machine speed setting is again 620 revs/min, stirs 4.5 minutes, and then to improve stirring dispersion machine speed setting be 1000 revs/min, and control temperature is no more than 50 DEG C.
For achieving the above object, the present invention proposes a kind of using method of no-solvent type ultraviolet (UV) photocuring texture paint, comprise the following steps:
A) be coated on base material by no-solvent type ultraviolet (UV) photocuring texture paint by coating machine, glue spread is 20 ~ 25 grams/every square metre;
B), there is texture through the wrinkling lamp of LED in the base material of coated described no-solvent type ultraviolet (UV) photocuring texture paint;
C) base material of the texture patterns of formation no-solvent type ultraviolet (UV) photocuring texture paint enters the photo solidification machine with two medium pressure mercury lamps, and carry out photocuring complete drying, photocuring energy ensures 250 ~ 350mJ/cm
2, obtain the fine and smooth shape visual effect of clean mark of described no-solvent type ultraviolet (UV) photocuring texture paint.
As preferably, in described a) step, base material is PVC pad pasting ash wall body plate, and coating machine is single roll coater, and glue spread is 23 grams/every square metre.
As preferably, in described c) step, photocuring energy ensures 300mJ/cm
2.
Beneficial effect of the present invention: the present invention can energy-conserving and environment-protective, simple to operation, form that textured, rapid solidification are dry, good visual effect, be particularly suited for the use of PVC pad pasting body of wall flat board decoration in the room in master builder room, parlor by simple roller coat coating method.
[embodiment]
Embodiment 1
A kind of no-solvent type ultraviolet (UV) of the present invention photocuring texture paint, comprise following component and the quality proportioning of each component is: aromatic urethane 3 functional group acrylated oligomer: 10 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 30 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 40 parts, tripropylene glycol diacrylate monomer (TPGDA): 8 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6.5 parts, pentaerythritol triacrylate monomer (PET3A): 5 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 3 parts, response type tertiary amine aided initiating: 3 parts, polyether-modified polydimethylsiloxane flow agent: 0.5 part.
Embodiment 2
A kind of no-solvent type ultraviolet (UV) of the present invention photocuring texture paint, comprise following component and the quality proportioning of each component is: aromatic urethane 3 functional group acrylated oligomer: 9 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 28 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 36 parts, tripropylene glycol diacrylate monomer (TPGDA): 7.5 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6 parts, pentaerythritol triacrylate monomer (PET3A): 4 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 2 parts, response type tertiary amine aided initiating: 2 parts, polyether-modified polydimethylsiloxane flow agent: 0.48 part.
Embodiment 3
A kind of no-solvent type ultraviolet (UV) of the present invention photocuring texture paint, comprise following component and the quality proportioning of each component is: aromatic urethane 3 functional group acrylated oligomer: 11 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 33 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 44 parts, tripropylene glycol diacrylate monomer (TPGDA): 8.5 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 7 parts, pentaerythritol triacrylate monomer (PET3A): 6 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 3.5 parts, response type tertiary amine aided initiating: 4 parts, polyether-modified polydimethylsiloxane flow agent: 0.58 part.
A preparation method for no-solvent type ultraviolet (UV) photocuring texture paint, comprises the following steps:
A) add tripropylene glycol diacrylate monomer (TPGDA) in stirring dispersion machine in the ratio in formula, and to open stirring dispersion machine setting speed be 320 revs/min;
B) adding 1,6-hexylene glycol two acrylic ester monomer (HDDA) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
C) adding pentaerythritol triacrylate monomer (PET3A) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
D) aromatic urethane 3 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 2 ~ 3 minutes;
E) aliphatic polyurethane 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2 ~ 3 minutes, then stirring 2 ~ 3 minutes of reversing;
F) bisphenol-A epoxy 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
G) response type tertiary amine aided initiating is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
H) polyether-modified polydimethylsiloxane flow agent is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
I) 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173) is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2.5 minutes, then stirring 2.5 minutes of reversing; Improving stirring dispersion machine speed setting is again 620 revs/min, stirs 4.5 minutes, and then to improve stirring dispersion machine speed setting be 1000 revs/min, and control temperature is no more than 50 DEG C, is stirred to evenly, obtained a kind of no-solvent type ultraviolet (UV) photocuring texture paint;
J) a kind of no-solvent type ultraviolet (UV) photocuring texture paint grenadine obtained in i) step is filtered and packs.
A using method for no-solvent type ultraviolet (UV) photocuring texture paint, comprises the following steps:
A) be coated on base material by no-solvent type ultraviolet (UV) photocuring texture paint by coating machine, glue spread is 23 grams/every square metre;
B), there is texture through the wrinkling lamp of LED in the base material of coated described no-solvent type ultraviolet (UV) photocuring texture paint;
C) base material of the texture patterns of formation no-solvent type ultraviolet (UV) photocuring texture paint enters the photo solidification machine with two medium pressure mercury lamps, and carry out photocuring complete drying, photocuring energy ensures 300mJ/cm
2, obtain the fine and smooth shape visual effect of clean mark of described no-solvent type ultraviolet (UV) photocuring texture paint.
The present invention can energy-conserving and environment-protective, simple to operation, form that textured, rapid solidification are dry, good visual effect, be particularly suited for the use of PVC pad pasting body of wall flat board decoration in the room in master builder room, parlor by simple roller coat coating method.
Above-described embodiment is to explanation of the present invention, is not limitation of the invention, anyly all belongs to protection scope of the present invention to the scheme after simple transformation of the present invention.
Claims (7)
1. a no-solvent type ultraviolet (UV) photocuring texture paint, it is characterized in that: comprise following component and the quality proportioning of each component is: aromatic urethane 3 functional group acrylated oligomer: 9 ~ 11 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 28 ~ 33 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 36 ~ 44 parts, tripropylene glycol diacrylate monomer (TPGDA): 7.5 ~ 8.5 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6 ~ 7 parts, pentaerythritol triacrylate monomer (PET3A): 4 ~ 6 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 2 ~ 3.5 parts, response type tertiary amine aided initiating: 2 ~ 4 parts, polyether-modified polydimethylsiloxane flow agent: 0.48 ~ 0.58 part.
2. a kind of no-solvent type ultraviolet (UV) photocuring texture paint as claimed in claim 1, it is characterized in that: the quality proportioning of described each component is: aromatic urethane 3 functional group acrylated oligomer: 10 parts, aliphatic polyurethane 2 functional group acrylated oligomer: 30 parts, bisphenol-A epoxy 2 functional group acrylated oligomer: 40 parts, tripropylene glycol diacrylate monomer (TPGDA): 8 parts, 1, 6-hexylene glycol two acrylic ester monomer (HDDA) 6.5 parts, pentaerythritol triacrylate monomer (PET3A): 5 parts, 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173): 3 parts, response type tertiary amine aided initiating: 3 parts, polyether-modified polydimethylsiloxane flow agent: 0.5 part.
3. a preparation method for no-solvent type ultraviolet (UV) photocuring texture paint, is characterized in that: comprise the following steps:
A) add tripropylene glycol diacrylate monomer (TPGDA) in stirring dispersion machine in the ratio in formula, and to open stirring dispersion machine setting speed be 320 revs/min;
B) adding 1,6-hexylene glycol two acrylic ester monomer (HDDA) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
C) adding pentaerythritol triacrylate monomer (PET3A) in stirring dispersion machine in the ratio in formula, keeping stirring dispersion machine setting speed to be 320 revs/min, stir 2 ~ 3 minutes;
D) aromatic urethane 3 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 2 ~ 3 minutes;
E) aliphatic polyurethane 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2 ~ 3 minutes, then stirring 2 ~ 3 minutes of reversing;
F) bisphenol-A epoxy 2 functional group acrylated oligomer is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
G) response type tertiary amine aided initiating is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
H) polyether-modified polydimethylsiloxane flow agent is being added in stirring dispersion machine in the ratio in formula; Keep stirring dispersion machine speed setting to be 320 revs/min, stir 5 ~ 6 minutes;
I) 2-hydroxy-2-methyl-1-phenyl-1-acetone light trigger (1173) is being added in stirring dispersion machine in the ratio in formula; Stirring dispersion machine speed setting is kept to be 320 revs/min; First rotate forward stirring 2 ~ 3 minutes, then stirring 2 ~ 3 minutes of reversing; Improving stirring dispersion machine speed setting is again 520 ~ 620 revs/min, stir 4 ~ 5 minutes, and then to improve stirring dispersion machine speed setting be 950 ~ 1000 revs/min, control temperature is no more than 48 ~ 53 DEG C, be stirred to evenly, obtained a kind of no-solvent type ultraviolet (UV) photocuring texture paint;
J) a kind of no-solvent type ultraviolet (UV) photocuring texture paint grenadine obtained in i) step is filtered and packs.
4. the preparation method of a kind of no-solvent type ultraviolet (UV) photocuring texture paint as claimed in claim 3, is characterized in that: first rotate forward stirring 2.5 minutes in described i) step, then stirring 2.5 minutes of reversing; Improving stirring dispersion machine speed setting is again 620 revs/min, stirs 4.5 minutes, and then to improve stirring dispersion machine speed setting be 1000 revs/min, and control temperature is no more than 50 DEG C.
5. a using method for no-solvent type ultraviolet (UV) photocuring texture paint, is characterized in that: comprise the following steps:
A) be coated on base material by no-solvent type ultraviolet (UV) photocuring texture paint by coating machine, glue spread is 20 ~ 25 grams/every square metre;
B), there is texture through the wrinkling lamp of LED in the base material of coated described no-solvent type ultraviolet (UV) photocuring texture paint;
C) base material of the texture patterns of formation no-solvent type ultraviolet (UV) photocuring texture paint enters the photo solidification machine with two medium pressure mercury lamps, and carry out photocuring complete drying, photocuring energy ensures 250 ~ 350mJ/cm
2, obtain the fine and smooth shape visual effect of clean mark of described no-solvent type ultraviolet (UV) photocuring texture paint.
6. the using method of a kind of no-solvent type ultraviolet (UV) photocuring texture paint as claimed in claim 5, is characterized in that: in described a) step, base material is PVC pad pasting ash wall body plate, and coating machine is single roll coater, and glue spread is 23 grams/every square metre.
7. the using method of a kind of no-solvent type ultraviolet (UV) photocuring texture paint according to any one of claim 5 to 6, is characterized in that: in described c) step, photocuring energy ensures 300mJ/cm
2.
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| CN201510697937.3A CN105153926A (en) | 2015-10-23 | 2015-10-23 | Solvent-free type ultraviolet (UV) photocuring texture paint and preparation and use method thereof |
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| CN201510697937.3A CN105153926A (en) | 2015-10-23 | 2015-10-23 | Solvent-free type ultraviolet (UV) photocuring texture paint and preparation and use method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105925170A (en) * | 2016-06-29 | 2016-09-07 | 海盐三田科技有限公司 | Solvent-free ultraviolet photocuring anti-flouring easily cleaned paint as well as preparation method and application thereof |
| CN106085083A (en) * | 2016-06-23 | 2016-11-09 | 苏州吉人高新材料股份有限公司 | A kind of aqueous composite paint of environmental protection and preparation method thereof |
| CN106362916A (en) * | 2016-08-26 | 2017-02-01 | 索菲亚家居股份有限公司 | Spraying technology utilizing LED lamp for curing |
| CN114525069A (en) * | 2022-03-21 | 2022-05-24 | 小森新材料科技有限公司 | UV light-cured texture paint for similar 3D printing, preparation method and use method thereof |
| CN114633334A (en) * | 2022-03-21 | 2022-06-17 | 小森新材料科技有限公司 | Anti-yellowing matte surface coating process for UV (ultraviolet) photocureable coating of solid wood composite board |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106085083A (en) * | 2016-06-23 | 2016-11-09 | 苏州吉人高新材料股份有限公司 | A kind of aqueous composite paint of environmental protection and preparation method thereof |
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| CN105925170A (en) * | 2016-06-29 | 2016-09-07 | 海盐三田科技有限公司 | Solvent-free ultraviolet photocuring anti-flouring easily cleaned paint as well as preparation method and application thereof |
| CN106362916A (en) * | 2016-08-26 | 2017-02-01 | 索菲亚家居股份有限公司 | Spraying technology utilizing LED lamp for curing |
| CN114525069A (en) * | 2022-03-21 | 2022-05-24 | 小森新材料科技有限公司 | UV light-cured texture paint for similar 3D printing, preparation method and use method thereof |
| CN114633334A (en) * | 2022-03-21 | 2022-06-17 | 小森新材料科技有限公司 | Anti-yellowing matte surface coating process for UV (ultraviolet) photocureable coating of solid wood composite board |
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Application publication date: 20151216 |