CN105968942A - LED-solidified water transfer printing ink and preparation method thereof - Google Patents
LED-solidified water transfer printing ink and preparation method thereof Download PDFInfo
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- CN105968942A CN105968942A CN201610544262.3A CN201610544262A CN105968942A CN 105968942 A CN105968942 A CN 105968942A CN 201610544262 A CN201610544262 A CN 201610544262A CN 105968942 A CN105968942 A CN 105968942A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses LED-solidified water transfer printing ink and a preparation method thereof. The ink is mainly prepared from the following raw materials in parts by weight: 10-50 parts of urethane acrylate resin, 15-80 parts of epoxy acrylate resin, 5-30 parts of acrylic resin, 5-50 parts of 1,6-hexanediol diacrylate, 2-20 parts of trimethylolpropane triacrylate and 2-20 parts of photosensitive initiator. The components are sequentially added according to the parts, stirred at fixed time and constant speed and finally ground by a three-roller machine and stirred. The ink disclosed by the invention meets the customer requirements on the surface decoration of the plastic, carbon fiber and metal stainless steel toys, sports equipment, bicycles and electric vehicle cores.
Description
Technical field
The present invention relates to a kind of ink, particularly relate to water transfer ink of a kind of LED solidification and preparation method thereof,
Specifically refer to one apply and become a full member the anti-labeling industry of patch at plastics, carbon fibre, rustless steel, pottery, metal class water
Printing-ink and preparation method thereof.
Background technology
Water transfer materials refer to substrate surface processing can the print film of global transfer picture and text, base material is permissible
It is plastic sheeting, it is also possible to be water-transfer printing paper.This print film is as text carrier, and its appearance should be print
One much progress of brush technology, because there being a lot of product to be difficult to directly print, and has had this carrier, people
Picture and text first can be imprinted on the carrier of easily printing by ripe printing technology, then picture and text are transferred to
On stock.As having certain altitude, relatively heavier, grotesque article or area is the least
Article can use transfer printing process.Single for water transfer printing technique, its adaptability is very wide, almost without
The product that cannot transfer.
At present, most of mode of printings are both for plane or the decorating printing of almost plane stock, as thin
Film gravure, paper offset printing etc.；The stock of silk screen printing is more, can print some irregular curved surfaces,
Such as plastic bottle；The adaptability of bat printing makes progress again than silk screen printing, but coverage is too narrow.Water transfer technique
It it is a kind of special trans-printing new technique.Water transfer technique be utilize hydraulic pressure by the transfer paper of band multicolour pattern/
Plastic foil carries out a kind of printing of macromolecule hydrolysis.Along with people's raising to product packaging with the requirement of decoration,
The purposes of water transfer is more and more extensive, can be used for Automobile Products, electronic product, room articles for use, daily fine work,
Indoor building materials etc..The principle of its indirect printing and perfect printing effect solve many product surface decorations
A difficult problem, is mainly used in all kinds of pottery, applique, the transfer of metal class material etc..
Transfer ink then with the dyestuff of special nature be main make the pattern being imprinted on special paper, word etc.,
Can be allowed to transfer to the ink that other base materials get on because of heating.At present, domestic water transfer ink uses
Resin, the solid propenoic acid resin of the most external import, price is high, uses existing defects, due to
The vitrification point of solid propenoic acid resin is 32 DEG C, and during summer, resin particle easily melts conglomeration, need to break into pieces
After could dissolve with solvent.And domestic thermoplastic acrylic resin, mostly use dimethylbenzene, butyl acetate
Make solvent, there is penetrating odor, it is difficult to for printing industry；And, existing thermoplastic acrylic tree
Fat, due to molecular weight, causes being difficult to reach balance in hardness and hot strength.For cost consideration,
Some producer water transfer ink in utilize acrylic resin to replace acrylic resin, but it is big to there is fragility
Defect, toughener need to be added and carry out toughness reinforcing, but toughener easily migrates, cause produce water transfer
The marble paper short time becomes fragile after depositing.Additionally, the production of existing acrylic resin be from liquid to solid again to
The process of liquid, more to energy resource consumption.
And, at present at plastic toy, plastics sports equipment, carbon fibre sports equipment, metal leg treadmill, electricity
Environment, human body are caused certain hazardness by the solvent-borne type water transfer ink that the industries such as motor-car commonly use；Giving birth to
The speed of production. art, efficiency is by a certain degree of restriction.
Summary of the invention
For solving the problems referred to above, it is an object of the invention to provide the water transfer ink of a kind of LED solidification.This
The ink of bright offer uses the solidification of non-volatile pollution-free LED UV cold light source, thus has the excellent of low-energy environment-friendly
Gesture.
For reaching above-mentioned purpose, the present invention adopts the following technical scheme that
The water transfer ink of a kind of LED solidification, is made up of the raw material comprising following parts by weight:
The amount of polyurethane acrylate resin can be such as 12 parts, 18 parts, 23 parts, 28 parts, 33 parts, 39
Part, 45 parts, 49 parts etc..
The amount of Epocryl can be such as 18 parts, 23 parts, 28 parts, 33 parts, 39 parts, 45 parts,
50 parts, 55 parts, 62 parts, 69 parts, 74 parts, 78 parts etc..
The amount of acrylic resin can be such as 7 parts, 11 parts, 16 parts, 19 parts, 22 parts, 27 parts etc..
The amount of 1,6-HD dipropyl dilute acid ester can be such as 7 parts, 11 parts, 18 parts, 23 parts, 28 parts, 33
Part, 39 parts, 45 parts, 49 parts etc..
The amount of trimethylolpropane trimethacrylate can be such as 3 parts, 7 parts, 11 parts, 16 parts, 19 parts etc..
The amount of photoinitiator can be such as 3 parts, 7 parts, 11 parts, 16 parts, 19 parts etc..
As preferably, the water transfer ink of the present invention, it is made up of the raw material comprising following parts by weight:
The present invention uses polyurethane acrylate resin and Epocryl and 1,6-HD two propylene
The combination of acid esters can ensure the adhesive force of ink.
As preferably, the water transfer ink of the present invention, also comprise: organic pigment, defoamer, dispersant or
One kind or two or more combination in levelling agent.
As preferably, the water transfer ink of the present invention, raw material by weight also comprises:
The amount of organic pigment can be such as 0.08 part, 0.15 part, 0.5 part, 1.2 parts, 2 parts, 5 parts, 8 parts,
11 parts, 14 parts etc..
The amount of defoamer can be such as 0.07 part, 0.12 part, 0.2 part, 0.7 part, 1.3 parts, 2 parts, 2.5
Part, 3.6 parts, 4.1 parts, 4.8 parts etc..
The amount of dispersant can be such as 0.07 part, 0.12 part, 0.2 part, 0.7 part, 1.3 parts, 2 parts, 2.5
Part, 3.6 parts, 4.1 parts, 4.8 parts etc..
The amount of levelling agent can be such as 0.07 part, 0.12 part, 0.2 part, 0.7 part, 1.3 parts, 2 parts, 2.5
Part, 3.6 parts, 4.1 parts, 4.8 parts etc..
As preferably, the water transfer ink of the present invention, raw material by weight also comprises:
As preferably, the water transfer ink of the present invention, described photoinitiator be 4-phenyl benzophenone and/or
Diphenyl phosphate oxygen.
As preferably, the water transfer ink of the present invention, described organic pigment is permanent bordeaux, permanent yellow, forever consolidates
One kind or two or more combination in purple, phthalocyanine blue, green, carbon black.
As preferably, the water transfer ink of the present invention, described defoamer is a kind in polymer-type defoamer
Or combination of more than two kinds.Defoamer can help froth breaking and printing off-network effect, makes printing effect more attractive in appearance.
As preferably, the water transfer ink of the present invention, described dispersant is that the block containing pigment affinity groups is total to
One kind or two or more combination in polymers.
As preferably, the water transfer ink of the present invention, described levelling agent is polyether-modified polydimethylsiloxane
The one kind or two or more combination of blend apoplexy due to endogenous wind, the most polyether-modified polydimethylsiloxane.
As preferably, the water transfer ink of the present invention, it is made up of the raw material comprising following parts by weight:
An object of the present invention also resides in the preparation method providing water transfer ink of the present invention, including
Following steps:
(1) by polyurethane acrylate resin, Epocryl, acrylic resin, 1,6-oneself two
Alcohol dipropyl dilute acid ester, trimethylolpropane trimethacrylate are stirred until homogeneous；
Optionally (2) addition organic pigment, stirring；
(3) surplus materials is added, stirring；
(4) grinding steps (3) gained mixture.
As preferably, preparation method of the present invention, in step (1), the speed of stirring is 800-1000
Rev/min, the time of stirring is more than 5 minutes, preferably 10-30 minute.
As preferably, preparation method of the present invention, described in step (2), organic pigment is at stirring
Under be slowly added to.
Preferably, the speed of described stirring is 800-1000 rev/min, and the time of stirring is more than 5 minutes, excellent
Elect 10-30 minute as.
As preferably, preparation method of the present invention, in step (3) speed of stirring be 500-800 turn/
Point, the time of stirring is more than 2 minutes, preferably 5-10 minute.
As preferably, preparation method of the present invention, in step (4), use three-roller is ground.
Preferably, the number of times of grinding is more than 2 times, preferably 4-6 time.
Preferably, survey 3, left, center, right thickness between machine discharging blade and the preliminary roller machine of grinding, should be less than
50 μm, preferably smaller than 35 μm.Preferably, final finished ink records ink fineness on Hegman grind gage
Less than 5 μm, preferably smaller than 3 μm.
Present invention have the advantage that the ink of the present invention uses non-volatile pollution-free LED UV cold light source solid
Change, thus there is the advantage of low-energy environment-friendly.
Detailed description of the invention
For the present invention is better described, it is simple to understand technical scheme, the typical case of the present invention but non-limit
The embodiment of property processed is as follows:
Embodiment 1
Raw material contains by weight: polyurethane acrylate resin 20 parts, Epocryl 30
Part, acrylic resin 10 parts, 1,6-hexanediol dipropyl dilute acid ester 10 parts, trimethylolpropane trimethacrylate
5 parts, photoinitiator 5 parts, organic pigment 0 part, defoamer 0.1 part, dispersant 0.2 part, levelling agent
0.1 part.
Photoinitiator is 4-phenyl benzophenone, diphenyl phosphate oxygen；Defoamer is polymer-type defoamer；
Dispersant is the block copolymer containing pigment affinity groups；Levelling agent is polyether-modified dimethione.
Concrete preparation method is as follows:
(1) number is pressed by polyurethane acrylate resin, Epocryl, acrylic resin, 1,6-
Hexanediol dipropyl dilute acid ester, trimethylolpropane trimethacrylate blanking successively stir 10-30 minute to uniformly,
Mixing speed is 800-1000 rev/min.
(2) adding its remainder by number, stir 5-10 minute, mixing speed is 500-800 rev/min.
(3) use three-roller to be ground 4-6 time by mixed ink, survey between grinder discharging blade and preliminary roller machine
3, left, center, right thickness, should be in 20 μm-35 μm, and it is thin that final finished ink records ink on Hegman grind gage
Degree is less than 1 μm-3 μm.
Printing process and drying condition thereof:
1) add diluent and adjust ink viscosity, stir 10 minutes, then stand 10 minutes.
2) use 250-300 mesh grid (100-120T) screen printing, be printed on water-transfer printing paper.
3) turn dry with the solidification of LED machine cold light source on paper by print and water.
4) dried transfer paper is just transferring through soaked patterned layer disengaging and is being attached to material (glass, pottery)
On.Forward on glass, pottery through baking in 170 DEG C to 30 minutes.
Embodiment 2
Raw material contains by weight: polyurethane acrylate resin 25 parts, Epocryl 40
Part, acrylic resin 15 parts, 1,6-hexanediol dipropyl dilute acid ester 20 parts, trimethylolpropane trimethacrylate
8 parts, photoinitiator 8 parts, organic pigment 5 parts, defoamer 1 part, dispersant 1 part, levelling agent 1 part.
Photoinitiator is diphenyl phosphate oxygen；Organic pigment is permanent bordeaux；Defoamer is polymer-type froth breaking；
Dispersant is the block copolymer containing pigment affinity groups；Levelling agent is polyether-modified polydimethylsiloxane.
Concrete preparation process is same as in Example 1, increases the step adding organic pigment.
Concrete printing process and drying condition thereof are same as in Example 1.
Embodiment 3
Raw material contains by weight: polyurethane acrylate resin 30 parts, Epocryl 50
Part, acrylic resin 20 parts, 1,6-hexanediol dipropyl dilute acid ester 30 parts, trimethylolpropane trimethacrylate
10 parts, photoinitiator 10 parts, organic pigment 8 parts, defoamer 2 parts, dispersant 2 parts, levelling agent 2
Part.
Photoinitiator is 4-phenyl benzophenone；Organic pigment is carbon black；Defoamer is polymer-type froth breaking
Agent；Dispersant is the block copolymer containing pigment affinity groups；Levelling agent is polyether-modified polydimethylsiloxanes
Alkane.
Concrete preparation process is same as in Example 1, increases the step adding organic pigment.
Concrete printing process and drying condition thereof are same as in Example 1.
Embodiment 4
Raw material contains by weight: polyurethane acrylate resin 10 parts, Epocryl 80
Part, acrylic resin 5 parts, 1,6-hexanediol dipropyl dilute acid ester 50 parts, trimethylolpropane trimethacrylate 2
Part, photoinitiator 2 parts, organic pigment 15 parts.
Photoinitiator is 4-phenyl benzophenone, diphenyl phosphate oxygen；Organic pigment is that phthalein is Dracocephalum moldabium.
Concrete preparation process is same as in Example 1, increases the step adding organic pigment.
Concrete printing process and drying condition thereof are same as in Example 1.
Embodiment 5
Raw material contains by weight: polyurethane acrylate resin 50 parts, Epocryl 15
Part, acrylic resin 30 parts, 1,6-hexanediol dipropyl dilute acid ester 5 parts, trimethylolpropane trimethacrylate 20
Part, photoinitiator 20 parts, dispersant 5 parts, levelling agent part 5 parts.
Photoinitiator is diphenyl phosphate oxygen；Dispersant is the block copolymer containing pigment affinity groups；Levelling
Agent is polyether-modified polydimethylsiloxane.
Concrete preparation process is same as in Example 1.
Concrete printing process and drying condition thereof are same as in Example 1.
The ink that the embodiment of the present invention prepares can use non-volatile pollution-free LED UV cold light source to solidify, thus
There is the advantage of low-energy environment-friendly.
Applicant states, the present invention illustrates the method detailed of the present invention by above-described embodiment, but the present invention
It is not limited to above-mentioned method detailed, does not i.e. mean that the present invention has to rely on above-mentioned method detailed and could implement.
Person of ordinary skill in the field is it will be clearly understood that any improvement in the present invention, each former to product of the present invention
The equivalence of material is replaced and the interpolation of auxiliary element, concrete way choice etc., all falls within the protection model of the present invention
Within the scope of enclosing and disclosing.
Claims (10)
1. a water transfer ink, it is characterised in that be made up of the raw material comprising following parts by weight:
Water transfer ink the most according to claim 1, it is characterised in that by comprising following parts by weight
Raw material make:
Water transfer ink the most according to claim 1 and 2, it is characterised in that also comprise: You Jiyan
One kind or two or more combination in material, defoamer, dispersant or levelling agent.
Water transfer ink the most according to claim 1 and 2, it is characterised in that raw material by weight
Also comprise:
Preferably, raw material also comprises by weight:
5. according to the water transfer ink described in any one of claim 1-4, it is characterised in that described photosensitive draw
Sending out agent is 4-phenyl benzophenone and/or diphenyl phosphate oxygen.
6. according to the water transfer ink described in claim 3 or 4, it is characterised in that described organic pigment is
One kind or two or more combination in permanent bordeaux, permanent yellow, permanent violet, phthalocyanine blue, green, carbon black；
Preferably, the one kind or two or more combination during described defoamer is polymer-type defoamer；
Preferably, one kind or two or more during described dispersant is the block copolymer containing pigment affinity groups
Combination；
Preferably, described levelling agent be that polyether-modified polydimethylsiloxane is blended in species defoamer a kind
Or combination of more than two kinds, the most polyether-modified polydimethylsiloxane.
Water transfer ink the most according to claim 1, it is characterised in that by comprising following parts by weight
Raw material make:
8. the preparation method of the water transfer ink described in any one of claim 1-7, comprises the steps:
(1) by polyurethane acrylate resin, Epocryl, acrylic resin, dipropylene glycol
Diacrylate, trimethylolpropane trimethacrylate are stirred until homogeneous；
Optionally (2) addition organic pigment, stirring；
(3) surplus materials is added, stirring；
(4) grinding steps (3) gained mixture.
Preparation method the most according to claim 8, it is characterised in that the speed of stirring in step (1)
Degree is for 800-1000 rev/min, and the time of stirring is more than 5 minutes, preferably 10-30 minute；
Preferably, described in step (2), organic pigment is slowly added under stirring；
Preferably, the speed of described stirring is 800-1000 rev/min, and the time of stirring is more than 5 minutes, excellent
Elect 10-30 minute as.
Preparation method the most according to claim 8 or claim 9, it is characterised in that stirring in step (3)
Speed be 500-800 rev/min, the time of stirring is more than 2 minutes, preferably 5-10 minute；
Preferably, step (4) use three-roller be ground；
Preferably, the number of times of grinding is more than 2 times, preferably 4-6 time；
Preferably, survey 3, left, center, right thickness between machine discharging blade and the preliminary roller machine of grinding, should be less than
50 μm, preferably smaller than 35 μm；
Preferably, final finished ink records ink fineness on Hegman grind gage and is less than 5 μm, preferably smaller than
3μm。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610544262.3A CN105968942A (en) | 2016-07-12 | 2016-07-12 | LED-solidified water transfer printing ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610544262.3A CN105968942A (en) | 2016-07-12 | 2016-07-12 | LED-solidified water transfer printing ink and preparation method thereof |
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| CN105968942A true CN105968942A (en) | 2016-09-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610544262.3A Pending CN105968942A (en) | 2016-07-12 | 2016-07-12 | LED-solidified water transfer printing ink and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108912816A (en) * | 2018-09-20 | 2018-11-30 | 永修县利君科技有限公司 | A kind of cured water transfer ink of LED |
| CN108912815A (en) * | 2018-09-10 | 2018-11-30 | 东莞市美吉高分子材料有限公司 | A kind of novel environment friendly LED-UV water transfer plastic glue ink and its production method |
| CN108997824A (en) * | 2018-09-10 | 2018-12-14 | 东莞市美吉高分子材料有限公司 | A kind of novel environment friendly LED-UV water transfer glass ink and its production method |
| CN108997826A (en) * | 2018-09-10 | 2018-12-14 | 东莞市美吉高分子材料有限公司 | A kind of environment-friendly energy-saving LED-UV toy car plastic uptake ink and its production method |
| US10982103B2 (en) * | 2016-12-09 | 2021-04-20 | Sicpa Holding Sa | Low energy curing offset and letterpress printing inks and printing process |
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| CN101696332A (en) * | 2009-10-28 | 2010-04-21 | 东周化学工业（昆山）有限公司 | Ultra-violet curing transfer ink |
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| CN101696332A (en) * | 2009-10-28 | 2010-04-21 | 东周化学工业（昆山）有限公司 | Ultra-violet curing transfer ink |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10982103B2 (en) * | 2016-12-09 | 2021-04-20 | Sicpa Holding Sa | Low energy curing offset and letterpress printing inks and printing process |
| CN108912815A (en) * | 2018-09-10 | 2018-11-30 | 东莞市美吉高分子材料有限公司 | A kind of novel environment friendly LED-UV water transfer plastic glue ink and its production method |
| CN108997824A (en) * | 2018-09-10 | 2018-12-14 | 东莞市美吉高分子材料有限公司 | A kind of novel environment friendly LED-UV water transfer glass ink and its production method |
| CN108997826A (en) * | 2018-09-10 | 2018-12-14 | 东莞市美吉高分子材料有限公司 | A kind of environment-friendly energy-saving LED-UV toy car plastic uptake ink and its production method |
| CN108912816A (en) * | 2018-09-20 | 2018-11-30 | 永修县利君科技有限公司 | A kind of cured water transfer ink of LED |
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Effective date of registration: 20180116 Address after: 330300 Yunshan Industrial Park, Yunshan Economic Development Zone, Yongxiu County, Jiujiang, Jiangxi Applicant after: Yongxiu County Lijun science and Technology Co., Ltd. Address before: Suzhou City, Jiangsu province 215334, Kunshan City Development Zone, No. 350 Honghu Road Applicant before: Kunshan Shuguang Lighting Equipment Co., Ltd. |
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