CN102267839A - Plant organic nutrient solution containing saccharicterpenin and preparation method thereof - Google Patents
Plant organic nutrient solution containing saccharicterpenin and preparation method thereof Download PDFInfo
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Abstract
A saccharicterpenin contained plant organic nutrient solution comprises in per liter 10-100g of saccharicterpenin raw powder, 200-800g of bamboo vinegar, 50-250g of amino acid stock solution powder, 2-20g of oligosaccharide, 70-300g of chemical fertilizer, 10-35g of trace element fertilizer, 2-5g of surfactant and the balance of water. The plant organic nutrient solution of the invention is suitable for using as a plant nutrition agent.
Description
Technical field
The present invention relates to a kind of farm crop fertilizer, especially a kind of organic nutrition of plant liquid that contains saccharicter-penin and preparation method thereof.
Background technology
Oil tea is a kind of important oilseed plant.Tea oil tree is extensively planted in various places, China south.After from the oil tea fruit, squeezing edible oil, obtain a large amount of tea seed cakes.Tea seed cake also has camellia seedcake except that tea-seed pancake.Owing to tea-seed pancake bitter, reason such as poisonous, cause a large amount of grouts to go out of use, cause the very big wasting of resources.
Saccharicter-penin (Saccharicterpenin) is made up of the triterpenoid saponin that extracts from the Theaceae fruit (〉=30), carbohydrate natural bioactivity substances such as (〉=30), is a kind of pale brown look, ashless, fine shape crystallisate.It is insoluble to ether, chloroform, acetone benzene, sherwood oil, dissolves in warm water, dithiocarbonic anhydride, vinyl acetic monomer, is soluble in aqueous methanol, aqueous ethanol, propyl carbinol and Glacial acetic acid.Saccharicter-penin is easily molten in aqueous alcohols, and solubleness maximum in 70%～80% methyl alcohol, ethanol can be dissolved in hot water, and solubleness significantly increases in alkaline aqueous solution, and is almost insoluble in non-polar solvents such as ether and sherwood oil.
The triterpenes oligosaccharide that the researchist of animal science institute of Zhejiang University extracts from plant, commodity are called saccharicter-penin (SHP), be the triterpenoid saponin that from the grouts after the plant of theaceae seed processing, extracts and the mixture of carbohydrate, the natural bioactivity substance of forming by carbohydrate (I＞30%), glycoside (〉=30%) and organic acid.It belongs to green feed additive, and the saccharicter-penin fodder additives obtains first new feed additive certification of China (No. 199816, agriculture and animal husbandry letter) in May, 1998, has now obtained the patent of invention of states such as China, the U.S., Israel, Australia and Russia.On July 6th, 2000, GFDC is that saccharicter-penin has been issued AA level fully natural green fodder additives certificate.
Our result of study shows in recent years, and an important feature of the triterpenoid saponin in the saccharicter-penin is to suppress urease activity, improves utilization rate of fertilizer, has surfactivity, can increase drug effect.It also has the plant of stimulation vivo immuning system, promotes the infiltration and the absorption of nutritive ingredient, accelerates albumen synthetic effect.Saccharicter-penin has obvious removing free radical and anti-oxidant function.According to the study, the oxidation voluntarily of fat (acid) is because radical such as generation such as the effect of high temperature, radioactive rays, metal ion etc. begins, saccharicter-penin can stop proceeding of oxidation voluntarily with this radical generation effect, and it has the effect of removing superoxide radical, hydroxy radical qiao and alicyclic diradical.Data shows that many Plant diseasess such as virus disease, bacterial disease, early ageing, physiological disease, continuous cropping disease etc. are all relevant with the toxic reaction of oxyradical, and biomacromolecules such as oxyradical and DNA react, and cause cellularstructure and function destroyed.Saccharicter-penin also has anticancer, antivirus action except having obvious removing free radical and anti-oxidant function, can suppress the growth of virosome, and is obvious to alleviating the virus disease effect.
Therefore, whole immune performance and the body interior sugared nitrogen metabolism system function of saccharicter-penin by improving plant improves the disease-resistant level of system of plant, and then improves the production performance of plant.Saccharicter-penin can obviously improve the plant body's immunological function and effect is coerced in disease-resistant, degeneration-resistant border, promote protein synthesis and the active physiological function of plurality of enzymes, saccharicter-penin can also obviously improve quality of agricultural product, reduce the agricultural-food melon, really, heavy metal content in the vegetables, sugar, grain, oil crops.Obviously, the mechanism of action of saccharicter-penin obviously is different from sterilant (sterilant is prevented and treated disease by suppressing or killing the dip-dye of plant harmful microbe, growth and breeding, and its effects of action phase is short).
But with the saccharicter-penin is that core material manufacturing fertilizer does not appear in the newspapers so far, especially with saccharicter-penin as core material, cooperate bamboo charcoal tankage bamboo vinegar liquid as carrier, add nitrogen phosphorus potassium, amino acid, trace element, oligosaccharide etc. and make a kind of organic nutrition of plant liquid that contains saccharicter-penin, be used for agriculture production, improve crop yield, more belong to a novel invention.
Summary of the invention
The present invention will solve the problem that present tea seed cake could not efficiently utilize and lack the organic nutrition of plant liquid that contains saccharicter-penin, a kind of organic nutrition of plant liquid that contains saccharicter-penin of the present invention and preparation method thereof is provided for this reason, the present invention has expanded the range of application of saccharicter-penin, makes the forest tree resource recycle; The present invention has tangible stiffening effect to disease-resistant crops, resistance, can improve output and the agricultural product quality of farm crop; The present invention does not contain any hormone, and is pollution-free, and no hazard residue is without any side effects, to safety in production, optimizes agricultural-food, and protection human health etc. are significant.
For addressing the above problem, the technical solution used in the present invention comprises a kind of organic nutrition of plant liquid of saccharicter-penin and preparation method of this nutritive medium of containing.
A kind of organic nutrition of plant liquid that contains saccharicter-penin of the present invention, its special character are to be that benchmark contains with every liter of described nutritive medium:
Former powder 10～100 grams of saccharicter-penin,
Bamboo vinegar liquid 200～800 grams,
Amino acid primary liquid powder 50～250 grams,
Oligosaccharide 2～20 grams,
Chemical fertilizer 70～300 grams,
Trace element fertilizer 10～35 grams,
Tensio-active agent 2～5 grams,
Water surplus.
Described oligosaccharide be in xylo-oligosaccharide, chitosan, soybean oligosaccharide, the oligofructose one or both, three kinds mixture.
Described chemical fertilizer is urea 50～200 grams, saltpetre and/or potassium primary phosphate 20～100 grams.
Described trace element fertilizer is the mixture of one or more (containing two kinds) in boron fertilizer, zinc fertilizer, iron fertilizer, manganese fertilizer, the copper fertilizer.
Described tensio-active agent is tween 80, Sodium dodecylbenzene sulfonate or Sodium dodecylbenzene sulfonate.
A kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin of the present invention, its special character is to be benchmark with every liter of described nutritive medium,
(1) 200-800 is restrained bamboo vinegar liquid and insert reactor, be warming up to 40-60 ℃, drop into the former powder 10-100 gram of saccharicter-penin, be dissolved in the bamboo vinegar liquid;
(2) in above-mentioned solution, add amino acid powder 50-250 gram, mix;
(3) above-mentioned mixed solution adds chemical fertilizer 70～300 grams under agitation condition, keeps 40-60 ℃ of temperature, fully after the dissolving, adds trace element fertilizer 10～50 grams while stirring, to fully dissolving;
(4) get a stainless steel vessel in addition,, be soaked in 50～100 milliliters 30～50 ℃ the warm water 1.5～4 hours oligosaccharide 2～20 gram;
(5) the 4th step gained solution is joined in the 3rd step solution, mix, add tensio-active agent 2～5 grams then, stirring, emulsification pretreatment 15～45 minutes add water to 1000 milliliters, stir.
Described oligosaccharide is the mixture of one or more (containing two kinds) in xylo-oligosaccharide, chitosan, soybean oligosaccharide, the oligofructose etc.
Described chemical fertilizer is urea 50～200 grams, saltpetre and/or potassium primary phosphate 20～100 grams.
Described trace element fertilizer is the mixture of one or more (containing two kinds) in boron fertilizer, zinc fertilizer, iron fertilizer, manganese fertilizer, the copper fertilizer.
Described tensio-active agent is tween 80, Sodium dodecylbenzene sulfonate or Sodium dodecylbenzene sulfonate.
The present invention compared with prior art has following positively effect:
1, the present invention has opened up out the range of application of saccharicter-penin, takes the lead in that saccharicter-penin is prepared into plant nutrition liquid as the nutrition agent core material and is applied to plant husbandry.
2, the present invention is on the basis of saccharicter-penin, adds bamboo charcoal tankage fermented liquid, has solved the approach of forest tree resource cycling and reutilization, meets requirements such as the national green ecological Agricultural Development demand and the ecological agriculture.Enlarged the development mode of water-soluble fertilizer simultaneously, the two is worked in coordination, and mutually promotes.
3, saccharicter-penin plant growth nutrient fluid of the present invention is aided with oligosaccharide as a kind of triterpenoid saponin and carbohydrate admixture, and mutually synergy has tangible stiffening effect to inducing plant or disease-resistant crops, resistance.
4, a kind of saccharicter-penin plant growth nutrient fluid of being prepared into of the present invention, comprehensive nutrition, the organic content height, rich trace elements is a kind of organic nutritive medium.Be used for plant husbandry; has tangible enhancing immunity effect; can improve output and the agricultural product quality of farm crop; do not contain any hormone; environmental protection; pollution-free noresidue is without any side effects, to production safety, high quality agricultural products, protection human health and strengthen high quality agricultural products grain, dish, really, outlets such as tea, sugar, cigarette are significant.
4, the present invention is used for soil treatment, irritates root and dash and execute, and can improve the crop micro-ecological environment, has anti-continuous cropping, kills subterranean pest-insect, kills nematode, takes root, the effect of mulch, has and improves the effect that output is promoted quality.
5, the present invention is as a kind of organic nutritive medium, compatibleness is good, can reduce the surface tension of liquid, with agricultural chemicals, other foliage fertilizers, water-soluble fertilizer is composite has significant synergies, reduce the input of effective constituents such as fungicide insecticide, abridged edition, synergy, residual low.
Embodiment
Embodiment 1:
(1) 700 gram refined bamboo vinegars is squeezed into reactor, be warming up to 50～60 ℃, get former powder 100 grams of saccharicter-penin, in 50～60 ℃ of the being dissolved in heating bamboo vinegar liquid;
(2) adding former powder 50 grams of amino acid in above-mentioned solution mixes;
(3) above-mentioned mixed solution adds urea 50 grams under agitation condition, potassium primary phosphate 50 grams, and saltpetre 40 grams keep 50～60 ℃ of temperature, fully after the dissolving, add boric acid 10 grams while stirring, iron vitriol 10 grams, citric acid 8 grams are to fully dissolving;
(4) get a stainless steel vessel in addition, with xylo-oligosaccharide 4 gram, chitosan 6 grams are soaked in 50 milliliters 30～50 ℃ the warm water 1.5～4 hours;
(5) the 4th step gained solution is joined in the 3rd step solution, mix, add tensio-active agent Sodium dodecylbenzene sulfonate 3 grams then, stirring, emulsification pretreatment 30 minutes add water to 1000 milliliters, stir, and promptly finish the present invention.
Embodiment 2: the organic nutrition of plant liquid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 20 grams; The former powder of amino acid: 250 grams;
Urea: 100 grams; Saltpetre: 60 grams;
Refined bamboo vinegar: 300 grams; Citric acid: 10 grams;
Boric acid: 5 grams; Sodium lauryl sulphate: 5 grams
Zinc Sulphate Heptahydrate: 10 grams; Xylo-oligosaccharide: 5 grams
Seven water manganous sulfates: 5 grams; Water: surplus;
Production stage and technology are with shining embodiment 1.
Embodiment 3: the plant that contains saccharicter-penin of present embodiment has flour nutrition liquid, contains following component in every liter of solution:
The former powder of saccharicter-penin: 50 grams; The former powder of amino acid: 125 grams;
Urea: 150 grams; Dipotassium hydrogen phosphate: 50 grams;
Refined bamboo vinegar: 400 grams; Citric acid: 5 grams;
Five water Sodium Tetraboratees: 10 grams; Sodium dodecylbenzene sulfonate: 3 grams;
Zinc Sulphate Heptahydrate: 8 grams; Water: surplus;
Chitosan: 10 grams;
Xylo-oligosaccharide: 10 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 4: the organic nutrition of plant liquid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 10 grams; The former powder of amino acid: 250 grams;
Urea: 200 grams; Saltpetre: 100 grams;
Refined bamboo vinegar: 300 grams; Citric acid: 6 grams;
Four water, eight Sodium Tetraboratees: 5 grams; Sodium dodecylbenzene sulfonate: 3 grams
Zinc nitrate: 10 gram water: surplus;
Soybean oligosaccharide: 6 grams;
Xylo-oligosaccharide: 14 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 5: the plant growth nutrient fluid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 60 grams; The former powder of amino acid: 250 grams;
Urea: 150 grams; Potassium primary phosphate: 100 grams;
Refined bamboo vinegar: 350 grams; Citric acid: 8 grams;
Boric acid: 10 grams; Sodium dodecylbenzene sulfonate: 4 grams;
Zinc Sulphate Heptahydrate: 8 grams; Water: surplus;
Chitosan: 10 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 6: the organic nutrition of plant liquid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 40 grams; The former powder of amino acid: 150 grams;
Urea: 150 grams; Saltpetre: 70 grams;
Refined bamboo vinegar: 350 grams; Citric acid: 5 grams;
Boric acid: 10 grams; Sodium dodecylbenzene sulfonate: 3 grams;
Xylo-oligosaccharide: 10 grams; Water: surplus;
Iron-amino acid chelate: 20 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 7: the organic nutrition of plant liquid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 40 grams; The former powder of amino acid: 150 grams;
Urea: 150 grams; Saltpetre: 50 grams;
Refined bamboo vinegar: 300 grams; Citric acid: 5 grams;
Boric acid: 10 grams; Tween 80: 3 grams;
Chitosan: 2 grams; Water: surplus;
Iron-amino acid chelate: 20 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 8: the plant growth nutrient fluid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 10 grams; Urea: 200 grams;
Saltpetre: 100 grams; Citric acid: 6 grams;
Refined bamboo vinegar: gram 250 grams; Sodium dodecylbenzene sulfonate: 3 grams;
Four water, eight Sodium Tetraboratees: 5 grams; Water: surplus;
Zinc nitrate: 10 grams
Oligofructose: 6 grams;
Xylo-oligosaccharide: 14 grams;
Production stage and technology are with shining embodiment 1.
Embodiment 9: the organic nutrition of plant liquid that contains saccharicter-penin of present embodiment, contain following component in every liter of solution:
The former powder of saccharicter-penin: 40 grams; The former powder of amino acid: 150 grams;
Urea: 150 grams; Saltpetre: 50 grams;
Refined bamboo vinegar: 300 grams; Citric acid: 5 grams;
Boric acid: 10 grams; Sodium dodecylbenzene sulfonate: 3 grams;
Iron-amino acid chelate: 20 grams; Soybean oligosaccharide: 1 gram;
Oligofructose: 1 gram; Water: surplus;
Production stage and technology are with shining embodiment 1.
Embodiment 10
Present embodiment is field test embodiment
1, romaine lettuce is used saccharicter-penin plant growth nutrient fluid field simultaneous test:
In late October, 2009 applicant selected two neighbor cells in the auspicious booth of town Li Hong on May Day, the identical farm manure of quantity is all used in 222 square metres of every sub-districts, " east lucky star " romaine lettuce that plantation is introduced from the U.S..Beginning in the 10th day after field planting, experimental group used the organic nutrition of plant liquid that contains saccharicter-penin of the present invention to carry out foliar spray one time in per 10 days, and totally 3 times, 100 milliliters of each consumptions are converted 30 kg of water foliar sprays.Control group uses clear water spraying, totally 3 times, each 50 kilograms.Carried out comparative analysis when gather mid-December.
It is as follows that table 1 romaine lettuce is used saccharicter-penin plant growth nutrient fluid field comparative test result:
As can be seen from Table 1, use plant that the organic nutrition of plant liquid contain saccharicter-penin handles than control group sturdy tall and big, blade distributes closely, leaf area increases the single plant yield height.The industrialization of this science and technology item will bring remarkable economic efficiency and social benefit.
2,2009 plastic tent cucumber saccharicter-penin plant growth nutrient fluid interpretations
Two processing are established in test, four repetitions, and the test site physical features is smooth, neatly, middle fertility on the upper side, and is evenly, representative in the locality, the organic nutrition of plant liquid model field (handling 1) that contains saccharicter-penin sprays more than 5 mu, every mu time with 50 milliliters of this product, converts water 15k gram-25k and restrain, after field planting 30 days, 60 days, 90 days, each spray is once sprayed 3 times altogether.1 same period is sprayed the equivalent clear water with handling more than 1 mu in contrast field (handle 2).
The organic nutrition of plant liquid experimental result that plastic tent cucumber in 2009 contains saccharicter-penin is carried out the t check
Table 2
The single standard deviation
Mean standard deviation
t＝|x
1～x
2|/sd＝3.45/0.2705＝12.75
Degree of freedom n～1=4～1=3, table look-up t0.05=3.18, t0.01=5.84t=12.75＞t0.01=5.84.Processing 1 and processing 2 level of difference reach extremely remarkable, illustrate that the saccharicter-penin plant growth nutrient fluid has significant effect.
Table 3
Can find out from table 3, contain the organic nutrition of plant liquor ratio clear water contrast cucumber production promoting amplitude 14.79% of saccharicter-penin.
Test-results shows, uses the organic nutrition of plant liquid that contains saccharicter-penin that cucumber production promoting is had unusual effect.
By above two field tests as seen, if contain of the achievements conversion of the organic nutrition of plant liquid of saccharicter-penin, will bring remarkable economic efficiency and social benefit as science and technology item.By annual crop rotation twice, every batch of crop only sprays 3 times at the florescence, 6 bags of annual consumptions, and the organic nutrition of plant liquid that the peasant just contains saccharicter-penin drops into 15 yuan altogether.Every mu of volume increase 10% promptly increases by 450 kilograms of output as one batch of cucumber is pressed, increases by 900 yuan of net return.Every mu of volume increase 10% of another batch autumn kidney bean promptly increases by 300 kilograms of output, increases by 600 yuan of net return.Two batches of totals increase by 1500 yuan of net return altogether, and it is 1: 100 that the peasant uses the comparative effectiveness of the organic nutrition of plant liquid input and output that contains saccharicter-penin.
In addition, use to contain during the organic nutrition of plant liquid of saccharicter-penin, can use less, without chemical pesticide.Routinely, the peasant will use chemical pesticide 1 time in per 7～10 days, spent 8 yuan at every turn.After use contains the organic nutrition of plant liquid of saccharicter-penin, can save 50 1 80 yuan of chemical pesticides.Since few with, without chemical pesticide, agricultural-food can reach pollution-free food, and even A level, AA level green food standard, actual benefit can be higher.Simultaneously, promote the use of the organic nutrition of plant liquid that contains saccharicter-penin, also will promote green agriculture, the ecological agriculture, agriculture oriented for export and foreign exchange earnings effectively.Help ensureing that domestic and international consumers in general's is healthy.
Claims (10)
1. organic nutrition of plant liquid that contains saccharicter-penin is characterized in that with every liter of described nutritive medium being that benchmark contains:
Former powder 10～100 grams of saccharicter-penin,
Bamboo vinegar liquid 200～800 grams,
Amino acid primary liquid powder 50～250 grams,
Oligosaccharide 2～20 grams,
Chemical fertilizer 70～300 grams,
Trace element fertilizer 10～35 grams,
Tensio-active agent 2～5 grams,
Water surplus.
2. a kind of organic nutrition of plant liquid that contains saccharicter-penin as claimed in claim 1, it is characterized in that described oligosaccharide be in xylo-oligosaccharide, chitosan, soybean oligosaccharide, the oligofructose one or both, three kinds mixture.
3. a kind of organic nutrition of plant liquid that contains saccharicter-penin as claimed in claim 1 is characterized in that described chemical fertilizer is urea 50～200 grams, saltpetre and/or potassium primary phosphate 20～100 grams.
4. a kind of organic nutrition of plant liquid that contains saccharicter-penin as claimed in claim 1 is characterized in that described trace element fertilizer is the mixture of one or more (containing two kinds) in boron fertilizer, zinc fertilizer, iron fertilizer, manganese fertilizer, the copper fertilizer.
5. a kind of organic nutrition of plant liquid that contains saccharicter-penin as claimed in claim 1 is characterized in that described tensio-active agent is tween 80, Sodium dodecylbenzene sulfonate or Sodium dodecylbenzene sulfonate.
6. a kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin as claimed in claim 1 is characterized in that with every liter of described nutritive medium be benchmark,
(1) 200-800 is restrained bamboo vinegar liquid and insert reactor, be warming up to 40-60 ℃, drop into the former powder 10-100 gram of saccharicter-penin, be dissolved in the bamboo vinegar liquid;
(2) in above-mentioned solution, add amino acid powder 50-250 gram, mix;
(3) above-mentioned mixed solution adds chemical fertilizer 70～300 grams under agitation condition, keeps 40-60 ℃ of temperature, fully after the dissolving, adds trace element fertilizer 10～50 grams while stirring, to fully dissolving;
(4) get a stainless steel vessel in addition,, be soaked in 50～100 milliliters 30～50 ℃ the warm water 1.5～4 hours oligosaccharide 2～20 gram;
(5) the 4th step gained solution is joined in the 3rd step solution, mix, add tensio-active agent 2～5 grams then, stirring, emulsification pretreatment 15～45 minutes add water to 1000 milliliters, stir.
7. a kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin as claimed in claim 6 is characterized in that described oligosaccharide is the mixture of one or more (containing two kinds) in xylo-oligosaccharide, chitosan, soybean oligosaccharide, the oligofructose etc.
8. a kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin as claimed in claim 6 is characterized in that described chemical fertilizer is urea 50～200 grams, saltpetre and/or potassium primary phosphate 20～100 grams.
9. a kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin as claimed in claim 6 is characterized in that described trace element fertilizer is the mixture of one or more (containing two kinds) in boron fertilizer, zinc fertilizer, iron fertilizer, manganese fertilizer, the copper fertilizer.
10. a kind of preparation method who contains the organic nutrition of plant liquid of saccharicter-penin as claimed in claim 6 is characterized in that described tensio-active agent is tween 80, Sodium dodecylbenzene sulfonate or Sodium dodecylbenzene sulfonate.
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| CN103408351A (en) * | 2013-07-09 | 2013-11-27 | 天津市星河系科技有限公司 | Polysaccharide composition and preparation method thereof |
| CN103570472A (en) * | 2013-11-10 | 2014-02-12 | 湖州艺萌城市农业发展有限公司 | Leafy vegetable culture liquor in micro agriculture |
| CN104447074A (en) * | 2014-12-30 | 2015-03-25 | 尤素梅 | Preparation method and application of green and environment-friendly and composite functional plant leaf fertilizer |
| CN104557338A (en) * | 2015-02-03 | 2015-04-29 | 舟山源丰海洋生物科技有限公司 | Fish protein fermentation liquor |
| CN110790611A (en) * | 2019-12-03 | 2020-02-14 | 杭州三得农业科技有限公司 | Manufacturing process of special organic soluble fertilizer for leguminous plants |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103408351A (en) * | 2013-07-09 | 2013-11-27 | 天津市星河系科技有限公司 | Polysaccharide composition and preparation method thereof |
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| CN104447074A (en) * | 2014-12-30 | 2015-03-25 | 尤素梅 | Preparation method and application of green and environment-friendly and composite functional plant leaf fertilizer |
| CN104557338A (en) * | 2015-02-03 | 2015-04-29 | 舟山源丰海洋生物科技有限公司 | Fish protein fermentation liquor |
| CN110790611A (en) * | 2019-12-03 | 2020-02-14 | 杭州三得农业科技有限公司 | Manufacturing process of special organic soluble fertilizer for leguminous plants |
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