CN102240340A - Method for processing prepared rehmannia root - Google Patents
Method for processing prepared rehmannia root Download PDFInfo
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- CN102240340A CN102240340A CN2011101675759A CN201110167575A CN102240340A CN 102240340 A CN102240340 A CN 102240340A CN 2011101675759 A CN2011101675759 A CN 2011101675759A CN 201110167575 A CN201110167575 A CN 201110167575A CN 102240340 A CN102240340 A CN 102240340A
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Abstract
The invention belongs to the field of traditional Chinese medicines, relating to a process for processing prepared rehmannia root which is Chinese herbal pieces for decoction. The process comprises the following steps of: soaking rehmannia root for 12 to 36 hours, and then taking out and draining; adding water 5 to 8 times more than the rehmannia root, and stewing for 6 to 24 hours; adding 0.5 to 4kg of amomum fruit and 1 to 6kg of tangerine peel into every 100kg of the stewed rehmannia root, continuing to stew for 6 hours, airing till the surfaces of the rehmannia root is slightly dry, and mixing with the remaining decoction; after the decoction is completely absorbed, drying at a temperature within a range of 60-80 DEG C till the moisture content is 12% to 20%, adding 10 to 30g of yellow rice wine into every 100kg of a dried product, moistening until the yellow rice wine is completely absorbed, steaming for 4 to 12 hours, pouring out, and airing to the room temperature; cutting the obtained rehmannia root into slices of 2 to 4mm in thickness, and drying at a temperature within the range of 60 to 80 DEG C till the moisture content is 8% to 15%, thereby obtaining the prepared rehmannia root. The prepared rehmannia root produced in the invention has the characteristics of black and bright surface, moist, soft and flexible texture, brilliantly black section, less smell and sweet taste, and is high in the contents of reducing sugars, polysaccharides and trace elements. The yield of the prepared rehmannia root is 60%-70%.
Description
Technical field
The invention belongs to the field of Chinese medicines, relate to a kind of processing procedure of prepared slices of Chinese crude drugs Radix Rehmanniae Preparata.
Background technology
Radix Rehmanniae Preparata is the large kind in prepared slices of Chinese crude drugs market, is scrophulariaceae rehmannia glutinosa plant
Rehmannia glubinosaLibosch. rhizome processes through the process of preparing Chinese medicine.Radix Rehmanniae is the name Radix Rehmanniae Preparata after steaming, and has nourishing YIN and supplementing blood, and beneficial essence is filled out the merit of marrow.Be widely used in treating the hepatic and renal YIN deficiency clinically, blurred vision tinnitus, soreness of the waist and knees is quenched one's thirst, seminal emission, metrorrhagia, early whitening of beard and hair etc.Modern pharmacological research shows that Radix Rehmanniae Preparata has diuresis, calmness, blood pressure lowering, cholesterol reducing, improves the effect of cerebral blood flow and coronary insufficiency.
Chinese crude drug is used as medicine after concocting, and is characteristics of tcm clinical practice medication, also is a big characteristic of Chinese medicine and pharmacy, and purpose is to strengthen drug effect, reduces or the elimination toxic and side effects, makes it be more suitable for the clinical application requirement.But each factor all might directly influence clinical efficacy in different concocting methods, the concocting process.Various and the disunity of concocting method of present various places Radix Rehmanniae Preparata, and different concocting methods causes the quality of processed product to differ, and directly has influence on clinical efficacy.In Jiangxi, Fujian and surrounding area commonly use the stew method for making and concoct Radix Rehmanniae, technology shows unique characteristics, product quality abnormal smells from the patient purity, nourishing power are strong, compare more with steaming method, cooking method or stewed method to have one's own knack, and enjoy a very good reputation at medicine circle.But because enterprise does not use traditional technical advantage, the processing procedure technology is still rule of thumb controlled, and can't adapt with the development of big production and modern Chinese medicine.
Therefore, stew prepared glutinous rehmannia processing procedure is furtherd investigate, thereby the industrialization and the large-scale production of the stew system of realization Radix Rehmanniae Preparata promote the fast development of local Chinese medicine industry by modern analysis means and method.This is an urgent demand of inheriting with development Chinese medicine tradition processing procedure, also is to promote the march toward necessary behave of standardization, standardization and process of industrialization of Chinese medicine processing.
Summary of the invention
The object of the present invention is to provide a kind of technology that adopts the stew method for making to concoct Radix Rehmanniae Preparata.By the preferred processing procedure parameter of orthogonal test, and realize purpose of the present invention by following step.
Concocting method of the present invention is as follows:
(1), get the Radix Rehmanniae, select stepping, place in the container, add water to and flood the Radix Rehmanniae fully, soaked 12～36 hours, taking-up, drain the water step 1 make thing;
(2), the thing that makes of step 1 is placed in the heating container, amount of water is 5～8 times of the weight that makes thing of step 1, being heated to the boiling back and adjusting firepower to little boiling, stew system 6～24 hours;
(3), add adjuvant, adjuvant is Fructus Amomi and Pericarpium Citri Reticulatae, the thing that makes of every 100kg step 1 adds Fructus Amomi 0.5～4kg and Pericarpium Citri Reticulatae 1～6kg, continue stew system more than 6 hours, and medicine juice be will use up the time, the self-heating container introversion goes out, the airing epidermis is dried slightly, will remain medicine juice and admix;
(4), treat that medicine juice exhausts after, under 60～80 ℃ temperature, be dried to water content 12%～20%, get the dry thing that makes, place in the heating container again, add yellow wine, it is 10～30kg that every 100kg drying makes thing adding yellow wine amount, mixes thoroughly, shuts pot cover, moistening to yellow wine exhausts, steam 4～12 hours again, inclining, and airing to room temperature gets the thing that makes of step 4;
(5), get the thing that makes of step 4, section is dried to water content 8%～15% at 60～80 ℃, promptly.
Be preferably:
(1), get the Radix Rehmanniae, select stepping, place in the container, add water to and flood the Radix Rehmanniae fully, soaked 20～30 hours, taking-up, drain the water step 1 make thing;
(2), the thing that makes of step 1 is placed in the heating container, amount of water is 6～7 times of the weight that makes thing of step 1, being heated to the boiling back and adjusting firepower to little boiling, stew system 12～20 hours;
(3), add adjuvant, adjuvant is Fructus Amomi and Pericarpium Citri Reticulatae, the thing that makes of every 100kg step 1 adds Fructus Amomi 1～3kg and Pericarpium Citri Reticulatae 3～5kg, continues stew system more than 6 hours, and medicine juice be will use up the time, the self-heating container introversion goes out, the airing epidermis is dried slightly, will remain medicine juice and admix;
(4), treat that medicine juice exhausts after, under 66～75 ℃ temperature, be dried to water content 14%～18%, get the dry thing that makes, place in the heating container again, add yellow wine, it is 20～25kg that every 100kg drying makes thing adding yellow wine amount, mixes thoroughly, shuts pot cover, moistening to yellow wine exhausts, steam 4～8 hours again, inclining, and airing to room temperature gets the thing that makes of step 4;
(5), get the thing that makes of step 4, be cut into 2～4mm sheet, be dried to water content 10%～14% at 65～75 ℃, promptly.
Advantage of the present invention:
(1) character.Optimize the processing procedure parameter of stew prepared glutinous rehmannia by orthogonal test, the shiny black as lacquer in Radix Rehmanniae Preparata surface of production, quality is moistened soft and is had toughness, section corvinus.Feeble QI, sweet in the mouth such as maltosemalt sugar.
(2) reducing sugar and polyoses content height.The Radix Rehmanniae Preparata reducing sugar and the polyoses content that adopt this method to produce are higher than the system of stewing and steam two kinds of methods, and significant difference has been analysed in credit by statistics.The results are shown in Table 1, table 2.
Content of reducing sugar measurement result in table 1 sample
| Sample | Sample number | Content %(￣
 |
Significance |
| Stew system Radix Rehmanniae Preparata | 28 | 33.88±2.81 | ? |
| Steam Radix Rehmanniae Preparata | 10 | 30.09±2.13** | With the group comparison of Jianchang group, P＜0.01 |
| Stewed with wine system Radix Rehmanniae Preparata | 11 | 30.83±2.63* | With the group comparison of Jianchang group, P＜0.05 |
Annotate: warp
tCheck, *
P＜0.05.
Determination of polysaccharide result in the table 2 body sample
| Sample | Sample number | Content %(
 |
Significance |
| Radix Rehmanniae | 5 | 2.69±0.18 | ? |
| Stew system Radix Rehmanniae Preparata | 28 | 3.94±0.56*** | P＜0.001 |
| Steam Radix Rehmanniae Preparata | 10 | 3.28±0.51 | With the group comparison of Jianchang group, P＜0.05 |
| Stewed with wine system Radix Rehmanniae Preparata | 11 | 2.75±0.74 | With the group comparison of Jianchang group, P＜0.01 |
Annotate: warp
tCheck, *
P＜0.05.
(3) micronutrient levels height.Two kinds of methods are made and steamed to K, Zn, Cu, Fe, Mn content apparently higher than stewing in the Radix Rehmanniae Preparata that employing this method is produced.Wherein Zn content increases by 8% than Radix Rehmanniae, increases by 25% than wine with cooking, and the power of nourishing kidney-yin, yin nourishing blood is strong; Zinc-copper ratio, manganese value be all apparently higher than the stewed with wine Radix Rehmanniae Preparata, and there are certain relation in zinc-copper ratio and enriching yin and nourishing kidney, slow down aging, and the returning through having dependency of zinc, manganese value and kidney-nourishing tcm drug.The results are shown in Table 3, table 4.
Table 3 sample Determination of trace elements result (
)
| Constituent content | Sample number (n) | K（mg/g） | Zn（mg/g） | Cu（mg/g） | Fe（mg/g） | Mn（mg/g） | Ni（mg/g） |
| Stew system Radix Rehmanniae Preparata | 8 | 4.2180±1.6944 | 0.0712±0.0066 | 0.0130±0.0038 | 0.4038±0.0590 | 0.0525±0.0152 | 0.0009±0.0002 |
| Steam Radix Rehmanniae Preparata | 6 | 2.8495±0.2821* | 0.0200±0.0014* | 0.0090±0.0057 | 0.3055±0.1351* | 0.0260±0.0071* | 0 |
| Stewed with wine system Radix Rehmanniae Preparata | 6 | 3.3653±2.2239* | 0.0370±0.0070* | 0.0063±0.0025 | 0.3680±0.1476 | 0.0427±0.0168 | 0 |
Annotate: warp
tCheck, *
P＜0.05.
Zinc/copper ratio tentatively compares in the Radix Rehmanniae Preparata of table 4 different process preparation
| Group | Sample number (n) | Content (
 |
Remarks |
| Stew system Radix Rehmanniae Preparata | 8 | 6.2924±2.0559 | ? |
| Steam Radix Rehmanniae Preparata | 6 | 2.7077±1.5448* | P＜0.05 |
| Stewed with wine system Radix Rehmanniae Preparata | 6 | 6.5185±2.6124 | ? |
Annotate: warp
tCheck, *
P＜0.05.
(4) selling point.Employing adds its property of Radix Rehmanniae Preparata of adjuvant Fructus Amomi and Pericarpium Citri Reticulatae stew system by the cold temperature of changeing, and its flavor changes sweet by hardship, the abnormal smells from the patient purity, and nourishing YIN and supplementing blood, the merit that beneficial essence is filled out marrow is strong, compares more and has one's own knack with steaming method, method.Add the purpose of yellow wine, Fructus Amomi, Pericarpium Citri Reticulatae, get the gas that its hot Wen Xiang scurries, with the spleen invigorating row stagnate, improving inspiration by invigorating kidney-QI returns kidney, and borrows the capacity for liquor row to loose, promoting blood circulation makes abnormal smells from the patient pure and solely thick, enriches blood and does not stagnate.
(5) adopt the Radix Rehmanniae Preparata of stew system explained hereafter to meet that " 2010 editions Radix Rehmanniae Preparata prepared slice quality requirements of Chinese pharmacopoeia, yield is 60%～70%.
The specific embodiment
The present invention is by the following examples can the invention will be further described, yet scope of the present invention is not limited to following embodiment.
Embodiment 1: the Radix Rehmanniae Preparata processing procedure:
The first step: get clean Radix Rehmanniae, select stepping, place in the container, add water to and flood medical material fully, soaked 24 hours, take out, drain the water.
Second step: the clean Radix Rehmanniae that will drain, to put in the digester, gradation adds the water of 6 times of medical material amounts, is heated to the boiling back and adjusts firepower to little boiling, and stew system 12 hours is admixed adjuvant Fructus Amomi 1.5 kg, Pericarpium Citri Reticulatae 4kg respectively by every 100kg medical material.Continued stew system 12 hours, and medicine juice goes out will use up the time from the digester introversion, the airing epidermis is dried slightly, will remain medicine juice and admix.
The 3rd step: after treating that medicine juice exhausts, it is about 15%～18% that 70 ℃ of medical materials are dried to the decoction pieces water content, puts in the tilting-type digester, add yellow wine 20kg by every 100kg medical material, mix thoroughly, shut pot cover, moistening to yellow wine exhausts, steam 4 hours, inclining, and airing is to room temperature, be cut into 2～4mm sheet, 75 ℃ are dried to water content 10%～14%, quality examination, packing.
Embodiment 2:
Claims (2)
1. the concocting method of a Radix Rehmanniae Preparata is characterized in that concocting method is as follows:
(1), get the Radix Rehmanniae, select stepping, place in the container, add water to and flood the Radix Rehmanniae fully, soaked 12～36 hours, taking-up, drain the water step 1 make thing;
(2), the thing that makes of step 1 is placed in the heating container, amount of water is 5～8 times of the weight that makes thing of step 1, being heated to the boiling back and adjusting firepower to little boiling, stew system 6～24 hours;
(3), add adjuvant, adjuvant is Fructus Amomi and Pericarpium Citri Reticulatae, the thing that makes of every 100kg step 1 adds Fructus Amomi 0.5～4kg and Pericarpium Citri Reticulatae 1～6kg, continue stew system more than 6 hours, and medicine juice be will use up the time, the self-heating container introversion goes out, the airing epidermis is dried slightly, will remain medicine juice and admix;
(4), treat that medicine juice exhausts after, under 60～80 ℃ temperature, be dried to water content 12%～20%, get the dry thing that makes, place in the heating container again, add yellow wine, it is 10～30kg that every 100kg drying makes thing adding yellow wine amount, mixes thoroughly, shuts pot cover, moistening to yellow wine exhausts, steam 4～12 hours again, inclining, and airing to room temperature gets the thing that makes of step 4;
(5), get the thing that makes of step 4, section is dried to water content 8%～15% at 60～80 ℃, promptly.
2. according to the concocting method of power 1 described a kind of Radix Rehmanniae Preparata, it is characterized in that concocting method is as follows:
(1), get the Radix Rehmanniae, select stepping, place in the container, add water to and flood the Radix Rehmanniae fully, soaked 20～30 hours, taking-up, drain the water step 1 make thing;
(2), the thing that makes of step 1 is placed in the heating container, amount of water is 6～7 times of the weight that makes thing of step 1, being heated to the boiling back and adjusting firepower to little boiling, stew system 12～20 hours;
(3), add adjuvant, adjuvant is Fructus Amomi and Pericarpium Citri Reticulatae, the thing that makes of every 100kg step 1 adds Fructus Amomi 1～3kg and Pericarpium Citri Reticulatae 3～5kg, continues stew system more than 6 hours, and medicine juice be will use up the time, the self-heating container introversion goes out, the airing epidermis is dried slightly, will remain medicine juice and admix;
(4), treat that medicine juice exhausts after, under 66～75 ℃ temperature, be dried to water content 14%～18%, get the dry thing that makes, place in the heating container again, add yellow wine, it is 20～25kg that every 100kg drying makes thing adding yellow wine amount, mixes thoroughly, shuts pot cover, moistening to yellow wine exhausts, steam 4～8 hours again, inclining, and airing to room temperature gets the thing that makes of step 4;
(5), get the thing that makes of step 4, be cut into 2～4mm sheet, be dried to water content 10%～14% at 65～75 ℃, promptly.
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102614304A (en) * | 2012-04-24 | 2012-08-01 | 劲牌有限公司 | Prepared rehmannia root preparation method |
| CN103316137A (en) * | 2012-03-19 | 2013-09-25 | 陕西天士力植物药业有限责任公司 | Prepared rehmannia root processing technology |
| CN103349706A (en) * | 2013-07-03 | 2013-10-16 | 亳州市豪门中药饮片有限公司 | Traditional Chinese medicine processing method for prepared rehmannia root |
| CN105983003A (en) * | 2016-01-25 | 2016-10-05 | 安徽亿源药业股份有限公司 | Processing method of Radix Rehmanniae Preparata |
| CN107375606A (en) * | 2017-08-31 | 2017-11-24 | 广州资生生物科技有限公司 | A kind of blood tonifying compound and stem cell health products of enriching blood |
| CN107412438A (en) * | 2017-08-03 | 2017-12-01 | 青海九康中药饮片有限公司 | A kind of processing method of matrimony vine herbal mixture material |
| CN108175803A (en) * | 2018-03-12 | 2018-06-19 | 汕头市粤东药业有限公司 | A kind of processing procedure of prepared rehmannia root |
| CN108968057A (en) * | 2018-08-28 | 2018-12-11 | 邓中林 | It is a kind of can it is instant bosom glutinous rehmannia production method |
| CN111602809A (en) * | 2020-04-10 | 2020-09-01 | 建昌帮药业有限公司 | Instant braised polygonatum odoratum food and preparation method thereof |
| CN111939206A (en) * | 2020-10-15 | 2020-11-17 | 河南华夏药材有限公司 | Preparation process of prepared rehmannia root traditional Chinese medicine decoction pieces |
| CN114306460A (en) * | 2021-11-23 | 2022-04-12 | 江西纳弗堂制药有限公司 | Fructus amomi steamed rehmannia decoction pieces and preparation method thereof |
| CN115671184A (en) * | 2022-11-03 | 2023-02-03 | 广东鼎铭药业有限公司 | Method for preparing nine-steamed and nine-prepared rehmannia root and processing device |
| CN117357585A (en) * | 2023-12-08 | 2024-01-09 | 南昌大学 | Processing method of traditional Chinese medicine rehmannia |
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2011
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| CN103316137A (en) * | 2012-03-19 | 2013-09-25 | 陕西天士力植物药业有限责任公司 | Prepared rehmannia root processing technology |
| CN103316137B (en) * | 2012-03-19 | 2017-06-27 | 陕西天士力植物药业有限责任公司 | A kind of prepared rhizome of rehmannia processing procedure |
| CN102614304A (en) * | 2012-04-24 | 2012-08-01 | 劲牌有限公司 | Prepared rehmannia root preparation method |
| CN103349706A (en) * | 2013-07-03 | 2013-10-16 | 亳州市豪门中药饮片有限公司 | Traditional Chinese medicine processing method for prepared rehmannia root |
| CN105983003A (en) * | 2016-01-25 | 2016-10-05 | 安徽亿源药业股份有限公司 | Processing method of Radix Rehmanniae Preparata |
| CN107412438A (en) * | 2017-08-03 | 2017-12-01 | 青海九康中药饮片有限公司 | A kind of processing method of matrimony vine herbal mixture material |
| CN107375606A (en) * | 2017-08-31 | 2017-11-24 | 广州资生生物科技有限公司 | A kind of blood tonifying compound and stem cell health products of enriching blood |
| CN108175803A (en) * | 2018-03-12 | 2018-06-19 | 汕头市粤东药业有限公司 | A kind of processing procedure of prepared rehmannia root |
| CN108968057A (en) * | 2018-08-28 | 2018-12-11 | 邓中林 | It is a kind of can it is instant bosom glutinous rehmannia production method |
| CN111602809A (en) * | 2020-04-10 | 2020-09-01 | 建昌帮药业有限公司 | Instant braised polygonatum odoratum food and preparation method thereof |
| CN111602809B (en) * | 2020-04-10 | 2023-06-09 | 建昌帮药业有限公司 | Instant braised fragrant solomonseal rhizome food and preparation method thereof |
| CN111939206A (en) * | 2020-10-15 | 2020-11-17 | 河南华夏药材有限公司 | Preparation process of prepared rehmannia root traditional Chinese medicine decoction pieces |
| CN114306460A (en) * | 2021-11-23 | 2022-04-12 | 江西纳弗堂制药有限公司 | Fructus amomi steamed rehmannia decoction pieces and preparation method thereof |
| CN115671184A (en) * | 2022-11-03 | 2023-02-03 | 广东鼎铭药业有限公司 | Method for preparing nine-steamed and nine-prepared rehmannia root and processing device |
| CN117357585A (en) * | 2023-12-08 | 2024-01-09 | 南昌大学 | Processing method of traditional Chinese medicine rehmannia |
| CN117357585B (en) * | 2023-12-08 | 2024-03-29 | 南昌大学 | Processing method of traditional Chinese medicine rehmannia |
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