CN107308218A - A kind of nine steam the processing procedure method of nine prepared fleece flower roots - Google Patents
A kind of nine steam the processing procedure method of nine prepared fleece flower roots Download PDFInfo
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Abstract
The invention discloses the processing procedure method that a kind of nine steam nine prepared fleece flower roots.The first step, selection；Second step, wash；3rd step, cutting and drying；4th step, decoction of black soybean processed；5th step, nine steam nine processes processed；6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained is fried with small fire sand；7th step, adds vegetable oil in pot, is taken the dish out of the pot after stir-frying；9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, 20 35min of stirring mixing under the conditions of 55 80 DEG C；Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, is uniformly mixed；11st step, by said mixture at 100 125 DEG C evaporation drying, obtain mixed-powder；12nd step, packaging.The processing procedure method of nine steamings, nine prepared fleece flower roots is reasonable in design, is compared by experiment, it is determined that optimal processing procedure, improves fleece-flower root medical value, greatly improve Business Economic Benefit.
Description
Technical field
The processing procedure method of nine prepared fleece flower roots is steamed the present invention relates to traditional Chinese medicine processing technique field, specifically a kind of nine.
Background technology
The fleece-flower root（Scientific name：Fallopia multiflora (Thunb.) Harald.）, also known as spend more knotweed, purple black rattan,
Polygonum multiflower knotweed etc..It is that the polygonaceae knotweed race fleece-flower root belongs to perennial winding liana, root tuber is plump, oblong, dark brown.Raw mountain valley
Shrubbery, hillside sylvan life, ditch curb gap.Produce Southern Shaanxi, SOUTH OF GANSU, East China, Central China, south China, Sichuan, Yunnan and Guizhou.Its
Root tuber is used as medicine, and can be calmed the nerves, blood-nourishing, active, removing toxic substances（Preventing malaria）, disappear carbuncle；RADIX POLYGONI MULTIFLORI PREPARATA can help essence and blood, black beard and hair, strengthening the bones and muscles, tonifying liver
Kidney, is your common detail medicinal material.
The fleece-flower root exists《Compendium of Materia Medica》It is early on the books：" fleece-flower root energy replenishing qi and blood, black beard and hair, happy color, long muscles and bones, strengthening the essence
Marrow, macrobiosis be not old ".Since the Tang Dynasty, the favor of the fleece-flower root extremely common people.It is among the people to be widely used as physical fitness, promote longevity it
Good merchantable brand.In recent years, medical scholar's achievement in research confirms that the fleece-flower root contains more lecithin both at home and abroad, and lecithin is to constitute god
Through tissue, particularly encephalomyelic main component, in addition, the fleece-flower root has the effect for reducing lipofuscin generation, and lipofuscin is
The material of spontaneous generation in human body, its content rises with the growth at the age of people, is one of important aging reason, the fleece-flower root
With the generation for reducing lipofuscin.
The fleece-flower root processes purpose：Radix Polygoni Multiflori hardship lets out mild-natured and diverging, and with removing toxic substances, disappear carbuncle, effect (the fresh head relaxed bowel
Crow removing toxic substances ease constipation effect is more preferably).For scrofula sore carbuncle, rubella itch, dry constipation of intestines；Hyperlipemia.It is sweet and thick after black soya bean system
Then enter the moon, strengthen enriching yin and nourishing kidney, nourishing liver and replenishing blood, black beard and hair, the function of strengthening the bones and muscles.For blood deficiency chlorosis, dizziness and tinnitus, beard and hair is early
In vain, under soreness and weakness of waist and knees, extremity numbness, uterine bleeding band, chronic malaria body void；Hyperlipemia.The pair of Radix Polygoni Multiflori laxation lead to diarrhea is eliminated simultaneously
Effect, makes chronic patient long-term taking without diarrhoea.
The Tang Dynasty have black soya bean steam, vinegar boil, water be cooked black soya bean wine boil (《Reason wound》) etc. concocting method, and propose " cut with bitter bamboo knife,
It is rice swill leaching one night, suddenly and violently dry, avoid iron " (《Bencao Tujing》).Song Dynasty add it is single steam, after water in which rice has been washed leaching nine steam it is nine sudden and violent (《Sheng Hui
Side》), ginger radix glycyrrhizae system (《Zhu Shi》), root of bidentate achyranthes system (《Lv Cliff rocks》) etc. method.Gold dollar have meter swill dried black bean jujube with system (《Scholar door》).
The Ming Dynasty add again black soya bean human milk system (《Rejuvenate》), black soya bean root of bidentate achyranthes human milk system (《Awake vegetarian》), human milk mix steaming, steeping in wine steam (《Scape
High mountain》).The Qing Dynasty also add black mutton system (《Good friend》), cow's milk system (《Cut use》).Now, its concocting method is planted up to more than 30.Closely
What is recorded over year in the concocted specification of various regions is that black soya bean steams method mostly, also has decoction of black soybean yellow rice wine to mix stewed method, it is believed that wine can promote blood circulation network,
Its dispelling, collateral-activating is provided, cold numbness arthralgia is controlled.It is universal due to stewing the application of the method whole nation,《Chinese Pharmacopoeia》After record fleece-flower root black soya bean
Juice is stewed or steaming method and deposited after mixing thoroughly, and wherein black soya bean is mixed steaming method and used till today always from the Tang Dynasty, and its applicating history is most long.
In the processing procedure of the fleece-flower root, although the conventional system of nine steaming nine reaches requirement in appearance luster, due to its work
Skill is complicated, and condition is various, and cost is high, and processing procedure process is based on the experience of clinical medicine work, random big, is easiest to occur
The not good situation of effect is processed, the increase of its active ingredient, the reduction of toxic component can not be optimal, and therefore, not be
A kind of processing procedure of main flow, but also just because of this fine concocting method, once condition is suitable, the fleece-flower root processed out
Drug effect is extremely effective.Therefore, the present invention is optimized in the processing procedure to nine nine prepared fleece flower roots of steaming, finds out optimal processing bar
Part, and quality verification is carried out to processing product by more specifically parameter index, obtain optimal processing procedure.
The content of the invention
It is an object of the invention to provide the processing procedure method that a kind of nine steam nine prepared fleece flower roots, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：
A kind of nine steam the processing procedure method of nine prepared fleece flower roots, comprise the following steps：
The first step, selection：Perform《Clean post standard practice instructions》, impurity is sorted out, is put in clean transfer container, is weighed；Cut
Piece, thickness is in 25-30mm；
Second step, wash：Perform《Wash post standard practice instructions》And《Medicine-washing machine standard practice instructions》, wash post operation
The fleece-flower root is put into machine by work, with meet the water washing 3 times of drinking water standard to it is clean, without silt, load clean plastics turnover
Container；
3rd step, cutting and drying；Cutting is performed《Cutting post standard practice instructions》《High speed severing reciprocating medicine cutter standard
Operational procedure》Cut sheet or cut into fourth, piece thickness 2-4mm or 8-12mm fourths by hand；Dry and perform《Dry post standard operation rule
Journey》,《Heated-air circulation oven standard practice instructions》Or《Opened type baking oven standard practice instructions》, 60-75 DEG C of design temperature, time
About 35 hours, dried moisture control was within 15.0 ﹪；
4th step, decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:（5-20）, add water appropriate, intense fire is boiled
25-40min, then the 1-3h that simmers in water, the bean dregs of filtering and filtrate, bean dregs, which are added water, to be boiled about 3 hours, filtering, merges institute twice
Filtrate is obtained, alpha-linolenic acid is added dropwise, stirring mixing 20-55min, produces decoction of black soybean under the conditions of 45-80 DEG C；Alpha-linolenic acid matter
Measure as the 1-3% of fleece-flower root quality；
5th step, nine steam nine processes processed, and nine steaming, nine processes processed include：The system of one steaming one, two steamings two are made, three steamings three are made, four steam
Four are made, five steamings five are made, six steamings six are made, seven steamings seven are made, eight steamings eight are made, the system of nine steaming nine；Obtain dry RADIX POLYGONI MULTIFLORI PREPARATA and the liquid steamed
Body；
6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained fries 8-15min with small fire sand, takes out, weeds out sand, cools down；
7th step, adds vegetable oil in pot, plant oil quality why the 15-28% of tuber of multiflower knotweed quality, vegetable oil is warming up to 105-
125 DEG C, taken the dish out of the pot in addition after step gained RADIX POLYGONI MULTIFLORI PREPARATA, the 2-8min that stir-fries, leach oil；8th step, by above-mentioned RADIX POLYGONI MULTIFLORI PREPARATA grinds
End, RADIX POLYGONI MULTIFLORI PREPARATA powder sieving 60-150 mesh；
9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, the stirring mixing 20- under the conditions of 55-80 DEG C
35min, obtains mixed liquor；Astaxanthin quality is the 0.3-1% of fleece-flower root quality；
Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 200-500r/min, and
Using ultrasonic oscillation 25-40min, mixture is obtained；
11st step, by said mixture at 100-125 DEG C evaporation drying, obtain mixed-powder；
12nd step, packaging：With packaging directive packaging, perform《Pack post standard practice instructions》, it is desirable to it is accurate to weigh, sealing
Tightly, no folder medicine, leakage medicine phenomenon, often pack and post the quality certification, quality certification content complete display.
It is used as further scheme of the invention：4th step, decoction of black soybean processed：Take black soya bean, black soya bean quality and fleece-flower root matter
Amount is than being 1:15, add water appropriate, intense fire boils 30min, then the 1.5h that simmers in water, the bean dregs of filtering and filtrate, and bean dregs, which are added water, to be boiled
About 3 hours, filtering merged gained filtrate twice, alpha-linolenic acid is added dropwise, and stirring mixing 40min, is produced under the conditions of 65 DEG C
Decoction of black soybean.
It is used as further scheme of the invention：The alpha-linolenic acid quality is the 2.8% of fleece-flower root quality.
It is used as further scheme of the invention：Nine steaming, nine processes processed are specifically included：First, mix：By what head cleaned
Crow mixes infiltration to the fleece-flower root thoroughly with decoction of black soybean and run through, and infiltrates 2-5 hours, juice is fully absorbed, and half an hour is stirred once, obtains
Middle product, middle product are put into tilting-type digester or uniformly inserted in food steamer；2nd, steam：Perform《Steam post standard behaviour
Make code》And《Digester standard practice instructions》Or《Food steamer standard practice instructions》, it is passed through the steam that pressure is 0.5-0.8Mpa
About 8 hours, pressure is preferably pressed into for 0.6Mpa, and steaming temperature scope is 155-170 DEG C, preferably 160 DEG C, is steamed to inside and outside in taste
Moisten black, pour out liquid and RADIX POLYGONI MULTIFLORI PREPARATA that the inside is steamed；Then RADIX POLYGONI MULTIFLORI PREPARATA is dried：Temperature is 60-75 DEG C, is dried about 25 hours
It is dry or spread out and shone naturally near dry in threshing ground to eighty per cant；Continuously steam nine times；RADIX POLYGONI MULTIFLORI PREPARATA is obtained in the liquid steamed after steaming for 9th time
12-24h is soaked in body, then pulls RADIX POLYGONI MULTIFLORI PREPARATA out drying, liquid is standby.
It is used as further scheme of the invention：7th step, adds vegetable oil in pot, plant oil quality why the tuber of multiflower knotweed
The 22% of quality, vegetable oil is warming up to 115 DEG C, is taken the dish out of the pot in addition after step gained RADIX POLYGONI MULTIFLORI PREPARATA, the 5min that stir-fries, leaches oil.
It is used as further scheme of the invention：The vegetable oil is safflower seed oil, grape-kernel oil or brave macadamia nut oil.
It is used as further scheme of the invention：The astaxanthin quality is the 0.5% of fleece-flower root quality.
It is used as further scheme of the invention：Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirred
Mixing, mixing speed 300r/min are mixed, and uses ultrasonic oscillation 35min, mixture is obtained.
A kind of fleece-flower root processed using the nine processing procedure concocting methods for steaming nine prepared fleece flower roots.
Compared with prior art, the beneficial effects of the invention are as follows：
The processing procedure method of nine steamings, nine prepared fleece flower roots is reasonable in design, is compared by experiment, it is determined that optimal processing
Technique, is of great significance for the optimal concocting method tool for setting up the fleece-flower root；Performance for its main body drug effect is established
Basis；Fleece-flower root medical value is improved, fleece-flower root resource is preferably rationally utilized, enables it to play bigger curative effect, greatly
Improve Business Economic Benefit.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Embodiment 1
A kind of nine steam the processing procedure method of nine prepared fleece flower roots, specifically include following steps：
The first step, selection：Perform《Clean post standard practice instructions》, impurity is sorted out, is put in clean transfer container, is weighed；Cut
Piece, thickness is in 25-30mm；
Second step, wash：Perform《Wash post standard practice instructions》And《Medicine-washing machine standard practice instructions》, wash post operation
The fleece-flower root is put into machine by work, with meet the water washing 3 times of drinking water standard to it is clean, without silt, load clean plastics turnover
Container；
3rd step, cutting and drying；Cutting is performed《Cutting post standard practice instructions》《High speed severing reciprocating medicine cutter standard
Operational procedure》Cut sheet, piece thickness 2-4mm；Dry and perform《Dry post standard practice instructions》,《Heated-air circulation oven standard is grasped
Make code》Or《Opened type baking oven standard practice instructions》, 60 DEG C of design temperature, about 35 hours time, dried moisture control
Within 15.0 ﹪；
4th step, decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:5, add water appropriate, intense fire boils 25min,
Simmered in water 1h again, the bean dregs of filtering and filtrate, and bean dregs, which are added water, to be boiled about 3 hours, filtering, merges gained filtrate twice, dropwise
Alpha-linolenic acid is added, stirring mixing 20min, produces decoction of black soybean under the conditions of 45 DEG C；Alpha-linolenic acid quality is fleece-flower root quality
1%；
5th step, nine steam nine processes processed, and nine steaming, nine processes processed include：The system of one steaming one, two steamings two are made, three steamings three are made, four steam
Four are made, five steamings five are made, six steamings six are made, seven steamings seven are made, eight steamings eight are made, the system of nine steaming nine；Obtain dry RADIX POLYGONI MULTIFLORI PREPARATA and the liquid steamed
Body；Nine steaming, nine processes processed are specifically included：First, mix：The clean fleece-flower root and decoction of black soybean is mixed thoroughly infiltration to the fleece-flower root to moisten
Thoroughly, infiltrate 2 hours, juice is fully absorbed, and half an hour is stirred once, obtains middle product, middle product are put into tilting-type boiling
In pot or uniformly insert in food steamer；2nd, steam：Perform《Steam post standard practice instructions》And《Digester standard practice instructions》
Or《Food steamer standard practice instructions》, the steam about 8 hours that pressure is 0.5Mpa is passed through, steaming temperature scope is 155 DEG C, is steamed to interior
Outer is in moisten black, pours out liquid and RADIX POLYGONI MULTIFLORI PREPARATA that the inside is steamed；Then RADIX POLYGONI MULTIFLORI PREPARATA is dried：Temperature is 60 DEG C, dries about 25
Hour to eighty per cant it is dry or spread out in threshing ground shines naturally to closely do；Continuously steam nine times；RADIX POLYGONI MULTIFLORI PREPARATA is obtained after steaming for 9th time steaming
Liquid in soak 12h, then pull RADIX POLYGONI MULTIFLORI PREPARATA out drying, liquid is standby；
6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained fries 8min with small fire sand, takes out, weeds out sand, cools down；
7th step, adds vegetable oil in pot, plant oil quality why the 15% of tuber of multiflower knotweed quality, vegetable oil is warming up to 105 DEG C, plus
Taken the dish out of the pot after entering RADIX POLYGONI MULTIFLORI PREPARATA obtained by upper step, the 2min that stir-fries, leach oil；The vegetable oil is that safflower seed oil, grape-kernel oil or tiger are hard
Fruit oil；
8th step, above-mentioned RADIX POLYGONI MULTIFLORI PREPARATA is clayed into power, RADIX POLYGONI MULTIFLORI PREPARATA powder 60 mesh of sieving；
9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, and stirring mixing 20min, is obtained under the conditions of 55 DEG C
Mixed liquor；Astaxanthin quality is the 0.3% of fleece-flower root quality；
Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 200r/min, and use
Ultrasonic oscillation 25min, obtains mixture；
11st step, by said mixture at 100 DEG C evaporation drying, obtain mixed-powder；
12nd step, packaging：With packaging directive packaging, perform《Pack post standard practice instructions》, it is desirable to it is accurate to weigh, sealing
Tightly, no folder medicine, leakage medicine phenomenon, often pack and post the quality certification, quality certification content complete display.
Embodiment 2
A kind of nine steam the processing procedure method of nine prepared fleece flower roots, specifically include following steps：
The first step, selection：Perform《Clean post standard practice instructions》, impurity is sorted out, is put in clean transfer container, is weighed；Cut
Piece, thickness is in 25-30mm；
Second step, wash：Perform《Wash post standard practice instructions》And《Medicine-washing machine standard practice instructions》, wash post operation
The fleece-flower root is put into machine by work, with meet the water washing 3 times of drinking water standard to it is clean, without silt, load clean plastics turnover
Container；
3rd step, cutting and drying；Cutting is performed《Cutting post standard practice instructions》《High speed severing reciprocating medicine cutter standard
Operational procedure》Cut into 8-12mm fourths by hand；Dry and perform《Dry post standard practice instructions》,《Heated-air circulation oven standard
Operational procedure》Or《Opened type baking oven standard practice instructions》, 75 DEG C of design temperature, about 35 hours time, dried moisture control
System is within 15.0 ﹪；
4th step, decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:20, add water appropriate, intense fire boils 40min,
Simmered in water 3h again, the bean dregs of filtering and filtrate, and bean dregs, which are added water, to be boiled about 3 hours, filtering, merges gained filtrate twice, dropwise
Alpha-linolenic acid is added, stirring mixing 55min, produces decoction of black soybean under the conditions of 80 DEG C；Alpha-linolenic acid quality is fleece-flower root quality
3%；
5th step, nine steam nine processes processed, and nine steaming, nine processes processed include：The system of one steaming one, two steamings two are made, three steamings three are made, four steam
Four are made, five steamings five are made, six steamings six are made, seven steamings seven are made, eight steamings eight are made, the system of nine steaming nine；Obtain dry RADIX POLYGONI MULTIFLORI PREPARATA and the liquid steamed
Body；Nine steaming, nine processes processed are specifically included：First, mix：The clean fleece-flower root and decoction of black soybean is mixed thoroughly infiltration to the fleece-flower root to moisten
Thoroughly, infiltrate 5 hours, juice is fully absorbed, and half an hour is stirred once, obtains middle product, middle product are put into tilting-type boiling
In pot or uniformly insert in food steamer；2nd, steam：Perform《Steam post standard practice instructions》And《Digester standard practice instructions》
Or《Food steamer standard practice instructions》, the steam about 8 hours that pressure is 0.8Mpa is passed through, steaming temperature scope is 70 DEG C, is steamed to interior
Outer is in moisten black, pours out liquid and RADIX POLYGONI MULTIFLORI PREPARATA that the inside is steamed；Then RADIX POLYGONI MULTIFLORI PREPARATA is dried：Temperature is 75 DEG C, dries about 25
Hour to eighty per cant it is dry or spread out in threshing ground shines naturally to closely do；Continuously steam nine times；RADIX POLYGONI MULTIFLORI PREPARATA is obtained after steaming for 9th time steaming
Liquid in soak 24h, then pull RADIX POLYGONI MULTIFLORI PREPARATA out drying, liquid is standby；
6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained fries 15min with small fire sand, takes out, weeds out sand, cools down；
7th step, adds vegetable oil in pot, plant oil quality why the 28% of tuber of multiflower knotweed quality, vegetable oil is warming up to 125 DEG C, plus
Taken the dish out of the pot after entering RADIX POLYGONI MULTIFLORI PREPARATA obtained by upper step, the 8min that stir-fries, leach oil；The vegetable oil is that safflower seed oil, grape-kernel oil or tiger are hard
Fruit oil；
8th step, above-mentioned RADIX POLYGONI MULTIFLORI PREPARATA is clayed into power, RADIX POLYGONI MULTIFLORI PREPARATA powder 150 mesh of sieving；
9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, and stirring mixing 35min, is obtained under the conditions of 80 DEG C
Mixed liquor；Astaxanthin quality is the 1% of fleece-flower root quality；
Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 500r/min, and use
Ultrasonic oscillation 40min, obtains mixture；
11st step, by said mixture at 125 DEG C evaporation drying, obtain mixed-powder；
12nd step, packaging：With packaging directive packaging, perform《Pack post standard practice instructions》, it is desirable to it is accurate to weigh, sealing
Tightly, no folder medicine, leakage medicine phenomenon, often pack and post the quality certification, quality certification content complete display.
Embodiment 3
A kind of nine steam the processing procedure method of nine prepared fleece flower roots, specifically include following steps：
The first step, selection：Perform《Clean post standard practice instructions》, impurity is sorted out, is put in clean transfer container, is weighed；Cut
Piece, thickness is in 25-30mm；
Second step, wash：Perform《Wash post standard practice instructions》And《Medicine-washing machine standard practice instructions》, wash post operation
The fleece-flower root is put into machine by work, with meet the water washing 3 times of drinking water standard to it is clean, without silt, load clean plastics turnover
Container；
3rd step, cutting and drying；Cutting is performed《Cutting post standard practice instructions》《High speed severing reciprocating medicine cutter standard
Operational procedure》Cut sheet, piece thickness 2-4mm；Dry and perform《Dry post standard practice instructions》,《Heated-air circulation oven standard is grasped
Make code》Or《Opened type baking oven standard practice instructions》, 70 DEG C of design temperature, about 35 hours time, dried moisture control
Within 15.0 ﹪；
4th step, decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:15, add water appropriate, intense fire boils 30min,
Simmered in water 1.5h again, the bean dregs of filtering and filtrate, and bean dregs, which are added water, to be boiled about 3 hours, filtering, merges gained filtrate twice, by
Alpha-linolenic acid is added dropwise to, stirring mixing 40min, produces decoction of black soybean under the conditions of 65 DEG C；Alpha-linolenic acid quality is fleece-flower root quality
2.8%；
5th step, nine steam nine processes processed, and nine steaming, nine processes processed include：The system of one steaming one, two steamings two are made, three steamings three are made, four steam
Four are made, five steamings five are made, six steamings six are made, seven steamings seven are made, eight steamings eight are made, the system of nine steaming nine；Obtain dry RADIX POLYGONI MULTIFLORI PREPARATA and the liquid steamed
Body；Nine steaming, nine processes processed are specifically included：First, mix：The clean fleece-flower root and decoction of black soybean is mixed thoroughly infiltration to the fleece-flower root to moisten
Thoroughly, infiltrate 3 hours, juice is fully absorbed, and half an hour is stirred once, obtains middle product, middle product are put into tilting-type boiling
In pot or uniformly insert in food steamer；2nd, steam：Perform《Steam post standard practice instructions》And《Digester standard practice instructions》
Or《Food steamer standard practice instructions》, the steam about 8 hours that pressure is 0.6Mpa is passed through, steaming temperature scope is 160 DEG C, is steamed to interior
Outer is in moisten black, pours out liquid and RADIX POLYGONI MULTIFLORI PREPARATA that the inside is steamed；Then RADIX POLYGONI MULTIFLORI PREPARATA is dried：Temperature is 70 DEG C, dries about 25
Hour to eighty per cant it is dry or spread out in threshing ground shines naturally to closely do；Continuously steam nine times；RADIX POLYGONI MULTIFLORI PREPARATA is obtained after steaming for 9th time steaming
Liquid in soak 18h, then pull RADIX POLYGONI MULTIFLORI PREPARATA out drying, liquid is standby；
6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained fries 13min with small fire sand, takes out, weeds out sand, cools down；
7th step, adds vegetable oil in pot, plant oil quality why the 22% of tuber of multiflower knotweed quality, vegetable oil is warming up to 115 DEG C, plus
Taken the dish out of the pot after entering RADIX POLYGONI MULTIFLORI PREPARATA obtained by upper step, the 5min that stir-fries, leach oil；The vegetable oil is that safflower seed oil, grape-kernel oil or tiger are hard
Fruit oil；
8th step, above-mentioned RADIX POLYGONI MULTIFLORI PREPARATA is clayed into power, RADIX POLYGONI MULTIFLORI PREPARATA powder 110 mesh of sieving；
9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, and stirring mixing 30min, is obtained under the conditions of 75 DEG C
Mixed liquor；Astaxanthin quality is the 0.5% of fleece-flower root quality；
Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 300r/min, and use
Ultrasonic oscillation 35min, obtains mixture；
11st step, by said mixture at 118 DEG C evaporation drying, obtain mixed-powder；
12nd step, packaging：With packaging directive packaging, perform《Pack post standard practice instructions》, it is desirable to it is accurate to weigh, sealing
Tightly, no folder medicine, leakage medicine phenomenon, often pack and post the quality certification, quality certification content complete display.
Comparative example 1
Identical with the preparation method of embodiment 3, difference is not add alpha-linolenic acid during the 4th step decoction of black soybean.
Comparative example 2
Identical with the preparation method of embodiment 3, difference is that the 7th step vegetable oil is warming up to step gained RADIX POLYGONI MULTIFLORI PREPARATA in 90 DEG C, addition and entered
Row stir-fries.
Comparative example 3
Identical with the preparation method of embodiment 3, difference is that the 7th step vegetable oil is warming up to step gained RADIX POLYGONI MULTIFLORI PREPARATA in 140 DEG C, addition
Stir-fried.
Comparative example 4
Identical with the preparation method of embodiment 3, difference is not carry out the operation of the 7th step, and RADIX POLYGONI MULTIFLORI PREPARATA stir-fried without vegetable oil is added
Journey.
Comparative example 5
Identical with the preparation method of embodiment 3, difference is not carry out the operation of the 9th step, i.e., do not add in the liquid that the 5th step is steamed
Enter astaxanthin.
Experimental example 1
Nine steam nine prepared fleece flower roots and the comparison of commercially available fleece-flower root active ingredient
Medicinal material：Embodiment 3 is processed in the present invention nine steam nine prepared fleece flower roots.
Commercially available Radix Polygoni Multiflori, one prepared fleece flower root of a commercially available steaming, nine prepared fleece flower roots of commercially available nine steaming are purchased from the market, purchased from conjunction
Fertile large-scale pharmacy of city, every kind of medicinal material purchases 3 batches, and all medicinal materials, through Anguo City Chinese medicine row expert appraisal, are certified products.
Detection method：Using Chinese invention patent：A kind of detection method of Radix Polygoni Multiflori and prepared fleece flower root, application number：
200910059024.3.Experimental result is shown in Table 1.
Table 1 nine steams nine prepared fleece flower roots and commercially available fleece-flower root active ingredient comparative result
| Medicinal material title | THSG (percentage by weight %) | Rheum emodin (percentage by weight %) |
| Radix Polygoni Multiflori（It is commercially available） | 5.321±0.021 | 0.089±0.018 |
| Nine steam nine prepared fleece flower roots（It is commercially available） | 3.810±0.041 | 0.115±0.038 |
| One steams a prepared fleece flower root（It is commercially available） | 3.645±0.051 | 0.102±0.015 |
| Nine steam nine prepared fleece flower roots | 4.524±0.037 | 0.158±0.048 |
Judging index component content criterion of acceptability：It is required that 2,3 in Radix Polygoni Multiflori medicinal material to be measured, 4 ', 5- tetrahydroxystilbenes-
2-O- β-D- glucopyranosides（THSG）Percentage composition >=3.00% and rheum emodin percentage composition >=0.050%, then sentence
Fixed Radix Polygoni Multiflori medicinal material to be measured is qualified, otherwise unqualified.It is required that 2,3 in prepared fleece flower root medicinal material to be measured, 4 ', 5- tetrahydroxys two
Percentage composition >=1.93% of styrene -2-O- β-D- glucopyranosides, and percentage composition >=0.067% of rheum emodin.By
Upper table is visible, and nine nine prepared fleece flower root medicinal materials of steaming of the invention are qualified products.
Experimental example 2
Nine steam the comparison of the different preparation condition active ingredients of nine prepared fleece flower roots
What head nine nine prepared fleece flower roots of steaming that the Chinese medicine preparation method of the embodiment of the present invention 1 is processed, nine steamings nine that comparative example 1 is processed make
Crow, nine nine prepared fleece flower roots of steaming that comparative example 2 is processed, nine nine prepared fleece flower roots of steaming that comparative example 3 is processed.
Detection method：Using Chinese invention patent：A kind of detection method of Radix Polygoni Multiflori and prepared fleece flower root, application number：
200910059024.3.Experimental result is shown in Table 2.Every kind of sample is repeated three times, and experimental result takes three average values.
Table 2 nine steams the comparative result of the different preparation condition active ingredients of nine prepared fleece flower roots
| Medicinal material title | THSG (percentage by weight %) | Rheum emodin (percentage by weight %) |
| Embodiment 3 | 4.524 | 0.158 |
| Comparative example 1 | 3.257 | 0.115 |
| Comparative example 2 | 3.184 | 0.121 |
| Comparative example 3 | 1.081 | 0.065 |
| Comparative example 4 | 3.378 | 0.098 |
| Comparative example 5 | 3.415 | 0.113 |
The different preparation condition character pair ratios of nine nine prepared fleece flower roots of steaming the results are shown in Table 3：
Table 3 nine steams the different preparation condition character pair ratios of nine prepared fleece flower roots
| Sample | Color | Smell |
| Embodiment 3 | Pitch-black, gloss | It is fragrant |
| Comparative example 1 | Pitch-black, gloss | Light perfume (or spice) |
| Comparative example 2 | Black, tarnish | Light perfume (or spice) |
| Comparative example 3 | It is pitch-black, be charred | It is charred |
| Comparative example 4 | Pitch-black, gloss | Light perfume (or spice) |
| Comparative example 5 | Pitch-black, gloss | It is fragrant |
It can be drawn by the data of table 2 and table 3, if the 7th step stir-fries, not enough, the conversion of its THSG and rheum emodin is not enough for temperature；
If the 7th step stir-fries, temperature is too high, and its active ingredient declines rapidly, and possible active ingredient is destroyed rapidly by high temperature, if occurring burnt
Paste, secondary medicine will be destroyed by the gross, otherwise not only without drug effect, or even have harmful components generation.It can also be seen that by add α-
Leukotrienes and astaxanthin can effectively improve the conversion ratio of THSG and rheum emodin.
Nine steaming nine prepared fleece flower roots, three effective substances prepared by embodiment 3 the results are shown in Table 4：
Nine steaming nine prepared fleece flower roots, three effective substance results prepared by the embodiment 3 of table 4
| Kind | THSG (percentage by weight %) | Rheum emodin (percentage by weight %) |
| The batch of 3 fleece-flower root of embodiment one | 4.519±0.032 | 0.157±0.015 |
| The batch of 3 fleece-flower root of embodiment two | 4.528±0.018 | 0.159±0.025 |
| The batch of 3 fleece-flower root of embodiment three | 4.525±0.026 | 0.158±0.036 |
All data are with sample of the same race, and three batch the data obtained averages are defined.
Drawn by the data of table 4, the THSG and emodin content prepared by the optimal preparation technology of three batches are stable, have
Repeatability, illustrates that experiment condition is objective.
The processing procedure method of nine steamings, nine prepared fleece flower roots is reasonable in design, is compared by experiment, it is determined that optimal
Processing procedure, is of great significance for the optimal concocting method tool for setting up the fleece-flower root；Performance for its main body drug effect is established
Set basis；Fleece-flower root medical value is improved, fleece-flower root resource is preferably rationally utilized, enables it to play bigger curative effect, greatly
The earth improves Business Economic Benefit.
, it is necessary to illustrate, unless otherwise clear and definite in the description of this nine processing procedure method for steaming nine prepared fleece flower roots
Regulation and limit, term " setting ", " connected " and " connection " should be interpreted broadly, for example, it may be fixedly connected or
It is detachably connected, or is integrally connected；Can be joined directly together, can also be indirectly connected to by intermediary, can be two
The connection of element internal.For the ordinary skill in the art, with concrete condition above-mentioned term can be understood in the present invention
In concrete meaning.
The better embodiment to this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
, can also be on the premise of this patent objective not be departed from formula, the knowledge that one skilled in the relevant art possesses
Make a variety of changes.
Claims (9)
1. a kind of nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that comprise the following steps：
The first step, selection：Perform《Clean post standard practice instructions》, impurity is sorted out, is put in clean transfer container, is weighed；Cut
Piece, thickness is in 25-30mm；
Second step, wash：Perform《Wash post standard practice instructions》And《Medicine-washing machine standard practice instructions》, wash post operation
The fleece-flower root is put into machine by work, with meet the water washing 3 times of drinking water standard to it is clean, without silt, load clean plastics turnover
Container；
3rd step, cutting and drying；Cutting is performed《Cutting post standard practice instructions》《High speed severing reciprocating medicine cutter standard
Operational procedure》Cut sheet or cut into fourth, piece thickness 2-4mm or 8-12mm fourths by hand；Dry and perform《Dry post standard operation rule
Journey》,《Heated-air circulation oven standard practice instructions》Or《Opened type baking oven standard practice instructions》, 60-75 DEG C of design temperature, time
About 35 hours, dried moisture control was within 15.0 ﹪；
4th step, decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:（5-20）, add water appropriate, intense fire is boiled
25-40min, then the 1-3h that simmers in water, the bean dregs of filtering and filtrate, bean dregs, which are added water, to be boiled about 3 hours, filtering, merges institute twice
Filtrate is obtained, alpha-linolenic acid is added dropwise, stirring mixing 20-55min, produces decoction of black soybean under the conditions of 45-80 DEG C；Alpha-linolenic acid matter
Measure as the 1-3% of fleece-flower root quality；
5th step, nine steam nine processes processed, and nine steaming, nine processes processed include：The system of one steaming one, two steamings two are made, three steamings three are made, four steam
Four are made, five steamings five are made, six steamings six are made, seven steamings seven are made, eight steamings eight are made, the system of nine steaming nine；Obtain dry RADIX POLYGONI MULTIFLORI PREPARATA and the liquid steamed
Body；
6th step, the RADIX POLYGONI MULTIFLORI PREPARATA that upper step is obtained fries 8-15min with small fire sand, takes out, weeds out sand, cools down；
7th step, adds vegetable oil in pot, plant oil quality why the 15-28% of tuber of multiflower knotweed quality, vegetable oil is warming up to 105-
125 DEG C, taken the dish out of the pot in addition after step gained RADIX POLYGONI MULTIFLORI PREPARATA, the 2-8min that stir-fries, leach oil；8th step, by above-mentioned RADIX POLYGONI MULTIFLORI PREPARATA grinds
End, RADIX POLYGONI MULTIFLORI PREPARATA powder sieving 60-150 mesh；
9th step, astaxanthin is added dropwise in the liquid that the 5th step is steamed, the stirring mixing 20- under the conditions of 55-80 DEG C
35min, obtains mixed liquor；Astaxanthin quality is the 0.3-1% of fleece-flower root quality；
Tenth step, RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 200-500r/min, and
Using ultrasonic oscillation 25-40min, mixture is obtained；
11st step, by said mixture at 100-125 DEG C evaporation drying, obtain mixed-powder；
12nd step, packaging：With packaging directive packaging, perform《Pack post standard practice instructions》, it is desirable to it is accurate to weigh, sealing
Tightly, no folder medicine, leakage medicine phenomenon, often pack and post the quality certification, quality certification content complete display.
2. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the 4th step,
Decoction of black soybean processed：Black soya bean is taken, black soya bean quality is 1 with fleece-flower root mass ratio:15, add water appropriate, intense fire boils 30min, then simmers in water
1.5h, the bean dregs of filtering and filtrate, bean dregs, which are added water, to be boiled about 3 hours, filtering, merges gained filtrate twice, α-Asia is added dropwise
Numb acid, stirring mixing 40min, produces decoction of black soybean under the conditions of 65 DEG C.
3. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the alpha-linolenic acid
Quality is the 2.8% of fleece-flower root quality.
4. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that described nine, which steam nine, makes
Process is specifically included：First, mix：Mix the clean fleece-flower root and decoction of black soybean thoroughly infiltration to the fleece-flower root to run through, infiltrate 2-5 hours,
Juice is fully absorbed, and half an hour is stirred once, obtains middle product, and middle product are put into tilting-type digester or uniformly inserted
In food steamer；2nd, steam：Perform《Steam post standard practice instructions》And《Digester standard practice instructions》Or《Food steamer standard is grasped
Make code》, the steam about 8 hours that pressure is 0.5-0.8Mpa is passed through, pressure is preferably pressed into for 0.6Mpa, steaming temperature scope is
155-170 DEG C, preferably 160 DEG C, steam to inside and outside in black is moistened, pour out liquid and RADIX POLYGONI MULTIFLORI PREPARATA that the inside is steamed；Then will system
The tuber of multiflower knotweed is dried：Temperature be 60-75 DEG C, dry about 25 hours to eighty per cant it is dry or spread out in threshing ground shines naturally to closely do；Continuously steam nine
It is secondary；RADIX POLYGONI MULTIFLORI PREPARATA being obtained after steaming for 9th time 12-24h being soaked in the liquid steamed, then pull RADIX POLYGONI MULTIFLORI PREPARATA out drying, liquid is standby
With.
5. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the 7th step,
Add vegetable oil in pot, plant oil quality why the 22% of tuber of multiflower knotweed quality, vegetable oil is warming up to 115 DEG C, and step gained is made in addition
Taken the dish out of the pot after the tuber of multiflower knotweed, the 5min that stir-fries, leach oil.
6. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the vegetable oil is
Safflower seed oil, grape-kernel oil or brave macadamia nut oil.
7. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the astaxanthin matter
Measure as the 0.5% of fleece-flower root quality.
8. according to claim 1 nine steam the processing procedure method of nine prepared fleece flower roots, it is characterised in that the tenth step,
RADIX POLYGONI MULTIFLORI PREPARATA powder is added in step gained mixed liquor, stirring mixing, mixing speed 300r/min, and use ultrasonic oscillation
35min, obtains mixture.
9. the fleece-flower root processed using concocting method described in claim 1-8.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108542967A (en) * | 2018-04-26 | 2018-09-18 | 安徽亿源药业股份有限公司 | A kind of concocting method of Radix picrorrhizae medicine materical crude slice |
| CN109045118A (en) * | 2018-11-07 | 2018-12-21 | 陕西广济堂医药集团股份有限公司 | A kind of production method of prepared fleece flower root purification medicine materical crude slice |
| CN109999084A (en) * | 2019-04-19 | 2019-07-12 | 河南省青山药业股份有限公司 | A kind of preparation method of the fleece-flower root |
-
2017
- 2017-06-01 CN CN201710403884.9A patent/CN107308218A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108542967A (en) * | 2018-04-26 | 2018-09-18 | 安徽亿源药业股份有限公司 | A kind of concocting method of Radix picrorrhizae medicine materical crude slice |
| CN109045118A (en) * | 2018-11-07 | 2018-12-21 | 陕西广济堂医药集团股份有限公司 | A kind of production method of prepared fleece flower root purification medicine materical crude slice |
| CN109999084A (en) * | 2019-04-19 | 2019-07-12 | 河南省青山药业股份有限公司 | A kind of preparation method of the fleece-flower root |
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