CN102227392B - 使用酸洗涤系统的尿素成粒过程和氨盐到尿素颗粒中的相应集成 - Google Patents
使用酸洗涤系统的尿素成粒过程和氨盐到尿素颗粒中的相应集成 Download PDFInfo
- Publication number
- CN102227392B CN102227392B CN200980147420.XA CN200980147420A CN102227392B CN 102227392 B CN102227392 B CN 102227392B CN 200980147420 A CN200980147420 A CN 200980147420A CN 102227392 B CN102227392 B CN 102227392B
- Authority
- CN
- China
- Prior art keywords
- granulator
- urea
- washer
- ammonia
- stage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
- C05C9/005—Post-treatment
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
- C05C3/005—Post-treatment
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
- Treating Waste Gases (AREA)
- Gas Separation By Absorption (AREA)
- Separation Of Particles Using Liquids (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP08020708.7 | 2008-11-28 | ||
| EP08020708A EP2192099A1 (en) | 2008-11-28 | 2008-11-28 | Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules |
| PCT/EP2009/007953 WO2010060535A1 (en) | 2008-11-28 | 2009-11-06 | Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102227392A CN102227392A (zh) | 2011-10-26 |
| CN102227392B true CN102227392B (zh) | 2014-04-09 |
Family
ID=40521831
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200980147420.XA Active CN102227392B (zh) | 2008-11-28 | 2009-11-06 | 使用酸洗涤系统的尿素成粒过程和氨盐到尿素颗粒中的相应集成 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8466315B2 (enExample) |
| EP (2) | EP2192099A1 (enExample) |
| JP (1) | JP5723782B2 (enExample) |
| CN (1) | CN102227392B (enExample) |
| AR (1) | AR075554A1 (enExample) |
| BR (1) | BRPI0921863B1 (enExample) |
| CA (1) | CA2743488C (enExample) |
| PE (1) | PE20120243A1 (enExample) |
| RU (1) | RU2485077C2 (enExample) |
| WO (1) | WO2010060535A1 (enExample) |
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2192099A1 (en) * | 2008-11-28 | 2010-06-02 | Uhde Fertilizer Technology B.V. | Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules |
| EP2301917A1 (en) | 2009-09-16 | 2011-03-30 | Stamicarbon B.V. | Removal of urea and ammonia from exhaust gases |
| DE102011016759A1 (de) | 2011-04-12 | 2012-10-18 | Thyssenkrupp Uhde Gmbh | Verfahren zur Herstellung von NH3 |
| WO2013165245A1 (en) | 2012-05-03 | 2013-11-07 | Stamicarbon B.V. | Urea production plant |
| EP2662349A1 (en) | 2012-05-08 | 2013-11-13 | Uhde Fertilizer Technology B.V. | Urea granulation process with scrubbing system |
| NL2009295C2 (en) * | 2012-08-08 | 2014-02-11 | Green Granulation Technology Ltd | Method for manufacturing granules from a liquid. |
| EP2746244A1 (en) * | 2012-12-21 | 2014-06-25 | Uhde Fertilizer Technology B.V. | Method for reducing the visible downwind detached plume opacity |
| ITMI20130847A1 (it) * | 2013-05-24 | 2014-11-25 | Saipem Spa | Metodo e sistema per il recupero di solfato di ammonio da un flusso gassoso di un impianto urea |
| BR112016000017B1 (pt) * | 2013-07-05 | 2020-02-18 | Stamicarbon B.V. | Método para a remoção de poeira de ureia do efluente gasoso, equipamento de acabamento para uma planta de ureia e planta de ureia |
| US9394210B2 (en) | 2013-08-23 | 2016-07-19 | Koch Agronomic Services, Llc | Urea and nitrogen stabilizer compositions and methods and systems of making and using thereof |
| CN103432847B (zh) * | 2013-09-10 | 2016-08-03 | 安徽淮化股份有限公司 | 一种处理硝酸铵造粒塔尾气的方法及装置 |
| CN110013717B (zh) | 2013-11-15 | 2022-03-22 | 斯塔米卡邦有限公司 | 用于从气体流捕集颗粒的设备和方法以及从气体中去除可溶颗粒的方法 |
| US9586169B2 (en) | 2014-02-05 | 2017-03-07 | Green Granulation Technology Limited | Method for manufacturing granules from a liquid |
| DE102014108703A1 (de) | 2014-06-20 | 2015-12-24 | Thyssenkrupp Ag | Harnstoffzusammensetzung und Verfahren zu ihrer Herstellung |
| EP3020702A1 (en) | 2014-11-12 | 2016-05-18 | Casale SA | Urea finishing process with acid scrubbing |
| EA033176B1 (ru) * | 2014-11-27 | 2019-09-30 | Стамикарбон Б.В. | Способ и установка для производства карбамидоаммониевого нитрата (uan) |
| DE102015122070A1 (de) * | 2015-12-17 | 2017-06-22 | Thyssenkrupp Ag | Harnstoffhaltige Düngemittel und Verfahren zu ihrer Herstellung |
| WO2017111585A1 (en) | 2015-12-21 | 2017-06-29 | Stamicarbon B.V. | Urea ammonium nitrate production |
| US10730002B2 (en) * | 2016-05-09 | 2020-08-04 | Stamicarbon B.V. | Submicron particle removal from gas streams |
| NL2016915B1 (en) * | 2016-06-08 | 2017-12-18 | Green Granulation Tech Limited | Fluidized bed granulation |
| LT3484601T (lt) | 2016-07-15 | 2021-04-26 | Thyssenkrupp Fertilizer Technology Gmbh | Karbamido kompozicijos panaudojimas dyzelio išmetamųjų dujų skysčio gavimui |
| EP3315192B1 (en) * | 2016-10-27 | 2021-12-15 | YARA International ASA | Fluidized bed granulation |
| DE102017203251A1 (de) | 2017-02-28 | 2018-08-30 | Thyssenkrupp Ag | Verfahren zur Reinigung der Abluft einer Granulierungsanlage zur Herstellung eines harnstoffhaltigen Granulats |
| JP6851869B2 (ja) * | 2017-03-17 | 2021-03-31 | 東洋エンジニアリング株式会社 | 尿素の造粒方法 |
| CN107715676A (zh) * | 2017-10-10 | 2018-02-23 | 鲁西化工集团股份有限公司煤化工分公司 | 一种降低尿素造粒塔尾气氨含量的生产工艺 |
| EP3508465B1 (de) | 2018-01-08 | 2023-11-29 | thyssenkrupp Fertilizer Technology GmbH | Prallbleche im fliessbettkühler |
| JP2021516154A (ja) * | 2018-03-23 | 2021-07-01 | ティッセンクルップ フェルティリツァー テクノロジー ゲゼルシャフト ミット ベシュレンクテル ハフツング | 尿素造粒プラントの空気システム内のダスト蓄積を防止するためのコーティング材料を備えた流動層造粒機システム |
| JP7144528B2 (ja) | 2018-03-23 | 2022-09-29 | ティッセンクルップ フェルティリツァー テクノロジー ゲゼルシャフト ミット ベシュレンクテル ハフツング | 流動層造粒機または流動層クーラ用の分割された有孔板 |
| EP3542893A1 (de) | 2018-03-23 | 2019-09-25 | thyssenkrupp Fertilizer Technology GmbH | Fliessbettgranulator oder fliessbettkühler mit beschichteter perforierter platte |
| EP3560907B1 (en) | 2018-04-23 | 2021-01-06 | thyssenkrupp Fertilizer Technology GmbH | Urea production plant and scrubbing system |
| EP3790654B2 (en) | 2018-05-08 | 2025-09-24 | thyssenkrupp Uhde Fertilizer Technology GmbH | Internal cooling system for fluid-bed granulation plants |
| EP3581265B1 (de) | 2018-06-12 | 2024-12-04 | thyssenkrupp Fertilizer Technology GmbH | Sprühdüse zur herstellung eines harnstoff-schwefel düngers |
| EP3593898B1 (en) | 2018-07-13 | 2021-09-01 | thyssenkrupp Fertilizer Technology GmbH | Producing fertilizer granules with a defined size distribution |
| DE102019216894A1 (de) | 2019-10-31 | 2021-05-06 | Thyssenkrupp Ag | Fließbettgranulator |
| DE102019216931A1 (de) * | 2019-11-04 | 2021-05-06 | Thyssenkrupp Ag | Verfahren und Anlage zur Herstellung von Harnstoffgranulat |
| CA3166402C (en) | 2019-12-30 | 2023-08-15 | Stamicarbon B.V. | Ammonia removal from urea finishing |
| US11332437B2 (en) | 2019-12-30 | 2022-05-17 | Stamicarbon B.V. | Urea production with multiple evaporators |
| AU2020416395B2 (en) | 2019-12-30 | 2023-02-02 | Stamicarbon B.V. | Urea plant with chilled condensation section |
| PL3848341T3 (pl) | 2020-01-08 | 2024-06-24 | Thyssenkrupp Fertilizer Technology Gmbh | Sposób i urządzenie do wytwarzania nawozu |
| EP3907208A1 (en) | 2020-05-08 | 2021-11-10 | Yara International ASA | Urea ammonium sulfate-based composition |
| CN112742303B (zh) * | 2021-01-07 | 2022-06-10 | 黄超 | 集成式氧化铝粉造粒系统 |
| EP4029601A1 (en) * | 2021-01-13 | 2022-07-20 | Green Granulation Ltd. | Plant and process of granulating urea ammonia sulphate |
| DE102021202869A1 (de) * | 2021-03-24 | 2022-09-29 | Thyssenkrupp Ag | Anlage und Verfahren zur Herstellung von Harnstoffgranulat |
| US20250145543A1 (en) * | 2022-02-22 | 2025-05-08 | Tessenderlo Group Nv | Methods for the production of a solid urea-thiosulfate fertilizer |
| US20250178913A1 (en) * | 2023-07-27 | 2025-06-05 | Stamicarbon B.V. | System and processs for the production of uan |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3798021A (en) * | 1972-08-21 | 1974-03-19 | Foster Wheeler Corp | Pollution elimination for fertilizer process |
| US4370198A (en) | 1980-03-13 | 1983-01-25 | Mta Muszaki Kemiai Kutato Intezet | Method and apparatus for the recovery of the solid material content of solutions and/or suspensions as granules in a gas fluidized bed |
| US4493820A (en) * | 1982-10-01 | 1985-01-15 | Gardinier, Inc. | Process for partial removing of impurities from a wet process phosphoric acid |
| FI70202C (fi) * | 1984-06-20 | 1986-09-15 | Kemira Oy | Saett att aotervinna naeringsmedel fraon avgaserna av en np-konstgoedselfabrik |
| CN85100950A (zh) * | 1985-04-01 | 1987-01-10 | 基米勒公司 | 混合肥料的生产方法 |
| IT1249057B (it) * | 1991-05-22 | 1995-02-11 | Agrimont Spa | Processo per abbattere con un liquido l'ammoniaca contenuta in uno sfiato. |
| EP0653961B1 (en) * | 1992-08-07 | 1996-06-19 | Hydro Agri Sluiskil B.V. | Process for the production of urea granules |
| JPH09227493A (ja) * | 1996-02-27 | 1997-09-02 | Toyo Eng Corp | 排ガス中からの尿素ダスト及びアンモニアの回収方法 |
| NL1002862C2 (nl) | 1996-04-15 | 1997-10-17 | Dsm Nv | Werkwijze voor het bereiden van granules. |
| JPH09313860A (ja) | 1996-05-27 | 1997-12-09 | Shigeru Saito | 湿式同時除害、除塵ガス処理装置及び方法 |
| JP2000001466A (ja) * | 1998-06-12 | 2000-01-07 | Toyo Eng Corp | 排ガス中の尿素ダスト及びアンモニアの回収・利用方法 |
| JP2000095591A (ja) * | 1998-09-18 | 2000-04-04 | Chiyoda Corp | ダスト含有空気の洗浄設備 |
| JP2000279736A (ja) * | 1999-03-29 | 2000-10-10 | Toyo Eng Corp | 尿素ダスト及びアンモニアを含有する流体の処理装置、それを用いた処理方法及びそれを付設した尿素製造装置 |
| FI116288B (fi) * | 1999-07-08 | 2005-10-31 | Kemira Growhow Oyj | Ureafosfaattiprosessin emäliuoksen käsittelymenetelmä |
| NL1020665C2 (nl) | 2002-05-23 | 2003-11-25 | Dsm Nv | Werkwijze voor het verwijderen van ammoniak uit een ammoniak-bevattende gasstroom. |
| DE10346519A1 (de) * | 2003-10-02 | 2005-05-04 | Uhde Gmbh | Verfahren zur Entfernung von Ammoniak und Staub aus einem Abgas, das bei der Herstellung von Düngemitteln anfällt |
| CN1303041C (zh) * | 2004-02-06 | 2007-03-07 | 河北天人化工股份有限公司 | 一种氮磷或氮磷钾复合肥的制备方法 |
| CN100556503C (zh) * | 2006-08-01 | 2009-11-04 | 智胜化工股份有限公司 | 一种净化尿素造粒塔粉尘的方法 |
| CN200974818Y (zh) * | 2006-12-07 | 2007-11-14 | 张军保 | 尿素造粒尾气的气液并流式冷却洗涤器 |
| EP2192099A1 (en) * | 2008-11-28 | 2010-06-02 | Uhde Fertilizer Technology B.V. | Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules |
-
2008
- 2008-11-28 EP EP08020708A patent/EP2192099A1/en not_active Withdrawn
-
2009
- 2009-11-06 WO PCT/EP2009/007953 patent/WO2010060535A1/en not_active Ceased
- 2009-11-06 CN CN200980147420.XA patent/CN102227392B/zh active Active
- 2009-11-06 EP EP09756253.2A patent/EP2362863B1/en active Active
- 2009-11-06 BR BRPI0921863-7A patent/BRPI0921863B1/pt active IP Right Grant
- 2009-11-06 PE PE2011001076A patent/PE20120243A1/es not_active Application Discontinuation
- 2009-11-06 JP JP2011537866A patent/JP5723782B2/ja active Active
- 2009-11-06 CA CA2743488A patent/CA2743488C/en active Active
- 2009-11-06 RU RU2011126345/13A patent/RU2485077C2/ru active
- 2009-11-06 US US12/998,733 patent/US8466315B2/en active Active
- 2009-11-27 AR ARP090104595A patent/AR075554A1/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| CN102227392A (zh) | 2011-10-26 |
| PE20120243A1 (es) | 2012-04-14 |
| EP2192099A1 (en) | 2010-06-02 |
| JP2012509833A (ja) | 2012-04-26 |
| US20110229394A1 (en) | 2011-09-22 |
| BRPI0921863B1 (pt) | 2020-12-15 |
| CA2743488A1 (en) | 2010-06-03 |
| RU2011126345A (ru) | 2013-01-10 |
| CA2743488C (en) | 2017-12-05 |
| AR075554A1 (es) | 2011-04-20 |
| BRPI0921863A2 (pt) | 2020-08-11 |
| EP2362863A1 (en) | 2011-09-07 |
| US8466315B2 (en) | 2013-06-18 |
| WO2010060535A1 (en) | 2010-06-03 |
| EP2362863B1 (en) | 2017-06-14 |
| JP5723782B2 (ja) | 2015-05-27 |
| RU2485077C2 (ru) | 2013-06-20 |
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