Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of hair treatment composition and method of making the same is provided, wherein pass through mix and match and the protein of Chinese medicine medicines, the adding of the trichotrophy compositions such as aminoacid, can effectively reduce dandruff generation and scalp infects, promote piliation, comprehensively solve the hair problem.
A kind of hair treatment compositions of the present invention, the quality sum of each component is 100 mass parts, is comprised of following component:
Described component A is nature moisturizing factor, the nature moisturizing factor H109 of Shanghai Laibo Bio-chemical Co. Ltd. for example, and Main Ingredients and Appearance is water, glycerol, lactic acid, carbamide, Anjidew NL50, sodium chloride, 1, the 2-hexanediol, caprylyl glycol, allantoin, hyaluronate sodium, use as wetting agent, be applicable in the product of various Moisturizers and sun-proof, crease-resistant, resisting fatigue.
Described B component is the compositions that is comprised of dimethiconol and tridecyl ether-5, the 979E of German Wacker Chemie GmbH for example, belong to the large granule silicone oil emulsion, outstanding conditioning additive, be used for hair care product, excellent wet and slippery sense and wet cardability is provided, salubrious dry sliding sense is provided, keep the shampoo foam abundant.
Described component C is the compositions that is comprised of polydimethylsiloxane and dodecylbenzene sodium sulfonate, and for example the 3112VP of German Wacker Chemie GmbH can improve wet comb property, and the gloss hair keeps moisture, and smooth feeling is provided, and strengthens the glossiness of product.
Described component D is Methylisothiazolinone or iodine propilolic alcohol butyl mephenesin Carbamate, for example the MTI of Bristol special chemical article company limited (THOR SPECIALTIES (UK) LTD).
Described Radix Polygoni Multiflori extract prepares according to following step: at first Radix Polygoni Multiflori is put in the reactor, add sterile deionized water to the submergence Radix Polygoni Multiflori, soak and remove impurity after 1-3 hour, add again the sterile deionized water that fleece-flower root total quality 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Polygoni Multiflori extract.
Described Radix Ginseng extract prepares according to following step: at first Radix Ginseng is put in the reactor, add sterile deionized water to the submergence Radix Ginseng, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Ginseng gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Ginseng extract.
Described Radix Angelicae Sinensis extract prepares according to following step: at first Radix Angelicae Sinensis is put in the reactor, add sterile deionized water to the submergence Radix Angelicae Sinensis, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Angelicae Sinensis gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Angelicae Sinensis extract.
Described Fructus Lycii extract prepares according to following step: at first Fructus Lycii is put in the reactor, add sterile deionized water to the submergence Fructus Lycii, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Fructus Lycii gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Fructus Lycii extract.
Described Radix Rehmanniae Preparata extract prepares according to following step: at first Radix Rehmanniae Preparata is put in the reactor, add sterile deionized water to the submergence Radix Rehmanniae Preparata, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Rehmanniae Preparata gross mass 10-12 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains the Radix Rehmanniae Preparata extract.
A kind of hair treatment compositions of the present invention, the quality sum of each component is 100 mass parts, constituent content is preferably as follows:
A kind of method for preparing the hair treatment compositions of the present invention, carry out according to following step:
(1) cetearyl alcohol, hydrogenated polydecene, polydimethylsiloxane, Astrocaryum Murumuru Butter, the two stearyl alkyl dimethyl ammonium chlorides of hydroxypropyl, two cetyl alkyl dimethyl ammonium chlorides are warming up to 75-85 ℃, and stir;
(2) propylene glycol, 1,3 butylene glycol, component A, mountain Yu base trimethyl ammonium chloride, B component, component C, pantothenylol, palmitamide oxypropyl trimethyl ammonium chloride, sterile deionized water are warming up to 75-85 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs 10-20 minute at 80-85 ℃ of lower high speed homogenization, then naturally is cooled to 40-42 ℃;
(5) in emulsion reactor, add successively Radix Polygoni Multiflori extract, Radix Ginseng extract, Radix Angelicae Sinensis extract, Fructus Lycii extract, Radix Rehmanniae Preparata extract, Silk Amino Acids, component D and essence again, and high speed homogenization is stirred to evenly;
When (6) treating that mixture temperature is down to 36-38 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions of the present invention.
In the described step (1), be warming up to 80-85 ℃.
In the described step (2), be warming up to 80-85 ℃.
In described step (4) and (5), the high speed homogenization mixing speed is 3000-6000 rev/min.
Compared with prior art, hair treatment compositions of the present invention, contain the water extract of raw medicinal material of cosmetic conduct and learning or pharmaceutically acceptable carrier and effective dose or the extract of organic solvent, described raw medicinal material comprises Radix Rehmanniae Preparata, Fructus Lycii, Radix Polygoni Multiflori, Radix Angelicae Sinensis, Radix Ginseng, generation and the scalp that can reduce dandruff infect, remove pruritus and sense of discomfort, strengthen scalp nutrition, promote piliation, make the direct Absorption of nourishment composition of hair, impel hair sturdy, elegant long, submissive shiny black gloss, nontoxic nonirritant, safe and reliable.Wherein:
1. Radix Rehmanniae Preparata has the YIN nourishing of enriching blood effect, and is sweet, tepor, the yin nourishing of enriching blood, black beard and hair has the effect that improves tyrosinase activity, and extracting solution can play the hair blackening, impel the hair black pigment to generate, can be used as nutrient and the conditioner of hair, have antioxidation.
2. Fructus Lycii contains carotene, betanin, vitamin A, vitamin B1, vitamin B2, vitamin C and calcium, phosphorus, ferrum etc., and having increases the pharmacological action that leukocyte is active, promote hepatocyte new life, but also blood pressure lowering, blood sugar lowering, blood fat.
3. Radix Polygoni Multiflori, contain the nutritional labelings such as lecithin, effect with nourishing blood to expel wind, scalable neural and endocrine function and hairy root nourishing can impel the hair black pigment to generate the hair blackening, the effect of nutritious root of hair, impel the melanic generation of hair, can make the hair blackening, can be used as hair nutritional agent and conditioner and antibacterial.
4. Radix Angelicae Sinensis, include multiple volatile oil, sucrose, vitamin B12 and its function of retinoid material mainly contain brighten, defying age.Hair there is protective effect, promotes the scalp cells growth, have simultaneously the clean skin effect of speckle dispelling.
5. Radix Ginseng, contain multiple ginsenoside and volatile oil in the root, Main Ingredients and Appearance is panacene C15H24 in the oil, can increase cell viability, and can enhance metabolism and the effect of peripheral vessel circulation, improve the intensity of hair, prevent the usefulness of alopecia and poliosis regeneration, life-time service makes hair pitch-black glossy.
6. Silk Amino Acids, include 17 seed amino acids, skin there is very strong permeability, be applied to the skin very permeable and cross the epidermal keratinocyte of skin and hair, and then for skin absorbs, therefore have skin nutrition, strengthen the epidermis cell vigor, the function of delaying skin aging is outstanding especially, can make hair flexible, has gloss, soft and smooth, enhancing hair conditioning.
The specific embodiment
Further specify technical scheme of the present invention below in conjunction with specific embodiment.
At first adopt the Chinese medicine extraction process, Radix Polygoni Multiflori, Radix Ginseng, Radix Angelicae Sinensis, Fructus Lycii and Radix Rehmanniae Preparata are processed, to obtain its extract, wherein: (1) is put into Radix Polygoni Multiflori in the reactor, adds sterile deionized water to the submergence Radix Polygoni Multiflori, soaks and removes impurity after 1-3 hour, add again the sterile deionized water that fleece-flower root total quality 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Polygoni Multiflori extract; (2) Radix Ginseng is put in the reactor, added sterile deionized water to the submergence Radix Ginseng, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Ginseng gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Ginseng extract; (3) Radix Angelicae Sinensis is put in the reactor, added sterile deionized water to the submergence Radix Angelicae Sinensis, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Angelicae Sinensis gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Radix Angelicae Sinensis extract; (4) Fructus Lycii is put in the reactor, added sterile deionized water to the submergence Fructus Lycii, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Fructus Lycii gross mass 8-10 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains Fructus Lycii extract; (5) Radix Rehmanniae Preparata is put in the reactor, added sterile deionized water to the submergence Radix Rehmanniae Preparata, soak and remove impurity after 1-3 hour, add again the sterile deionized water that Radix Rehmanniae Preparata gross mass 10-12 doubly measures, heat boil 2-4 hour after, discharging is also filtered, and obtains the Radix Rehmanniae Preparata extract.
Then utilize Chinese medicine extract, the H109 (component A) of Shanghai Laibo Bio-chemical Co. Ltd., the 979E (B component) of German Wacker Chemie GmbH, the 3112VP (component C) of German Wacker Chemie GmbH, the MTI (component D) of Bristol special chemical article company limited (THOR SPECIALTIES (UK) LTD) of above-mentioned technique preparation, each constituent mass sum is that 100kg is example, prepares hair treatment compositions of the present invention.
Embodiment 1
(1) with cetearyl alcohol 5kg, hydrogenated polydecene 4kg, polydimethylsiloxane 2kg, Astrocaryum Murumuru Butter 1kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 1kg, two cetyl alkyl dimethyl ammonium chloride 3kg, is warming up to 85 ℃, and stirs;
(2) with propylene glycol 3kg, 1,3-butanediol 3kg, component A4kg, mountain Yu base trimethyl ammonium chloride 3kg, B component 4kg, component C 1kg, pantothenylol 1kg, palmitamide oxypropyl trimethyl ammonium chloride 1kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 85 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (6000 rev/mins) 10 minutes at 85 ℃ of lower high speed homogenizations, then naturally is cooled to 42 ℃;
(5) in emulsion reactor, add successively Radix Polygoni Multiflori extract 2kg, Radix Ginseng extract 1kg, Radix Angelicae Sinensis extract 1.5kg, Fructus Lycii extract 2kg, Radix Rehmanniae Preparata extract 1kg, Silk Amino Acids 0.5kg, component D 0.1kg and essence 0.5kg again, and high speed homogenization stirs (5000 rev/mins) to even;
When (6) treating that mixture temperature is down to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 1.
Embodiment 2
(1) with cetearyl alcohol 4kg, hydrogenated polydecene 3kg, polydimethylsiloxane 0.5kg, Astrocaryum Murumuru Butter 0.5kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 2kg, two cetyl alkyl dimethyl ammonium chloride 1kg, is warming up to 75 ℃, and stirs;
(2) with propylene glycol 5kg, 1,3-butanediol 5kg, component A 1kg, mountain Yu base trimethyl ammonium chloride 1kg, B component 1kg, component C 2kg, pantothenylol 2kg, palmitamide oxypropyl trimethyl ammonium chloride 0.5kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 75 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (3000 rev/mins) 15 minutes at 80 ℃ of lower high speed homogenizations, then naturally is cooled to 40 ℃;
(5) add successively Radix Polygoni Multiflori extract 0.5kg, Radix Ginseng extract 0.5kg, Radix Angelicae Sinensis extract 0.5kg, Fructus Lycii extract 1kg, Radix Rehmanniae Preparata extract 0.5kg, Silk Amino Acids 1kg, component D 0.05kg and essence 1kg again in emulsion reactor, high speed homogenization stirs (3000 rev/mins) to even;
When (6) treating that mixture temperature is down to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 2.
Embodiment 3
(1) with cetearyl alcohol 5kg, hydrogenated polydecene 4kg, polydimethylsiloxane 1kg, Astrocaryum Murumuru Butter 1kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 0.5kg, two cetyl alkyl dimethyl ammonium chloride 2kg, is warming up to 80 ℃, and stirs;
(2) with propylene glycol 4kg, 1,3-butanediol 4kg, component A 2kg, mountain Yu base trimethyl ammonium chloride 2kg, B component 3kg, component C 1.5kg, pantothenylol 1.5kg, palmitamide oxypropyl trimethyl ammonium chloride 1.5kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 85 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (4000 rev/mins) 15 minutes at 85 ℃ of lower high speed homogenizations, then naturally is cooled to 40 ℃;
(5) add successively Radix Polygoni Multiflori extract 2kg, Radix Ginseng extract 1.5kg, Radix Angelicae Sinensis extract 1kg, Fructus Lycii extract 0.5kg, Radix Rehmanniae Preparata extract 0.5kg, Silk Amino Acids 0.5kg, component D 0.08kg and essence 0.2kg again in emulsion reactor, high speed homogenization stirs (5000 rev/mins) to even;
When (6) treating that mixture temperature is down to 37 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 3.
Embodiment 4
(1) with cetearyl alcohol 4.5kg, hydrogenated polydecene 3.5kg, polydimethylsiloxane 1kg, Astrocaryum Murumuru Butter 1.5kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 1.5kg, two cetyl alkyl dimethyl ammonium chloride 1.5kg, be warming up to 75 ℃, and stir;
(2) with propylene glycol 3.5kg, 1,3-butanediol 4kg, component A 2kg, mountain Yu base trimethyl ammonium chloride 1.5kg, B component 3kg, component C 0.5kg, pantothenylol 0.5kg, palmitamide oxypropyl trimethyl ammonium chloride 1.5kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 85 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (5000 rev/mins) 10 minutes at 80 ℃ of lower high speed homogenizations, then naturally is cooled to 42 ℃;
(5) add successively Radix Polygoni Multiflori extract 1kg, Radix Ginseng extract 1.5kg, Radix Angelicae Sinensis extract 1kg, Fructus Lycii extract 1.5kg, Radix Rehmanniae Preparata extract 0.5kg, Silk Amino Acids 1kg, component D 0.1kg and essence 0.5kg again in emulsion reactor, high speed homogenization stirs (3000 rev/mins) to even;
When (6) treating that mixture temperature is down to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 4.
Embodiment 5
(1) with cetearyl alcohol 5kg, hydrogenated polydecene 4.5kg, polydimethylsiloxane 1kg, Astrocaryum Murumuru Butter 0.5kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 1kg, two cetyl alkyl dimethyl ammonium chloride 3kg, is warming up to 85 ℃, and stirs;
(2) with propylene glycol 3kg, 1,3-butanediol 4kg, component A 2.5kg, mountain Yu base trimethyl ammonium chloride 1kg, B component 1.5kg, component C 1kg, pantothenylol 1kg, palmitamide oxypropyl trimethyl ammonium chloride 1kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 75 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (3000 rev/mins) 20 minutes at 85 ℃ of lower high speed homogenizations, then naturally is cooled to 42 ℃;
(5) add successively Radix Polygoni Multiflori extract 2kg, Radix Ginseng extract 1kg, Radix Angelicae Sinensis extract 1kg, Fructus Lycii extract 1kg, Radix Rehmanniae Preparata extract 1.5kg, Silk Amino Acids 1kg, component D 0.05kg and essence 0.5kg again in emulsion reactor, high speed homogenization stirs (5000 rev/mins) to even;
When (6) treating that mixture temperature is down to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 5.
Embodiment 6
(1) with cetearyl alcohol 4kg, hydrogenated polydecene 3kg, polydimethylsiloxane 2kg, Astrocaryum Murumuru Butter 1kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 0.5kg, two cetyl alkyl dimethyl ammonium chloride 2kg, is warming up to 85 ℃, and stirs;
(2) with propylene glycol 4kg, 1,3-butanediol 5kg, component A 1kg, mountain Yu base trimethyl ammonium chloride 3kg, B component 2kg, component C 1.5kg, pantothenylol 2kg, palmitamide oxypropyl trimethyl ammonium chloride 1kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 85 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (6000 rev/mins) 12 minutes at 80 ℃ of lower high speed homogenizations, then naturally is cooled to 42 ℃;
(5) add successively Radix Polygoni Multiflori extract 2kg, Radix Ginseng extract 2kg, Radix Angelicae Sinensis extract 1kg, Fructus Lycii extract 1kg, Radix Rehmanniae Preparata extract 1kg, Silk Amino Acids 2kg, component D 0.1kg and essence 1kg again in emulsion reactor, high speed homogenization stirs (6000 rev/mins) to even;
When (6) treating that mixture temperature is down to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 6.
Embodiment 7
(1) with cetearyl alcohol 4kg, hydrogenated polydecene 3kg, polydimethylsiloxane 1kg, Astrocaryum Murumuru Butter 1.8kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 1.2kg, two cetyl alkyl dimethyl ammonium chloride 1kg, is warming up to 85 ℃, and stirs;
(2) with propylene glycol 5kg, 1,3-butanediol 3kg, component A 1kg, mountain Yu base trimethyl ammonium chloride 2kg, B component 1kg, component C 2kg, pantothenylol 1kg, palmitamide oxypropyl trimethyl ammonium chloride 2kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 78 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (6000 rev/mins) 15 minutes at 83 ℃ of lower high speed homogenizations, then naturally is cooled to 41 ℃;
(5) add successively Radix Polygoni Multiflori extract 1.5kg, Radix Ginseng extract 1.5kg, Radix Angelicae Sinensis extract 2kg, Fructus Lycii extract 2kg, Radix Rehmanniae Preparata extract 1.5kg, Silk Amino Acids 1kg, component D 0.08kg and essence 0.8kg again in emulsion reactor, high speed homogenization stirs (4000 rev/mins) to even;
When (6) treating that mixture temperature is down to 37 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 7.
Embodiment 8
(1) with cetearyl alcohol 5kg, hydrogenated polydecene 3kg, polydimethylsiloxane 0.5kg, Astrocaryum Murumuru Butter 1kg, hydroxypropyl two stearyl alkyl dimethyl ammonium chloride 0.5kg, two cetyl alkyl dimethyl ammonium chloride 1kg, is warming up to 80 ℃, and stirs;
(2) with propylene glycol 4kg, 1,3-butanediol 4kg, component A 4kg, mountain Yu base trimethyl ammonium chloride 1kg, B component 2kg, component C 2kg, pantothenylol 1kg, palmitamide oxypropyl trimethyl ammonium chloride 1kg, sterile deionized water are (according to addition and the quality sum 100kg of other components, calculate its concrete addition) be warming up to 80 ℃, and stir;
(3) with the mixture of step (1) preparation, join in the mixture of step (2) preparation, and stir;
(4) mixture that step (3) is stirred places the airtight and evacuation of emulsion reactor, stirs (4000 rev/mins) 20 minutes at 85 ℃ of lower high speed homogenizations, then naturally is cooled to 40 ℃;
(5) add successively Radix Polygoni Multiflori extract 1kg, Radix Ginseng extract 1kg, Radix Angelicae Sinensis extract 0.5kg, Fructus Lycii extract 2kg, Radix Rehmanniae Preparata extract 0.5kg, Silk Amino Acids 1kg, component D 0.05kg and essence 0.5kg again in emulsion reactor, high speed homogenization stirs (6000 rev/mins) to even;
When (6) treating that mixture temperature is down to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and namely gets hair treatment compositions 8.
Investigate the action effect of hair treatment composition sample 1-8 of the present invention, the personnel that choose 50 all ages and classes use, life cycle is fortnight, 99% user is good to above-mentioned sample performance, sample can effectively reduce the dandruff generation and scalp infects, promote piliation, comprehensively solve the hair problem.
More than the present invention has been done exemplary description; should be noted that; in the situation that does not break away from core of the present invention, the replacement that is equal to that any simple distortion, modification or other those skilled in the art can not spend creative work all falls into protection scope of the present invention.